CN103013695B - Degerming laundry detergent containing marine organism degerming component and preparation method of degerming laundry detergent - Google Patents
Degerming laundry detergent containing marine organism degerming component and preparation method of degerming laundry detergent Download PDFInfo
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- CN103013695B CN103013695B CN201210559662.3A CN201210559662A CN103013695B CN 103013695 B CN103013695 B CN 103013695B CN 201210559662 A CN201210559662 A CN 201210559662A CN 103013695 B CN103013695 B CN 103013695B
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Abstract
The invention discloses a degerming laundry detergent containing a marine organism degerming component and a preparation method of the degerming laundry detergent. The degerming laundry detergent comprises the following components by weight percentage: 2.0-3.5% of marine organism degerming agent, 10.0-13.0% of coconut oil fatty acid diethanol amide, 4.0-6.0% of alkyl glycoside, 6.0-8.0% of fatty alcohol polyoxyethylene ether sodium sulfate, 0.5-1.0% of disodium EDTA (ethylene diamine tetraacetic acid), 0.5-1.0% of sodium chloride, 0-1.0% of essence and the balance of water. The degerming laundry detergent containing the marine organism degerming component can degerm effectively and has a strong dirt-removing ability.
Description
Technical field
The present invention relates to washing liquid, relate in particular to a kind of degerming washing liquid that contains marine organisms degerming composition and preparation method thereof.
Background technology
Along with the enhancing of people to health perception, can not meet cleaning efficacy only to cleaning of clothing, when clean clothing, energy degerming sterilization has become human consumer's first-selection, baby's skin is very tender and lovely, passive protective physical fitness is low, it is improper that washing liquid is selected, and skin and health more easily come to harm.On market, have and possess functional baby's washing liquid antibacterial, sterilization, but generally the disinfection composition of interpolation is chlorine-containing disinfectant, oxygen-containing disinfectant or contains alcohol disinfectant, and the tensio-active agent that these washing liquids adopt and sterilizing agent all have unpleasant irritating smell; Irritant to fabric and skin, be corrosive; Poor stability; Compatibleness with other raw materials is poor; To the shortcoming such as environment is unfriendly, very easily hurt the healthy of baby.
In Chinese patent, CN200710179670 discloses " antimicrobial laundry liquid of a kind of disinfecting and decontaminating simultaneously and preparation method thereof ", the composition for sterilization of announcing in formula is poly hexamethylene biguanide PHMB, be fatty alcohol-polyoxyethylene ether AEO-7 for clean tensio-active agent, fatty alcohol-polyoxyethylene ether AEO-9, fatty alcohol-polyoxyethylene ether AEO-5, fatty alcohol-polyoxyethylene ether XL-80, more than be nonionogenic tenside, this formula is subject to the impact of sterilization component to be subject to limitation in the selection of tensio-active agent, can only select similar fatty alcohol-polyoxyethylene ether nonionogenic tenside, therefore, the detersive power of this patent formulation has been subject to impact.
Summary of the invention
An object of the present invention is to provide one and there is sterilizing function, and the degerming washing liquid that contains marine organisms degerming composition of strong detergency.
Another object of the present invention is to provide one sterilizing function, and the preparation method of the degerming washing liquid that contains marine organisms degerming composition of strong detergency.
The degerming washing liquid that contains marine organisms degerming composition of the present invention, percentage ratio meter proportioning is as follows by weight:
Marine organisms degerming agent 2.0-3.5%;
Cocoanut fatty acid diethanolamide 10.0-13.0%;
Alkyl glycoside 4.0-6.0%;
Polyoxyethylenated alcohol sodium sulfate 6.0-8.0%;
Disodium ethylene diamine tetraacetate 0.5-1.0%;
Sodium-chlor 0.5-1.0%;
Essence 0-1.0%;
Surplus is water.
The preparation method of the degerming washing liquid that contains marine organisms degerming composition of the present invention, comprises the following steps:
Step S10: to the disodium ethylene diamine tetraacetate that adds proportional quantity in the water of 35 ~ 45 DEG C, be uniformly mixed to obtain mixed liquor A;
Step S20: add cocoanut fatty acid diethanolamide, alkyl glycoside and polyoxyethylenated alcohol sodium sulfate in mixed liquor A, be uniformly mixed to obtain mixed liquid B under the temperature condition of 35 ~ 45 DEG C;
Step S30: to the marine organisms degerming agent that adds proportional quantity in mixed liquid B, be uniformly mixed to obtain the mixed solution C of institute under 25 ~ 35 DEG C of temperature condition;
Step S40: to the sodium-chlor and the essence that add proportional quantity in mixed solution C, mix described in contain marine organisms degerming composition degerming washing liquid.
The degerming washing liquid that contains marine organisms degerming composition of the present invention not only has excellent bactericidal property, and strong detergency.Cocoanut fatty acid diethanolamide is nonionogenic tenside, has wetting, washing, the performance such as antistatic and soft, is good suds-stabilizing agent.Alkyl glycoside is the more comprehensive new non-ionic surfactants of a kind of performance, has the characteristic of common nonionic and anion surfactant concurrently, can complete biodegradable and to skin without any pungency.Polyoxyethylenated alcohol sodium sulfate is that anion surfactant has good decontamination, emulsification, foam performance.Disodium ethylene diamine tetraacetate belongs to sequestrant, can make stain remove rapidly surface tension, thereby dissolves, comes off.Sodium-chlor, as thickening material, can improve the adsorption of tensio-active agent to fabric, improves its detersive power, reduces the micelle-forming concentration of tensio-active agent.Therefore, owing to adopting marine organisms degerming agent in the present invention, unrestricted for the selection of tensio-active agent, contain ionogenic surfactant and nonionic surface active agent, overcome the defect of bactericidal liquid detergent of the prior art, there is the effect that soil removability is strong.
The preparation method of the degerming washing liquid that contains marine organisms degerming composition of the present invention, because order by merging and the mixing condition of each material are comparatively reasonable, the each component of degerming washing liquid that contains marine organisms degerming composition making by preparation method of the present invention is mixed, good stability.
Embodiment
Embodiment 1
A degerming washing liquid that contains marine organisms degerming composition, is characterized in that, percentage ratio meter proportioning is as follows by weight:
Marine organisms degerming agent 2.0-3.5%;
Cocoanut fatty acid diethanolamide 10.0-13.0%;
Alkyl glycoside 4.0-6.0%;
Polyoxyethylenated alcohol sodium sulfate 6.0-8.0%;
Disodium ethylene diamine tetraacetate 0.5-1.0%;
Sodium-chlor 0.5-1.0%;
Essence 0-1.0%;
Surplus is water.
The degerming washing liquid that contains marine organisms degerming composition of the present embodiment not only has excellent bactericidal property, and strong detergency.Cocoanut fatty acid diethanolamide is nonionogenic tenside, has wetting, washing, the performance such as antistatic and soft, is good suds-stabilizing agent.Alkyl glycoside is the more comprehensive new non-ionic surfactants of a kind of performance, has the characteristic of common nonionic and anion surfactant concurrently, can complete biodegradable and to skin without any pungency.Polyoxyethylenated alcohol sodium sulfate is that anion surfactant has good decontamination, emulsification, foam performance.Disodium ethylene diamine tetraacetate belongs to sequestrant, can make stain remove rapidly surface tension, thereby dissolves, comes off.Sodium-chlor, as thickening material, can improve the adsorption of tensio-active agent to fabric, improves its detersive power, reduces the micelle-forming concentration of tensio-active agent.Therefore, owing to adopting marine organisms degerming agent in the present invention, unrestricted for the selection of tensio-active agent, contain ionogenic surfactant and nonionic surface active agent, overcome the defect of bactericidal liquid detergent of the prior art, there is the effect that soil removability is strong.
In the present embodiment, in order to obtain better degerming and clean effect, the described degerming washing liquid that contains marine organisms degerming composition, is characterized in that, percentage ratio meter proportioning is as follows by weight:
Marine organisms degerming agent 2.5-3.0%;
Cocoanut fatty acid diethanolamide 11.0-12.0%;
Alkyl glycoside 4.5-5.5%;
Polyoxyethylenated alcohol sodium sulfate 6.5-7.5%;
Disodium ethylene diamine tetraacetate 0.6-0.8%;
Sodium-chlor 0.6-0.8%;
Essence 0.2-0.4%;
Surplus is water.
In the present embodiment, optional, in order to obtain the moderate degerming washing liquid that contains marine organisms degerming composition of fragrance, percentage ratio meter proportioning is as follows by weight for this degerming washing liquid that contains marine organisms degerming composition:
Marine organisms degerming agent 2.5-3.0%;
Cocoanut fatty acid diethanolamide 11.0-12.0%;
Alkyl glycoside 4.5-5.5%;
Polyoxyethylenated alcohol sodium sulfate 6.5-7.5%;
Disodium ethylene diamine tetraacetate 0.6-0.8%;
Sodium-chlor 0.6-0.8%;
Essence 0.2-0.4%;
Surplus is water.
In the present embodiment, in order to obtain better bacteria-eliminating efficacy, optional, described marine organisms degerming agent by weight percentage ratio meter proportioning is as follows:
Cm-chitosan 1.0 ~ 2.0%;
Sargassum polysaccharides 2.0 ~ 4.0%;
Cecropin 6.0 ~ 8.0%;
N-acetylmuramide lycanohydrlase 1.5 ~ 3.5%;
Water 82.5 ~ 89.5%.
In the present embodiment, in order to make the mixed effect of each component better, optional, described water is deionized water.
It is the cecropin described in CN101104637B that described cecropin can adopt notification number, can certainly adopt other cecropin.
Described marine organisms degerming agent can be prepared as follows:
Step S10: to the cm-chitosan and the Sargassum polysaccharides that add proportional quantity in the water of 30 ~ 35 DEG C, be uniformly mixed 10 ~ 20 minutes mixed liquor A;
Step S20: toward the cecropin that adds proportional quantity in mixed liquor A, the time being uniformly mixed be 3 ~ 7 minutes mixed liquid B;
Step S30: toward the N-acetylmuramide lycanohydrlase that adds proportional quantity in mixed liquid B, be uniformly mixed 3 ~ 7 minutes described degerming marine organisms degerming agent.
Embodiment 2
The present embodiment provides a kind of preparation method of the degerming washing liquid that contains marine organisms degerming composition for embodiment 1, it is characterized in that, comprises the following steps:
Step S10: to the disodium ethylene diamine tetraacetate that adds proportional quantity in the water of 35 ~ 45 DEG C, be uniformly mixed to obtain mixed liquor A;
Step S20: add cocoanut fatty acid diethanolamide, alkyl glycoside and polyoxyethylenated alcohol sodium sulfate in mixed liquor A, be uniformly mixed to obtain mixed liquid B under the temperature condition of 35 ~ 45 DEG C;
Step S30: to the marine organisms degerming agent that adds proportional quantity in mixed liquid B, be uniformly mixed to obtain the mixed solution C of institute under 25 ~ 35 DEG C of temperature condition;
Step S40: to the sodium-chlor and the essence that add proportional quantity in mixed solution C, mix described in contain marine organisms degerming composition degerming washing liquid.
The preparation method of the degerming washing liquid that contains marine organisms degerming composition of the present embodiment, because order by merging and the mixing condition of each material are comparatively reasonable, the each component of degerming washing liquid that contains marine organisms degerming composition making by preparation method of the present invention is mixed, good stability.
In the present embodiment, optional, in order to make each component obtain better mixed effect, in described step S10, the temperature of described water is 40 DEG C.
In the present embodiment, optional, in order to make each component obtain better mixed effect, in described step S20, the time being uniformly mixed is 25-35 minute; In described step S30, the time being uniformly mixed is 3-7 minute.
In the present embodiment, optionally, be easy to carry and the degerming washing liquid of the better marine organisms degerming of performance composition in order to obtain, after step S40, also comprise step S50: the degerming washing liquid of marine organisms degerming composition is lowered the temperature and froth breaking after, carry out packing.
Embodiment 3
The present embodiment provides a kind of degerming washing liquid that contains marine organisms degerming composition, and percentage ratio meter proportioning is as follows by weight:
Marine organisms degerming agent 2.0%;
Cocoanut fatty acid diethanolamide 10.0%;
Alkyl glycoside 4.0%;
Polyoxyethylenated alcohol sodium sulfate 6.0%;
Disodium ethylene diamine tetraacetate 0.5%;
Sodium-chlor 0.5%;
Water 77%.
Marine organisms degerming agent in the present embodiment by weight percentage ratio meter proportioning is: cm-chitosan 1.0%; Sargassum polysaccharides 2.0%; Cecropin 6.0%; N-acetylmuramide lycanohydrlase 1.5%; Water 89.5%.
The preparation method of the degerming washing liquid that contains marine organisms degerming composition of the present embodiment carries out as follows:
Step S301: to the disodium ethylene diamine tetraacetate that adds proportional quantity in the water of 35 DEG C, be uniformly mixed to obtain mixed liquor A;
Step S302: add cocoanut fatty acid diethanolamide, alkyl glycoside and polyoxyethylenated alcohol sodium sulfate in mixed liquor A, be uniformly mixed 25 minutes and obtain mixed liquid B under the temperature condition of 35 DEG C;
Step S303: to the marine organisms degerming agent that adds proportional quantity in mixed liquid B, under 25 DEG C of temperature condition, be uniformly mixed 3 minutes the mixed solution C of institute;
Step S304: to the sodium-chlor that adds proportional quantity in mixed solution C, mix to obtain the degerming washing liquid of described marine organisms degerming composition.
After testing, active constituent content is greater than 12%, ph8.1 to the degerming washing liquid that contains marine organisms degerming composition in the present embodiment, meets the requirement of GB/T1224-2007 GB to washing liquid.
According to the Ministry of Health " 2002 disinfection technology standard ", this product 1:50 diluent, acts on 2 minutes the average bacteriostasis rate of intestinal bacteria, streptococcus aureus, Candida albicans is respectively to 99.45%, 99.53%, 99.46%, has stronger degerming bacteriostatic action.
White dyes does not detect.
The normal temperature quality guaranteed period is 24 months.
In addition, the degerming washing liquid that contains marine organisms degerming composition in experiment the present embodiment also has stronger clean effect.
Embodiment 4
The present embodiment provides a kind of degerming washing liquid that contains marine organisms degerming composition, and percentage ratio meter proportioning is as follows by weight:
Marine organisms degerming agent 3.5%;
Cocoanut fatty acid diethanolamide 13.0%;
Alkyl glycoside 6.0%;
Polyoxyethylenated alcohol sodium sulfate 8.0%;
Disodium ethylene diamine tetraacetate 1.0%;
Sodium-chlor 1.0%;
Essence 1.0%;
Water 66.5%.
Marine organisms degerming agent in the present embodiment by weight percentage ratio meter proportioning is: cm-chitosan 2.0%; Sargassum polysaccharides 4.0%; Cecropin 8.0%; N-acetylmuramide lycanohydrlase 3.5%; Water 82.5%.
The preparation method of the degerming washing liquid that contains marine organisms degerming composition of the present embodiment carries out as follows:
Step S401: to the disodium ethylene diamine tetraacetate that adds proportional quantity in the water of 45 DEG C, be uniformly mixed to obtain mixed liquor A;
Step S402: add cocoanut fatty acid diethanolamide, alkyl glycoside and polyoxyethylenated alcohol sodium sulfate in mixed liquor A, be uniformly mixed 35 minutes and obtain mixed liquid B under the temperature condition of 45 DEG C;
Step S403: to the marine organisms degerming agent that adds proportional quantity in mixed liquid B, under 35 DEG C of temperature condition, be uniformly mixed 7 minutes the mixed solution C of institute;
Step S404: to the sodium-chlor and the essence that add proportional quantity in mixed solution C, mix described in contain marine natural product baby's washing liquid.
Step S405: the degerming washing liquid that contains marine organisms degerming composition that contains marine natural product is lowered the temperature and froth breaking after, carry out packing.
After testing, active constituent content is greater than 12%, ph8.0 to the degerming washing liquid that contains marine organisms degerming composition in the present embodiment, meets the requirement of GB/T1224-2007 GB to washing liquid.
According to the Ministry of Health " 2002 disinfection technology standard ", this product 1:50 diluent, acts on 2 minutes the average bacteriostasis rate of intestinal bacteria, streptococcus aureus, Candida albicans is respectively to 99.43%, 99.55%, 99.48%, has stronger degerming bacteriostatic action.
White dyes does not detect.
The normal temperature quality guaranteed period is 24 months.
In addition, the degerming washing liquid that contains marine organisms degerming composition in experiment the present embodiment also has stronger clean effect.
Embodiment 5
The present embodiment provides a kind of degerming washing liquid that contains marine organisms degerming composition, and percentage ratio meter proportioning is as follows by weight:
Marine organisms degerming agent 2.5%;
Cocoanut fatty acid diethanolamide 11.0%;
Alkyl glycoside 4.5%;
Polyoxyethylenated alcohol sodium sulfate 6.5%;
Disodium ethylene diamine tetraacetate 0.6%;
Sodium-chlor 0.6%;
Essence 0.2%;
Water 74.1%.
Marine organisms degerming agent in the present embodiment by weight percentage ratio meter proportioning is: cm-chitosan 1.5%; Sargassum polysaccharides 3.0%; Cecropin 7.0%; N-acetylmuramide lycanohydrlase 2.0%; Water 86.5%.
The preparation method of the degerming washing liquid that contains marine organisms degerming composition of the present embodiment carries out as follows:
Step S501: to the disodium ethylene diamine tetraacetate that adds proportional quantity in the water of 40 DEG C, be uniformly mixed to obtain mixed liquor A;
Step S502: add cocoanut fatty acid diethanolamide, alkyl glycoside and polyoxyethylenated alcohol sodium sulfate in mixed liquor A, be uniformly mixed 30 minutes and obtain mixed liquid B under the temperature condition of 40 DEG C;
Step S503: to the marine organisms degerming agent that adds proportional quantity in mixed liquid B, under 30 DEG C of temperature condition, be uniformly mixed 5 minutes the mixed solution C of institute;
Step S504: to the sodium-chlor that adds proportional quantity in mixed solution C, mix described in contain marine organisms degerming composition degerming washing liquid.
Step S505: the degerming washing liquid that contains marine organisms degerming composition is lowered the temperature and froth breaking after, carry out packing.
After testing, active constituent content is greater than 12%, ph7.99 to the degerming washing liquid that contains marine organisms degerming composition in the present embodiment, meets the requirement of GB/T1224-2007 GB to washing liquid.
According to the Ministry of Health " 2002 disinfection technology standard ", this product 1:50 diluent, acts on 2 minutes the average bacteriostasis rate of intestinal bacteria, streptococcus aureus, Candida albicans is respectively to 99.52%, 99.60%, 99.51%, has stronger degerming bacteriostatic action.
White dyes does not detect.
The normal temperature quality guaranteed period is 24 months.
In addition, the degerming washing liquid that contains marine organisms degerming composition in experiment the present embodiment also has stronger clean effect.
Embodiment 6
The present embodiment provides a kind of degerming washing liquid that contains marine organisms degerming composition, and percentage ratio meter proportioning is as follows by weight:
Marine organisms degerming agent 3.0%;
Cocoanut fatty acid diethanolamide 12.0%;
Alkyl glycoside 5.5%;
Polyoxyethylenated alcohol sodium sulfate 7.5%;
Disodium ethylene diamine tetraacetate 0.8%;
Sodium-chlor 0.8%;
Essence 0.4%;
Water 70%.
Marine organisms degerming agent in the present embodiment by weight percentage ratio meter proportioning is: cm-chitosan 1.5%; Sargassum polysaccharides 3.0%; Cecropin 7.0%; N-acetylmuramide lycanohydrlase 2.0%; Water 86.5%.
The preparation method of the degerming washing liquid that contains marine organisms degerming composition of the present embodiment carries out as follows:
Step S601: to the disodium ethylene diamine tetraacetate that adds proportional quantity in the water of 40 DEG C, be uniformly mixed to obtain mixed liquor A;
Step S602: add cocoanut fatty acid diethanolamide, alkyl glycoside and polyoxyethylenated alcohol sodium sulfate in mixed liquor A, be uniformly mixed 30 minutes and obtain mixed liquid B under the temperature condition of 40 DEG C;
Step S603: to the marine organisms degerming agent that adds proportional quantity in mixed liquid B, under 30 DEG C of temperature condition, be uniformly mixed 5 minutes the mixed solution C of institute;
Step S604: to the sodium-chlor and the essence that add proportional quantity in mixed solution C, mix described in contain marine organisms degerming composition degerming washing liquid.
Step S605: the degerming washing liquid that contains marine organisms degerming composition is lowered the temperature and froth breaking after, carry out packing.
After testing, active constituent content is greater than 12%, ph7.97 to the degerming washing liquid that contains marine organisms degerming composition in the present embodiment, meets the requirement of GB/T1224-2007 GB to washing liquid.
According to the Ministry of Health " 2002 disinfection technology standard ", this product 1:50 diluent, acts on 2 minutes the average bacteriostasis rate of intestinal bacteria, streptococcus aureus, Candida albicans is respectively to 99.53%, 99.62%, 99.52%, has stronger degerming bacteriostatic action.
White dyes does not detect.
The normal temperature quality guaranteed period is 24 months.
In addition, the degerming washing liquid that contains marine organisms degerming composition in experiment the present embodiment also has stronger clean effect.
Finally it should be noted that: above embodiment only, in order to technical scheme of the present invention to be described, is not intended to limit; Although the present invention is had been described in detail with reference to previous embodiment, those of ordinary skill in the art is to be understood that: its technical scheme that still can record aforementioned each embodiment is modified, or part technical characterictic is wherein equal to replacement; And these amendments or replacement do not make the essence of appropriate technical solution depart from the spirit and scope of various embodiments of the present invention technical scheme.
Claims (8)
3. the degerming washing liquid that contains marine organisms degerming composition according to claim 1 and 2, is characterized in that, described essence is plant essence.
4. the degerming washing liquid that contains marine organisms degerming composition according to claim 1 and 2, is characterized in that, described water is deionized water.
5. a preparation method for the degerming washing liquid that contains marine organisms degerming composition as described in claim 1-4 any one, is characterized in that, comprises the following steps:
Step S10: to the disodium ethylene diamine tetraacetate that adds proportional quantity in the water of 35~45 DEG C, be uniformly mixed to obtain mixed liquor A;
Step S20: add cocoanut fatty acid diethanolamide, alkyl glycoside and polyoxyethylenated alcohol sodium sulfate in mixed liquor A, be uniformly mixed to obtain mixed liquid B under the temperature condition of 35~45 DEG C;
Step S30: to the marine organisms degerming agent that adds proportional quantity in mixed liquid B, be uniformly mixed to obtain the mixed solution C of institute under 25~35 DEG C of temperature condition;
Step S40: to the sodium-chlor and the essence that add proportional quantity in mixed solution C, mix described in contain marine organisms degerming composition degerming washing liquid.
6. the preparation method of the degerming washing liquid that contains marine organisms degerming composition according to claim 5, is characterized in that: in described step S10, the temperature of described water is 40 DEG C.
7. the preparation method of the degerming washing liquid that contains marine organisms degerming composition according to claim 5, is characterized in that: in described step S20, the time being uniformly mixed is 25-35 minute; In described step S30, the time being uniformly mixed is 3-7 minute.
8. the preparation method of the degerming washing liquid that contains marine organisms degerming composition according to claim 5, it is characterized in that: after step S40, also comprise step S50: the degerming washing liquid that contains marine organisms degerming composition is lowered the temperature and froth breaking after, carry out packing.
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CN105441240A (en) * | 2015-12-16 | 2016-03-30 | 无锡吉进环保科技有限公司 | Preparation method of household oil stain cleaning agent |
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