CN106366207A - Fenugreek water-soluble polysaccharide hand sanitizer and preparation method thereof - Google Patents
Fenugreek water-soluble polysaccharide hand sanitizer and preparation method thereof Download PDFInfo
- Publication number
- CN106366207A CN106366207A CN201610810774.XA CN201610810774A CN106366207A CN 106366207 A CN106366207 A CN 106366207A CN 201610810774 A CN201610810774 A CN 201610810774A CN 106366207 A CN106366207 A CN 106366207A
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- CN
- China
- Prior art keywords
- soluble polysaccharide
- semen trigonellae
- handwashing liquid
- water soluble
- water
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/0003—General processes for their isolation or fractionation, e.g. purification or extraction from biomass
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
Abstract
The invention provides a fenugreek water-soluble polysaccharide hand sanitizer and a preparation method thereof. The fenugreek water-soluble polysaccharide hand sanitizer is prepared from the following raw materials in percentage by weight: 15 to 20 percent of cocamidopropyl betaine, 5 to 10 percent of dodecyl polyglucoside, 1 to 4 percent of glycerinum, 10 to 20 percent of a fenugreek water-soluble polysaccharide solution, 1 to 6 percent of cocoanut fatty acid diethanolamide, 0.1 to 0.5 percent of isopropyl myristate, 0.2 to 0.5 percent of citric acid, 0.5 to 1 percent of sodium citrate 0.005 to 0.05 percent of essence and the balance deionized water. The fenugreek water-soluble polysaccharide hand sanitizer provided by the invention has the effects of cleaning skin, sterilizing, moisturizing and the like; the added fenugreek water-soluble polysaccharide has high moisture absorbability and moisture retentivity, has a good film-forming effect, reduces loss of water on the surface of skin, has high antibacterial property and maintains double hands to be sanitary.
Description
Technical field
The invention belongs to daily living article field, especially relate to a kind of Semen Trigonellae water soluble polysaccharide handwashing liquid and its system
Preparation Method.
Background technology
Continuous improvement with people's living standard and the continuous intensification of health understanding, washing one's hands, it is daily to have become as people
Habitual program in life.Handwashing liquid replaces traditional hand-washing articles such as fancy soap to become important cleaning supplies in daily life.
Nowadays, people increasingly pay attention to the conditioning liquid of hand skin, and handss are referred to as " second face " of woman, thus right
The Functional Requirement of handwashing liquid also gets more and more.And reaching its maturity with handwashing liquid production technology, the washing of various specific functions
Handss liquid also constantly comes out, and wherein comprises a large amount of products containing natural plant composition and is more obtained extensively due to pollution-free, low stimulation
Big consumer is liked.
Semen Trigonellae, also known as Trigonella foenum-graecum, Rhizoma et radix valerianae, is pulse family Papillionoideae frenugreek spp plant.Contain in calabash graecum seed
40% about locust beam gum, in interior plumule breast, locust beam gum is widely used in food, medicine, the field such as oil field compression fracture, carries residue after locust beam gum
Middle insoluble polysaccharide at present nearly as offal treatment, it has been investigated that, calabash graecum seed through enzymolysis water soluble polysaccharide tool
There are good non-oxidizability, moisturizing, sterilization and thickening power.
Content of the invention
In view of this, it is contemplated that proposing a kind of Semen Trigonellae water soluble polysaccharide handwashing liquid and preparation method thereof, this is washed one's hands
Liquid has bactericidal action, and the cleaning maintenance of hand skin is had functions that good, nontoxic, non-stimulated；Meanwhile, also increase
Semen Trigonellae puies forward value and the market value of the residue after glue.
For reaching above-mentioned purpose, the technical scheme is that and be achieved in that:
A kind of Semen Trigonellae water soluble polysaccharide, this Semen Trigonellae water soluble polysaccharide is obtained by the method including the steps: will
Residue after Semen Trigonellae carries locust beam gum is carried out defat, after alcohol extraction, adds cellulase, mixed with water, then carry out extracting, enzyme denaturing,
After filtration, obtain the solution containing Semen Trigonellae water soluble polysaccharide.
Further, the temperature of described extraction step is 45 DEG C.
The purposes of described Semen Trigonellae water soluble polysaccharide, described Semen Trigonellae water soluble polysaccharide in preparing handwashing liquid should
With.
A kind of handwashing liquid, contains the described solution containing Semen Trigonellae water soluble polysaccharide in this handwashing liquid.
Further, the mass percent of the solution containing Semen Trigonellae water soluble polysaccharide in described handwashing liquid is 10-20%.
Further, described handwashing liquid is made up of the raw material including following percentage by weight:
Preferably, described handwashing liquid is made up of the raw material including following percentage by weight:
Further, in the described solution containing Semen Trigonellae water soluble polysaccharide, the content of Semen Trigonellae water soluble polysaccharide is 5%.
The preparation method of described handwashing liquid, comprises the steps:
(1) by cocamidopropyl betaine, glycerol, the solution of Semen Trigonellae water soluble polysaccharide, Dodecyl Glucoside, coconut palm
Seed oil fatty diglycollic amide is dissolved in deionized water, and mix homogeneously is stirred at room temperature；
(2) citric acid, sodium citrate are slowly added to, are slowly stirred 10-20min so as to mix uniformly；
(3) be slowly added to isopropyl myristate, be stirred continuously mixing, ultrasonic to non-foam, stand, obtain final product Semen Trigonellae water
Soluble polysaccharide handwashing liquid.
Further, the ph value of the Semen Trigonellae water soluble polysaccharide handwashing liquid being obtained in described step (3) is 6-7.
With respect to prior art, Semen Trigonellae water soluble polysaccharide handwashing liquid of the present invention and preparation method thereof has following
Advantage:
(1) Semen Trigonellae water soluble polysaccharide handwashing liquid of the present invention has the effects such as cleaning skin and sterilization, moisturizing；Add
Plus Semen Trigonellae water soluble polysaccharide have a good moisture absorbability and moisture retentivity, good filming effect reduces scattering and disappearing of skin surface moisture, good
Good bacteria resistance, keeps both hands health.
(2) Semen Trigonellae water soluble polysaccharide handwashing liquid of the present invention is raw materials used includes Semen Trigonellae water soluble polysaccharide, coconut palm
The good group of the biocompatibility of oleamidopropyl betaine, Dodecyl Glucoside and cocoanut fatty acid diethanolamide etc.
Point, gentle environmental protection, environmentally safe.
(3) preparation method of Semen Trigonellae water soluble polysaccharide handwashing liquid of the present invention is simply it is easy to operate.
Specific embodiment
Unless otherwise indicated, term used herein is respectively provided with the conventional implication understanding of those skilled in the art, in order to
Readily appreciate the present invention, some terms used herein have been carried out following definitions.
All of Digital ID, such as ph, temperature, time, concentration, including scope, are all approximations.It is to be understood that although
Term " about " is all added before always clearly not describing all of Digital ID.Simultaneously it will also be understood that although always not clear and definite
Narration, reagent described herein is only example, and its equivalent is known in the art.
To describe the present invention with reference to embodiment in detail.
Embodiment 1
Described Semen Trigonellae water soluble polysaccharide is obtained by the method including the steps: takes 10g Semen Trigonellae to carry after locust beam gum
Residue carry out defat, after alcohol extraction, add 200g distilled water, 0.1g cellulase, citric acid adjusts ph value=6,45 DEG C of stirrings carry
Take 2 hours, filter, filtrate keeps 30 minutes enzyme denaturing, 5 μm of membrane filtrations under the conditions of 80 DEG C, and filtrate rotary evaporation is concentrated into about
50ml, obtains 5% solution containing Semen Trigonellae water soluble polysaccharide.
Described handwashing liquid, is made up of the raw material including following percentage by weight:
The preparation method of described handwashing liquid, comprises the steps:
(1) by cocamidopropyl betaine, glycerol, the solution of Semen Trigonellae water soluble polysaccharide, Dodecyl Glucoside, coconut palm
Seed oil fatty diglycollic amide is dissolved in deionized water, and mix homogeneously is stirred at room temperature；
(2) citric acid, sodium citrate are slowly added to, are slowly stirred 10min so as to mix uniformly；
(3) be slowly added to isopropyl myristate, be stirred continuously mixing, ultrasonic to non-foam, stand, obtain final product Semen Trigonellae water
Soluble polysaccharide handwashing liquid.
Embodiment 2
Described Semen Trigonellae water soluble polysaccharide is obtained by the method including the steps: takes 10g Semen Trigonellae to carry after locust beam gum
Residue carry out defat, after alcohol extraction, add 200g distilled water, 0.1g cellulase, citric acid adjusts ph value=6,45 DEG C of stirrings carry
Take 2 hours, filter, filtrate keeps 30 minutes enzyme denaturing, 5 μm of membrane filtrations under the conditions of 80 DEG C, and filtrate rotary evaporation is concentrated into about
50ml, obtains 5% solution containing Semen Trigonellae water soluble polysaccharide.
Described handwashing liquid, is made up of the raw material including following percentage by weight:
The preparation method of described handwashing liquid, comprises the steps:
(1) by cocamidopropyl betaine, glycerol, the solution of Semen Trigonellae water soluble polysaccharide, Dodecyl Glucoside, coconut palm
Seed oil fatty diglycollic amide is dissolved in deionized water, and mix homogeneously is stirred at room temperature；
(2) citric acid, sodium citrate are slowly added to, are slowly stirred 10min so as to mix uniformly；
(3) be slowly added to isopropyl myristate, be stirred continuously mixing, ultrasonic to non-foam, stand, obtain final product Semen Trigonellae water
Soluble polysaccharide handwashing liquid.
Embodiment 3
Described Semen Trigonellae water soluble polysaccharide is obtained by the method including the steps: takes 10g Semen Trigonellae to carry after locust beam gum
Residue carry out defat, after alcohol extraction, add 200g distilled water, 0.1g cellulase, citric acid adjusts ph value=6,45 DEG C of stirrings carry
Take 2 hours, filter, filtrate keeps 30 minutes enzyme denaturing, 5 μm of membrane filtrations under the conditions of 80 DEG C, and filtrate rotary evaporation is concentrated into about
50ml, obtains 5% solution containing Semen Trigonellae water soluble polysaccharide.
Described handwashing liquid, is made up of the raw material including following percentage by weight:
The preparation method of described Semen Trigonellae water soluble polysaccharide handwashing liquid, comprises the steps:
(1) by cocamidopropyl betaine, glycerol, the solution of Semen Trigonellae water soluble polysaccharide, Dodecyl Glucoside, coconut palm
Seed oil fatty diglycollic amide is dissolved in deionized water, and mix homogeneously is stirred at room temperature；
(2) citric acid, sodium citrate are slowly added to, are slowly stirred 10min so as to mix uniformly；
(3) be slowly added to isopropyl myristate, be stirred continuously mixing, ultrasonic to non-foam, stand, obtain final product Semen Trigonellae water
Soluble polysaccharide handwashing liquid.
Embodiment 4
Described Semen Trigonellae water soluble polysaccharide is obtained by the method including the steps: takes 10g Semen Trigonellae to carry after locust beam gum
Residue carry out defat, after alcohol extraction, add 200g distilled water, 0.1g cellulase, citric acid adjusts ph value=6,45 DEG C of stirrings carry
Take 2 hours, filter, filtrate keeps 30 minutes enzyme denaturing, 5 μm of membrane filtrations under the conditions of 80 DEG C, and filtrate rotary evaporation is concentrated into about
50ml, obtains 5% solution containing Semen Trigonellae water soluble polysaccharide.
Described handwashing liquid, is made up of the raw material including following percentage by weight:
The preparation method of described Semen Trigonellae water soluble polysaccharide handwashing liquid, comprises the steps:
(1) by cocamidopropyl betaine, glycerol, the solution of Semen Trigonellae water soluble polysaccharide, Dodecyl Glucoside, coconut palm
Seed oil fatty diglycollic amide is dissolved in deionized water, and mix homogeneously is stirred at room temperature；
(2) citric acid, sodium citrate are slowly added to, are slowly stirred 10min so as to mix uniformly；
(3) be slowly added to isopropyl myristate, be stirred continuously mixing, ultrasonic to non-foam, stand, obtain final product Semen Trigonellae water
Soluble polysaccharide handwashing liquid.
Comparative example 1
A kind of handwashing liquid, is made up of the raw material including following percentage by weight: by the raw material including following percentage by weight
Make:
The preparation method of described handwashing liquid, comprises the steps:
(1) cocamidopropyl betaine, glycerol, Dodecyl Glucoside are dissolved in deionized water, stir at room temperature
Mix mix homogeneously；
(2) citric acid, sodium citrate are slowly added to, are slowly stirred 10min so as to mix uniformly；
(3) be slowly added to isopropyl myristate, be stirred continuously mixing, ultrasonic to non-foam, stand, obtain final product handwashing liquid.
Obtained by above step and material proportioning and do not contain Semen Trigonellae water soluble polysaccharide aqueous solution, Cocamidopropyl
The handwashing liquid comparative example of Radix Betae alkali composition.
Comparative example 2
A kind of handwashing liquid, is made up of the raw material including following percentage by weight:
The preparation method of described handwashing liquid, comprises the steps:
(1) will be molten to cocamidopropyl betaine, glycerol, Dodecyl Glucoside, cocoanut fatty acid diethanolamide
In deionized water, mix homogeneously is stirred at room temperature；
(2) citric acid, sodium citrate are slowly added to, are slowly stirred 10min so as to mix uniformly；
(3) be slowly added to isopropyl myristate, be stirred continuously mixing, ultrasonic to non-foam, stand, obtain final product handwashing liquid.
By the corresponding test specification present invention is carried out in bactericidal property, moisture absorbability and moisture retentivity to above-described embodiment and comparative example
Can all there is excellent performance.
Test event includes:
(1) the bactericidal property test of Semen Trigonellae water soluble polysaccharide handwashing liquid.
" experimentatioies of several wash product bactericidal effects " that experimental technique is write with reference to Zhao Yanan etc., select from " Jilin
Medicine and pharmacy college journal " -2009,30 (3), the bactericidal property using embodiment 2 is as shown in table 1.
Table 1 handwashing liquid bactericidal effect
Visible according to table 1 data, due to the addition of Semen Trigonellae water soluble polysaccharide, prolongation over time, bactericidal effect increases
Plus.The bactericidal effect of the handwashing liquid that embodiment 1-4 and comparative example 1-2 prepare is shown in Table 2, and the time of washing one's hands is 20s.
The different embodiment handwashing liquid bactericidal effect of table 2
Visible according to table 2 data, with the increase of Semen Trigonellae water soluble polysaccharide amount, bactericidal effect substantially increases, therefore, through surveying
The bactericidal property of the examination embodiment of the present invention is better than comparative example；Comparative example 2 and 3 finds out, cocamidopropyl betaine adds
Amount has an impact to bactericidal effect, cocamidopropyl betaine and Semen Trigonellae water soluble polysaccharide dosage phase in embodiment 1 and 4
With bactericidal effect is basically identical, illustrates that other components biocidal efficacies are little.
(2) the moisture-absorbing moisture-keeping performance test of the handwashing liquid of water soluble polysaccharide containing Semen Trigonellae.
Under room temperature (25 DEG C) relative humidity (rh) be 81% saturated ammonium sulfate aqueous solution exsiccator be super-humid conditions, satisfy
The exsiccator being 43% for relative humidity (rh) with potassium carbonate is low humidity conditions, the moisture sorption effect of determination sample；By sample preparation
Become 50% aqueous solution, measure moistening effect in above-mentioned two situations, result is as shown in table 3.
The moisture-absorbing moisture-keeping effect of table 3 sample
The preferable composition of moistening effect that glycerol, Polyethylene Glycol, Aloe polysaccharide are conventional, is found out by table 3, high humidity
Lower Semen Trigonellae water soluble polysaccharide hygroscopicity does not project, but moistening effect is preferable；Under low humidity conditions, Semen Trigonellae water solublity is many
The moisture absorption of sugar, moisture retention are very prominent, especially have good hygroscopicity.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all essences in the present invention
Within god and principle, any modification, equivalent substitution and improvement made etc., should be included within the scope of the present invention.
Claims (9)
1. a kind of Semen Trigonellae water soluble polysaccharide it is characterised in that: this Semen Trigonellae water soluble polysaccharide is by the side including the steps
Method is obtained: Semen Trigonellae is carried the residue after locust beam gum and carries out defat, after alcohol extraction, add cellulase, mix with water, then carried
Take, enzyme denaturing, after filtration, obtain the solution containing Semen Trigonellae water soluble polysaccharide.
2. Semen Trigonellae water soluble polysaccharide according to claim 1 it is characterised in that: the temperature of described extraction step be 45
℃.
3. the Semen Trigonellae water soluble polysaccharide described in claim 1 or 2 purposes it is characterised in that: described Semen Trigonellae water solublity
Application in preparing handwashing liquid for the polysaccharide.
4. a kind of handwashing liquid it is characterised in that: many containing water solublity containing Semen Trigonellae described in claim 1 or 2 in this handwashing liquid
The solution of sugar.
5. handwashing liquid according to claim 4 it is characterised in that: the water soluble polysaccharide containing Semen Trigonellae in described handwashing liquid
Solution mass percent be 10-20%.
6. handwashing liquid according to claim 5 it is characterised in that: described handwashing liquid is by including following percentage by weight
Raw material is made:
7. handwashing liquid according to claim 6 it is characterised in that: described handwashing liquid is by including following percentage by weight
Raw material is made:
8. the handwashing liquid according to any one of claim 4-6 it is characterised in that: described water soluble polysaccharide containing Semen Trigonellae
Solution in Semen Trigonellae water soluble polysaccharide content be 5%.
9. the handwashing liquid any one of claim 4-6 preparation method it is characterised in that: comprise the steps:
(1) by cocamidopropyl betaine, glycerol, the solution of Semen Trigonellae water soluble polysaccharide, Dodecyl Glucoside, Oleum Cocois
Fatty diglycollic amide is dissolved in deionized water, and mix homogeneously is stirred at room temperature；
(2) citric acid, sodium citrate are slowly added to, are slowly stirred 10-20min so as to mix uniformly；
(3) be slowly added to isopropyl myristate, be stirred continuously mixing, ultrasonic to non-foam, stand, obtain final product Semen Trigonellae water solublity
Polysaccharide handwashing liquid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610810774.XA CN106366207B (en) | 2016-09-08 | 2016-09-08 | A kind of faenum graecum water-soluble polysaccharide hand cleanser and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610810774.XA CN106366207B (en) | 2016-09-08 | 2016-09-08 | A kind of faenum graecum water-soluble polysaccharide hand cleanser and preparation method thereof |
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| CN106366207A true CN106366207A (en) | 2017-02-01 |
| CN106366207B CN106366207B (en) | 2019-04-12 |
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| CN201610810774.XA Expired - Fee Related CN106366207B (en) | 2016-09-08 | 2016-09-08 | A kind of faenum graecum water-soluble polysaccharide hand cleanser and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107157801A (en) * | 2017-06-13 | 2017-09-15 | 甘肃民族师范学院 | Containing natural Radix Salviae Miltiorrhizae polysaccharide compound antibacterial hand sanitizer and preparation method thereof |
| CN107744495A (en) * | 2017-11-01 | 2018-03-02 | 吕凤鹏 | A kind of medical inspection section hand cleanser and preparation method thereof |
| CN110591825A (en) * | 2019-10-30 | 2019-12-20 | 鹰潭华宝香精有限公司 | Preparation method of fenugreek concentrate |
| CN110755347A (en) * | 2019-11-11 | 2020-02-07 | 中国科学院西北高原生物研究所 | Skin moistening humectant and preparation method and application thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107157801A (en) * | 2017-06-13 | 2017-09-15 | 甘肃民族师范学院 | Containing natural Radix Salviae Miltiorrhizae polysaccharide compound antibacterial hand sanitizer and preparation method thereof |
| CN107744495A (en) * | 2017-11-01 | 2018-03-02 | 吕凤鹏 | A kind of medical inspection section hand cleanser and preparation method thereof |
| CN110591825A (en) * | 2019-10-30 | 2019-12-20 | 鹰潭华宝香精有限公司 | Preparation method of fenugreek concentrate |
| CN110755347A (en) * | 2019-11-11 | 2020-02-07 | 中国科学院西北高原生物研究所 | Skin moistening humectant and preparation method and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106366207B (en) | 2019-04-12 |
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