CN103013695A - Degerming laundry detergent containing marine organism degerming component and preparation method of degerming laundry detergent - Google Patents
Degerming laundry detergent containing marine organism degerming component and preparation method of degerming laundry detergent Download PDFInfo
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- CN103013695A CN103013695A CN2012105596623A CN201210559662A CN103013695A CN 103013695 A CN103013695 A CN 103013695A CN 2012105596623 A CN2012105596623 A CN 2012105596623A CN 201210559662 A CN201210559662 A CN 201210559662A CN 103013695 A CN103013695 A CN 103013695A
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Abstract
The invention discloses a degerming laundry detergent containing a marine organism degerming component and a preparation method of the degerming laundry detergent. The degerming laundry detergent comprises the following components by weight percentage: 2.0-3.5% of marine organism degerming agent, 10.0-13.0% of coconut oil fatty acid diethanol amide, 4.0-6.0% of alkyl glycoside, 6.0-8.0% of fatty alcohol polyoxyethylene ether sodium sulfate, 0.5-1.0% of disodium EDTA (ethylene diamine tetraacetic acid), 0.5-1.0% of sodium chloride, 0-1.0% of essence and the balance of water. The degerming laundry detergent containing the marine organism degerming component can degerm effectively and has a strong dirt-removing ability.
Description
Technical field
The present invention relates to washing liquid, relate in particular to a kind of degerming washing liquid that contains marine organisms degerming composition and preparation method thereof.
Background technology
Along with the enhancing of people to health perception, can not satisfy only cleaning efficacy to the cleaning of clothing, energy degerming sterilization has become human consumer's first-selection in the time of the cleaning clothing, baby's skin is very tender and lovely, passive protective physical fitness is low, it is improper that washing liquid is selected, and skin and health more easily come to harm.Have on the market and possess functional baby's washing liquid antibiotic, sterilization, but generally the disinfection composition of interpolation is chlorine-containing disinfectant, oxygen-containing disinfectant or contains alcohol disinfectant, and the tensio-active agent that these washing liquids adopt and sterilizing agent all have unpleasant irritating smell; Fabric and skin there are pungency, are corrosive; Poor stability; Compatibleness with other raw materials is poor; To the shortcoming such as environment is unfriendly, very easily hurt the healthy of baby.
CN200710179670 discloses " antimicrobial laundry liquid of a kind of simultaneously disinfecting and decontaminating and preparation method thereof " in the Chinese patent, the composition that is used for sterilization of announcing in the prescription is poly hexamethylene biguanide PHMB, the tensio-active agent that is used for cleaning is fatty alcohol-polyoxyethylene ether AEO-7, fatty alcohol-polyoxyethylene ether AEO-9, fatty alcohol-polyoxyethylene ether AEO-5, fatty alcohol-polyoxyethylene ether XL-80, more than be nonionogenic tenside, this prescription is subjected to the impact of sterilization component to be subject to limitation in the selection of tensio-active agent, can only select similar fatty alcohol-polyoxyethylene ether nonionogenic tenside, therefore, the detersive power of this patent formulation has been subject to impact.
Summary of the invention
An object of the present invention is to provide a kind of sterilizing function that has, and the degerming washing liquid that contains marine organisms degerming composition of strong detergency.
Another object of the present invention provides a kind of sterilizing function that has, and the preparation method of the degerming washing liquid that contains marine organisms degerming composition of strong detergency.
The degerming washing liquid that contains marine organisms degerming composition of the present invention, percentage ratio meter proportioning is as follows by weight:
Marine organisms degerming agent 2.0-3.5%;
Cocoanut fatty acid diethanolamide 10.0-13.0%;
Alkyl glycoside 4.0-6.0%;
Polyoxyethylenated alcohol sodium sulfate 6.0-8.0%;
Disodium ethylene diamine tetraacetate 0.5-1.0%;
Sodium-chlor 0.5-1.0%;
Essence 0-1.0%;
Surplus is water.
The preparation method who contains the degerming washing liquid of marine organisms degerming composition of the present invention may further comprise the steps:
Step S10: add the disodium ethylene diamine tetraacetate of proportional quantity in 35 ~ 45 ℃ the water, mix to get mixed liquor A;
Step S20: in mixed liquor A, add cocoanut fatty acid diethanolamide, alkyl glycoside and polyoxyethylenated alcohol sodium sulfate, under 35 ~ 45 ℃ temperature condition, mix to get mixed liquid B;
Step S30: add the marine organisms degerming agent of proportional quantity in the mixed liquid B, under 25 ~ 35 ℃ of temperature condition, mix to get the mixed solution C of institute;
Step S40: add sodium-chlor and the essence of proportional quantity in the mixed solution C, mix to get the described degerming washing liquid that contains marine organisms degerming composition.
The degerming washing liquid that contains marine organisms degerming composition of the present invention not only has excellent bactericidal property, and strong detergency.Cocoanut fatty acid diethanolamide is nonionogenic tenside, has wetting, washing, the performance such as antistatic and soft, is good suds-stabilizing agent.Alkyl glycoside is the more comprehensive new non-ionic surfactants of a kind of performance, has the characteristic of common nonionic and anion surfactant concurrently, can complete biodegradable and to skin without any pungency.Polyoxyethylenated alcohol sodium sulfate is that anion surfactant has good decontamination, emulsification, foam performance.Disodium ethylene diamine tetraacetate belongs to sequestrant, can make stain remove rapidly surface tension, thereby dissolves, comes off.Sodium-chlor can improve tensio-active agent to the adsorption of fabric as thickening material, improves its detersive power, reduces the micelle-forming concentration of tensio-active agent.Therefore, since adopt the marine organisms degerming agent among the present invention, unrestricted for the selection of tensio-active agent, contain ionogenic surfactant and nonionic surface active agent, overcome the defective of bactericidal liquid detergent of the prior art, had the strong effect of soil removability.
The preparation method who contains the degerming washing liquid of marine organisms degerming composition of the present invention, because order by merging and the mixing condition of each material are comparatively reasonable, so that each component of degerming washing liquid that contains marine organisms degerming composition that makes by preparation method of the present invention mixes good stability.
Embodiment
Embodiment 1
A kind of degerming washing liquid that contains marine organisms degerming composition is characterized in that, percentage ratio meter proportioning is as follows by weight:
Marine organisms degerming agent 2.0-3.5%;
Cocoanut fatty acid diethanolamide 10.0-13.0%;
Alkyl glycoside 4.0-6.0%;
Polyoxyethylenated alcohol sodium sulfate 6.0-8.0%;
Disodium ethylene diamine tetraacetate 0.5-1.0%;
Sodium-chlor 0.5-1.0%;
Essence 0-1.0%;
Surplus is water.
The degerming washing liquid that contains marine organisms degerming composition of the present embodiment not only has excellent bactericidal property, and strong detergency.Cocoanut fatty acid diethanolamide is nonionogenic tenside, has wetting, washing, the performance such as antistatic and soft, is good suds-stabilizing agent.Alkyl glycoside is the more comprehensive new non-ionic surfactants of a kind of performance, has the characteristic of common nonionic and anion surfactant concurrently, can complete biodegradable and to skin without any pungency.Polyoxyethylenated alcohol sodium sulfate is that anion surfactant has good decontamination, emulsification, foam performance.Disodium ethylene diamine tetraacetate belongs to sequestrant, can make stain remove rapidly surface tension, thereby dissolves, comes off.Sodium-chlor can improve tensio-active agent to the adsorption of fabric as thickening material, improves its detersive power, reduces the micelle-forming concentration of tensio-active agent.Therefore, since adopt the marine organisms degerming agent among the present invention, unrestricted for the selection of tensio-active agent, contain ionogenic surfactant and nonionic surface active agent, overcome the defective of bactericidal liquid detergent of the prior art, had the strong effect of soil removability.
In the present embodiment, in order to obtain better degerming and clean effect, the described degerming washing liquid that contains marine organisms degerming composition is characterized in that, percentage ratio meter proportioning is as follows by weight:
Marine organisms degerming agent 2.5-3.0%;
Cocoanut fatty acid diethanolamide 11.0-12.0%;
Alkyl glycoside 4.5-5.5%;
Polyoxyethylenated alcohol sodium sulfate 6.5-7.5%;
Disodium ethylene diamine tetraacetate 0.6-0.8%;
Sodium-chlor 0.6-0.8%;
Essence 0.2-0.4%;
Surplus is water.
In the present embodiment, optional, in order to obtain the moderate degerming washing liquid that contains marine organisms degerming composition of fragrance, this contains the degerming washing liquid of marine organisms degerming composition, and percentage ratio meter proportioning is as follows by weight:
Marine organisms degerming agent 2.5-3.0%;
Cocoanut fatty acid diethanolamide 11.0-12.0%;
Alkyl glycoside 4.5-5.5%;
Polyoxyethylenated alcohol sodium sulfate 6.5-7.5%;
Disodium ethylene diamine tetraacetate 0.6-0.8%;
Sodium-chlor 0.6-0.8%;
Essence 0.2-0.4%;
Surplus is water.
In the present embodiment, in order to obtain better bacteria-eliminating efficacy, optional, described marine organisms degerming agent by weight percentage ratio meter proportioning is as follows:
Cm-chitosan 1.0 ~ 2.0%;
Sargassum polysaccharides 2.0 ~ 4.0%;
Cecropin 6.0 ~ 8.0%;
N-acetylmuramide lycanohydrlase 1.5 ~ 3.5%;
Water 82.5 ~ 89.5%.
In the present embodiment, better for the mixed effect that makes each component, optional, described water is deionized water.
It is the cecropin described in the CN101104637B that described cecropin can adopt notification number, can certainly adopt other cecropin.
Described marine organisms degerming agent can prepare as follows:
Step S10: add cm-chitosan and the Sargassum polysaccharides of proportional quantity in 30 ~ 35 ℃ the water, mix 10 ~ 20 minutes mixed liquor A;
Step S20: add the cecropin of proportional quantity in the mixed liquor A, the time that mixes be 3 ~ 7 minutes mixed liquid B;
Step S30: add the N-acetylmuramide lycanohydrlase of proportional quantity in the mixed liquid B, mix 3 ~ 7 minutes described degerming marine organisms degerming agent.
Embodiment 2
The present embodiment provides a kind of preparation method of the degerming washing liquid that contains marine organisms degerming composition for embodiment 1, it is characterized in that, may further comprise the steps:
Step S10: add the disodium ethylene diamine tetraacetate of proportional quantity in 35 ~ 45 ℃ the water, mix to get mixed liquor A;
Step S20: in mixed liquor A, add cocoanut fatty acid diethanolamide, alkyl glycoside and polyoxyethylenated alcohol sodium sulfate, under 35 ~ 45 ℃ temperature condition, mix to get mixed liquid B;
Step S30: add the marine organisms degerming agent of proportional quantity in the mixed liquid B, under 25 ~ 35 ℃ of temperature condition, mix to get the mixed solution C of institute;
Step S40: add sodium-chlor and the essence of proportional quantity in the mixed solution C, mix to get the described degerming washing liquid that contains marine organisms degerming composition.
The preparation method of the degerming washing liquid that contains marine organisms degerming composition of the present embodiment, because order by merging and the mixing condition of each material are comparatively reasonable, so that each component of degerming washing liquid that contains marine organisms degerming composition that makes by preparation method of the present invention mixes good stability.
In the present embodiment, optional, obtain better mixed effect in order to make each component, among the described step S10, the temperature of described water is 40 ℃.
In the present embodiment, optional, obtain better mixed effect in order to make each component, among the described step S20, the time that mixes is 25-35 minute; Among the described step S30, the time that mixes is 3-7 minute.
In the present embodiment, optionally, in order to obtain to be easy to carry and the degerming washing liquid of the better marine organisms degerming of performance composition, after step S40, also comprise step S50: the degerming washing liquid of marine organisms degerming composition is lowered the temperature and froth breaking after, carry out packing.
Embodiment 3
The present embodiment provides a kind of degerming washing liquid that contains marine organisms degerming composition, and percentage ratio meter proportioning is as follows by weight:
Marine organisms degerming agent 2.0%;
Cocoanut fatty acid diethanolamide 10.0%;
Alkyl glycoside 4.0%;
Polyoxyethylenated alcohol sodium sulfate 6.0%;
Disodium ethylene diamine tetraacetate 0.5%;
Sodium-chlor 0.5%;
Water 77%.
Marine organisms degerming agent in the present embodiment by weight percentage ratio meter proportioning is: cm-chitosan 1.0%; Sargassum polysaccharides 2.0%; Cecropin 6.0%; N-acetylmuramide lycanohydrlase 1.5%; Water 89.5%.
The preparation method of the degerming washing liquid that contains marine organisms degerming composition of the present embodiment carries out as follows:
Step S301: add the disodium ethylene diamine tetraacetate of proportional quantity in 35 ℃ the water, mix to get mixed liquor A;
Step S302: in mixed liquor A, add cocoanut fatty acid diethanolamide, alkyl glycoside and polyoxyethylenated alcohol sodium sulfate, under 35 ℃ temperature condition, mix 25 minutes and get mixed liquid B;
Step S303: add the marine organisms degerming agent of proportional quantity in the mixed liquid B, under 25 ℃ of temperature condition, mix 3 minutes the mixed solution C of institute;
Step S304: add the sodium-chlor of proportional quantity in the mixed solution C, mix to get the degerming washing liquid of described marine organisms degerming composition.
The degerming washing liquid that contains marine organisms degerming composition in the present embodiment after testing, active constituent content meets the GB/T1224-2007 GB to the requirement of washing liquid greater than 12%, ph8.1.
According to the Ministry of Health " 2002 disinfection technology standard ", this product 1:50 diluent acts on 2 minutes average bacteriostasis rates to intestinal bacteria, streptococcus aureus, Candida albicans and is respectively 99.45%, 99.53%, 99.46%, has stronger degerming bacteriostatic action.
White dyes does not detect.
The normal temperature quality guaranteed period is 24 months.
In addition, the degerming washing liquid that contains marine organisms degerming composition in experiment the present embodiment also has stronger clean effect.
Embodiment 4
The present embodiment provides a kind of degerming washing liquid that contains marine organisms degerming composition, and percentage ratio meter proportioning is as follows by weight:
Marine organisms degerming agent 3.5%;
Cocoanut fatty acid diethanolamide 13.0%;
Alkyl glycoside 6.0%;
Polyoxyethylenated alcohol sodium sulfate 8.0%;
Disodium ethylene diamine tetraacetate 1.0%;
Sodium-chlor 1.0%;
Essence 1.0%;
Water 66.5%.
Marine organisms degerming agent in the present embodiment by weight percentage ratio meter proportioning is: cm-chitosan 2.0%; Sargassum polysaccharides 4.0%; Cecropin 8.0%; N-acetylmuramide lycanohydrlase 3.5%; Water 82.5%.
The preparation method of the degerming washing liquid that contains marine organisms degerming composition of the present embodiment carries out as follows:
Step S401: add the disodium ethylene diamine tetraacetate of proportional quantity in 45 ℃ the water, mix to get mixed liquor A;
Step S402: in mixed liquor A, add cocoanut fatty acid diethanolamide, alkyl glycoside and polyoxyethylenated alcohol sodium sulfate, under 45 ℃ temperature condition, mix 35 minutes and get mixed liquid B;
Step S403: add the marine organisms degerming agent of proportional quantity in the mixed liquid B, under 35 ℃ of temperature condition, mix 7 minutes the mixed solution C of institute;
Step S404: add sodium-chlor and the essence of proportional quantity in the mixed solution C, mix to get the described baby's washing liquid that contains marine natural product.
Step S405: the degerming washing liquid that contains marine organisms degerming composition that will contain marine natural product lower the temperature and froth breaking after, carry out packing.
The degerming washing liquid that contains marine organisms degerming composition in the present embodiment after testing, active constituent content meets the GB/T1224-2007 GB to the requirement of washing liquid greater than 12%, ph8.0.
According to the Ministry of Health " 2002 disinfection technology standard ", this product 1:50 diluent acts on 2 minutes average bacteriostasis rates to intestinal bacteria, streptococcus aureus, Candida albicans and is respectively 99.43%, 99.55%, 99.48%, has stronger degerming bacteriostatic action.
White dyes does not detect.
The normal temperature quality guaranteed period is 24 months.
In addition, the degerming washing liquid that contains marine organisms degerming composition in experiment the present embodiment also has stronger clean effect.
Embodiment 5
The present embodiment provides a kind of degerming washing liquid that contains marine organisms degerming composition, and percentage ratio meter proportioning is as follows by weight:
Marine organisms degerming agent 2.5%;
Cocoanut fatty acid diethanolamide 11.0%;
Alkyl glycoside 4.5%;
Polyoxyethylenated alcohol sodium sulfate 6.5%;
Disodium ethylene diamine tetraacetate 0.6%;
Sodium-chlor 0.6%;
Essence 0.2%;
Water 74.1%.
Marine organisms degerming agent in the present embodiment by weight percentage ratio meter proportioning is: cm-chitosan 1.5%; Sargassum polysaccharides 3.0%; Cecropin 7.0%; N-acetylmuramide lycanohydrlase 2.0%; Water 86.5%.
The preparation method of the degerming washing liquid that contains marine organisms degerming composition of the present embodiment carries out as follows:
Step S501: add the disodium ethylene diamine tetraacetate of proportional quantity in 40 ℃ the water, mix to get mixed liquor A;
Step S502: in mixed liquor A, add cocoanut fatty acid diethanolamide, alkyl glycoside and polyoxyethylenated alcohol sodium sulfate, under 40 ℃ temperature condition, mix 30 minutes and get mixed liquid B;
Step S503: add the marine organisms degerming agent of proportional quantity in the mixed liquid B, under 30 ℃ of temperature condition, mix 5 minutes the mixed solution C of institute;
Step S504: add the sodium-chlor of proportional quantity in the mixed solution C, mix to get the described degerming washing liquid that contains marine organisms degerming composition.
Step S505: the degerming washing liquid that will contain marine organisms degerming composition lower the temperature and froth breaking after, carry out packing.
The degerming washing liquid that contains marine organisms degerming composition in the present embodiment after testing, active constituent content meets the GB/T1224-2007 GB to the requirement of washing liquid greater than 12%, ph7.99.
According to the Ministry of Health " 2002 disinfection technology standard ", this product 1:50 diluent acts on 2 minutes average bacteriostasis rates to intestinal bacteria, streptococcus aureus, Candida albicans and is respectively 99.52%, 99.60%, 99.51%, has stronger degerming bacteriostatic action.
White dyes does not detect.
The normal temperature quality guaranteed period is 24 months.
In addition, the degerming washing liquid that contains marine organisms degerming composition in experiment the present embodiment also has stronger clean effect.
Embodiment 6
The present embodiment provides a kind of degerming washing liquid that contains marine organisms degerming composition, and percentage ratio meter proportioning is as follows by weight:
Marine organisms degerming agent 3.0%;
Cocoanut fatty acid diethanolamide 12.0%;
Alkyl glycoside 5.5%;
Polyoxyethylenated alcohol sodium sulfate 7.5%;
Disodium ethylene diamine tetraacetate 0.8%;
Sodium-chlor 0.8%;
Essence 0.4%;
Water 70%.
Marine organisms degerming agent in the present embodiment by weight percentage ratio meter proportioning is: cm-chitosan 1.5%; Sargassum polysaccharides 3.0%; Cecropin 7.0%; N-acetylmuramide lycanohydrlase 2.0%; Water 86.5%.
The preparation method of the degerming washing liquid that contains marine organisms degerming composition of the present embodiment carries out as follows:
Step S601: add the disodium ethylene diamine tetraacetate of proportional quantity in 40 ℃ the water, mix to get mixed liquor A;
Step S602: in mixed liquor A, add cocoanut fatty acid diethanolamide, alkyl glycoside and polyoxyethylenated alcohol sodium sulfate, under 40 ℃ temperature condition, mix 30 minutes and get mixed liquid B;
Step S603: add the marine organisms degerming agent of proportional quantity in the mixed liquid B, under 30 ℃ of temperature condition, mix 5 minutes the mixed solution C of institute;
Step S604: add sodium-chlor and the essence of proportional quantity in the mixed solution C, mix to get the described degerming washing liquid that contains marine organisms degerming composition.
Step S605: the degerming washing liquid that will contain marine organisms degerming composition lower the temperature and froth breaking after, carry out packing.
The degerming washing liquid that contains marine organisms degerming composition in the present embodiment after testing, active constituent content meets the GB/T1224-2007 GB to the requirement of washing liquid greater than 12%, ph7.97.
According to the Ministry of Health " 2002 disinfection technology standard ", this product 1:50 diluent acts on 2 minutes average bacteriostasis rates to intestinal bacteria, streptococcus aureus, Candida albicans and is respectively 99.53%, 99.62%, 99.52%, has stronger degerming bacteriostatic action.
White dyes does not detect.
The normal temperature quality guaranteed period is 24 months.
In addition, the degerming washing liquid that contains marine organisms degerming composition in experiment the present embodiment also has stronger clean effect.
It should be noted that at last: above embodiment only in order to technical scheme of the present invention to be described, is not intended to limit; Although with reference to previous embodiment the present invention is had been described in detail, those of ordinary skill in the art is to be understood that: it still can be made amendment to the technical scheme that aforementioned each embodiment puts down in writing, and perhaps part technical characterictic wherein is equal to replacement; And these modifications or replacement do not make the essence of appropriate technical solution break away from the spirit and scope of various embodiments of the present invention technical scheme.
Claims (9)
1. a degerming washing liquid that contains marine organisms degerming composition is characterized in that, percentage ratio meter proportioning is as follows by weight:
Marine organisms degerming agent 2.0-3.5%;
Cocoanut fatty acid diethanolamide 10.0-13.0%;
Alkyl glycoside 4.0-6.0%;
Polyoxyethylenated alcohol sodium sulfate 6.0-8.0%;
Disodium ethylene diamine tetraacetate 0.5-1.0%;
Sodium-chlor 0.5-1.0%;
Essence 0-1.0%;
Surplus is water.
2. the degerming washing liquid that contains marine organisms degerming composition according to claim 1 is characterized in that, percentage ratio meter proportioning is as follows by weight:
Marine organisms degerming agent 2.5-3.0%;
Cocoanut fatty acid diethanolamide 11.0-12.0%;
Alkyl glycoside 4.5-5.5%;
Polyoxyethylenated alcohol sodium sulfate 6.5-7.5%;
Disodium ethylene diamine tetraacetate 0.6-0.8%;
Sodium-chlor 0.6-0.8%;
Essence 0.2-0.4%;
Surplus is water.
3. the degerming washing liquid that contains marine organisms degerming composition according to claim 1 and 2 is characterized in that, described marine organisms degerming agent by weight percentage ratio meter proportioning is as follows:
Cm-chitosan 1.0 ~ 2.0%;
Sargassum polysaccharides 2.0 ~ 4.0%;
Cecropin 6.0 ~ 8.0%;
N-acetylmuramide lycanohydrlase 1.5 ~ 3.5%;
Water 82.5 ~ 89.5%.
4. the degerming washing liquid that contains marine organisms degerming composition according to claim 1 and 2 is characterized in that, described essence is plant essence.
5. the degerming washing liquid that contains marine organisms degerming composition according to claim 1 and 2 is characterized in that, described water is deionized water.
6. one kind such as each described preparation method who contains the degerming washing liquid of marine organisms degerming composition of claim 1-5, it is characterized in that, may further comprise the steps:
Step S10: add the disodium ethylene diamine tetraacetate of proportional quantity in 35 ~ 45 ℃ the water, mix to get mixed liquor A;
Step S20: in mixed liquor A, add cocoanut fatty acid diethanolamide, alkyl glycoside and polyoxyethylenated alcohol sodium sulfate, under 35 ~ 45 ℃ temperature condition, mix to get mixed liquid B;
Step S30: add the marine organisms degerming agent of proportional quantity in the mixed liquid B, under 25 ~ 35 ℃ of temperature condition, mix to get the mixed solution C of institute;
Step S40: add sodium-chlor and the essence of proportional quantity in the mixed solution C, mix to get the described degerming washing liquid that contains marine organisms degerming composition.
7. the preparation method who contains the degerming washing liquid of marine organisms degerming composition according to claim 6, it is characterized in that: among the described step S10, the temperature of described water is 40 ℃.
8. the preparation method who contains the degerming washing liquid of marine organisms degerming composition according to claim 6, it is characterized in that: among the described step S20, the time that mixes is 25-35 minute; Among the described step S 30, the time that mixes is 3-7 minute.
9. the preparation method who contains the degerming washing liquid of marine organisms degerming composition according to claim 6, it is characterized in that: after step S40, also comprise step S50: the degerming washing liquid that will contain marine organisms degerming composition lower the temperature and froth breaking after, carry out packing.
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