CN103690404B - Baby bath agent containing marine biomaterial and compositions, preparation method - Google Patents
Baby bath agent containing marine biomaterial and compositions, preparation method Download PDFInfo
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- CN103690404B CN103690404B CN201310719933.1A CN201310719933A CN103690404B CN 103690404 B CN103690404 B CN 103690404B CN 201310719933 A CN201310719933 A CN 201310719933A CN 103690404 B CN103690404 B CN 103690404B
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Abstract
The invention discloses a kind of the baby bath agent and compositions, the preparation method that contain marine biomaterial, comprise the component of following weight percentage: marine biological sterilization agent 2.0-4.0%; Sargassum polysaccharides 5.0-10.0%; Chitin 1.0-2.0%; Alkyl polyglucoside 9.0-15.0%; Cocamido propyl betaine 4.0-8.0%; Alcohol ether carboxylate 11.0-16.0%; Sodium chloride 1.0-1.5%; Citric acid 0.5%-2.0%; Edible essence 0.5-2.0%; Surplus is pure water.This preparation method comprises: in pure water, add alkyl polyglucoside, cocamido propyl betaine and alcohol ether carboxylate, stirs, carries out emulsifying, obtain mixed liquor A; In mixed liquor A, add marine biological sterilization agent, Sargassum polysaccharides and chitin, be uniformly mixed, obtain mixed liquid B; In mixed liquid B, add sodium chloride, citric acid and edible essence, be uniformly mixed, obtain the baby bath agent containing marine biomaterial.The baby bath agent of marine biomaterial of the present invention does not contain antiseptic, to infant skin without pessimal stimulation.
Description
Technical field
The present invention relates to bath preparation, particularly relate to a kind of the baby bath agent and compositions, the preparation method that contain marine biomaterial.
Background technology
At present, the kind of existing baby bath articles for use is a lot, and main adding ingredient is: surfactant and antiseptic.Infant skin has skin thin, and lipid is few, and skin resistance is poor, the feature that metabolism is fast, bath article as strong in frequent thigmic stimulus, can cause pessimal stimulation, cause xerosis cutis, dermatitis, eczema or allergic phenomena babies skin.
Summary of the invention
Provide hereinafter about brief overview of the present invention, to provide about the basic comprehension in some of the present invention.Should be appreciated that this general introduction is not summarize about exhaustive of the present invention.It is not that intention determines key of the present invention or pith, and nor is it intended to limit the scope of the present invention.Its object is only provide some concept in simplified form, in this, as the preorder in greater detail discussed after a while.
The object of the embodiment of the present invention is the defect for above-mentioned prior art, provides one not containing antiseptic, to the baby bath agent containing marine biomaterial of infant skin without pessimal stimulation.
Another object of the present invention is to provide a kind of preparation method of the baby bath agent containing marine biomaterial.
To achieve these goals, the technical scheme that the present invention takes is:
The invention provides a kind of compositions for the baby bath agent containing marine biomaterial, comprise the component of following weight percentage:
The present invention also provides a kind of method using the above-mentioned baby bath agent of compositions preparation containing marine biomaterial, comprises the following steps:
Step S10: add the alkyl polyglucoside of proportional quantity, cocamido propyl betaine and alcohol ether carboxylate in pure water, stirs, carries out emulsifying, obtain mixed liquor A;
Step S20: add the marine biological sterilization agent of proportional quantity, Sargassum polysaccharides and chitin in mixed liquor A, be uniformly mixed, obtain mixed liquid B;
Step S30: add the sodium chloride of proportional quantity, citric acid and edible essence in mixed liquid B, mix homogeneously obtains the baby bath agent containing marine biomaterial.
The present invention also provides a kind of baby bath agent containing marine biomaterial prepared according to above-mentioned method.
Compared with prior art, the invention has the beneficial effects as follows:
Baby bath agent containing marine biomaterial of the present invention, due to containing marine biological sterilization agent composition, therefore, after using, can be effectively degerming, and then the interpolation of alternative antiseptic there is antibacterial action.
The Sargassum polysaccharides contained and chitin are known marine biomaterial, as natural immunostimulant, not only can the immunity of enhancing body and the ability of resist the disease, and the generation of body patience can be reduced, promote the growth of animal, the complexation of Sargassum polysaccharides and mineral element, can not only improve the utilization rate of mineral element, reduce residual, can also cooperative effect be produced.Simultaneously; Sargassum polysaccharides is a kind of excellent emollient; its active matter mass-energy is combined the gel forming moisture retention with skin protein; and it can also form protecting film by hydration on the surface of skin; prevent moisture from evaporating; there is obvious moisture-keeping function, therefore, well can protect the tender and lovely skin of baby.
The preparation method of the baby bath agent containing marine biomaterial of the present invention, due to the order by merging of each material and mixing condition comparatively reasonable, make each component mix homogeneously of baby bath agent containing marine biomaterial obtained by preparation method of the present invention, good stability.
Detailed description of the invention
For making the object of the embodiment of the present invention, technical scheme and advantage clearly, be clearly and completely described below to the technical scheme in the embodiment of the present invention, obviously, described embodiment is the present invention's part embodiment, instead of whole embodiments.The element described in one embodiment of the invention and feature can combine with the element shown in one or more embodiment and feature.It should be noted that for purposes of clarity, in explanation, eliminate expression and the description of unrelated to the invention, parts known to persons of ordinary skill in the art and process.Based on the embodiment in the present invention, those of ordinary skill in the art, not paying the every other embodiment obtained under creative work prerequisite, belong to the scope of protection of the invention.
The invention provides a kind of compositions for the baby bath agent containing marine biomaterial, comprise the component of following weight percentage:
Edible essence of the present invention can select edible strawberry essence, edible apple essence or edible Fructus Citri Limoniae essence.
Baby bath agent containing marine biomaterial of the present invention, due to containing marine biological sterilization agent composition, therefore, can substitute the interpolation of chemical preservative completely, the Sargassum polysaccharides contained and chitin effectively can moisten infant skin.
The surfactant selected by baby bath agent containing marine biomaterial of the present invention is all environment-friendly type, the novel surfactant non-stimulated to skin, and therefore, bath shampoo of the present invention is non-stimulated to infant skin.
In the present embodiment, in order to obtain better antibacterial and antiseptic effect, optionally, for the compositions of the baby bath agent containing marine biomaterial, comprise the component of following weight percentage:
Preferred technical scheme: for the compositions of the baby bath agent containing marine biomaterial, comprise the component of following weight percentage:
Each component of the present invention is not containing antiseptic, and be applicable to baby, to infant skin without pessimal stimulation, scientific formulation is reasonable.
In the present embodiment, in order to obtain bacteria-eliminating efficacy of better sterilizing, optionally, described marine biological sterilization agent percentage proportioning is as follows:
In the present embodiment, in order to make the mixed effect of each component better, described hydromining pure water.
Described cecropin can adopt notification number for the cecropin described in CN101104637B, can certainly adopt other cecropin.
The present invention also provides a kind of method using the above-mentioned baby bath agent of compositions preparation containing marine biomaterial, comprises the following steps:
Step S10: add the alkyl polyglucoside of proportional quantity, cocamido propyl betaine and alcohol ether carboxylate in pure water, stirs, carries out emulsifying, obtain mixed liquor A;
Step S20: add the marine biological sterilization agent of proportional quantity, Sargassum polysaccharides and chitin in mixed liquor A, be uniformly mixed, obtain mixed liquid B;
Step S30: add the sodium chloride of proportional quantity, citric acid and edible essence in mixed liquid B, mix homogeneously obtains the baby bath agent containing marine biomaterial.
The preparation method of the baby bath agent containing marine biomaterial of the present embodiment, due to the order by merging of each material and mixing condition reasonable, make each component mix homogeneously of baby bath agent containing marine biomaterial obtained by preparation method of the present invention, good stability.
Preferably, described marine biological sterilization agent is prepared as follows:
Step S101: the carboxymethyl chitosan and the Sargassum polysaccharides that add proportional quantity in the water of 30 ~ 35 DEG C, carries out stirring and obtains the first mixed liquor in 10 ~ 20 minutes;
Step S102: the cecropin adding proportional quantity in the first mixed liquor, stirs and obtains the second mixed liquor in 3 ~ 7 minutes;
Step S103: the N-acetylmuramide lycanohydrlase adding proportional quantity in the second mixed liquor, stirs and within 3 ~ 7 minutes, obtains described degerming marine biological sterilization agent.
In the present embodiment, in order to make each component obtain better mixed effect, in described step S10: the temperature of described pure water is 40-50 DEG C, the time of stirring is 30-40 minute, and the speed of stirring is 80-90 rev/min.
In the present embodiment, in order to make each component obtain better mixed effect, in described step S20: the temperature of stirring is 25-35 DEG C, the time of stirring is 15-20 minute, and the speed of stirring is 70-80 rev/min; In described step S30: the time of stirring is 10-15 minute, the speed of stirring is 70-80 rev/min.
In the present embodiment, in order to obtain portable shampoo, after step S30, also comprise step S40: after the baby bath agent cooling containing marine biomaterial, carry out subpackage.
The present invention also provides a kind of baby bath agent containing marine biomaterial prepared according to above-mentioned method.
Below by specific embodiment, the present invention is further illustrated:
Embodiment 1
The present embodiment provides a kind of baby bath agent containing marine biomaterial, and percentage proportioning is as follows:
The edible essence that the embodiment of the present invention is added can select the essence added in shampoo in prior art or bath gel.Preferably edible apple essence.
Marine biological sterilization agent percentage proportioning in the present embodiment is: carboxymethyl chitosan 1.5%; Sargassum polysaccharides 3.0%; Cecropin 7.0%; N-acetylmuramide lycanohydrlase 2.0%; Water 86.5%.
Marine biological sterilization agent is prepared as follows:
Step S101: the carboxymethyl chitosan and the Sargassum polysaccharides that add proportional quantity in the water of 32 DEG C, carries out stirring and obtains the first mixed liquor in 15 minutes;
Step S102: the cecropin adding proportional quantity in the first mixed liquor, stirs and obtains the second mixed liquor in 6 minutes;
Step S103: the N-acetylmuramide lycanohydrlase adding proportional quantity in the second mixed liquor, stirs and within 5 minutes, obtains described degerming marine biological sterilization agent.
The preparation method of the baby bath agent containing marine biomaterial of the present embodiment is carried out as follows:
Step S10: add the alkyl polyglucoside of proportional quantity, cocamido propyl betaine, alcohol ether carboxylate AEC in the pure water of 45 DEG C is 85 revs/min with speed.Stir 35 minutes, carry out emulsifying and obtain mixed liquor A;
Step S20: add the marine biological sterilization agent of proportional quantity, Sargassum polysaccharides and chitin in mixed liquor A, at 35 DEG C, is 75 revs/min with speed.Stir 15 minutes, mix homogeneously obtains mixed liquid B;
Step S30: add the sodium chloride of proportional quantity, citrin and edible apple essence in mixed liquid B is 75 revs/min with speed.Stir 15 minutes, mix homogeneously obtains the baby bath agent containing marine biomaterial.
Through experiment, the baby bath agent containing marine biomaterial of the present embodiment can effectively decontamination, antibacterial, and after use, non-stimulated to skin, skin-moisturizing, skin is good.
Embodiment 2
The present embodiment provides a kind of baby bath agent containing marine biomaterial, and percentage proportioning is as follows:
Marine biological sterilization agent percentage proportioning in the present embodiment is: carboxymethyl chitosan 2.0%; Sargassum polysaccharides 4.0%; Cecropin 8.0%; N-acetylmuramide lycanohydrlase 3.5%; Water 82.5%.The present embodiment adopts Chinese notification number for the cecropin described in CN101104637B.
Marine biological sterilization agent is prepared as follows:
Step S101: the carboxymethyl chitosan and the Sargassum polysaccharides that add proportional quantity in the water of 30 DEG C, carries out stirring and obtains the first mixed liquor in 10 minutes;
Step S102: the cecropin adding proportional quantity in the first mixed liquor, stirs and obtains the second mixed liquor in 7 minutes;
Step S103: the N-acetylmuramide lycanohydrlase adding proportional quantity in the second mixed liquor, stirs and within 3 minutes, obtains described degerming marine biological sterilization agent.
The preparation method of the baby bath agent containing marine biomaterial of the present embodiment is carried out as follows:
Step S10: add the alkyl polyglucoside of proportional quantity, cocamido propyl betaine, alcohol ether carboxylate AEC in the pure water of 40 DEG C is 80 revs/min with speed, stirs 40 minutes, carries out emulsifying and obtain mixed liquor A;
Step S20: add the marine biological sterilization agent of proportional quantity, Sargassum polysaccharides and chitin in mixed liquor A, at 28 DEG C, is 80 revs/min with speed, and stir 13 minutes, mix homogeneously obtains mixed liquid B;
Step S30: add the sodium chloride of proportional quantity, citrin and edible strawberry essence in mixed liquid B is 70 revs/min with speed, and stir 14 minutes, mix homogeneously obtains the baby bath agent containing marine biomaterial.
Through test, the baby bath agent containing marine biomaterial of the present embodiment, smooth with rear skin.
Embodiment 3
The present embodiment provides a kind of baby bath agent containing marine biomaterial, and percentage proportioning is as follows:
Marine biological sterilization agent percentage proportioning in the present embodiment is: carboxymethyl chitosan 1.0%; Sargassum polysaccharides 2.0%; Cecropin 6.0%; N-acetylmuramide lycanohydrlase 1.5%; Water 89.5%.
Marine biological sterilization agent is prepared as follows:
Step S101: the carboxymethyl chitosan and the Sargassum polysaccharides that add proportional quantity in the water of 35 DEG C, carries out stirring and obtains the first mixed liquor in 20 minutes;
Step S102: the cecropin adding proportional quantity in the first mixed liquor, stirs and obtains the second mixed liquor in 3 minutes;
Step S103: the N-acetylmuramide lycanohydrlase adding proportional quantity in the second mixed liquor, stirs and within 7 minutes, obtains described degerming marine biological sterilization agent.
The preparation method of the baby bath agent containing marine biomaterial of the present embodiment is carried out as follows:
Step S10: add the alkyl polyglucoside of proportional quantity, cocamido propyl betaine, alcohol ether carboxylate AEC in the pure water of 50 DEG C is 90 revs/min with speed, stirs 30 minutes, carries out emulsifying and obtain mixed liquor A;
Step S20: add the marine biological sterilization agent of proportional quantity, Sargassum polysaccharides and chitin in mixed liquor A, at 25 DEG C, is 70 revs/min with speed, and stir 20 minutes, mix homogeneously obtains mixed liquid B;
Step S30: add the sodium chloride of proportional quantity, citrin and edible Fructus Citri Limoniae essence in mixed liquid B is 80 revs/min with speed, and stir 10 minutes, mix homogeneously obtains the baby bath agent containing marine biomaterial.
Through experiment, the baby bath agent containing marine biomaterial of the present embodiment can effectively decontamination, antibacterial, and after use, non-stimulated to infant skin, moistening effect is good.
Pharmacodynamics research of the present invention:
Antibacterial action of the present invention is verified from zoopery aspect:
1, material
Animal mice, regular grade, male and female half and half, body weight 18-22g, rat, male, body weight 180-220g.
2, external susceptibility minimum inhibitory concentration MIC determination test is carried out:
Test strain: fungus, Candida albicans, staphylococcus aureus, Escherichia coli.
Method: each test strain normal saline is made bacteria suspension, and to be diluted to turbidity be more than 2.0McF bacteria suspension, use normal saline dilution 100 times again, rev/min Ii640 culture fluid releases 10 times, test group (bath shampoo in the embodiment of the present invention 1) and matched group (baby Jinsui River bath gel) doubling dilution, cultivate 72-96h in 96 well culture plates, slightly shake, 490nm place carries out photoelectric colorimetry.
Table 1
2.3 conclusion
See table 1, can find out through external susceptibility MIC test: the present invention all has stronger antibacterial action to fungus, Candida albicans, staphylococcus aureus, Escherichia coli.
More than test shows: the present invention has antibacterial action, the interpolation of alternative antiseptic.
State in each embodiment on the invention, the sequence number of embodiment is only convenient to describe, and does not represent the quality of embodiment.The description of each embodiment is all emphasized particularly on different fields, in certain embodiment, there is no the part described in detail, can see the associated description of other embodiments.
In the embodiments such as apparatus and method of the present invention, obviously, each parts or each step reconfigure after can decomposing, combine and/or decomposing.These decompose and/or reconfigure and should be considered as equivalents of the present invention.Simultaneously, above in the description of the specific embodiment of the invention, the feature described for a kind of embodiment and/or illustrate can use in one or more other embodiment in same or similar mode, combined with the feature in other embodiment, or substitute the feature in other embodiment.
Should emphasize, term " comprises/comprises " existence referring to feature, key element, step or assembly when using herein, but does not get rid of the existence or additional of one or more further feature, key element, step or assembly.
Although last it is noted that described the present invention and advantage thereof in detail above, be to be understood that and can carry out various change when not exceeding the spirit and scope of the present invention limited by appended claim, substituting and converting.And scope of the present invention is not limited only to the specific embodiment of process, equipment, means, method and step described by description.One of ordinary skilled in the art will readily appreciate that from disclosure of the present invention, can use perform the function substantially identical with corresponding embodiment described herein or obtain and its substantially identical result, existing and that will be developed in the future process, equipment, means, method or step according to the present invention.Therefore, appended claim is intended to comprise such process, equipment, means, method or step in their scope.
Claims (8)
1. for a compositions for the baby bath agent containing marine biomaterial, it is characterized in that, comprise the component of following weight percentage:
Described marine biological sterilization agent percentage proportioning is as follows:
2. the compositions for the baby bath agent containing marine biomaterial according to claim 1, is characterized in that, comprise the component of following weight percentage:
3. the compositions for the baby bath agent containing marine biomaterial according to claim 1, is characterized in that, comprise the component of following weight percentage:
4. use a method for the baby bath agent of compositions preparation containing marine biomaterial described in any one of claim 1-3, it is characterized in that, comprise the following steps:
Step S10: add the alkyl polyglucoside of proportional quantity, cocamido propyl betaine and alcohol ether carboxylate in pure water, stirs, carries out emulsifying, obtain mixed liquor A;
In described step S10: the temperature of described pure water is 40-50 DEG C, the time of stirring is 30-40 minute, and the speed of stirring is 80-90 rev/min;
Step S20: add the marine biological sterilization agent of proportional quantity, Sargassum polysaccharides and chitin in mixed liquor A, be uniformly mixed, obtain mixed liquid B;
Step S30: add the sodium chloride of proportional quantity, citric acid and edible essence in mixed liquid B, be uniformly mixed, obtains the baby bath agent containing marine biomaterial.
5. method according to claim 4, is characterized in that, described marine biological sterilization agent is prepared as follows:
Step S101: the carboxymethyl chitosan and the Sargassum polysaccharides that add proportional quantity in the water of 30 ~ 35 DEG C, carries out stirring and obtains the first mixed liquor in 10 ~ 20 minutes;
Step S102: the cecropin adding proportional quantity in the first mixed liquor, stirs and obtains the second mixed liquor in 3 ~ 7 minutes;
Step S103: the N-acetylmuramide lycanohydrlase adding proportional quantity in the second mixed liquor, stirs and within 3 ~ 7 minutes, obtains described degerming marine biological sterilization agent.
6. the method according to claim 4 or 5, is characterized in that, in described step S20: the temperature of stirring is 25-35 DEG C, and the time of stirring is 15-20 minute, and the speed of stirring is 70-80 rev/min; Or/and; In described step S30: the time of stirring is 10-15 minute, the speed of stirring is 70-80 rev/min.
7. the method according to claim 4 or 5, is characterized in that, after step S30, also comprises step S40: after the baby bath agent cooling containing marine biomaterial, carry out subpackage.
8. the baby bath agent containing marine biomaterial prepared according to the method described in any one of claim 4-7.
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| CN201310719933.1A CN103690404B (en) | 2013-12-23 | 2013-12-23 | Baby bath agent containing marine biomaterial and compositions, preparation method |
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| CN201310719933.1A CN103690404B (en) | 2013-12-23 | 2013-12-23 | Baby bath agent containing marine biomaterial and compositions, preparation method |
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| CN103690404A CN103690404A (en) | 2014-04-02 |
| CN103690404B true CN103690404B (en) | 2016-04-20 |
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| CN106176380A (en) * | 2016-08-11 | 2016-12-07 | 王君 | A kind of enzyme natural ecological bath lotion |
| CN111743817A (en) * | 2020-08-20 | 2020-10-09 | 广州荃智美肤生物科技研究院有限公司 | Children washing and protecting composition containing algal polysaccharide |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103027857A (en) * | 2012-12-25 | 2013-04-10 | 青岛海芬海洋生物科技有限公司 | Shampoo containing marine biological degerming components and preparation method of shampoo |
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Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103027857A (en) * | 2012-12-25 | 2013-04-10 | 青岛海芬海洋生物科技有限公司 | Shampoo containing marine biological degerming components and preparation method of shampoo |
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