CN103614858B - 一种微米碳化硅纤维毡及其制备方法 - Google Patents
一种微米碳化硅纤维毡及其制备方法 Download PDFInfo
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- CN103614858B CN103614858B CN201310585839.1A CN201310585839A CN103614858B CN 103614858 B CN103614858 B CN 103614858B CN 201310585839 A CN201310585839 A CN 201310585839A CN 103614858 B CN103614858 B CN 103614858B
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- silicon carbide
- polycarbosilane
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- silica fibre
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- 229910010271 silicon carbide Inorganic materials 0.000 title claims abstract description 85
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 title claims abstract description 66
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims abstract description 56
- 239000000835 fiber Substances 0.000 title claims abstract description 55
- 238000002360 preparation method Methods 0.000 title claims abstract description 31
- 239000000377 silicon dioxide Substances 0.000 title claims abstract description 28
- 229920003257 polycarbosilane Polymers 0.000 claims abstract description 34
- 238000001914 filtration Methods 0.000 claims abstract description 6
- 229920001558 organosilicon polymer Polymers 0.000 claims abstract description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 32
- 229910052757 nitrogen Inorganic materials 0.000 claims description 16
- 230000005021 gait Effects 0.000 claims description 14
- 238000005245 sintering Methods 0.000 claims description 12
- 238000009413 insulation Methods 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 9
- 238000009987 spinning Methods 0.000 claims description 9
- 239000007789 gas Substances 0.000 claims description 7
- 238000002844 melting Methods 0.000 claims description 6
- 230000008018 melting Effects 0.000 claims description 6
- 238000010792 warming Methods 0.000 claims description 6
- ICSWLKDKQBNKAY-UHFFFAOYSA-N 1,1,3,3,5,5-hexamethyl-1,3,5-trisilinane Chemical compound C[Si]1(C)C[Si](C)(C)C[Si](C)(C)C1 ICSWLKDKQBNKAY-UHFFFAOYSA-N 0.000 claims description 5
- IKXDEFIEGAVNOZ-UHFFFAOYSA-N [SiH4].[C] Chemical compound [SiH4].[C] IKXDEFIEGAVNOZ-UHFFFAOYSA-N 0.000 claims description 4
- 229910052799 carbon Inorganic materials 0.000 claims description 4
- 238000007500 overflow downdraw method Methods 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 3
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 2
- 239000003595 mist Substances 0.000 claims description 2
- 229910052719 titanium Inorganic materials 0.000 claims description 2
- 239000010936 titanium Substances 0.000 claims description 2
- 229910052727 yttrium Inorganic materials 0.000 claims description 2
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 claims description 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims 2
- 239000011261 inert gas Substances 0.000 claims 2
- 229910052786 argon Inorganic materials 0.000 claims 1
- -1 polyborazine Chemical compound 0.000 claims 1
- 230000001681 protective effect Effects 0.000 claims 1
- 239000000463 material Substances 0.000 abstract description 7
- 239000011153 ceramic matrix composite Substances 0.000 abstract description 4
- 238000002074 melt spinning Methods 0.000 abstract description 4
- 239000000919 ceramic Substances 0.000 abstract description 2
- 230000003197 catalytic effect Effects 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 description 7
- 238000005516 engineering process Methods 0.000 description 6
- 229910003465 moissanite Inorganic materials 0.000 description 6
- 239000002131 composite material Substances 0.000 description 5
- 239000011160 polymer matrix composite Substances 0.000 description 5
- 229920013657 polymer matrix composite Polymers 0.000 description 5
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000013329 compounding Methods 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 238000002803 maceration Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 206010021143 Hypoxia Diseases 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000010041 electrostatic spinning Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 208000018875 hypoxemia Diseases 0.000 description 1
- 239000002075 main ingredient Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 229920000548 poly(silane) polymer Polymers 0.000 description 1
- 239000012925 reference material Substances 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
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Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105568427B (zh) * | 2016-03-01 | 2018-02-02 | 江苏赛菲新材料有限公司 | 一种高电阻率连续碳化硅纤维及其制备方法 |
CN106337211B (zh) * | 2016-08-29 | 2018-08-28 | 浙江惠侬丝针织内衣有限公司 | 一种陶瓷保健纱加工方法 |
CN109610045B (zh) * | 2018-08-23 | 2021-09-21 | 成都市宏智达科技有限公司 | 一种耐高温、高强度碳化硅纤维的制备方法 |
CN109797460B (zh) * | 2019-01-28 | 2021-07-30 | 江西嘉捷信达新材料科技有限公司 | 含铝硼SiC纤维及其超临界流体下的制备方法 |
CN109776096A (zh) * | 2019-01-28 | 2019-05-21 | 江西嘉捷信达新材料科技有限公司 | 硫化钼/石墨烯、铁共掺杂的碳化硅纤维及其制备方法与应用 |
CN110184662B (zh) * | 2019-05-29 | 2021-06-22 | 中国人民解放军国防科技大学 | 熔融纺丝用陶瓷先驱体聚合物熔体连续供料装置及方法 |
CN111575818B (zh) * | 2020-05-11 | 2022-01-11 | 宁波众兴新材料科技有限公司 | 一种大丝束连续碳化硅纤维制备装置及方法 |
CN111501114B (zh) * | 2020-05-15 | 2021-08-10 | 唐山开滦化工科技有限公司 | 一种酚醛纤维的制备方法 |
Citations (5)
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CN1410606A (zh) * | 2002-11-18 | 2003-04-16 | 中国人民解放军国防科学技术大学 | 耐高温多晶碳化硅纤维的制备方法 |
CN1715466A (zh) * | 2005-06-29 | 2006-01-04 | 中国人民解放军国防科学技术大学 | 含铝连续碳化硅纤维的制备方法 |
CN101319414A (zh) * | 2008-07-16 | 2008-12-10 | 中国人民解放军国防科学技术大学 | 一种高耐温性碳化硅纤维的制造方法 |
CN102634867A (zh) * | 2012-05-04 | 2012-08-15 | 中国人民解放军国防科学技术大学 | 一种近化学计量比的碳化硅纤维的制备方法 |
CN103320966A (zh) * | 2013-07-04 | 2013-09-25 | 厦门大学 | 一种柔性多晶碳化硅微纳米纤维毡的制备方法 |
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US20050031866A1 (en) * | 2001-10-03 | 2005-02-10 | Hiroyuki Yamaoka | Silicon carbide fiber having boron nitride layer in fiber surface and process for the production thereof |
JP2003113537A (ja) * | 2001-10-03 | 2003-04-18 | Ube Ind Ltd | 窒化ホウ素層を繊維表面に有する炭化珪素繊維及びその製造方法 |
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Patent Citations (5)
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CN1410606A (zh) * | 2002-11-18 | 2003-04-16 | 中国人民解放军国防科学技术大学 | 耐高温多晶碳化硅纤维的制备方法 |
CN1715466A (zh) * | 2005-06-29 | 2006-01-04 | 中国人民解放军国防科学技术大学 | 含铝连续碳化硅纤维的制备方法 |
CN101319414A (zh) * | 2008-07-16 | 2008-12-10 | 中国人民解放军国防科学技术大学 | 一种高耐温性碳化硅纤维的制造方法 |
CN102634867A (zh) * | 2012-05-04 | 2012-08-15 | 中国人民解放军国防科学技术大学 | 一种近化学计量比的碳化硅纤维的制备方法 |
CN103320966A (zh) * | 2013-07-04 | 2013-09-25 | 厦门大学 | 一种柔性多晶碳化硅微纳米纤维毡的制备方法 |
Non-Patent Citations (3)
Title |
---|
先驱体法制备含异质元素SiC陶瓷纤维的现状与进展;余煜玺;《硅酸盐学报》;20030430;第31卷(第4期);第371-375页 * |
同板多形碳化硅纤维的制备及其性能研究;殷玲玲;《中国优秀硕士学位论文全文数据库 工程科技Ⅰ辑》;20060315(第3期);B020-13 * |
含铝碳化硅纤维的连续化制备与研究;余煜玺;《中国博士学位论文全文数据库 工程科技Ⅰ辑》;20060315(第3期);B016-7 * |
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