CN104611150A - Clear and stable detergent containing high-concentration soapberry extract - Google Patents
Clear and stable detergent containing high-concentration soapberry extract Download PDFInfo
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Abstract
The invention discloses a clear and stable detergent containing a high-concentration soapberry extract. The detergent comprises a thickening composition comprising the following components: 0.05wt%-1.0wt% of cationic cellulose JR-400, 2wt%-4wt% of PEG-150 distearate and 1.0wt%-5.0wt% of polyglycerol-10. The high-concentration soapberry extract contains a large amount of high-purity saponin which is a non-ionic surfactant, when the large amount of saponin is added in the detergent, the detergent is difficult to be thickened; the compounded thickening composition is added into the detergent, the product is moderate in thickness, the detergent is thickened and meanwhile, the detergent maintains clear; the thickness of the detergent basically remains unchanged and the detergent is stable in performance; the detergent without the thickening composition is difficult to be thickened and the phenomena of precipitation, discoloration, turbidity and the like are easily caused during the thickening process.
Description
Technical field
The invention belongs to the preparation field of washing composition, be specifically related to a kind of clarification containing high density Seed of Chinese Soapberry extracting solution, stable washing composition.
Background technology
Sapindoside (Soapnut Saponin) is containing abundant glucosides class material, be mainly triterpene saponin, sesquiterpene glucosides class, be a kind of natural mild nonionogenic tenside, having confirmed to act on human body skin has antibacterial, sterilization, anti-inflammatory and dandruff-removing itching-relieve effect.In addition also containing many materials useful to human body, as: reducing sugar, lipid acid, grease, oleic acid, carotenoid, Yan acid, riboflavin, protein, 10 multiple amino acids such as vitamins C, vitamin A, vitamins B and Methionin, tyrosine, phenylalanine, L-glutamic acid, glycine and Histidine.Therefore sapindoside by a large amount of for the manufacture of natural nuisance-free articles for washing.
When general preparation is containing the washing composition of sapindoside composition, usually direct using sapindoside extracting solution as raw material, then be aided with other compositions and make washing composition.But in the pulp extracting solution of Seed of Chinese Soapberry, containing outside a large amount of saponins materials, also containing compositions such as some pigments, reducing sugar, amino acid.Saponin(e is nonionogenic tenside, when it makes an addition in washing composition in a large number, causes washing composition to be difficult to thickening.And because the existence of other compositions in extracting solution, when being made an addition in washing composition by the Seed of Chinese Soapberry extracting solution of high density, easily produce the phenomenons such as precipitation, variable color, muddiness.Therefore in order to ensure that the denseness of washing composition is moderate, clarification, in washing composition, generally all can not add the sapindoside extracting solution of high density, cause saponin content in washing composition lower like this, clean effect is not remarkable.
Summary of the invention
The object of the invention is to be difficult to thickening for the washing composition containing high density Seed of Chinese Soapberry extracting solution, do not clarify, and denseness is unstable when the temperature is changed, and a kind of clarification containing high density Seed of Chinese Soapberry extracting solution, stable washing composition are provided.By adding thickening combination in washing composition, make the washing composition denseness containing high density Seed of Chinese Soapberry extracting solution moderate, and denseness can not have very large change along with the change of temperature, and the clarification of product, stable can be kept in thickening.
For achieving the above object, the present invention adopts following technical scheme:
A kind of clarification containing high density Seed of Chinese Soapberry extracting solution, stable washing composition, containing thickening combination composed of the following components in described washing composition, the per-cent that each component accounts for washing composition total mass is: cationic cellulose JR-400 0.05 wt% ~ 1.0wt%, PEG-150 SUNSOFT Q-182S 2 wt% ~ 4wt%, Natrulon H-10 1.0 wt% ~ 5.0wt%; In described high density Seed of Chinese Soapberry extracting solution, saponin content is 65wt% ~ 85wt%.
Also containing anti-sensitive composition composed of the following components in described washing composition, the per-cent that each component accounts for washing composition total mass is: α-Hydagen B 2wt% ~ 5wt%, Rizinsan K2 A2 0.1 wt% ~ 0.5wt%, scutellarin 0.2 wt% ~ 0.4wt%, Herba portulacae extract 0.1 wt% ~ 0.5wt%.
Described washing composition also contains following component, by massfraction:
High density Seed of Chinese Soapberry extracting solution 65 wt% ~ 70wt%,
Polyoxyethylenated alcohol sodium sulfate 8 wt% ~ 10wt%,
Coco-nut oil fatty acid 2wt% ~ 4wt%,
Alkyl glycoside 0.5wt% ~ 2.0wt%,
AMONYL 380LC 3wt% ~ 5wt%,
Citric acid 0.05wt% ~ 0.3wt%,
Trisodium Citrate 0.05wt% ~ 0.3wt%,
Sodium D-isoascorbate 0.3wt% ~ 0.5wt%,
Tripoly phosphate sodium STPP 0.1wt% ~ 0.2wt%,
Disodium ethylene diamine tetraacetate 0.1wt% ~ 0.3wt%,
Methylisothiazolinone 0.005wt% ~ 0.01wt%,
Washing composition all components massfraction sum is 100%.
The preparation method of Herba portulacae extract is: get new fresh purslane, cleans, shreds, add the water of 10 ~ 15 times of quality, and 80 ~ 100 DEG C decoct 2 ~ 3 h, filter, get filtrate; Moisture is volatilized, obtains extract, 30 ~ 50 DEG C of oven dry.
A kind of preparation contains the clarification of high density Seed of Chinese Soapberry extracting solution, the method for stable washing composition as above: comprise the following steps:
(1) high density Seed of Chinese Soapberry extracting solution is placed in container, opens and stir, add thickening combination, be heated to 80 DEG C;
(2) then add polyoxyethylenated alcohol sodium sulfate, coco-nut oil fatty acid, fully after mixing, be down to room temperature;
(3) continue to add alkyl glycoside, AMONYL 380LC, anti-sensitive composition, stir 15 ~ 30 min;
(4) then add sodium D-isoascorbate, tripoly phosphate sodium STPP, disodium ethylene diamine tetraacetate carry out protecting look, protecting the look time is 5 ~ 10 min;
(5) add citric acid, Trisodium Citrate, regulate pH; Finally add and finally add methylisothiazolinone, after stirring 5 ~ 10 min, ageing, filling, obtained finished product.
Because the washing composition of the Seed of Chinese Soapberry extracting solution containing high density color when pH value is less is more shallow, when pH value is larger, color is darker, therefore adopt citric acid, sodium citrate buffer solution to regulate the pH value of washing composition, make the color of washing composition moderate, and keep stable.
Sapindoside is mainly based on Triterpene saponins, and the molecular structure of triterpenoid sapogenin is made up of two portions: a part is the saponin(e structure that carboxyl and glucosyl group (or other glycosyls) are connected to form, i.e. water-wet side; Another part is aglycon, i.e. non-hydrophilic end.Therefore made an addition in washing composition, washing composition can be made to subtract cunning, and play moisture-keeping function.
And α-Hydagen B, Rizinsan K2 A2, scutellarin, this several combinations of substances of Herba portulacae extract together, make an addition in washing composition, common contact anaphylactogen can be resisted, make can also use the crowd of the articles for washing allergy such as general shampoo, liquid detergent, hair dye, soap.
Beneficial effect of the present invention is:
(1) the present invention adds the Seed of Chinese Soapberry extracting solution of high density in washing composition, it is nonionogenic tenside, greatly reduce the usage quantity of anion surfactant, reduce the content of synthetic material, thus reduce the viscosity of product, humidity-holding effect is good, not satiny, performance is gentle, non-stimulated to skin, natural pollution-free, be a kind of environmentally friendly product;
(2) the present invention adds thickening combination in washing composition, solve and add (saponin(e is nonionogenic tenside) and the problem of not easily thickening because of high density Seed of Chinese Soapberry extracting solution, ensure that product denseness is moderate, and denseness can not vary with temperature and change, stable performance, can keep product to clarify simultaneously while thickening; And do not add the washing composition of thickening combination, be then difficult to thickening, and in thickening, be easy to occur the phenomenons such as precipitation, variable color, muddiness;
(3) more excellent, the present invention adds by α-Hydagen B in washing composition, Rizinsan K2 A2, scutellarin, the anti-sensitive composition of Herba portulacae extract composition, make product also be applicable to easy allergic human population to use, really achieve product natural pollution-free, not easily irritated, denseness is moderate, viscosity is little, humidity-holding effect is good.
Embodiment
The present invention's the following example further illustrates the present invention, but protection scope of the present invention is not limited to the following example.
Containing clarification, the stable washing composition of high density Seed of Chinese Soapberry extracting solution, composed of the following components:
High density Seed of Chinese Soapberry extracting solution 65 ~ 70 wt%, in described high density Seed of Chinese Soapberry extracting solution, saponin content is 65wt% ~ 85wt%;
Polyoxyethylenated alcohol sodium sulfate 8 ~ 10 wt%,
Coco-nut oil fatty acid 2 ~ 4 wt%,
Alkyl glycoside 0.5 ~ 2.0 wt%,
AMONYL 380LC 3 ~ 5 wt%,
Citric acid 0.05 ~ 0.3 wt%,
Trisodium Citrate 0.05 ~ 0.3 wt%,
Sodium D-isoascorbate 0.3 ~ 0.5 wt%,
Tripoly phosphate sodium STPP 0.1 ~ 0.2 wt%,
Disodium ethylene diamine tetraacetate 0.1 ~ 0.3 wt%,
Methylisothiazolinone 0.005 ~ 0.01 wt%,
Thickening combination (cationic cellulose JR-400 0.05 ~ 1.0wt%, PEG-150 SUNSOFT Q-182S 2 ~ 4wt%, Natrulon H-10 1.0 ~ 5.0wt%),
Anti-sensitive composition (α-Hydagen B 2 ~ 5 wt%, Rizinsan K2 A2 0.1 ~ 0.5wt%, scutellarin 0.2 ~ 0.4wt%, Herba portulacae extract 0.1 ~ 0.5wt%),
Washing composition all components massfraction sum is 100%.
embodiment 1
Containing clarification, the stable washing composition of high density Seed of Chinese Soapberry extracting solution, composed of the following components:
High density Seed of Chinese Soapberry extracting solution 70 wt%, in described high density Seed of Chinese Soapberry extracting solution, saponin content is 65.37wt%;
Polyoxyethylenated alcohol sodium sulfate 10 wt%,
Coco-nut oil fatty acid 4 wt%,
Alkyl glycoside 1.3 wt%,
AMONYL 380LC 3.0 wt%,
Citric acid 0.15 wt%,
Trisodium Citrate 0.15 wt%,
Sodium D-isoascorbate 0.4 wt%,
Tripoly phosphate sodium STPP 0.15 wt%,
Disodium ethylene diamine tetraacetate 0.2 wt%,
Methylisothiazolinone 0.005 wt%,
Thickening combination:
(cationic cellulose JR-400 0.5 wt%,
PEG-150 SUNSOFT Q-182S 4 wt%,
Natrulon H-10 3.245 wt%),
Anti-sensitive composition:
(α-Hydagen B 2 wt%,
Rizinsan K2 A2 0.3 wt%,
Scutellarin 0.3 wt%,
Herba portulacae extract 0.3 wt%);
A kind of preparation contains the clarification of high density Seed of Chinese Soapberry extracting solution, the method for stable washing composition as above: comprise the following steps:
(1) Seed of Chinese Soapberry extracting solution is placed in container, opens and stir, add thickening combination, be heated to 80 DEG C;
(2) then add polyoxyethylenated alcohol sodium sulfate, coco-nut oil fatty acid, fully after mixing, be down to room temperature;
(3) continue to add alkyl glycoside, AMONYL 380LC, anti-sensitive composition, stir 15 min;
(4) then add sodium D-isoascorbate, tripoly phosphate sodium STPP, disodium ethylene diamine tetraacetate carry out protecting look, protecting the look time is 5 min;
(5) add citric acid, Trisodium Citrate, adjust pH to 6.3, finally add methylisothiazolinone, after stirring 10 min, ageing, filling, obtained finished product.
embodiment 2
Containing clarification, the stable washing composition of high density Seed of Chinese Soapberry extracting solution, composed of the following components:
High density Seed of Chinese Soapberry extracting solution 65 wt%, in described high density Seed of Chinese Soapberry extracting solution, saponin content is 83.41wt%;
Polyoxyethylenated alcohol sodium sulfate 10 wt%,
Coco-nut oil fatty acid 3 wt%,
Alkyl glycoside 2.0 wt%,
AMONYL 380LC 4.0 wt%,
Citric acid 0.3 wt%,
Trisodium Citrate 0.29 wt%,
Sodium D-isoascorbate 0.5 wt%,
Tripoly phosphate sodium STPP 0.2 wt%,
Disodium ethylene diamine tetraacetate 0.3 wt%,
Methylisothiazolinone 0.01 wt%,
Thickening combination:
(cationic cellulose JR-400 1.0 wt%,
PEG-150 SUNSOFT Q-182S 4 wt%,
Natrulon H-10 5.0 wt%),
Anti-sensitive composition:
(α-Hydagen B 3 wt%,
Rizinsan K2 A2 0.5wt%,
Scutellarin 0.4wt%,
Herba portulacae extract 0.5wt%);
A kind of preparation contains the clarification of high density Seed of Chinese Soapberry extracting solution, the method for stable washing composition as above: comprise the following steps:
(1) Seed of Chinese Soapberry extracting solution is placed in container, opens and stir, add thickening combination, be heated to 80 DEG C;
(2) then add polyoxyethylenated alcohol sodium sulfate, coco-nut oil fatty acid, fully after mixing, be down to room temperature;
(3) continue to add alkyl glycoside, AMONYL 380LC, anti-sensitive composition, stir 20 min;
(4) then add sodium D-isoascorbate, tripoly phosphate sodium STPP, disodium ethylene diamine tetraacetate carry out protecting look, protecting the look time is 7 min;
(5) add citric acid, Trisodium Citrate, adjust pH to 6.5, finally add methylisothiazolinone, after stirring 5 min, ageing, filling, obtained finished product.
embodiment 3
Containing clarification, the stable washing composition of high density Seed of Chinese Soapberry extracting solution, composed of the following components:
High density Seed of Chinese Soapberry extracting solution 69 wt%, in described high density Seed of Chinese Soapberry extracting solution, saponin content is 70.18wt%;
Polyoxyethylenated alcohol sodium sulfate 8 wt%,
Coco-nut oil fatty acid 4 wt%,
Alkyl glycoside 2 wt%,
AMONYL 380LC 5 wt%,
Citric acid 0.3 wt%,
Trisodium Citrate 0.3 wt%,
Sodium D-isoascorbate 0.5 wt%,
Tripoly phosphate sodium STPP 0.2 wt%,
Disodium ethylene diamine tetraacetate 0.3 wt%,
Methylisothiazolinone 0.01 wt%,
Thickening combination:
(cationic cellulose JR-400 1.0 wt%,
PEG-150 SUNSOFT Q-182S 2 wt%,
Natrulon H-10 1.29 wt%),
Anti-sensitive composition:
(α-Hydagen B 5 wt%,
Rizinsan K2 A2 0.4wt%,
Scutellarin 0.3wt%,
Herba portulacae extract 0.4wt%);
A kind of preparation contains the clarification of high density Seed of Chinese Soapberry extracting solution, the method for stable washing composition as above: comprise the following steps:
(1) Seed of Chinese Soapberry extracting solution is placed in container, opens and stir, add thickening combination, be heated to 80 DEG C;
(2) then add polyoxyethylenated alcohol sodium sulfate, coco-nut oil fatty acid, fully after mixing, be down to room temperature;
(3) continue to add alkyl glycoside, AMONYL 380LC, anti-sensitive composition, stir 30 min;
(4) then add sodium D-isoascorbate, tripoly phosphate sodium STPP, disodium ethylene diamine tetraacetate carry out protecting look, protecting the look time is 7 min;
(5) add citric acid, Trisodium Citrate, adjust pH to 6.6, finally add methylisothiazolinone, after stirring 10 min, ageing, filling, obtained finished product.
comparative example 1
Other parameters are identical with embodiment 1, and difference is not add thickening combination, and only adds the thickening material of single component.
High density Seed of Chinese Soapberry extracting solution 70 wt%,
Polyoxyethylenated alcohol sodium sulfate 10 wt%,
Coco-nut oil fatty acid 4 wt%,
Alkyl glycoside 1.3 wt%,
AMONYL 380LC 3.0 wt%,
Citric acid 0.15 wt%,
Trisodium Citrate 0.15 wt%,
Sodium D-isoascorbate 0.4 wt%,
Tripoly phosphate sodium STPP 0.15 wt%,
Disodium ethylene diamine tetraacetate 0.2 wt%,
Methylisothiazolinone 0.005 wt%,
PEG-150 SUNSOFT Q-182S 7.745 wt%,
Anti-sensitive composition:
(α-Hydagen B 2 wt%,
Rizinsan K2 A2 0.3 wt%,
Scutellarin 0.3 wt%,
Herba portulacae extract 0.3 wt%);
A kind of preparation contains the clarification of high density Seed of Chinese Soapberry extracting solution, the method for stable washing composition as above: comprise the following steps:
(1) Seed of Chinese Soapberry extracting solution is placed in container, opens and stir, be heated to 80 DEG C;
(2) then add polyoxyethylenated alcohol sodium sulfate, coco-nut oil fatty acid, fully after mixing, be down to room temperature;
(3) continue to add alkyl glycoside, AMONYL 380LC, anti-sensitive composition, stir 15 min;
(4) then add sodium D-isoascorbate, tripoly phosphate sodium STPP, disodium ethylene diamine tetraacetate carry out protecting look, protecting the look time is 5 min;
(5) add citric acid, Trisodium Citrate, adjust pH to 6.3, finally add methylisothiazolinone, after stirring 10 min, ageing, filling, obtained finished product.
By finished product obtained for embodiment 1-3 compared with comparative example 1, the product denseness of embodiment 1-3 is moderate, and viscosity is lower, and clarification, stablizes 5 ~ 40 DEG C of denseness; And comparative example 1 adopts Conventional thickeners to carry out thickening, compared with the product of embodiment 1, be difficult to thickening, denseness is lower, and turbid phenomenon has appearred in washing composition in thickening, and when low temperature, denseness uprises, and denseness is thinning when high temperature.This its saponin(e purity of Seed of Chinese Soapberry extracting solution mainly due to high density is higher, and saponin(e belongs to nonionogenic tenside, adopts conventional thickening material to be difficult to the thickening effectiveness reached, and in thickening, there will be muddiness, the phenomenons such as variable color.And thickening combination disclosed by the invention exactly solves this problem, obtained a kind of clarification containing high density Seed of Chinese Soapberry extracting solution, stable washing composition, it belongs to All Pure Nature environmentfriendly products.
The foregoing is only preferred embodiment of the present invention, all equalizations done according to the present patent application the scope of the claims change and modify, and all should belong to covering scope of the present invention.
Claims (4)
1. one kind contains the clarification of high density Seed of Chinese Soapberry extracting solution, stable washing composition, it is characterized in that: containing thickening combination composed of the following components in described washing composition, the per-cent that each component accounts for washing composition total mass is: cationic cellulose JR-400 0.05wt% ~ 1.0wt%, PEG-150 SUNSOFT Q-182S 2wt% ~ 4wt%, Natrulon H-10 1.0wt% ~ 5.0wt%; Saponin content 65wt% ~ 85wt% in described high density Seed of Chinese Soapberry extracting solution.
2. the clarification containing high density Seed of Chinese Soapberry extracting solution according to claim 1, stable washing composition, it is characterized in that: also containing anti-sensitive composition composed of the following components in described washing composition, the per-cent that each component accounts for washing composition total mass is: α-Hydagen B 2wt% ~ 5wt%, Rizinsan K2 A2 0.1wt% ~ 0.5wt%, scutellarin 0.2wt% ~ 0.4wt%, Herba portulacae extract 0.1wt% ~ 0.5wt%.
3. the clarification containing high density Seed of Chinese Soapberry extracting solution according to claim 1, stable washing composition, is characterized in that: described washing composition also contains following component, by massfraction:
High density Seed of Chinese Soapberry extracting solution 65 wt% ~ 70 wt%,
Polyoxyethylenated alcohol sodium sulfate 8 wt% ~ 10 wt%,
Coco-nut oil fatty acid 2 wt% ~ 4 wt%,
Alkyl glycoside 0.5 wt% ~ 2.0 wt%,
AMONYL 380LC 3 wt% ~ 5 wt%,
Citric acid 0.05 wt% ~ 0.3 wt%,
Trisodium Citrate 0.05 wt% ~ 0.3 wt%,
Sodium D-isoascorbate 0.3 wt% ~ 0.5 wt%,
Tripoly phosphate sodium STPP 0.1 wt% ~ 0.2 wt%,
Disodium ethylene diamine tetraacetate 0.1 wt% ~ 0.3 wt%,
Methylisothiazolinone 0.005 wt% ~ 0.01 wt%,
Washing composition all components massfraction sum is 100%.
4. prepare as claimed in claim 1 containing the clarification of high density Seed of Chinese Soapberry extracting solution, a method for stable washing composition, it is characterized in that: comprise the following steps:
(1) high density Seed of Chinese Soapberry extracting solution is placed in container, opens and stir, add thickening combination, be heated to 80 DEG C;
(2) then add polyoxyethylenated alcohol sodium sulfate, coco-nut oil fatty acid, fully after mixing, be down to room temperature;
(3) continue to add alkyl glycoside, AMONYL 380LC, anti-sensitive composition, stir 15 ~ 30 min;
(4) then add sodium D-isoascorbate, tripoly phosphate sodium STPP, disodium ethylene diamine tetraacetate carry out protecting look, protecting the look time is 5 ~ 10 min;
(5) add citric acid, Trisodium Citrate, regulate pH; Finally add methylisothiazolinone, after stirring 5 ~ 10 min, ageing, filling, obtained finished product.
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CN106520415A (en) * | 2016-10-10 | 2017-03-22 | 福建省轻工业研究所 | Antidandruff itch-stopping shampoo soap containing sapindus saponin-nano silver complex |
CN106479748A (en) * | 2016-10-10 | 2017-03-08 | 福建省轻工业研究所 | A kind of medical detergent of the silver complex of nanometer containing sapindoside |
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