CN103027857A - Shampoo containing marine biological degerming components and preparation method of shampoo - Google Patents
Shampoo containing marine biological degerming components and preparation method of shampoo Download PDFInfo
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- CN103027857A CN103027857A CN2012105753893A CN201210575389A CN103027857A CN 103027857 A CN103027857 A CN 103027857A CN 2012105753893 A CN2012105753893 A CN 2012105753893A CN 201210575389 A CN201210575389 A CN 201210575389A CN 103027857 A CN103027857 A CN 103027857A
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Abstract
The invention discloses a shampoo containing marine biological degerming components and a preparation method of the shampoo. The shampoo comprises the following components by weight percent: 2.0-4.0% of marine biological degerming agent, 8.0-14.0% of alkyl glycoside, 7.0-10% of cocamidopropyl betaine, 6.0-10.0% of coco fatty acid diethanol amide, 0.5-2.0% of alkyl dimethyl polysiloxane, 1.0-1.5% of sodium chloride, 1.0-1.5% of sodium citrate, 0-5.0% of essence, and the balance of water. The shampoo containing the marine biological degerming components has itch relieving and dandruff removal functions and further has the advantages that the shampoo has no stimulation and corrosion to hairs.
Description
Technical field
The present invention relates to shampoo, relate in particular to a kind of shampoo that contains marine organisms degerming composition and preparation method thereof.
Background technology
Common scalp is uncomfortable, mainly is the dandruff and head pruritus, and the major reason that causes the dandruff is fungal infection, and is different according to the kind of individual variation and bacterial infection, is divided into:
1, seborrheic dermatitis: seborrheic dermatitis is to cause the topmost reason of the dandruff.Usually appear in the Adult Groups, showing as has thicker oiliness secretions or hair drying on the scalp.
2, tinea capitis: general thicker and tighter being attached on the scalp, the silvery white squama of surface coverage, normal journey speckle shape distributes.
3, chronic eczema: have the germ infection of scalp and hair to cause, show as the destruction of dandruff and hair.Can be with inflammatory reaction when serious.
4, atoipc dermatitis: show as the scalp diffusivity and do bits.
At present, existing shampoo kind is a lot, functional shampoo mainly is dandruff control shampoo containing and generating and nourishing hair class shampoo, main adding ingredient is: pyridine copper sulfate or other antifungal drugs (ketoconazole, climbazole, selenium sulfide etc. are arranged) and Chinese medicine preparation, antimycotic medicine life-time service can produce drug resistance, and production cost is high.The Chinese medicine preparation complex manufacturing, and sterilization, fungistatic effect are weak type.
Summary of the invention
An object of the present invention is to provide a kind of antipruritic and shampoo that the contains marine organisms degerming composition anti-dandruff function of having.
Another object of the present invention provides a kind of preparation method with shampoo that contains marine organisms degerming composition of antipruritic and anti-dandruff function.
The shampoo that contains marine organisms degerming composition of the present invention, percent meter proportioning is as follows by weight:
Marine organisms bacteria remover 2.0-4.0%;
Alkyl polyglucoside 8.0-14.0%;
Cocamido propyl betaine 7.0-10.0%;
Cocoanut fatty acid diethanolamide 6.0-10.0%;
Alkyl-dimethyl based polysiloxane 0.5-2.0%;
Sodium chloride 1.0-1.5%;
Sodium citrate 1.0-1.5%;
Essence 0-5.0%;
Surplus is water.
The preparation method that contains the shampoo of marine organisms degerming composition of the present invention may further comprise the steps:
Step S10: add alkyl polyglucoside, cocamido propyl betaine, cocoanut fatty acid diethanolamide, the alkyl-dimethyl based polysiloxane of proportional quantity in 35-40 ℃ the water, carry out emulsifying under the stirring condition and get mixed liquor A;
Step S20: add the marine organisms bacteria remover of proportional quantity in the mixed liquor A, under 25-35 ℃ of temperature conditions, mix to get institute's mixed liquid B;
Step S30: add sodium citrate, sodium chloride and the essence of proportional quantity in the mixed liquid B, mix homogeneously gets the described shampoo that contains marine organisms degerming composition.
The shampoo that contains marine organisms degerming composition of the present invention, owing to contain marine organisms bacteria remover composition, therefore, after the use, effectively degerming, and then have antipruritic and effect anti-dandruff, and owing to this each component that contains the shampoo of marine organisms degerming composition is nontoxic, non-stimulated, the free from corrosion material of skin, so this shampoo also has non-stimulated, the free from corrosion advantage of hair and hair.
The preparation method that contains the shampoo of marine organisms degerming composition of the present invention, because order by merging and the mixing condition of each material are comparatively reasonable, so that each the component mix homogeneously of the shampoo that contains marine organisms degerming composition that makes by preparation method of the present invention, good stability.
The specific embodiment
Embodiment 1
The shampoo that contains marine organisms degerming composition of present embodiment, percent meter proportioning is as follows by weight: marine organisms bacteria remover 2.0-4.0%;
Alkyl polyglucoside 8.0-14.0%;
Cocamido propyl betaine 7.0-10.0%;
Cocoanut fatty acid diethanolamide 6.0-10.0%;
Alkyl-dimethyl based polysiloxane 0.5-2.0%;
Sodium chloride 1.0-1.5%;
Sodium citrate 1.0-1.5%;
Essence 0-5.0%;
Surplus is water.
The shampoo that contains marine organisms degerming composition of present embodiment, owing to contain marine organisms bacteria remover composition, therefore, after the use, effectively degerming, and then have antipruritic and effect anti-dandruff, and owing to this each component that contains the shampoo of marine organisms degerming composition is nontoxic, non-stimulated, the free from corrosion material of skin, so this shampoo also has non-stimulated, the free from corrosion advantage of hair and hair.
In the present embodiment, in order to obtain better antipruritic and anti-dandruff effect, the described shampoo that contains marine organisms degerming composition, percent meter proportioning is as follows by weight:
Marine organisms bacteria remover 2.5-3.5%;
Alkyl polyglucoside 9.0-13.0%;
Cocamido propyl betaine 8.0-9.0%;
Cocoanut fatty acid diethanolamide 7.0-9.0%;
Alkyl-dimethyl based polysiloxane 1.0-1.5%;
Sodium chloride 1.1-1.4%;
Sodium citrate 1.1-1.4%;
Essence 0.5-2.0%;
Surplus is water.
In the present embodiment, in order to obtain better antipruritic and anti-dandruff effect, preferred, described marine organisms bacteria remover by weight percent meter proportioning is as follows:
Carboxymethyl chitosan 1.0 ~ 2.0%;
Sargassum polysaccharides 2.0 ~ 4.0%;
Cecropin 6.0 ~ 8.0%;
N-acetylmuramide lycanohydrlase 1.5 ~ 3.5%;
Water 82.5 ~ 89.5%.
In the present embodiment, preferred, described essence is plant essence.
In the present embodiment, for the mixed effect that makes each component better, described hydromining pure water.
It is the cecropin described in the CN101104637B that described cecropin can adopt notification number, can certainly adopt other cecropin.
Described marine organisms bacteria remover can prepare as follows:
Step S10: add carboxymethyl chitosan and the Sargassum polysaccharides of proportional quantity in 30 ~ 35 ℃ the water, mix 10 ~ 20 minutes mixed liquor A;
Step S20: add the cecropin of proportional quantity in the mixed liquor A, the time that mixes be 3 ~ 7 minutes mixed liquid B;
Step S30: add the N-acetylmuramide lycanohydrlase of proportional quantity in the mixed liquid B, mix 3 ~ 7 minutes described degerming marine organisms bacteria remover.
Embodiment 2
Present embodiment provides a kind of preparation method for the shampoo that contains marine organisms degerming composition described in the embodiment 1, may further comprise the steps:
Step S10: add alkyl polyglucoside, cocamido propyl betaine, cocoanut fatty acid diethanolamide, the alkyl-dimethyl based polysiloxane of proportional quantity in 35-40 ℃ the water, carry out emulsifying under the stirring condition and get mixed liquor A;
Step S20: add the marine organisms bacteria remover of proportional quantity in the mixed liquor A, under 25-35 ℃ of temperature conditions, mix to get institute's mixed liquid B;
Step S30: add sodium citrate, sodium chloride and the essence of proportional quantity in the mixed liquid B, mix homogeneously gets the described shampoo that contains marine organisms degerming composition.
The preparation method of the shampoo that contains marine organisms degerming composition of present embodiment, because order by merging and the mixing condition of each material are comparatively reasonable, so that each the component mix homogeneously of the shampoo that contains marine organisms degerming composition that makes by preparation method of the present invention, good stability.
In the present embodiment, obtain better mixed effect in order to make each component, among the described step S10, the temperature of described water is 40 ℃, and carrying out emulsification times under the stirring condition is 15-25 minute.
In the present embodiment, obtain better mixed effect in order to make each component, among the described step S20, the time that mixes is 3-7 minute.
In the present embodiment, obtain better mixed effect in order to make each component, among the described step S30, the time that mixes is 7-12 minute.
In the present embodiment, in order to obtain portable shampoo, after step S30, also comprise step S40: after will containing the shampoo cooling of marine organisms degerming composition, carry out packing.
Embodiment 3
Present embodiment provides a kind of shampoo that contains marine organisms degerming composition, and percent meter proportioning is as follows by weight:
Marine organisms bacteria remover 4.0%;
Alkyl polyglucoside 14.0%;
Cocamido propyl betaine 10.0%;
Cocoanut fatty acid diethanolamide 10.0%;
Alkyl-dimethyl based polysiloxane 2.0%;
Sodium chloride 1.5%;
Sodium citrate 1.5%;
Essence 5.0%;
Surplus is water.
Marine organisms bacteria remover in the present embodiment by weight percent meter proportioning is: carboxymethyl chitosan 1.0%; Sargassum polysaccharides 2.0%; Cecropin 6.0%; N-acetylmuramide lycanohydrlase 1.5%; Water 89.5%.
The preparation method of the shampoo that contains marine organisms degerming composition of present embodiment is carried out as follows:
Step S301: add alkyl polyglucoside, cocamido propyl betaine, cocoanut fatty acid diethanolamide, the alkyl-dimethyl based polysiloxane of proportional quantity in 35 ℃ the water, carry out under the stirring condition emulsifying 15 minutes mixed liquor A;
Step S302: add the marine organisms bacteria remover of proportional quantity in the mixed liquor A, under 25 ℃ of temperature conditions, mix 3 minutes institute's mixed liquid B;
Step S303: add sodium citrate, sodium chloride and the essence of proportional quantity in the mixed liquid B, mixes 7 minutes must the described shampoo that contains marine organisms degerming composition.
Through experiment, the shampoo that contains marine organisms degerming composition of present embodiment can be effectively antipruritic, anti-dandruff, and after using,, nothing corrosion non-stimulated to head, hair is submissiveer.
Embodiment 4
Present embodiment provides a kind of shampoo that contains marine organisms degerming composition, and percent meter proportioning is as follows by weight: marine organisms bacteria remover 2.0%;
Alkyl polyglucoside 8.0%;
Cocamido propyl betaine 7.0%;
Cocoanut fatty acid diethanolamide 6.0%;
Alkyl-dimethyl based polysiloxane 0.5%;
Sodium chloride 1.0%;
Sodium citrate 1.0%;
Surplus is water.
Marine organisms bacteria remover in the present embodiment by weight percent meter proportioning is: carboxymethyl chitosan 2.0%; Sargassum polysaccharides 4.0%; Cecropin 8.0%; N-acetylmuramide lycanohydrlase 3.5%; Water 82.5%.
The preparation method of the shampoo that contains marine organisms degerming composition of present embodiment is carried out as follows:
Step S401: add alkyl polyglucoside, cocamido propyl betaine, cocoanut fatty acid diethanolamide, the alkyl-dimethyl based polysiloxane of proportional quantity in 35 ℃ the water, carry out under the stirring condition emulsifying 25 minutes mixed liquor A;
Step S402: add the marine organisms bacteria remover of proportional quantity in the mixed liquor A, under 25 ℃ of temperature conditions, mix 7 minutes institute's mixed liquid B;
Step S403: add sodium citrate, sodium chloride and the essence of proportional quantity in the mixed liquid B, mixes 12 minutes must the described shampoo that contains marine organisms degerming composition.
Step S404: after will containing the shampoo cooling of marine organisms degerming composition, carry out packing.
Through experiment, the shampoo that contains marine organisms degerming composition of present embodiment can be effectively antipruritic, anti-dandruff, and after using,, nothing corrosion non-stimulated to head, hair is submissiveer.
Embodiment 5
Present embodiment provides a kind of shampoo that contains marine organisms degerming composition, and percent meter proportioning is as follows by weight:
Marine organisms bacteria remover 3.5%;
Alkyl polyglucoside 13.0%;
Cocamido propyl betaine 9.0%;
Cocoanut fatty acid diethanolamide 9.0%;
Alkyl-dimethyl based polysiloxane 1.5%;
Sodium chloride 1.4%;
Sodium citrate 1.4%;
Essence 2.0%;
Surplus is water.
Marine organisms bacteria remover in the present embodiment by weight percent meter proportioning is: carboxymethyl chitosan 1.5%; Sargassum polysaccharides 3.0%; Cecropin 7.0%; N-acetylmuramide lycanohydrlase 2.0%; Water 86.5%.
The preparation method of the shampoo that contains marine organisms degerming composition of present embodiment is carried out as follows:
Step S501: add alkyl polyglucoside, cocamido propyl betaine, cocoanut fatty acid diethanolamide, the alkyl-dimethyl based polysiloxane of proportional quantity in 40 ℃ the water, carry out under the stirring condition emulsifying 20 minutes mixed liquor A;
Step S502: add the marine organisms bacteria remover of proportional quantity in the mixed liquor A, under 35 ℃ of temperature conditions, mix 5 minutes institute's mixed liquid B;
Step S503: add sodium citrate, sodium chloride and the essence of proportional quantity in the mixed liquid B, mixes 10 minutes must the described shampoo that contains marine organisms degerming composition.
Step S504: after will containing the shampoo cooling of marine organisms degerming composition, carry out packing.
Through experiment, the shampoo that contains marine organisms degerming composition of present embodiment can be effectively antipruritic, anti-dandruff, and after using,, nothing corrosion non-stimulated to head, hair is submissiveer.
Embodiment 6
Present embodiment provides a kind of shampoo that contains marine organisms degerming composition, and percent meter proportioning is as follows by weight:
Marine organisms bacteria remover 2.5%;
Alkyl polyglucoside 9.0%;
Cocamido propyl betaine 8.0%;
Cocoanut fatty acid diethanolamide 7.0%;
Alkyl-dimethyl based polysiloxane 1.0%;
Sodium chloride 1.1%;
Sodium citrate 1.1%;
Essence 0.5%;
Surplus is water.
Marine organisms bacteria remover in the present embodiment by weight percent meter proportioning is: carboxymethyl chitosan 1.5%; Sargassum polysaccharides 3.0%; Cecropin 7.0%; N-acetylmuramide lycanohydrlase 2.0%; Water 86.5%.
The preparation method of the shampoo that contains marine organisms degerming composition of present embodiment is carried out as follows:
Step S601: add alkyl polyglucoside, cocamido propyl betaine, cocoanut fatty acid diethanolamide, the alkyl-dimethyl based polysiloxane of proportional quantity in 38 ℃ the water, carry out under the stirring condition emulsifying 20 minutes mixed liquor A;
Step S602: add the marine organisms bacteria remover of proportional quantity in the mixed liquor A, under 35 ℃ of temperature conditions, mix 5 minutes institute's mixed liquid B;
Step S603: add sodium citrate, sodium chloride and the essence of proportional quantity in the mixed liquid B, mixes 10 minutes must the described shampoo that contains marine organisms degerming composition.
Step S604: after will containing the shampoo cooling of marine organisms degerming composition, carry out packing.
Through experiment, the shampoo that contains marine organisms degerming composition of present embodiment can be effectively antipruritic, anti-dandruff, and after using,, nothing corrosion non-stimulated to head, hair is submissiveer.
Pharmacodynamics research of the present invention:
One, verify antipruritic and antibacterial action of the present invention from the zoopery aspect:
1 material
1.1 animal
Mice, regular grade, male and female half and half, body weight 18-22g, rat, male, body weight 180-220g.
1.2 medicine and reagent
Modeling reagent: depilatory cream: carrageenin: histamine phosphate; Dimethylbenzene.
Use medicine: the shampoo in the full example 5 of the invention process
Key instrument
Electronic balance, electric-heated thermostatic water bath, sufficient sole of the foot capacity measurer
2 methods and result
2.1 itching-relieving action:
Get 20 of mices and be divided at random two groups, 10 every group, male and female half and half are respectively matched group, test group.24h before the experiment shaves hair to each right back instep of group Cavia porcellus, smears 1 time each 5 seconds with cotton swab.Test the same day, abrade right back foot with coarse sandpaper and shave hair place, area 1c ㎡.Smear 1 time with cotton swab the part, and each 5 seconds 1 time, beginning is only dripped 0.01% 0.05ml/ of histamine phosphate behind the 10min at the wound surface place, after this every 3min0.02%, and 0.03% ... progressive concentration only is 0.05ml/ at every turn.Until later licking the right back histamine phosphate's total amount (μ g) that gives when sufficient, Cavia porcellus is itch-threshold.Record and itch-threshold of relatively respectively organizing.The result shows: dehumidifying itching-relieving gels group itch-threshold (321 ± 350.8) μ g, compare P＜0.01 with matrix group (55 ± 47.2) μ g.As seen product of the present invention has the effect of pruritus due to the obvious antagonism histamine phosphate.
2.2 bacteriostasis
Carry out external susceptibility MIC test:
Test strain: fungus, Candida albicans, staphylococcus aureus, Escherichia coli.
Method: each test strain is made bacteria suspension with normal saline, and to be diluted to turbidity be the above bacteria suspension of 2.0McF, use again 100 times of normal saline dilutions, 10 times of RPMII640 dilutions, test group (shampoo in the embodiment of the invention 5) and matched group (health king's washing liquid) doubling dilution, cultivate 72-96h in 96 well culture plates, slight concussion, the 490nm place carries out photoelectric colorimetry.
Table 1
2.3 conclusion
Referring to table 1, the present invention has the inhibitory action (P＜0.05 or P＜0.01) of highly significant to the guinea pig skin pruritus test due to the histamine phosphate; Have a look at out through external susceptibility MIC test: the present invention all has stronger antibacterial action to fungus, Candida albicans, staphylococcus aureus, Escherichia coli.
More than test shows: the present invention has the effect of antipruritic antibacterial, therefore, above each microbial dandruff is also had the effect of removal.
The main clinical research of the present invention:
The shampoo of getting among the embodiment of the invention 3, embodiment 4, embodiment 5, the embodiment 6 is tested, occupation mode be per two days once, duration is 16 days, the results are shown in Table 2, as seen the shampoo that contains marine organisms degerming composition of the present invention has effect antipruritic, anti-dandruff, and, nothing corrosion non-stimulated to scalp, hair is submissive after using.
Table 2
It should be noted that at last: above embodiment only in order to technical scheme of the present invention to be described, is not intended to limit; Although with reference to previous embodiment the present invention is had been described in detail, those of ordinary skill in the art is to be understood that: it still can be made amendment to the technical scheme that aforementioned each embodiment puts down in writing, and perhaps part technical characterictic wherein is equal to replacement; And these modifications or replacement do not make the essence of appropriate technical solution break away from the spirit and scope of various embodiments of the present invention technical scheme.
Claims (10)
1. a shampoo that contains marine organisms degerming composition is characterized in that, percent meter proportioning is as follows by weight:
Marine organisms bacteria remover 2.0-4.0%;
Alkyl polyglucoside 8.0-14.0%;
Cocamido propyl betaine 7.0-10.0%;
Cocoanut fatty acid diethanolamide 6.0-10.0%;
Alkyl-dimethyl based polysiloxane 0.5-2.0%;
Sodium chloride 1.0-1.5%;
Sodium citrate 1.0-1.5%;
Essence 0-5.0%;
Surplus is water.
2. the shampoo that contains marine organisms degerming composition according to claim 1 is characterized in that, percent meter proportioning is as follows by weight:
Marine organisms bacteria remover 2.5-3.5%;
Alkyl polyglucoside 9.0-13.0%;
Cocamido propyl betaine 8.0-9.0%;
Cocoanut fatty acid diethanolamide 7.0-9.0%;
Alkyl-dimethyl based polysiloxane 1.0-1.5%;
Sodium chloride 1.1-1.4%;
Sodium citrate 1.1-1.4%;
Essence 0.5-2.0%;
Surplus is water.
3. the shampoo that contains marine organisms degerming composition according to claim 1 and 2 is characterized in that, described marine organisms bacteria remover by weight percent meter proportioning is as follows:
Carboxymethyl chitosan 1.0 ~ 2.0%;
Sargassum polysaccharides 2.0 ~ 4.0%;
Cecropin 6.0 ~ 8.0%;
N-acetylmuramide lycanohydrlase 1.5 ~ 3.5%;
Water 82.5 ~ 89.5%.
4. the shampoo that contains marine organisms degerming composition according to claim 1 and 2 is characterized in that, described essence is plant essence.
5. the shampoo that contains marine organisms degerming composition according to claim 1 and 2 is characterized in that, described water pure water.
6. one kind such as each described preparation method that contains the shampoo of marine organisms degerming composition of claim 1-5, it is characterized in that, may further comprise the steps:
Step S10: add alkyl polyglucoside, cocamido propyl betaine, cocoanut fatty acid diethanolamide, the alkyl-dimethyl based polysiloxane of proportional quantity in 35-40 ℃ the water, carry out emulsifying under the stirring condition and get mixed liquor A;
Step S20: add the marine organisms bacteria remover of proportional quantity in the mixed liquor A, under 25-35 ℃ of temperature conditions, mix to get institute's mixed liquid B;
Step S30: add sodium citrate, sodium chloride and the essence of proportional quantity in the mixed liquid B, mix homogeneously gets the described shampoo that contains marine organisms degerming composition.
7. the preparation method that contains the shampoo of marine organisms degerming composition according to claim 6, it is characterized in that: among the described step S10, the temperature of described water is 40 ℃, carrying out emulsification times under the stirring condition is 15-25 minute.
8. the preparation method that contains the shampoo of marine organisms degerming composition according to claim 6, it is characterized in that: among the described step S20, the time that mixes is 3-7 minute.
9. the preparation method that contains the shampoo of marine organisms degerming composition according to claim 6, it is characterized in that: among the described step S30, the time that mixes is 7-12 minute.
10. the preparation method that contains the shampoo of marine organisms degerming composition according to claim 6 is characterized in that: after step S30, also comprise step S40: after will containing the shampoo cooling of marine organisms degerming composition, carry out packing.
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