CN103666014B - A kind of UV curable ink with antistatic property and preparation method thereof - Google Patents
A kind of UV curable ink with antistatic property and preparation method thereof Download PDFInfo
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- CN103666014B CN103666014B CN201310593211.6A CN201310593211A CN103666014B CN 103666014 B CN103666014 B CN 103666014B CN 201310593211 A CN201310593211 A CN 201310593211A CN 103666014 B CN103666014 B CN 103666014B
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- curable ink
- diatomite
- antistatic property
- auxiliary agent
- minute
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- 238000002360 preparation method Methods 0.000 title claims description 8
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 12
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000000843 powder Substances 0.000 claims abstract description 10
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 9
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 claims abstract description 7
- ZZTCPWRAHWXWCH-UHFFFAOYSA-N diphenylmethanediamine Chemical compound C=1C=CC=CC=1C(N)(N)C1=CC=CC=C1 ZZTCPWRAHWXWCH-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000000975 dye Substances 0.000 claims abstract description 7
- 239000003822 epoxy resin Substances 0.000 claims abstract description 7
- WSFSSNUMVMOOMR-UHFFFAOYSA-N formaldehyde Substances O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000000463 material Substances 0.000 claims abstract description 7
- 239000000049 pigment Substances 0.000 claims abstract description 7
- 229920000647 polyepoxide Polymers 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 229920005989 resin Polymers 0.000 claims abstract description 7
- 239000011347 resin Substances 0.000 claims abstract description 7
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000003112 inhibitor Substances 0.000 claims abstract description 6
- OWRCNXZUPFZXOS-UHFFFAOYSA-N 1,3-diphenylguanidine Chemical compound C=1C=CC=CC=1NC(=N)NC1=CC=CC=C1 OWRCNXZUPFZXOS-UHFFFAOYSA-N 0.000 claims abstract description 4
- DURPTKYDGMDSBL-UHFFFAOYSA-N 1-butoxybutane Chemical compound CCCCOCCCC DURPTKYDGMDSBL-UHFFFAOYSA-N 0.000 claims abstract description 4
- CTKINSOISVBQLD-UHFFFAOYSA-N Glycidol Chemical compound OCC1CO1 CTKINSOISVBQLD-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 4
- 230000003647 oxidation Effects 0.000 claims abstract description 4
- 238000007254 oxidation reaction Methods 0.000 claims abstract description 4
- 229920002239 polyacrylonitrile Polymers 0.000 claims abstract description 4
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 4
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 15
- 238000006243 chemical reaction Methods 0.000 claims description 10
- 239000012467 final product Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 3
- 244000077995 Coix lacryma jobi Species 0.000 claims description 3
- FQYUMYWMJTYZTK-UHFFFAOYSA-N Phenyl glycidyl ether Chemical compound C1OC1COC1=CC=CC=C1 FQYUMYWMJTYZTK-UHFFFAOYSA-N 0.000 claims description 3
- 229920002367 Polyisobutene Polymers 0.000 claims description 3
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 claims description 3
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 3
- DAKWPKUUDNSNPN-UHFFFAOYSA-N Trimethylolpropane triacrylate Chemical compound C=CC(=O)OCC(CC)(COC(=O)C=C)COC(=O)C=C DAKWPKUUDNSNPN-UHFFFAOYSA-N 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 239000010445 mica Substances 0.000 claims description 3
- 229910052618 mica group Inorganic materials 0.000 claims description 3
- GEMHFKXPOCTAIP-UHFFFAOYSA-N n,n-dimethyl-n'-phenylcarbamimidoyl chloride Chemical compound CN(C)C(Cl)=NC1=CC=CC=C1 GEMHFKXPOCTAIP-UHFFFAOYSA-N 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 3
- 230000003068 static effect Effects 0.000 abstract description 7
- 230000000694 effects Effects 0.000 abstract description 4
- 239000011358 absorbing material Substances 0.000 abstract description 2
- -1 methyl acrylic ester Chemical class 0.000 abstract description 2
- PWWSSIYVTQUJQQ-UHFFFAOYSA-N distearyl thiodipropionate Chemical compound CCCCCCCCCCCCCCCCCCOC(=O)CCSCCC(=O)OCCCCCCCCCCCCCCCCCC PWWSSIYVTQUJQQ-UHFFFAOYSA-N 0.000 abstract 1
- 240000001624 Espostoa lanata Species 0.000 description 2
- 235000009161 Espostoa lanata Nutrition 0.000 description 2
- 239000002932 luster Substances 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 101000831616 Homo sapiens Protachykinin-1 Proteins 0.000 description 1
- 240000008415 Lactuca sativa Species 0.000 description 1
- 206010034972 Photosensitivity reaction Diseases 0.000 description 1
- 102100024304 Protachykinin-1 Human genes 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 238000000016 photochemical curing Methods 0.000 description 1
- 230000036211 photosensitivity Effects 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 235000012045 salad Nutrition 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 150000003384 small molecules Chemical class 0.000 description 1
- 238000002211 ultraviolet spectrum Methods 0.000 description 1
Landscapes
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a kind of UV curable ink with antistatic property, it is characterized in that, be made up of the raw material of following weight part: pigment dyestuff 1-3, methyl methacrylate 12-15, diaminodiphenyl-methane 3-5, terpolycyantoamino-formaldehyde resin 20-24, E-12 epoxy resin 10-12, tetrafluoroethylene 2-3, diatomite 1-2, calcinated argil powder 2-4, citric acid 3-4, polyacrylonitrile microballoon 1-2, Racemic glycidol butyl ether 1-2, triethylene glycol 3-4, polyvinyl alcohol 1-2, oxidation inhibitor DSTP? 1-2, 184 light trigger 5-8, vulkacit D? 1.3-1.5, auxiliary agent 4-5, methyl acrylic ester static inhibitor is added in the present invention's formula, can the static charge on absorbing material surface preferably, thus play the effect of anti-electrostatic, and processing treatment is simple and convenient, the physicochemical property of base material is unaffected.
Description
Technical field
The present invention relates to a kind of ink and preparation method thereof, particularly a kind of UV curable ink with antistatic property and preparation method thereof.
Background technology
Ultraviolet light polymerization (UV) ink refers under uviolizing, utilizes the UV-light of different wave length and energy to make ink film forming and dry ink.Utilize different UV spectrum, can different-energy be produced, the monomer polymerization in different ink vehicle is become polymkeric substance, so the look film of UV ink has good machinery and chemical property.The major advantage of UV ink has: (1) is without solvent; (2) rate of drying is fast, and power consumption is few; (3) good luster, bright in luster; (4) water-fast, solvent resistant, wear resisting property is good.In UV ink, light trigger is that one is subject to light activated compound, after absorb light is shone, be excited into free radical, and energy trasfer, to photosensitivity molecule or photocrosslinking agent, makes UV ink that photocuring reaction occur.In order to reduce the harm that electrostatic brings, at present, people are typically employed in UV curable ink and add color stuffing to suppress the generation of static charge and to promote the leakage of static charge, thus be lowered into the surface resistivity of mould material to a certain extent, strengthen the antistatic property of film, but, because the reason of class coating material self structure and color stuffing are generally small molecules, the antistatic effect that this method produces is not very good, how to develop the good and antistatic lasting anti static additive of a kind of antistatic effect, and in UV curable ink, all UV curable ink field worker institutes problems faced.
Summary of the invention
The object of this invention is to provide a kind of UV curable ink with antistatic property and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
There is a UV curable ink for antistatic property, be made up of the raw material of following weight part: pigment dyestuff 1-3, methyl methacrylate 12-15, diaminodiphenyl-methane 3-5, terpolycyantoamino-formaldehyde resin 20-24, E-12 epoxy resin 10-12, tetrafluoroethylene 2-3, diatomite 1-2, calcinated argil powder 2-4, citric acid 3-4, polyacrylonitrile microballoon 1-2, Racemic glycidol butyl ether 1-2, triethylene glycol 3-4, polyvinyl alcohol 1-2, oxidation inhibitor DSTP1-2,184 light trigger 5-8, vulkacit D 1.3-1.5, auxiliary agent 4-5;
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, Silane coupling agent KH550 2-3, linking agent TAC2-3, polyisobutene 2-3, Resorcinol 1-2, Viscoat 295 10-12, acrylate 2-3, phenyl glycidyl ether 1-2, cobalt naphthenate 2-3, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 DEG C, and stirring reaction 30-40 minute, to obtain final product.
The UV curable ink with antistatic property of the present invention, be made up of following concrete steps: first add pigment dyestuff, methyl methacrylate, diaminodiphenyl-methane, terpolycyantoamino-formaldehyde resin, E-12 epoxy resin, tetrafluoroethylene, diatomite stirring and evenly mixing, be heated to 80-90 DEG C, stir 25-35 minute; Then all the other remaining components except 184 light triggers are added, stirring reaction 3-5 hour; Finally be cooled to 60-70 DEG C, add 184 light triggers, stirring reaction 40-50 minute, after cooling, grinding obtains 20-40 μm of slurry, to obtain final product.
The invention has the beneficial effects as follows: auxiliary agent of the present invention improves the toughness of ink, make distributes ink even, and maintain the stability of ink; Methyl acrylic ester static inhibitor is added in the present invention's formula, can the static charge on absorbing material surface preferably, thus play the effect of anti-electrostatic, and processing treatment is simple and convenient, the physicochemical property of base material is unaffected.
Specific embodiments
Below by specific examples, the present invention is described in detail.
There is a UV curable ink for antistatic property, be made up of the raw material of following weight part (kilogram): pigment dyestuff 2, methyl methacrylate 12, diaminodiphenyl-methane 3, terpolycyantoamino-formaldehyde resin 20, E-12 epoxy resin 10, tetrafluoroethylene 2, diatomite 1, calcinated argil powder 2, citric acid 3, polyacrylonitrile microballoon 1, Racemic glycidol butyl ether 1, triethylene glycol 3, polyvinyl alcohol 1, oxidation inhibitor DSTP1,184 light triggers 5, vulkacit D 1.3, auxiliary agent 4;
Described auxiliary agent is prepared from by the raw material of following weight part (kilogram): nano diatomite powder 0.2, nano mica powder 0.2, Silane coupling agent KH550 2, linking agent TAC2, polyisobutene 2, Resorcinol 1, Viscoat 295 10, acrylate 2, phenyl glycidyl ether 1, cobalt naphthenate 2, Tenox PG 2, coix seed oil 1; Its preparation method is by each mixing of materials, is heated to 60-70 DEG C, and stirring reaction 30-40 minute, to obtain final product.
The UV curable ink with antistatic property of the present invention, be made up of following concrete steps: first add pigment dyestuff, methyl methacrylate, diaminodiphenyl-methane, terpolycyantoamino-formaldehyde resin, E-12 epoxy resin, tetrafluoroethylene, diatomite stirring and evenly mixing, be heated to 80-90 DEG C, stir 25-35 minute; Then all the other remaining components except 184 light triggers are added, stirring reaction 3-5 hour; Finally be cooled to 60-70 DEG C, add 184 light triggers, stirring reaction 40-50 minute, after cooling, grinding obtains 20-40 μm of slurry, to obtain final product.
The ink of gained, uses cross-hatching ox-hide tape stripping, draws compartment apart from 1mm, 100% attachment; Use the spirituous cotton balls of leaching, 300 grams of pressure wipings 50 times, are as good as shape; To be soaked in salad oil (normal temperature) 8 hours, to be as good as shape; Use and be soaked with the cotton balls of salt solution, 300 grams of pressure wipings 50 times, are as good as shape.
Claims (2)
1. one kind has the UV curable ink of antistatic property, it is characterized in that, be prepared from by the raw material of following weight part: pigment dyestuff 1-3, methyl methacrylate 12-15, diaminodiphenyl-methane 3-5, terpolycyantoamino-formaldehyde resin 20-24, E-12 epoxy resin 10-12, tetrafluoroethylene 2-3, diatomite 1-2, calcinated argil powder 2-4, citric acid 3-4, polyacrylonitrile microballoon 1-2, Racemic glycidol butyl ether 1-2, triethylene glycol 3-4, polyvinyl alcohol 1-2, oxidation inhibitor DSTP1-2,184 light trigger 5-8, vulkacit D 1.3-1.5, auxiliary agent 4-5;
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, Silane coupling agent KH550 2-3, linking agent TAC2-3, polyisobutene 2-3, Resorcinol 1-2, Viscoat 295 10-12, acrylate 2-3, phenyl glycidyl ether 1-2, cobalt naphthenate 2-3, Tenox PG 2-3, coix seed oil 1-2; The preparation method of auxiliary agent is by each mixing of materials, and be heated to 60-70 DEG C, stirring reaction 30-40 minute, to obtain final product.
2. there is the UV curable ink of antistatic property according to claim 1, it is characterized in that, be made up of following concrete steps: first add pigment dyestuff, methyl methacrylate, diaminodiphenyl-methane, terpolycyantoamino-formaldehyde resin, E-12 epoxy resin, tetrafluoroethylene, diatomite stirring and evenly mixing, be heated to 80-90 DEG C, stir 25-35 minute; Then all the other remaining components except 184 light triggers are added, stirring reaction 3-5 hour; Finally be cooled to 60-70 DEG C, add 184 light triggers, stirring reaction 40-50 minute, after cooling, grinding obtains 20-40 μm of slurry, to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310593211.6A CN103666014B (en) | 2013-11-23 | 2013-11-23 | A kind of UV curable ink with antistatic property and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310593211.6A CN103666014B (en) | 2013-11-23 | 2013-11-23 | A kind of UV curable ink with antistatic property and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103666014A CN103666014A (en) | 2014-03-26 |
| CN103666014B true CN103666014B (en) | 2016-03-23 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310593211.6A Active CN103666014B (en) | 2013-11-23 | 2013-11-23 | A kind of UV curable ink with antistatic property and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN103666014B (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1260563A1 (en) * | 2001-05-21 | 2002-11-27 | Sicpa Holding S.A. | UV curing intaglio ink |
| CN1503829A (en) * | 2001-02-14 | 2004-06-09 | Ucb公司 | Waterfast ink jet inks containing UV curable resin |
| JP2004182933A (en) * | 2002-12-05 | 2004-07-02 | Riso Kagaku Corp | Ultraviolet light-curing type inkjet ink |
| CN101235235A (en) * | 2007-02-02 | 2008-08-06 | 日本精工油墨股份有限公司 | Ultraviolet solidifying type ink and decoration printed matter using the same |
| CN101805541A (en) * | 2010-04-09 | 2010-08-18 | 上海化工研究院 | Ultraviolet curing ink and production method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7449515B2 (en) * | 2005-11-30 | 2008-11-11 | Xerox Corporation | Phase change inks containing compounds derived from isocyanate, unsaturated alcohol, and polyol |
-
2013
- 2013-11-23 CN CN201310593211.6A patent/CN103666014B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1503829A (en) * | 2001-02-14 | 2004-06-09 | Ucb公司 | Waterfast ink jet inks containing UV curable resin |
| EP1260563A1 (en) * | 2001-05-21 | 2002-11-27 | Sicpa Holding S.A. | UV curing intaglio ink |
| JP2004182933A (en) * | 2002-12-05 | 2004-07-02 | Riso Kagaku Corp | Ultraviolet light-curing type inkjet ink |
| CN101235235A (en) * | 2007-02-02 | 2008-08-06 | 日本精工油墨股份有限公司 | Ultraviolet solidifying type ink and decoration printed matter using the same |
| CN101805541A (en) * | 2010-04-09 | 2010-08-18 | 上海化工研究院 | Ultraviolet curing ink and production method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103666014A (en) | 2014-03-26 |
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| PB01 | Publication | ||
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| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A UV curable ink with anti-static effect and its preparation method Effective date of registration: 20231113 Granted publication date: 20160323 Pledgee: Shanghai Yudi Aviation Supplies Co.,Ltd. Pledgor: TONGLING FOUNDER PLASTICS TECHNOLOGY Co.,Ltd. Registration number: Y2023980065339 |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
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Date of cancellation: 20231219 Granted publication date: 20160323 Pledgee: Shanghai Yudi Aviation Supplies Co.,Ltd. Pledgor: TONGLING FOUNDER PLASTICS TECHNOLOGY Co.,Ltd. Registration number: Y2023980065339 |
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Effective date of registration: 20240320 Address after: 236300 Yingshui Road, Economic Development Zone, Funan County, Fuyang City, Anhui Province Patentee after: Anhui Runhui Polymer Material Technology Co.,Ltd. Country or region after: Zhong Guo Address before: 244000 No. 3201, Cuihu Fourth Road, Tongling Economic Development Zone, Anhui Province Patentee before: TONGLING FOUNDER PLASTICS TECHNOLOGY Co.,Ltd. Country or region before: Zhong Guo |