CN106398883A - Laundry liquid for children, and preparation method thereof - Google Patents

Laundry liquid for children, and preparation method thereof Download PDF

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Publication number
CN106398883A
CN106398883A CN201610771468.XA CN201610771468A CN106398883A CN 106398883 A CN106398883 A CN 106398883A CN 201610771468 A CN201610771468 A CN 201610771468A CN 106398883 A CN106398883 A CN 106398883A
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China
Prior art keywords
extract
children
factor
laundry detergent
stain
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CN201610771468.XA
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Chinese (zh)
Inventor
张启明
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Bio Branch (shanghai) Biological Polytron Technologies Inc
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Bio Branch (shanghai) Biological Polytron Technologies Inc
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Priority to CN201610771468.XA priority Critical patent/CN106398883A/en
Publication of CN106398883A publication Critical patent/CN106398883A/en
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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/825Mixtures of compounds all of which are non-ionic
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/382Vegetable products, e.g. soya meal, wood flour, sawdust
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/386Preparations containing enzymes, e.g. protease or amylase
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/662Carbohydrates or derivatives

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention discloses a laundry liquid for children, and a preparation method thereof. The laundry liquid for children is prepared from Fucus serratus extract, Ascophyllum nodosum extract, Asparagopsis armata extract, natural ferment and a stain reduction and easy rinsing factor. The laundry liquid for children contains various natural components, provides softening, moistness and protection for children, is mild and friendly to skins, is harmless to hands, and can effectively clean clothing stubborn stains and nurse clothing fibers through a concentrated formula.

Description

Children laundry detergent and preparation method thereof
Technical field
The present invention relates to daily-use chemical industry technical field is and in particular to a kind of children laundry detergent and preparation method thereof.
Background technology
Often function is more single for the commonly used liquid detergent of people, substantially can only play cleaning action, have it simultaneously His laundry liquid product of function is more rare.And the skin of child is that ratio is more sensitive, need to enjoy care, and general laundry Very hard not soft of clothes that liquid comes out, simple de-sludging effect is to can not meet the market demand, special child Liquid detergent will be a kind of following development trend.
Content of the invention
For deficiency above-mentioned present in prior art, one of the technical problem to be solved is to provide a kind of youngster Virgin liquid detergent.
The two of the technical problem of the solution of the present invention are to provide a kind of preparation method of children laundry detergent.
The present invention seeks to be achieved through the following technical solutions:
A kind of children laundry detergent, is prepared from including following raw materials:Tip edge Fucus Vesiculosus extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract, natural ferment, stain is gone easily to float the factor.
A kind of children laundry detergent, is prepared from by the raw material of following weight parts:Tip edge Fucus Vesiculosus extract 0.3-3 part, bubble Leaf algae extract 0.3-3 part, thorn Asparagus toxiformis (Delile) Coll et Harv extract 0.3-3 part, glycerol 5-15 part, go stain easily to float factor 10-30 part, natural ferment Plain 2-20 part, EDETATE SODIUM 0.2-2 part, water 40-80 part.
Preferably, described stain of going easily floats the factor for Dodecyl Polyglucosides, myristic acid diglycollic amide, Cortex cocois radiciss oils and fatss One or more of mixture in fat acid diglycollic amide.
It is highly preferred that described stain of going easily floats the factor by Dodecyl Polyglucosides, myristic acid diglycollic amide, Oleum Cocois Fatty diglycollic amide mixes, described Dodecyl Polyglucosides, myristic acid diglycollic amide, coco-nut oil fatty acid two The mass ratio of glycollic amide is (1-3):(1-3):(1-3).
Present invention also offers the preparation method of above-mentioned children laundry detergent, comprise the following steps:
Heat water to 65-85 DEG C, sequentially add glycerol under stirring condition, go stain easily to float the factor to be uniformly mixed, fall Temperature to 45-55 DEG C, sequentially add tip edge Fucus Vesiculosus extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract, natural ferment, EDETATE SODIUM is uniformly mixed and obtains final product.
Specifically, in the present invention:
Natural ferment, the method system adopting embodiment 1 in number of patent application 201310512639.3 in the embodiment of the present invention Standby obtain.
Dodecyl Polyglucosides, No. CAS:110615-47-9.
Myristic acid diglycollic amide, No. CAS:7545-23-5.
Cocoanut fatty acid diethanolamide, No. CAS:68603-42-9.
EDETATE SODIUM, i.e. disodiumedetate, No. CAS:139-33-3.
Glycerol, No. CAS:56-81-5.
Tip edge Fucus Vesiculosus extract, English name:Fucus Serratus Extrac, from Boulez Brittany area Tip edge Fucus Vesiculosus, locals is referred to as " gold Sargassum ".This algae extract has reinforcing fiber archeocyte vigor, and protection mitochondrion is thin Born of the same parents, promote dermal respiration, are that skin brings powerful moisture-keeping efficacy, Cucumber Extract water storage function, also promotion organization can regenerate, increase Cell viability recovers skin life, promotes the metabolism of skin, is effective against free radical, antagonism cell senescence, discharges simultaneously Active-energy, improves and is dried, prevents microgroove, wrinkle to produce, delay skin aging.Tip edge Fucus Vesiculosus extract can be prepared or purchase Can buy, preparation method can be conventional water extraction or alcohol extracting method, according to solid-liquid after such as cleaning and crush tip edge Fucus Vesiculosus Than (g/ml) 1:10-1:30 immersion mass fractions are in 95% ethanol, soak 8-12h, are heated to reflux 4-6h, and cooling is filtered, will After filtrate concentrates, it is lyophilized into powder.Tip edge Fucus Vesiculosus extract used in the present invention is to buy from Nanjing Ze Lang medicine section Skill company limited, specification is 10:1, the 1g tip edge Fucus Vesiculosus extract that is, 10g tip edge Fucus Vesiculosus extract.
Yellow tang extract, English name:Ascophyllum Nodosum Extract, have antitumor, antiviral, Antibacterial, elimination free radical, anti-oxidation efficacy.Yellow tang extract can be prepared or be commercially available, and preparation method can be routine Water extraction or alcohol extracting method, according to solid-to-liquid ratio (g/ml) 1 after such as yellow tang being cleaned and crush:10-1:30 immersion mass fractions For, in 95% ethanol, soaking 8-12h, being heated to reflux 4-6h, cooling, filter, after filtrate is concentrated, be lyophilized into powder.The present invention Used in yellow tang extract be to buy from Xi'an all places bio tech ltd, specification is 10:1, i.e. 10g yellow tang The 1g yellow tang extract extracting.
Thorn Asparagus toxiformis (Delile) Coll et Harv Sargassum extract, English name:Asparagopsis Armata Extract, rich in activated silica, energy Effectively optimize skin cell metabolism, there is skin reconstruction, steatolysiss, opposing edema, skin quality moisture-keeping efficacy.Thorn Asparagus toxiformis (Delile) Coll et Harv Sargassum extract can be prepared or be commercially available, and preparation method can be conventional water extraction or alcohol extracting method, such as will pierce Haimen Winter Sargassum clean and crush after according to solid-to-liquid ratio (g/ml) 1:10-1:30 immersion mass fractions are in 95% ethanol, soak 8-12h, It is heated to reflux 4-6h, cooling, filter, after filtrate is concentrated, be lyophilized into powder.Thorn Asparagus toxiformis (Delile) Coll et Harv Sargassum used in the present invention carries Thing is taken to be to buy west (EXSYMOL) company of U.S. that regards for oneself, specification is 10:1, the 1g that is, 10g thorn Asparagus toxiformis (Delile) Coll et Harv Sargassum extract extracts Thorn Asparagus toxiformis (Delile) Coll et Harv Sargassum extract.
Children laundry detergent of the present invention, contains multiple natural components, gives child triple love:Shu Rou, moist, protection, temperature Do not hurt hands with pro-skin, Concentrated formulations, the effectively clean stupid stain of medicated clothing, care of laundry items fiber.
Specific embodiment
With reference to embodiment, the present invention is described further, described below, is only the preferable enforcement to the present invention Example, not does the restriction of other forms, any those skilled in the art are possibly also with the disclosure above to the present invention Technology contents be changed to the Equivalent embodiments that change on an equal basis.Every without departing from the present invention program content, according to the present invention Technical spirit following examples are made any simple modification or equivalent variations, all fall within protection scope of the present invention.
Embodiment 1
Children laundry detergent raw material (weight portion):0.8 part of tip edge Fucus Vesiculosus extract, 0.8 part of yellow tang extract, thorn Haimen 0.8 part of winter extract, 10 parts of glycerol, stain is gone easily to float 18 parts of the factor, 10 parts of natural ferment, 0.5 part of EDETATE SODIUM, 45 parts of water.
Described stain of going easily floats the factor by Dodecyl Polyglucosides, myristic acid diglycollic amide, coco-nut oil fatty acid two Glycollic amide is 1 in mass ratio:1:1 is uniformly mixed and obtains.
The preparation method of above-mentioned children laundry detergent, comprises the following steps:
Heat water to 75 DEG C, sequentially add glycerol under 500 revs/min of stirring conditions, go stain easily to float factor stirring mixing all Even, it is cooled to 48 DEG C, sequentially add tip edge Fucus Vesiculosus extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract, natural ferment Element, EDETATE SODIUM are uniformly mixed.Obtain the children laundry detergent of embodiment 1.
Embodiment 2
Children laundry detergent raw material (weight portion):1.2 parts of tip edge Fucus Vesiculosus extract, 1.2 parts of yellow tang extract, glycerol 10 Part, go stain easily to float 18 parts of the factor, 10 parts of natural ferment, 0.5 part of EDETATE SODIUM, 45 parts of water.
Described stain of going easily floats the factor by Dodecyl Polyglucosides, myristic acid diglycollic amide, coco-nut oil fatty acid two Glycollic amide is 1 in mass ratio:1:1 is uniformly mixed and obtains.
The preparation method of above-mentioned children laundry detergent, comprises the following steps:
Heat water to 75 DEG C, sequentially add glycerol under 500 revs/min of stirring conditions, go stain easily to float factor stirring mixing all Even, it is cooled to 48 DEG C, sequentially add tip edge Fucus Vesiculosus extract, yellow tang extract, natural ferment, EDETATE SODIUM stirring mixed Close uniformly.Obtain the children laundry detergent of embodiment 2.
Embodiment 3
Children laundry detergent raw material (weight portion):1.2 parts of tip edge Fucus Vesiculosus extract, 1.2 parts of Asparagus toxiformis (Delile) Coll et Harv extract of thorn, glycerol 10 parts, go stain easily to float 18 parts of the factor, 10 parts of natural ferment, 0.5 part of EDETATE SODIUM, 45 parts of water.
Described stain of going easily floats the factor by Dodecyl Polyglucosides, myristic acid diglycollic amide, coco-nut oil fatty acid two Glycollic amide is 1 in mass ratio:1:1 is uniformly mixed and obtains.
The preparation method of above-mentioned children laundry detergent, comprises the following steps:
Heat water to 75 DEG C, sequentially add glycerol under 500 revs/min of stirring conditions, go stain easily to float factor stirring mixing all Even, it is cooled to 48 DEG C, sequentially add tip edge Fucus Vesiculosus extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract, natural ferment, EDETATE SODIUM stirring Mix homogeneously.Obtain the children laundry detergent of embodiment 3.
Embodiment 4
Children laundry detergent raw material (weight portion):1.2 parts of yellow tang extract, 1.2 parts of Asparagus toxiformis (Delile) Coll et Harv extract of thorn, glycerol 10 Part, go stain easily to float 18 parts of the factor, 10 parts of natural ferment, 0.5 part of EDETATE SODIUM, 45 parts of water.
Described stain of going easily floats the factor by Dodecyl Polyglucosides, myristic acid diglycollic amide, coco-nut oil fatty acid two Glycollic amide is 1 in mass ratio:1:1 is uniformly mixed and obtains.
The preparation method of above-mentioned children laundry detergent, comprises the following steps:
Heat water to 75 DEG C, sequentially add glycerol under 500 revs/min of stirring conditions, go stain easily to float factor stirring mixing all Even, it is cooled to 48 DEG C, sequentially add yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract, natural ferment, EDETATE SODIUM stirring mixing Uniformly.Obtain the children laundry detergent of embodiment 4.
Embodiment 5
Substantially the same manner as Example 1, differ only in:Described stain of going easily floats the factor by myristic acid diethanol acyl Amine, cocoanut fatty acid diethanolamide are 1 in mass ratio:1 is uniformly mixed and obtains.Obtain child's laundry of embodiment 5 Liquid.
Embodiment 6
Substantially the same manner as Example 1, differ only in:Described stain of going easily floats the factor by Dodecyl Polyglucosides, coconut palm Seed oil fatty diglycollic amide is 1 in mass ratio:1 is uniformly mixed and obtains.Obtain the children laundry detergent of embodiment 6.
Embodiment 7
Substantially the same manner as Example 1, differ only in:Described stain of going easily floats the factor by Dodecyl Polyglucosides, meat Myristic acid diglycollic amide is 1 in mass ratio:1 is uniformly mixed and obtains.Obtain the children laundry detergent of embodiment 7.
Test case 1
According to industry standard QB/T 2850-2007 antibacterial bacteriostatic type detergent, carry out fungistatic effect test, activity It is 1wt%, be action time 20 minutes, concrete detection data, refer to table 1.
Table 1:Handwashing liquid fungistatic effect tests table
Comparing embodiment 1 and embodiment 2-4, embodiment 1 (tip edge Fucus Vesiculosus extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv Extract compound) fungistatic effect be substantially better than embodiment 2-4 (tip edge Fucus Vesiculosus extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv carry Take in thing arbitrarily that the two is compounding);Comparing embodiment 1 and embodiment 5-7, embodiment 1 (Dodecyl Polyglucosides, myristic acid two Glycollic amide, cocoanut fatty acid diethanolamide compound) fungistatic effect be substantially better than embodiment 5-7 (Dodecyl Polyglucosides, In myristic acid diglycollic amide, cocoanut fatty acid diethanolamide, arbitrarily the two is compounding).
Test case 2
The method specifying according to QB/T 1224-2007, detects going of the children laundry detergent that embodiment of the present invention 1-7 is obtained Dirty power.
Standard flour solution concentration is 0.2wt%, and liquid detergent solution concentration to be measured is 0.3wt%, hard with 250mg/kg respectively Water preparation, the method being specified using QB/T 13174-2008 and soiled cotton, measure laundry fluid samples and the decontamination of standard flour with machine Power.
Concrete detection data, refers to table 2.
Table 2:Detergency test result table
Decontamination ratio, (carbon black soiled cotton), P Decontamination ratio, (albumen soiled cotton), P
Embodiment 1 1.35 1.86
Embodiment 2 1.21 1.66
Embodiment 3 1.23 1.52
Embodiment 4 1.19 1.58
Embodiment 5 1.14 1.41
Embodiment 6 1.11 1.37
Embodiment 7 1.17 1.32
Standard flour 1.06 0.85
Comparing embodiment 1 and embodiment 2-4, embodiment 1 (tip edge Fucus Vesiculosus extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv Extract compound) detergency be substantially better than embodiment 2-4 (tip edge Fucus Vesiculosus extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract In thing, arbitrarily the two is compounding);Comparing embodiment 1 and embodiment 5-7, embodiment 1 (Dodecyl Polyglucosides, myristic acid diethyl Alkylolamides, cocoanut fatty acid diethanolamide compound) detergency is substantially better than embodiment 5-7 (Dodecyl Polyglucosides, lima bean In cool acid diglycollic amide, cocoanut fatty acid diethanolamide, arbitrarily the two is compounding).

Claims (5)

1. a kind of children laundry detergent is prepared from it is characterised in that including following raw materials:Tip edge Fucus Vesiculosus extract, yellow tang Extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract, natural ferment, go stain easily to float the factor.
2. a kind of children laundry detergent is it is characterised in that be prepared from by the raw material of following weight parts:Tip edge Fucus Vesiculosus extract 0.3-3 part, yellow tang extract 0.3-3 part, thorn Asparagus toxiformis (Delile) Coll et Harv extract 0.3-3 part, glycerol 5-15 part, go stain easily to float factor 10- 30 parts, natural ferment 2-20 part, EDETATE SODIUM 0.2-2 part, water 40-80 part.
3. children laundry detergent as claimed in claim 1 or 2 it is characterised in that:Described stain of going easily floats the factor for dodecyl One or more of mixture in glucoside, myristic acid diglycollic amide, cocoanut fatty acid diethanolamide.
4. children laundry detergent as claimed in claim 3 it is characterised in that:Described stain of going easily floats the factor by dodecyl glucose Glycosides, myristic acid diglycollic amide, cocoanut fatty acid diethanolamide mix, described Dodecyl Polyglucosides, lima bean Cool acid diglycollic amide, the mass ratio of cocoanut fatty acid diethanolamide are (1-3):(1-3):(1-3).
5. the preparation method of the children laundry detergent as any one of claim 1-4 is it is characterised in that include following walking Suddenly:
Heat water to 65-85 DEG C, sequentially add glycerol under stirring condition, go stain easily to float the factor to be uniformly mixed, be cooled to 45-55 DEG C, sequentially add tip edge Fucus Vesiculosus extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract, natural ferment, EDTA Disodium is uniformly mixed and obtains final product.
CN201610771468.XA 2016-08-30 2016-08-30 Laundry liquid for children, and preparation method thereof Withdrawn CN106398883A (en)

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Citations (7)

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Publication number Priority date Publication date Assignee Title
JP2002255790A (en) * 2001-03-05 2002-09-11 Nikko Seiyaku Kk Skin detergent
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CN103013699A (en) * 2012-12-20 2013-04-03 青岛海芬海洋生物科技有限公司 Infant laundry detergent containing marine organism component and preparation method of infant laundry detergent
CN103725441A (en) * 2013-12-04 2014-04-16 青岛海芬海洋生物科技有限公司 Marine animal disinfecting ingredient-containing dedicated cleaning agent for keyboards and mice
CN103881846A (en) * 2012-12-24 2014-06-25 青岛海芬海洋生物科技有限公司 Marine biological component-containing special detergent for underwear, and its preparation method
CN104257531A (en) * 2014-08-29 2015-01-07 何开远 Fresh peel ferment and preparation method thereof
CN104479934A (en) * 2014-12-11 2015-04-01 青岛海芬海洋生物科技有限公司 Marine alga enzyme detergent

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002255790A (en) * 2001-03-05 2002-09-11 Nikko Seiyaku Kk Skin detergent
CN103013695A (en) * 2012-12-20 2013-04-03 青岛海芬海洋生物科技有限公司 Degerming laundry detergent containing marine organism degerming component and preparation method of degerming laundry detergent
CN103013699A (en) * 2012-12-20 2013-04-03 青岛海芬海洋生物科技有限公司 Infant laundry detergent containing marine organism component and preparation method of infant laundry detergent
CN103881846A (en) * 2012-12-24 2014-06-25 青岛海芬海洋生物科技有限公司 Marine biological component-containing special detergent for underwear, and its preparation method
CN103725441A (en) * 2013-12-04 2014-04-16 青岛海芬海洋生物科技有限公司 Marine animal disinfecting ingredient-containing dedicated cleaning agent for keyboards and mice
CN104257531A (en) * 2014-08-29 2015-01-07 何开远 Fresh peel ferment and preparation method thereof
CN104479934A (en) * 2014-12-11 2015-04-01 青岛海芬海洋生物科技有限公司 Marine alga enzyme detergent

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Title
张德玉: "《海洋渔业知多少》", 31 January 2011, 中国时代经济出版社 *

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Application publication date: 20170215