CN106635566A - Enzymatic laundry soap containing natural antibacterial ingredient and preparation method of enzymatic laundry soap - Google Patents
Enzymatic laundry soap containing natural antibacterial ingredient and preparation method of enzymatic laundry soap Download PDFInfo
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- CN106635566A CN106635566A CN201611210746.0A CN201611210746A CN106635566A CN 106635566 A CN106635566 A CN 106635566A CN 201611210746 A CN201611210746 A CN 201611210746A CN 106635566 A CN106635566 A CN 106635566A
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- CN
- China
- Prior art keywords
- component
- soap
- natural bacteriostatic
- enzyme
- effect
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/045—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on non-ionic surface-active compounds and soap
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
The invention belongs to the field of daily use chemicals and particularly relates to an enzymatic laundry soap containing a natural antibacterial ingredient and a preparation method of the enzymatic laundry soap. The enzymatic laundry soap containing the natural antibacterial ingredient comprises the following components in percentage by weight: 38-60% of soap grains, 10-14% of enzyme, 10-14% of an enzyme stabilizer, 10-14% of the natural antibacterial ingredient, 5-10% of spice, and 5-10% of a chelating agent. The laundry soap realize effective and rapid decontamination, the natural antibacterial ingredient is used, so that the sterilizing effect is good, and the enzymatic laundry soap does not irritate or damage the skin, and can inhibit bacteria for a long period of time.
Description
Technical field
The invention belongs to household chemicals field, and in particular to a kind of enzymatic household soap of component of effect containing natural bacteriostatic and its preparation
Method.
Background technology
Soap has a long history, and is most ancient articles for washing, recently as people to product and Environmental security
Increasingly care, soap paid close attention to again by people, and people select soap to be mainly used to wash underwear and collar, sleeve
Buckle the stain in face, these dirts mainly by the groups of contaminants such as dust in the sebum and surrounding air of human secretory into, its
Main component is protein and grease.These protein combine with lipid components, are firmly attached on clothing, and common
Laundry soap is difficult to get rid of.
Enzyme is a kind of high-activity biological catalyst, its high catalytic efficiency, with very strong selectivity.With Enzymes Industry
Development, many enzyme preparations are applied in the middle of cleaning product, such as protease can rapid decomposition of protein class dirt, and by surface
The solubilising of activating agent, emulsification are removed；Lipase can remove oil dirt；Amylase can remove starch dirt；
Cellulase, this enzyme does not directly participate in decomposing dirt digestion, but with the increase of washing times, to the micro- of cotton fiber surface
Fine fibre is decomposed, and so just from slight part enhances the clean effect of detergent.
Chinese patent CN101319173B discloses a kind of enzymatic household soap and its production method, by neat soap, spices, coloring
Agent, chelating agent and enzyme are mixed, and the enzyme stabilizers that are made up of borax, glycerine or propane diols and citric acid of addition and spices are mixed
Close, stir in good time, then by refiner, three-roll grinder, last vacuum plodding roll printing is shaped to enzymatic household soap product,
Although inventing the washability that can keep higher it is contemplated that sterilization effect is not fine.
At present though with good clean effect, the sterilizing pesticide composition that it is used mostly is chemistry to existing laundry soap
Reagent so that have certain injury effect to skin, and can not long-time sterilizing pesticide.
The content of the invention
A kind of enzymatic household soap of the component of effect containing natural bacteriostatic of the present invention includes following components and its percentage by weight：
Neat soap 38～60%, enzyme 10～14%, enzyme stabilizers 10～14%, natural bacteriostatic effect component 10～14%, perfume
Material 5～10% and chelating agent 5～10%.
Preferably, the enzymatic household soap of described effect containing natural bacteriostatic component is by following components and its percentage by weight group
Into：
Neat soap 47.5%, enzyme 12.5%, enzyme stabilizers 12.5%, natural bacteriostatic effect component 12.5%, the and of spices 7.5%
Chelating agent 7.5%.
Preferably, described enzyme includes protease, cellulase, lipase and amylase by weight 3:4:2:6 compositions.
Preferably, described enzyme stabilizers are borax, glycerine and citric acid by weight 3:2:5 compositions.
Preferably, described natural bacteriostatic effect component is Tea Saponin.
Further preferably, described chelating agent is ethylenediamine tetramethylene phosphoric acid.
In addition, present invention also offers a kind of preparation method of the enzymatic household soap of effect containing natural bacteriostatic component, including
Following steps：
S1, addition neat soap stir in agitated kettle；
S2, addition natural bacteriostatic effect component and chelating agent, stir；
S3, addition enzyme and enzyme stabilizers, stir；
S4, spices is eventually adding, is stood after stirring；
S5, stirring product obtained in the previous step pass sequentially through refiner, three-roll grinder, last vacuum plodding roll printing into
Type.
Preferably, mixing time described in step S1 is 2～5 minutes；Mixing time described in step S2 is 2～4 minutes；Step
Mixing time described in rapid S3 is 2～4 minutes；Time of repose described in step S4 is 2～3 minutes.
Protease CAS：9025-49-4；Cellulase CAS：9012-54-8；Lipase CAS：9001-62-1；
Amylase CAS：9000-91-3；Borax CAS：1303-96-4；Citric acid CAS：77-92-9；Tea Saponin CAS：
8047-15-2。
Sugared body one end is hydrophilic radical in Tea Saponin molecular structure, is connected with other end hydrophobic group by ehter bond, hydrophobic
Group is made up of the group being connected in ester bond form and organic acid, thus has possessed the condition of surface-active action, therefore tea
Saponin has the kinds of surface such as emulsification, dispersion, wetting, decontamination, foaming, foam stabilizing activity, is a kind of self-faced of function admirable
Activating agent, in addition research shows that Tea Saponin also has functions that antibacterial desinsection is the natural antibacterial active component of function admirable.
Compared with prior art, the laundry soap that the present invention is provided can effective fast decontaminating, using natural sterilization efficacy group
Divide sterilization effect good, do not stimulate and injure skin, and can be antibacterial for a long time.
Specific embodiment
The present invention is described in further details below by specific embodiment, these embodiments are only used for the mesh of illustration
, it is in no way intended to limit protection scope of the present invention.
Neat soap is purchased from the happy biochemical technology Co., Ltd in Guangzhou Jiade；Spices is purchased from the limited public affairs of Shanghai Yi Kesaiting spices
Department.
Embodiment 1-3, comparative example 1-3
Embodiment 1-3 and comparative example 1-3 component and mass percent are as shown in table 1.
The component and its percentage by weight of the embodiment of table 1 and comparative example laundry soap
Comparative example 1 is with the difference of embodiment 2：Without Tea Saponin, increase the content of neat soap.
Comparative example 2 is with the difference of embodiment 2：Enzyme by protease, cellulase, lipase and amylase in mass ratio
1:1:1:1 composition.
Comparative example 3 is with the difference of embodiment 2：Enzyme stabilizers are by borax, glycerine and citric acid in mass ratio 1:1:1 group
Into.
The preparation method of laundry soap of the embodiment 1 containing natural activity component：
S1, addition neat soap stir in agitated kettle；
S2, addition natural bacteriostatic effect component and chelating agent, stir；
S3, addition enzyme and enzyme stabilizers, stir；
S4, spices is eventually adding, is stood after stirring；
S5, stirring product obtained in the previous step pass sequentially through refiner, three-roll grinder, last vacuum plodding roll printing into
Type.
The preparation method of embodiment 2-3 and comparative example 1-3 laundry soap is similar to Example 1.
Properties of product evaluation test
Test portion：
1. washing performance test
Method of testing：By embodiment and comparative example laundry soap, for international standard soiled cotton EMPA117 contrast test is carried out；
Wash conditions：Wash solution 250ppm hard water, sample wash concentration 3g/L, sampling amount is carried out by gold content during packaging in test
Conversion, 30 DEG C ± 1 DEG C, by GB/T13174《Dress material detergent detergency and the measure of circulation scourability》Method is washed, than
The whiteness of soiled cotton is poor before and after relatively washing, as a result such as table 2.
The embodiment of table 2 and comparative example washing performance test result of the test
From table 2 it can be seen that dirt-removing power of the embodiment laundry soap apparently higher than comparative example laundry soap, illustrates of the invention real
Apply the product for obtaining that cooperates of each component in example and there is more preferable dirt-removing power.
2. degerming experiment：According to《Disposable Sanitary Accessory hygienic practice》In sterilization rate method of testing experiment,
Under the conditions of 20 DEG C～21 DEG C of temperature, experimental concentration is 1% laundry detergent compositions, is acted on 5 minutes, and test strain is Staphylococcus aureus
Bacterium (Staphylococcus aureus, ATCC6538) and Escherichia coli (Escherichia coli, 8099) bacterial classification, as a result
It is shown in Table 3.
3. mould proof experiment：According to《Fabric product fungicidal properties is evaluated》Method of testing is tested, and experimental concentration is the laundry of 1% clothing
Soap, acts on 5 minutes, and test strain is aspergillus niger (Aspergillus, ATCC16404), Trichoderma viride (Trichoderma
Viride, AS3.2941), penicillium funiculosum (Penicillium funiculosum, GIM 3.103), Chaetomium globosum
(Chaetomium globasum, AS3.3601) four kinds of moulds, the results are shown in Table 4.
The embodiment of table 3 and the degerming result of the test of comparative example
As shown in Table 3, laundry soap of the present invention has degermation to Escherichia coli, staphylococcus aureus, and embodiment is more right
Ratio 1-3 sterilizing rate is higher, illustrates using Tea Saponin as bacteriostasis efficacy component and enzyme by protease, cellulase, fat
Enzyme and amylase in mass ratio 3:4:2:6 compositions, enzyme stabilizers are by borax, glycerine and citric acid in mass ratio 3:2:5 compositions
Laundry soap bactericidal effect is more preferable.
The embodiment of table 4 and comparative example mould proof test result
| Sample ID | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 |
| Mould proof grade | 0 | 0 | 0 | 2 | 1 | 1 |
Rating scale：0 grade-under magnifying glass without obvious fungus growth；1 grade-fungus growth rareness or local growth, in sample
The area coverage on product surface is less than 10%；2 grades-mould is 10%～30% in the area coverage of sample surfaces；3 grades-mould exists
The area coverage of sample surfaces is 30%～60%；Area coverage of the 4 grades-mould in sample surfaces>60%.
As shown in Table 4, it is higher compared with the mould proof grade of the laundry soap of comparative example using embodiment of the present invention laundry soap, mould proof effect
Fruit is more preferably.
The above is only the preferred embodiment of the present invention, it is noted that it is right that above-mentioned preferred embodiment is not construed as
The restriction of the present invention, protection scope of the present invention should be defined by claim limited range.For the art
For those of ordinary skill, without departing from the spirit and scope of the present invention, some improvements and modifications can also be made, these change
Enter and retouch also to should be regarded as protection scope of the present invention.
Claims (8)
1. a kind of enzymatic household soap of the component of effect containing natural bacteriostatic, it is characterised in that including following components and its weight percent
Than：
Neat soap 38～60%, enzyme 10～14%, enzyme stabilizers 10～14%, natural bacteriostatic effect component 10～14%, spices 5～
10% and chelating agent 5～10%.
2. the enzymatic household soap of the component of effect containing natural bacteriostatic according to claim 1, it is characterised in that by following components
And its percentage by weight composition：
Neat soap 47.5%, enzyme 12.5%, enzyme stabilizers 12.5%, natural bacteriostatic effect component 12.5%, spices 7.5% and chelating
Agent 7.5%.
3. the enzymatic household soap of the component of effect containing natural bacteriostatic according to claim 1 and 2, it is characterised in that described
Enzyme is by protease, cellulase, lipase and amylase by weight 3:4:2:6 compositions.
4. the enzymatic household soap of the component of effect containing natural bacteriostatic according to claim 1 and 2, it is characterised in that described
Enzyme stabilizers are by borax, glycerine and citric acid by weight 3:2:5 compositions.
5. the enzymatic household soap of the component of effect containing natural bacteriostatic according to claim 1 and 2, it is characterised in that described
Natural bacteriostatic effect component is Tea Saponin.
6. the enzymatic household soap of the component of effect containing natural bacteriostatic according to claim 1 and 2, it is characterised in that described
Chelating agent is ethylenediamine tetramethylene phosphoric acid.
7. the preparation method of the enzymatic household soap of the component of effect containing natural bacteriostatic according to any one of claim 1-6, its
It is characterised by, comprises the following steps：
S1, addition neat soap stir in agitated kettle；
S2, addition natural bacteriostatic effect component and chelating agent, stir；
S3, addition enzyme and enzyme stabilizers, stir；
S4, spices is eventually adding, is stood after stirring；
S5, stirring product obtained in the previous step pass sequentially through refiner, three-roll grinder, last vacuum plodding roll printing shaping.
8. the preparation method of the enzymatic household soap of natural bacteriostatic effect component according to claim 7, it is characterised in that step
Mixing time described in rapid S1 is 2～5 minutes；Mixing time described in step S2 is 2～4 minutes；During stirring described in step S3
Between be 2～4 minutes；Time of repose described in step S4 is 2～3 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611210746.0A CN106635566A (en) | 2016-12-24 | 2016-12-24 | Enzymatic laundry soap containing natural antibacterial ingredient and preparation method of enzymatic laundry soap |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611210746.0A CN106635566A (en) | 2016-12-24 | 2016-12-24 | Enzymatic laundry soap containing natural antibacterial ingredient and preparation method of enzymatic laundry soap |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106635566A true CN106635566A (en) | 2017-05-10 |
Family
ID=58826872
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611210746.0A Pending CN106635566A (en) | 2016-12-24 | 2016-12-24 | Enzymatic laundry soap containing natural antibacterial ingredient and preparation method of enzymatic laundry soap |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107418795A (en) * | 2017-06-23 | 2017-12-01 | 青岛元汇丰企业管理咨询服务有限公司 | Student's laundry soap and its production method |
| CN110194997A (en) * | 2019-04-18 | 2019-09-03 | 六安中达信息科技有限公司 | A kind of craft complex enzyme perfumed soap and its process units |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101319173A (en) * | 2008-07-21 | 2008-12-10 | 广州立白企业集团有限公司 | Enzymatic household soap and method of preparing the same |
| CN103695217A (en) * | 2013-12-20 | 2014-04-02 | 广州市浪奇实业股份有限公司 | Tea saponin washing soap |
-
2016
- 2016-12-24 CN CN201611210746.0A patent/CN106635566A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101319173A (en) * | 2008-07-21 | 2008-12-10 | 广州立白企业集团有限公司 | Enzymatic household soap and method of preparing the same |
| CN103695217A (en) * | 2013-12-20 | 2014-04-02 | 广州市浪奇实业股份有限公司 | Tea saponin washing soap |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107418795A (en) * | 2017-06-23 | 2017-12-01 | 青岛元汇丰企业管理咨询服务有限公司 | Student's laundry soap and its production method |
| CN110194997A (en) * | 2019-04-18 | 2019-09-03 | 六安中达信息科技有限公司 | A kind of craft complex enzyme perfumed soap and its process units |
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Application publication date: 20170510 |
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