CN106520415A - Antidandruff itch-stopping shampoo soap containing sapindus saponin-nano silver complex - Google Patents
Antidandruff itch-stopping shampoo soap containing sapindus saponin-nano silver complex Download PDFInfo
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- CN106520415A CN106520415A CN201610880138.4A CN201610880138A CN106520415A CN 106520415 A CN106520415 A CN 106520415A CN 201610880138 A CN201610880138 A CN 201610880138A CN 106520415 A CN106520415 A CN 106520415A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/225—Polymers
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/262—Organic compounds, e.g. vitamins containing oxygen containing carbohydrates
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/265—Organic compounds, e.g. vitamins containing oxygen containing glycerol
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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Abstract
The invention belongs to the field of preparation of shampoo soaps, and in particular relates to an antidandruff itch-stopping shampoo soap containing sapindus saponin-nano silver complex. The antidandruff itch-stopping shampoo soap contains 5wt%-10wt% of sapindus saponin-nano silver complex, 5wt%-10wt% of purslane extracting solution, 8wt%-12wt% of almond oil, 15wt%-20wt% of coix seed extracting solution and 0.05wt%-1.0wt% of cationic cellulose JR-400. The sapindus saponin is simultaneously used as a reducing agent and a protective agent of the Ag<+> so as to form a nano silver complex protected by the sapindus saponin, the shampoo soap is good in stability, obvious in antibacterial effect, and obvious in hair-protecting effect; meanwhile, the cationic cellulose can bring the hydrophobic components in the sapindus saponin and the purslane extracting solution and the almond oil to the scalp and the hairline so as to deeply clean the scalp and the hairline, the antidandruff effect is obvious, and the shampoo soap further has the antiallergic effect, can relieve the skin and inhibit the skin itch caused by dryness, and the itch-stopping effect is obvious.
Description
Technical field
The invention belongs to the preparation field of hair soap, and in particular to a kind of going containing sapindoside-nanometer silver complex
Consider antipruritic hairdressing soap to be worth doing.
Background technology
Dandruff is the dead cell come off after metabolism.Dandruff amount is little under normal circumstances, so seldom
It is noticeable；And somebody is accompanied by itching of the scalp because a variety of causes dandruff especially more, have a strong impact on individual humanoid
As.Dandruff can substantially be divided into two classes：A kind of is drying property, is caused the problems such as come off by dry scalp, scalp；One kind is
It is oleaginous, caused to produce by the bacteria breed with the cortex of scalp as nutrition.The approach of existing anti-dandruff is generally：Go
Oily, appropriate moisturizing suppresses fungi.It is general to suppress fungal product to have universal medicaments such as cave health azoles, but its large side effects, easily
Hair loss.And existing anti-dandruff shampoo product is also anti-dandruff thorough, easy recurrent exerbation；Or although anti-dandruff effect is good,
To sacrifice hair quality as cost so that withered and yellowish hairs, hair are dry.
Sapindoside（Soapnut Saponin）Containing abundant glucosides class material, mainly based on Triterpene saponins
（By taking structure Formulas I as an example）, the molecular structure of triterpenoid sapogenin is made up of two parts：A part is carboxyl and glucosyl group（Or
Other glycosyls）The saponin(e structure being connected to form, i.e. water-wet side；Another part is aglycon, i.e. non-hydrophilic end.
Structure Formulas I
Sapindoside is a kind of natural mild nonionic surfactant, and having proven to act on human body skin has antibacterial, kills
Bacterium, anti-inflammatory and dandruff-removing itching-relieve effect.Soapberry also contains many materials beneficial to human body in addition, such as：Reduced sugar, fat
Acid, grease, oleic acid, carotenoid, Yan are sour, riboflavin, protein, vitamin C, vitamin A, Cobastab and lysine, junket
10 several amino acids such as propylhomoserin, phenylalanine, glutamic acid, glycine and histidine.Therefore sapindoside is largely used to system
Make natural nuisance-free articles for washing.
Silver is with a long history as medical antibacterial agent, and silver ion has prominent bactericidal effect and preferable safety
Property, but silver ion is more unstable, limits its application to a certain extent.Nanometer technology is the important branch of modern science and technology
One of, the particle diameter for reducing Argent grain reaches nanoscale, can play its skin effect again, greatly improve its antibacterial activity.
Replace by the use of relatively stable nano-Ag particles silver ion as inorganic antibacterial material additive, have in anti-biotic material field
Wide application prospect.
The content of the invention
Present invention aims to existing anti-dandruff shampoo product is anti-dandruff not thoroughly, easily repeatedly, and hair quality is damaged
Deng not enough, there is provided a kind of anti-dandruff and itching-relieving hairdressing soap containing sapindoside-nanometer silver complex.Introduce by without trouble in hair soap
The nanometer silver complex of sub- saponin(e protection, can improve the anti-microbial property of hair soap；And as the hair soap of the present invention is in weak base
Property, do not hinder and send out, act on significant hairdressing；Simultaneously act synergistically with Portulaca water extract, apricot kernel oil etc., anti-dandruff and itching-relieving effect
Significantly.
For achieving the above object, the present invention is adopted the following technical scheme that：
A kind of anti-dandruff and itching-relieving hairdressing soap containing sapindoside-nanometer silver complex, its component are consisted of：
Sapindoside-nanometer silver complex 5wt% ~ 10wt%,
Purslane extract 5wt%-10wt%,
Apricot kernel oil 8wt%-12wt%,
Coix seed extract 15wt%-20wt%,
Cationic cellulose 0.05 wt% of JR-400 ~ 1.0wt%,
Stearic acid 14wt%-18wt%,
Palmitic acid 6wt%-10wt%,
Myristic acid 10wt%-12wt%,
Laurate 6wt%-8wt%,
NaOH 6.5wt%-9.5wt%,
Glycerine 4wt%-6wt%,
2 wt%-3wt% of triglycerides,
Scutelloside 0.2wt% ~ 0.4wt%,
Dipotassium glycyrrhizinate 0.1wt% ~ 0.5wt%；
All components weight fraction sum is 100%.
Described sapindoside-nanometer silver complex is using sapindoside as reducing agent and protective agent, by Ag+Also
Original is obtained complex compound into nano-Ag particles.
The preparation method of described sapindoside-nanometer silver complex is：100mL purified waters are taken, 40-60 mg are added
Sapindoside powder, is stirred with the rotating speed of 500r/min-1000r/min, then in sapindoside solution with
The speed of 0.01ml/s-0.02ml/s instills 0.05mL-0.1mL 0.05mol/LAgNO3Solution, after completion of dropping, continues to stir
40min-50min is mixed, sapindoside-nanometer silver complex of the silver nano-grain particle diameter for 10nm-70nm is obtained.
The preparation method of described coix seed extract is：Coix seed is taken, is crushed with pulverizer, add 4-6 times of quality
Water, in 80 DEG C of -90 DEG C of extraction 2-3h, is concentrated into the extract that solid content is 35-45wt%.
The preparation method of described Purslane extract is：Purslane is cleaned up, is crushed with pulverizer, add 5-6
The water of times quality, in 70 DEG C of -75 DEG C of extraction 2-3h, is concentrated into the extract that solid content is 50-60wt%.
A kind of method for preparing the anti-dandruff and itching-relieving hairdressing soap containing sapindoside-nanometer silver complex as above, bag
Include following steps：
1）Glycerine, stearic acid, palmitic acid, myristic acid, laurate and triglycerides are added into emulsification pot, 80～85 DEG C are heated to
Stirring and dissolving；
2）Apricot kernel oil is added in emulsification pot, 60 DEG C are cooled to, Purslane extract, coix seed is then slowly added into and is extracted
Liquid, cationic cellulose JR-400 and NaOH add emulsification pot saponification, insulated and stirred 30-40min；
3）Then 40 DEG C are cooled to, sapindoside-nanometer silver complex, scutelloside and dipotassium glycyrrhizinate is added to emulsification pot
In, stir 30-50min；
4）Inspection by sampling, in qualified rear discharging injection soap bucket, is obtained hairdressing soap.
Mainly based on Triterpene saponins, the molecular structure of triterpenoid sapogenin is made up of sapindoside two parts：One
Part is carboxyl and glucosyl group（Or other glycosyls）The saponin(e structure being connected to form, i.e. water-wet side；Another part is aglycon, i.e.,
Non-hydrophilic end.By sapindoside and Ag+Interact, sapindoside can be by Ag as pure-natural biological component+It is reduced to
Ag, and the nano-Ag particles after reduction can be protected；Mixing speed, the AgNO of sapindoside is controlled simultaneously3Rate of titration, can
To control the particle diameter of nano-Ag particles；The complex compound for being formed is made an addition in hair soap, stable performance, and nano-Ag particles can continue
Antibacterial action is played, sapindoside can be cleaned, nourish hair quality again, have significant hairdressing effect.
Significantly, aminoacid ingredient contained therein can be relaxed Purslane extract antiallergic effect with vasoconstriction smooth muscle
Slow skin and suppress the skin itching that causes of drying, effect of going to itch is obvious；Flavones and saponin can go free radical and it is anti-oxidant, prolong
Slow skin senescence；Alkaloid and flavones can be with antibacterial and suppression Common Pathogenic dermatophytes；Plant polyose and vitamin can be with
The physiological function of nutrition greasy skin and promotion epithelial cell tends to normal, increases the comfort level of skin.
Apricot kernel oil contains abundant vitamin E, wherein based on alpha tocopherol and gama tocopherol, with good anti-oxidant
Stability；Act on significant hairdressing simultaneously.
But Purslane extract, apricot kernel oil are made an addition in conventional hair washing product, difficult prospect is attached to hair and head
Pi Shang；And the present invention has using coixenolide, fat oil, amino acid, protein and carbohydrate etc. is rich in coix seed extract
Action of Surfactant, can be such that Purslane extract and apricot kernel oil fully merges, and pass through cationic cellulose JR-400（Sun
Ionomer）, can be by the band such as hydrophobic ingredient and apricot kernel oil of sapindoside and Portulaca water extract to anion
Hair and scalp on, the charges of different polarity are attracting, and action time is longer, deep layer cleaning, moisten scalp, and anti-dandruff, antipruritic effect is notable；
And there are anti-allergic effects, the skin itching that can releive skin and suppression drying cause, antipruritic effect are obvious.
Specific embodiment
The present invention further illustrates the present invention with the following example, but protection scope of the present invention is not limited to following reality
Apply example.
A kind of anti-dandruff and itching-relieving hairdressing soap containing sapindoside-nanometer silver complex, its component are consisted of：
Sapindoside-nanometer silver complex 5wt% ~ 10wt%,
Purslane extract 5wt%-10wt%,
Apricot kernel oil 8wt%-12wt%,
Coix seed extract 15wt%-20wt%,
Cationic cellulose 0.05 wt% of JR-400 ~ 1.0wt%,
Stearic acid 14wt%-18wt%,
Palmitic acid 6wt%-10wt%,
Myristic acid 10wt%-12wt%,
Laurate 6wt%-8wt%,
NaOH 6.5wt%-9.5wt%,
Glycerine 4wt%-6wt%,
2 wt%-3wt% of triglycerides,
Scutelloside 0.2wt% ~ 0.4wt%,
Dipotassium glycyrrhizinate 0.1wt% ~ 0.5wt%；
All components weight fraction sum is 100%.
The preparation method of described sapindoside-nanometer silver complex is：100mL purified waters are taken, 40-60 mg are added
Sapindoside powder, is stirred with the rotating speed of 500r/min-1000r/min, then in sapindoside solution with
The speed of 0.01ml/s-0.02ml/s instills 0.05mL-0.1mL 0.05mol/LAgNO3Solution, after completion of dropping, continues to stir
40min-50min is mixed, sapindoside-nanometer silver complex of the silver nano-grain particle diameter for 10nm-70nm is obtained.
The preparation method of described coix seed extract is：Coix seed is taken, is crushed with pulverizer, add 4-6 times of quality
Water, in 80 DEG C of -90 DEG C of extraction 2-3h, is concentrated into the extract that solid content is 35-45wt%.
The preparation method of described Purslane extract is：Purslane is cleaned up, is crushed with pulverizer, add 5-6
The water of times quality, in 70 DEG C of -75 DEG C of extraction 2-3h, is concentrated into the extract that solid content is 50-60wt%.
A kind of method for preparing the anti-dandruff and itching-relieving hairdressing soap containing sapindoside-nanometer silver complex as above, bag
Include following steps：
1）Glycerine, stearic acid, palmitic acid, myristic acid, laurate and triglycerides are added into emulsification pot, 80～85 DEG C are heated to
Stirring and dissolving；
2）Apricot kernel oil is added in emulsification pot, 60 DEG C are cooled to, Purslane extract, coix seed is then slowly added into and is extracted
Liquid, cationic cellulose JR-400 and NaOH add emulsification pot saponification, insulated and stirred 30-40min；
3）Then 40 DEG C are cooled to, sapindoside-nanometer silver complex, scutelloside and dipotassium glycyrrhizinate is added to emulsification pot
In, stir 30-50min；
4）Inspection by sampling, in qualified rear discharging injection soap bucket, is obtained hairdressing soap.
Embodiment 1
A kind of anti-dandruff and itching-relieving hairdressing soap containing sapindoside-nanometer silver complex, its component are consisted of：
Sapindoside-nanometer silver complex 5wt%,
Purslane extract 10wt%,
Apricot kernel oil 8wt%,
Coix seed extract 20wt%,
Cationic cellulose JR-400 0.05wt%,
Stearic acid 18wt%,
Palmitic acid 6wt%,
Myristic acid 12wt%,
Laurate 6wt%,
NaOH 7.05wt%,
Glycerine 4wt%,
Triglycerides 3wt%,
Scutelloside 0.4wt%,
Dipotassium glycyrrhizinate 0.5wt%；
All components weight fraction sum is 100%.
The preparation method of described sapindoside-nanometer silver complex is：100mL purified waters are taken, and 40 mg are added without trouble
Sub- saponin(e powder, is stirred with the rotating speed of 1000r/min, is then instilled with the speed of 0.01ml/s in sapindoside
0.05mL0.05mol/LAgNO3Solution, after completion of dropping, continues stirring 50min, and it is 10nm- that silver nano-grain particle diameter is obtained
The sapindoside of 70nm-nanometer silver complex.
The preparation method of described coix seed extract is：Coix seed is taken, is crushed with pulverizer, add the water of 4 times of quality,
2h is extracted at 90 DEG C, the extract that solid content is 40wt% is concentrated into.
The preparation method of described Purslane extract is：Purslane is cleaned up, is crushed with pulverizer, add 6 times
The water of quality, extracts 3h at 70 DEG C, is concentrated into the extract that solid content is 57wt%.
A kind of method for preparing the anti-dandruff and itching-relieving hairdressing soap containing sapindoside-nanometer silver complex as above, bag
Include following steps：
1）Glycerine, stearic acid, palmitic acid, myristic acid, laurate and triglycerides are added into emulsification pot, 80 DEG C of stirrings are heated to
Dissolving；
2）Apricot kernel oil is added in emulsification pot, 60 DEG C are cooled to, Purslane extract, coix seed is then slowly added into and is extracted
Liquid, cationic cellulose JR-400 and NaOH add emulsification pot saponification, insulated and stirred 30min；
3）Then 40 DEG C are cooled to, sapindoside-nanometer silver complex, scutelloside and dipotassium glycyrrhizinate is added to emulsification pot
In, stir 30min；
4）Inspection by sampling, in qualified rear discharging injection soap bucket, is obtained hairdressing soap.
Embodiment 2
A kind of anti-dandruff and itching-relieving hairdressing soap containing sapindoside-nanometer silver complex, its component are consisted of：
Sapindoside-nanometer silver complex 10wt%,
Purslane extract 5wt%,
Apricot kernel oil 12wt%,
Coix seed extract 15wt%,
Cationic cellulose JR-400 1.0wt%,
Stearic acid 14wt%,
Palmitic acid 10wt%,
Myristic acid 12wt%,
Laurate 6wt%,
NaOH 8.5wt%,
Glycerine 4wt%,
Triglycerides 2wt%,
Scutelloside 0.3wt%,
Dipotassium glycyrrhizinate 0.2wt%；
All components weight fraction sum is 100%.
Described sapindoside-nanometer silver complex is using sapindoside as reducing agent and protective agent, by Ag+Also
Original into nano-Ag particles, agitated polymerization and obtained complex compound.
The preparation method of described sapindoside-nanometer silver complex is：100mL purified waters are taken, and 60 mg are added without trouble
Sub- saponin(e powder, is stirred with the rotating speed of 500r/min, then instills 0.1mL with the speed of 0.02ml/s in sapindoside
0.05mol/LAgNO3Solution, after completion of dropping, continues stirring 40min-50min, and it is 10nm- that silver nano-grain particle diameter is obtained
The sapindoside of 70nm-nanometer silver complex.
The preparation method of described coix seed extract is：Coix seed is taken, is crushed with pulverizer, add 4-6 times of quality
Water, extracts 2h at 90 DEG C, is concentrated into the extract that solid content is 45wt%.
The preparation method of described Purslane extract is：Purslane is cleaned up, is crushed with pulverizer, add 5 times
The water of quality, extracts 2h at 75 DEG C, is concentrated into the extract that solid content is 60wt%.
A kind of method for preparing the anti-dandruff and itching-relieving hairdressing soap containing sapindoside-nanometer silver complex as above, bag
Include following steps：
1）Glycerine, stearic acid, palmitic acid, myristic acid, laurate and triglycerides are added into emulsification pot, 85 DEG C of stirrings are heated to
Dissolving；
2）Apricot kernel oil is added in emulsification pot, 60 DEG C are cooled to, Purslane extract, coix seed is then slowly added into and is extracted
Liquid, cationic cellulose JR-400 and NaOH add emulsification pot saponification, insulated and stirred 40min；
3）Then 40 DEG C are cooled to, sapindoside-nanometer silver complex, scutelloside and dipotassium glycyrrhizinate is added to emulsification pot
In, stir 50min；
4）Inspection by sampling, in qualified rear discharging injection soap bucket, is obtained hairdressing soap.
Embodiment 3
A kind of anti-dandruff and itching-relieving hairdressing soap containing sapindoside-nanometer silver complex, its component are consisted of：
Sapindoside-nanometer silver complex 8wt%,
Purslane extract 8wt%,
Apricot kernel oil 10wt%,
Coix seed extract 17wt%,
Cationic cellulose JR-400 0.5wt%,
Stearic acid 16wt%,
Palmitic acid 8wt%,
Myristic acid 11wt%,
Laurate 7wt%,
NaOH 6.5wt%,
Glycerine 5wt%,
Triglycerides 2.5wt%,
Scutelloside 0.3wt%,
Dipotassium glycyrrhizinate 0.2wt%；
All components weight fraction sum is 100%.
Described sapindoside-nanometer silver complex is using sapindoside as reducing agent and protective agent, by Ag+Also
Original into nano-Ag particles, agitated polymerization and obtained complex compound.
The preparation method of described sapindoside-nanometer silver complex is：100mL purified waters are taken, and 50 mg are added without trouble
Sub- saponin(e powder, is stirred with the rotating speed of 800r/min, is then instilled with the speed of 0.01ml/s in sapindoside
0.07mL 0.05mol/LAgNO3Solution, after completion of dropping, continues stirring 45min, and it is 10nm- that silver nano-grain particle diameter is obtained
The sapindoside of 70nm-nanometer silver complex.
The preparation method of described coix seed extract is：Coix seed is taken, is crushed with pulverizer, add the water of 5 times of quality,
2.5h is extracted at 85 DEG C, the extract that solid content is 41wt% is concentrated into.
The preparation method of described Purslane extract is：Purslane is cleaned up, is crushed with pulverizer, add 5 times
The water of quality, extracts 2.5h at 73 DEG C, is concentrated into the extract that solid content is 56wt%.
A kind of method for preparing the anti-dandruff and itching-relieving hairdressing soap containing sapindoside-nanometer silver complex as above, bag
Include following steps：
1）Glycerine, stearic acid, palmitic acid, myristic acid, laurate and triglycerides are added into emulsification pot, 83 DEG C of stirrings are heated to
Dissolving；
2）Apricot kernel oil is added in emulsification pot, 60 DEG C are cooled to, Purslane extract, coix seed is then slowly added into and is extracted
Liquid, cationic cellulose JR-400 and NaOH add emulsification pot saponification, insulated and stirred 30min；
3）Then 40 DEG C are cooled to, sapindoside-nanometer silver complex, scutelloside and dipotassium glycyrrhizinate is added to emulsification pot
In, stir 30min；
4）Inspection by sampling, in qualified rear discharging injection soap bucket, is obtained hairdressing soap.
1st, the bacteriostasis property test of product of the present invention：
With Escherichia coli and staphylococcus aureus as testing bacterial classification, using solid medium method（Colony counting method）Train with liquid
Foster base method evaluates the anti-microbial property of the stable Nano Silver of sapindoside.
As a result it is as follows：Under conditions of initial bacteria concentration is 100000 CFU/mL, to colibacillary minimum inhibitory concentration
Less than 40 ppm, 20 ppm are less than to the minimum inhibitory concentration of staphylococcus aureus.
2nd, anti-dandruff and itching-relieving measure of merit：
Tested using scalp test card, the hair soap of the present invention is relative to general anti-dandruff shampoo product, anti-dandruff and itching-relieving effect
Fruit is prominent, and after trying out one week, dandruff and fuel-displaced, drying regime are greatly reduced, and after trying out one month, anti-dandruff, antipruritic effect
Fruit very thoroughly, is not rebounded；And hair quality is submissive, glossy, it is short-tempered to be difficult.
The foregoing is only presently preferred embodiments of the present invention, all impartial changes done according to scope of the present invention patent with
Modification, should all belong to the covering scope of the present invention.
Claims (7)
1. a kind of anti-dandruff and itching-relieving hairdressing soap containing sapindoside-nanometer silver complex, it is characterised in that：Containing soapberry soap
Glycosides-nanometer silver complex 5wt% ~ 10wt%；Described sapindoside-nanometer silver complex is using sapindoside as reduction
Agent and protective agent, by Ag+It is reduced into nano-Ag particles and obtained complex compound.
2. the anti-dandruff and itching-relieving hairdressing soap containing sapindoside-nanometer silver complex according to claim 1, its feature exist
In：The preparation method of described sapindoside-nanometer silver complex is：100mL purified waters are taken, 40-60 mg soapberrys are added
Saponin(e powder, is stirred with the rotating speed of 500r/min-1000r/min, then in sapindoside solution with 0.01ml/s-
The speed of 0.02ml/s instills 0.05mL-0.1mL 0.05mol/LAgNO3Solution, after completion of dropping, continues stirring 40min-
50min, is obtained sapindoside-nanometer silver complex of the silver nano-grain particle diameter for 10nm-70nm.
3. the anti-dandruff and itching-relieving hairdressing soap containing sapindoside-nanometer silver complex according to claim 1, its feature exist
In：Also contain Purslane extract 5wt%-10wt%, apricot kernel oil 8wt%-12wt%, coix seed extract in described hairdressing soap
15wt%-20wt% and cationic cellulose 0.05 wt% of JR-400 ~ 1.0wt%.
4. the anti-dandruff and itching-relieving hairdressing soap containing sapindoside-nanometer silver complex according to claim 3, its feature exist
In：Also contain 14 wt%-18 wt% of stearic acid, palmitic acid 6wt%-10wt%, 10 wt%-12 of myristic acid in described hairdressing soap
Wt%, laurate 6wt%-8wt%, 6.5 wt%-9.5 wt% of NaOH, glycerine 5wt%, 2 wt%-3 wt% of triglycerides, the root of large-flowered skullcap
Glycosides 0.2wt% ~ 0.4wt%, dipotassium glycyrrhizinate 0.1wt% ~ 0.5wt%；All components weight fraction sum is 100%.
5. the anti-dandruff and itching-relieving hairdressing soap containing sapindoside-nanometer silver complex according to claim 3, its feature exist
In：The preparation method of described coix seed extract is：Coix seed is taken, is crushed with pulverizer, add the water of 4-6 times of quality,
80 DEG C of -90 DEG C of extraction 2-3h, are concentrated into the extract that solid content is 35-45wt%.
6. the anti-dandruff and itching-relieving hairdressing soap containing sapindoside-nanometer silver complex according to claim 3, its feature exist
In：The preparation method of described Purslane extract is：Purslane is cleaned up, is crushed with pulverizer, add 5-6 times of quality
Water, 70 DEG C -75 DEG C extraction 2-3h, be concentrated into solid content be 50-60wt% extract.
7. it is a kind of to prepare the side for containing the anti-dandruff and itching-relieving hairdressing soap of sapindoside-nanometer silver complex as claimed in claim 4
Method, it is characterised in that：Comprise the following steps：
1）Glycerine, stearic acid, palmitic acid, myristic acid, laurate and triglycerides are added into emulsification pot, 80～85 DEG C are heated to
Stirring and dissolving；
2）Apricot kernel oil is added in emulsification pot, 60 DEG C are cooled to, Purslane extract, coix seed is then slowly added into and is extracted
Liquid, cationic cellulose JR-400 and NaOH add emulsification pot saponification, insulated and stirred 30-40min；
3）Then 40 DEG C are cooled to, sapindoside-nanometer silver complex, scutelloside and dipotassium glycyrrhizinate is added to emulsification pot
In, stir 30-50min；
4）Inspection by sampling, in qualified rear discharging injection soap bucket, is obtained hairdressing soap.
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| CN201610880138.4A CN106520415B (en) | 2016-10-10 | 2016-10-10 | It is a kind of containing sapindoside-nanometer silver complex anti-dandruff and itching-relieving hairdressing soap |
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| CN201610880138.4A CN106520415B (en) | 2016-10-10 | 2016-10-10 | It is a kind of containing sapindoside-nanometer silver complex anti-dandruff and itching-relieving hairdressing soap |
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| CN106520415B CN106520415B (en) | 2019-06-21 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107177428A (en) * | 2017-07-27 | 2017-09-19 | 绵竹市天骄农业开发有限公司 | A kind of preparation method of basic zirconium phosphate handmade soap |
| CN107312655A (en) * | 2017-07-27 | 2017-11-03 | 绵竹市天骄农业开发有限公司 | A kind of basic zirconium phosphate handmade soap |
Citations (2)
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| CN104611150A (en) * | 2015-02-12 | 2015-05-13 | 福建省轻工业研究所 | Clear and stable detergent containing high-concentration soapberry extract |
| CN104921998A (en) * | 2015-06-24 | 2015-09-23 | 陈琳仁 | Process for simultaneously extracting pigments, saponins and polysaccharides of sapindus, and preparation and application of saponins of sapindus |
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| CN104611150A (en) * | 2015-02-12 | 2015-05-13 | 福建省轻工业研究所 | Clear and stable detergent containing high-concentration soapberry extract |
| CN104921998A (en) * | 2015-06-24 | 2015-09-23 | 陈琳仁 | Process for simultaneously extracting pigments, saponins and polysaccharides of sapindus, and preparation and application of saponins of sapindus |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107177428A (en) * | 2017-07-27 | 2017-09-19 | 绵竹市天骄农业开发有限公司 | A kind of preparation method of basic zirconium phosphate handmade soap |
| CN107312655A (en) * | 2017-07-27 | 2017-11-03 | 绵竹市天骄农业开发有限公司 | A kind of basic zirconium phosphate handmade soap |
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| Publication number | Publication date |
|---|---|
| CN106520415B (en) | 2019-06-21 |
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