CN109576081A - A kind of Soapberry liquid laundry detergent and preparation method thereof - Google Patents
A kind of Soapberry liquid laundry detergent and preparation method thereof Download PDFInfo
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- CN109576081A CN109576081A CN201811491547.0A CN201811491547A CN109576081A CN 109576081 A CN109576081 A CN 109576081A CN 201811491547 A CN201811491547 A CN 201811491547A CN 109576081 A CN109576081 A CN 109576081A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/29—Sulfates of polyoxyalkylene ethers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/38—Cationic compounds
- C11D1/62—Quaternary ammonium compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/667—Neutral esters, e.g. sorbitan esters
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
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- Oil, Petroleum & Natural Gas (AREA)
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- Cosmetics (AREA)
- Detergent Compositions (AREA)
Abstract
The invention belongs to field of fine chemical, in particular to a kind of Soapberry liquid laundry detergent and preparation method thereof；It is mixed with dodecyl ether sulfate, linear alkyl benzene sulfonic acid, glycerin monostearate, lauroylamidopropyl betaine, part polyquaternium -7 according to special ratios, and the soapberry extract of specific quantity is added, the irritation of linear alkyl benzene sulfonic acid is reduced by reasonably matching, pH value is neutralized to neutrality, it is mild skin friendly, pass through the cooperation of a variety of chemicals, make liquid detergent that there is outstanding emulsification, foam performance, and antifoam performance, there is stronger dirt-removing power and antibacterial ability compared to traditional liquid detergent, and have the characteristics that easily to rinse；This application involves Soapberry liquid laundry detergent ingredient in chemicals is all made of in addition to soapberry extract, compare pure natural liquid detergent, while greatly reducing production cost, ensure that its mild skin friendly characteristic.
Description
Technical field
The invention belongs to field of fine chemical, in particular to a kind of Soapberry liquid laundry detergent and preparation method thereof.
Background technique
Soapberry sequiterpene glucosides class Alto glucosides substance rich in, has the function of cleaning skin, is natural
Emollient is cleaned, has the effect of antibacterial, sterilization, anti-inflammatory to human skin；With the exploitation of natural component, soapberry starts to be answered
For in liquid detergent ingredient, application publication number be the Chinese patent of CN105419961A disclose a kind of Soapberry liquid laundry detergent and its
Preparation method, almost all uses natural component in ingredient；Think that chemicals all has irritation, wound can be generated to skin
Evil, there are allergy hidden danger, but completely using natural component as liquid detergent raw material on the one hand be difficult to ensure its it is good emulsify,
Foam performance, cleaning ability is limited, and the higher cost of natural products.
Summary of the invention
The technical problems to be solved by the present invention are: providing the soapberry of a kind of low irritant, low cost, high-cleanness ability
Liquid detergent and preparation method thereof.
In order to solve the above-mentioned technical problem, the technical solution adopted by the present invention are as follows:
The present invention relates to a kind of Soapberry liquid laundry detergents, are prepared by the raw material of following parts by weight:
3-5 parts of dodecyl ether sulfates；3-5 parts of linear alkyl benzene sulfonic acids；20-40 portions of dodecanamide propyl beets
Alkali；3-5 parts of glycerin monostearates；0.2-0.5 parts of polyquaterniums -7；3-4 parts of sodium citrates；0.5-3 parts of soapberry extracts；
0.01-0.05 portions of preservatives；50-70 parts of deionized waters.
The invention further relates to a kind of preparation methods of Soapberry liquid laundry detergent, comprising the following steps:
Step 1: taking out soapberry seed, its pericarp is placed in baking oven, after 80-100 DEG C of drying, be crushed to 60-100
Mesh；
Step 2: it will be mixed by drying, smashed soapberry pericarp powder with the water of 2 times of quality, impregnate 22-26h,
Obtain soapberry pericarp mixed liquor；
Step 3: the soapberry pericarp mixed liquor boiling 4-6h after impregnating will be mixed with water, addition is equivalent to soapberry pericarp
The ethyl alcohol of 3-5 times of quality of mixed liquor, refluxing extraction 2-4h, refluxing extraction temperature are 50-70 DEG C；
Step 4: after the ethyl alcohol in the extracting solution of refluxing extraction volatilizees completely, obtaining soapberry extract；
Step 5: using obtained 0.5-3 part soapberry extract as raw material and 3-5 parts of dodecyl ether sulfates；3-
5 parts of linear alkyl benzene sulfonic acids；20-40 parts of lauroylamidopropyl betaines；3-5 parts of glycerin monostearates；0.2-0.5 parts of poly- seasons
Ammonium salt -7；3-4 parts of sodium citrates；0.01-0.05 portions of preservatives；50-70 parts of deionized waters are uniformly mixed, and soapberry laundry is made
Liquid.
The beneficial effects of the present invention are: in Soapberry liquid laundry detergent ingredient provided by the invention, with dodecyl alcohol ether sulphur
Sour sodium, linear alkyl benzene sulfonic acid, glycerin monostearate, lauroylamidopropyl betaine, part polyquaternium -7 are according to specific ratio
Example mixing, and the soapberry extract of specific quantity is added, the irritation of linear alkyl benzene sulfonic acid is reduced by reasonably matching, it will
PH value is neutralized to neutrality, mild skin friendly, by the cooperation of a variety of chemicals, make liquid detergent have outstanding emulsification,
Foam performance and antifoam performance have stronger dirt-removing power and antibacterial ability compared to traditional liquid detergent, and have easily drift
The characteristics of washing；This application involves Soapberry liquid laundry detergent ingredient in chemicals is all made of in addition to soapberry extract, compared to pure
Natural liquid detergent while greatly reducing production cost, ensure that its mild skin friendly characteristic.
Specific embodiment
To explain the technical content, the achieved purpose and the effect of the present invention in detail, it is explained below in conjunction with embodiment.
The most critical design of the present invention is: sweet with dodecyl ether sulfate, linear alkyl benzene sulfonic acid, monostearate
Grease, lauroylamidopropyl betaine, part polyquaternium -7 are mixed according to special ratios, and the soapberry that specific quantity is added extracts
Object.
The present invention relates to a kind of Soapberry liquid laundry detergents, are prepared by the raw material of following parts by weight:
3-5 parts of dodecyl ether sulfates；3-5 parts of linear alkyl benzene sulfonic acids；20-40 portions of dodecanamide propyl beets
Alkali；3-5 parts of glycerin monostearates；0.2-0.5 parts of polyquaterniums -7；3-4 parts of sodium citrates；0.5-3 parts of soapberry extracts；
0.01-0.05 portions of preservatives；50-70 parts of deionized waters.
The invention further relates to a kind of preparation methods of Soapberry liquid laundry detergent, comprising the following steps:
Step 1: taking out soapberry seed, its pericarp is placed in baking oven, after 80-100 DEG C of drying, be crushed to 60-100
Mesh；
Step 2: it will be mixed by drying, smashed soapberry pericarp powder with the water of 2 times of quality, impregnate 22-26h,
Obtain soapberry pericarp mixed liquor；
Step 3: the soapberry pericarp mixed liquor boiling 4-6h after impregnating will be mixed with water, addition is equivalent to soapberry pericarp
The ethyl alcohol of 3-5 times of quality of mixed liquor, refluxing extraction 2-4h, refluxing extraction temperature are 50-70 DEG C；
Step 4: after the ethyl alcohol in the extracting solution of refluxing extraction volatilizees completely, obtaining soapberry extract；
Step 5: using obtained 0.5-3 part soapberry extract as raw material and 3-5 parts of dodecyl ether sulfates；3-
5 parts of linear alkyl benzene sulfonic acids；20-40 parts of lauroylamidopropyl betaines；3-5 parts of glycerin monostearates；0.2-0.5 parts of poly- seasons
Ammonium salt -7；3-4 parts of sodium citrates；0.01-0.05 portions of preservatives；50-70 parts of deionized waters are uniformly mixed, and soapberry laundry is made
Liquid.
It is sweet with dodecyl ether sulfate, linear alkyl benzene sulfonic acid, monostearate in above-mentioned Soapberry liquid laundry detergent ingredient
Grease, lauroylamidopropyl betaine, part polyquaternium -7 are mixed according to special ratios, and the soapberry that specific quantity is added extracts
Object reduces the irritation of linear alkyl benzene sulfonic acid by reasonably matching, pH value is neutralized to neutrality, mild skin friendly,
By the cooperation of a variety of chemicals, make liquid detergent that there is outstanding emulsification, foam performance and antifoam performance, compared to tradition
Liquid detergent have stronger dirt-removing power and antibacterial ability, and have the characteristics that easily rinsing；This application involves soapberry wash
It is all made of chemicals in addition to soapberry extract in clothing liquid ingredient, compares pure natural liquid detergent, greatly reduces production cost
While, it ensure that its mild skin friendly characteristic.
Further, above-mentioned Soapberry liquid laundry detergent is specifically prepared by the raw material of following parts by weight:
4 parts of dodecyl ether sulfates；4 parts of linear alkyl benzene sulfonic acids；30 parts of lauroylamidopropyl betaines；4 parts of lists
Tristerin；0.3 part of polyquaternium -7；3.5 parts of sodium citrates；2 parts of soapberry extracts；0.03 portion of preservative；60 parts
Deionized water.
Further, above-mentioned Soapberry liquid laundry detergent is specifically prepared by the raw material of following parts by weight:
3 parts of dodecyl ether sulfates；3 parts of linear alkyl benzene sulfonic acids；20 parts of lauroylamidopropyl betaines；3 parts of lists
Tristerin；0.2 part of polyquaternium -7；3 parts of sodium citrates；0.5 part of soapberry extract；0.01 portion of preservative；50 parts
Deionized water.
Further, above-mentioned Soapberry liquid laundry detergent is specifically prepared by the raw material of following parts by weight:
5 parts of dodecyl ether sulfates；5 parts of linear alkyl benzene sulfonic acids；40 parts of lauroylamidopropyl betaines；5 parts of lists
Tristerin；0.5 part of polyquaternium -7；4 parts of sodium citrates；3 parts of soapberry extracts；0.05 portion of preservative；70 parts are gone
Ionized water.
Further, above-mentioned Soapberry liquid laundry detergent preparation method specifically includes the following steps:
Step 1: taking out soapberry seed, its pericarp is placed in baking oven, after 80 DEG C of drying, be crushed to 60 mesh；
Step 2: will be mixed by drying, smashed soapberry pericarp powder with the water of 2 times of quality, impregnate 22h, obtain
Soapberry pericarp mixed liquor；
Step 3: the soapberry pericarp mixed liquor boiling 4h after impregnating will be mixed with water, it is mixed that addition is equivalent to soapberry pericarp
The ethyl alcohol of 3 times of quality of liquid, refluxing extraction 2-4h are closed, refluxing extraction temperature is 50 DEG C；
Step 4: after the ethyl alcohol in the extracting solution of refluxing extraction volatilizees completely, obtaining soapberry extract；
Step 5: using obtain 0.5 part of soapberry extract as raw material and 3 parts of dodecyl ether sulfates；3 parts straight
Alkyl group benzene sulfonic acid；20 parts of lauroylamidopropyl betaines；3 parts of glycerin monostearates；0.2 part of polyquaternium -7；3 portions of lemons
Sour sodium；0.01 portion of preservative；50 parts of deionized waters are uniformly mixed, and Soapberry liquid laundry detergent is made.
Further, above-mentioned Soapberry liquid laundry detergent preparation method specifically includes the following steps:
Step 1: taking out soapberry seed, its pericarp is placed in baking oven, after 90 DEG C of drying, be crushed to 80 mesh；
Step 2: will be mixed by drying, smashed soapberry pericarp powder with the water of 2 times of quality, impregnate for 24 hours, obtain
Soapberry pericarp mixed liquor；
Step 3: the soapberry pericarp mixed liquor boiling 5h after impregnating will be mixed with water, it is mixed that addition is equivalent to soapberry pericarp
The ethyl alcohol of 4 times of quality of liquid, refluxing extraction 3h are closed, refluxing extraction temperature is 60 DEG C；
Step 4: after the ethyl alcohol in the extracting solution of refluxing extraction volatilizees completely, obtaining soapberry extract；
Step 5: using obtain 2 parts of soapberry extracts as raw material and 4 parts of dodecyl ether sulfates；4 parts of straight chains
Alkyl benzene sulphonate；30 parts of lauroylamidopropyl betaines；4 parts of glycerin monostearates；0.3 part of polyquaternium -7；3.5 portions of lemons
Sour sodium；0.03 portion of preservative；60 parts of deionized waters are uniformly mixed, and Soapberry liquid laundry detergent is made.
Further, above-mentioned Soapberry liquid laundry detergent preparation method specifically includes the following steps:
Step 1: taking out soapberry seed, its pericarp is placed in baking oven, after 100 DEG C of drying, be crushed to 100 mesh；
Step 2: will be mixed by drying, smashed soapberry pericarp powder with the water of 2 times of quality, impregnate 26h, obtain
Soapberry pericarp mixed liquor；
Step 3: the soapberry pericarp mixed liquor boiling 6h after impregnating will be mixed with water, it is mixed that addition is equivalent to soapberry pericarp
The ethyl alcohol of 5 times of quality of liquid, refluxing extraction 4h are closed, refluxing extraction temperature is 70 DEG C；
Step 4: after the ethyl alcohol in the extracting solution of refluxing extraction volatilizees completely, obtaining soapberry extract；Step 5: will
3 parts of obtained soapberry extracts are as raw material and 5 parts of dodecyl ether sulfates；5 parts of linear alkyl benzene sulfonic acids；40 parts months
Osmanthus amido propyl betaine；5 parts of glycerin monostearates；0.5 part of polyquaternium -7；4 parts of sodium citrates；0.05 portion of preservative；
70 parts of deionized waters are uniformly mixed, and Soapberry liquid laundry detergent is made.
Embodiment 1
A kind of Soapberry liquid laundry detergent is prepared by the raw material of following parts by weight:
4 parts of dodecyl ether sulfates；4 parts of linear alkyl benzene sulfonic acids；30 parts of lauroylamidopropyl betaines；4 parts of lists
Tristerin；0.3 part of polyquaternium -7；3.5 parts of sodium citrates；2 parts of soapberry extracts；0.03 portion of preservative；60 parts
Deionized water.
The preparation method of above-mentioned Soapberry liquid laundry detergent the following steps are included:
Step 1: taking out soapberry seed, its pericarp is placed in baking oven, after 90 DEG C of drying, be crushed to 80 mesh；
Step 2: will be mixed by drying, smashed soapberry pericarp powder with the water of 2 times of quality, impregnate for 24 hours, obtain
Soapberry pericarp mixed liquor；
Step 3: the soapberry pericarp mixed liquor boiling 5h after impregnating will be mixed with water, it is mixed that addition is equivalent to soapberry pericarp
The ethyl alcohol of 4 times of quality of liquid, refluxing extraction 3h are closed, refluxing extraction temperature is 60 DEG C；
Step 4: after the ethyl alcohol in the extracting solution of refluxing extraction volatilizees completely, obtaining soapberry extract；
Step 5: using obtain 2 parts of soapberry extracts as raw material and 3-5 parts of dodecyl ether sulfates；4 parts straight
Alkyl group benzene sulfonic acid；30 parts of lauroylamidopropyl betaines；4 parts of glycerin monostearates；0.3 part of polyquaternium -7；3.5 parts of lemons
Lemon acid sodium；0.03 portion of preservative；60 parts of deionized waters are uniformly mixed, and Soapberry liquid laundry detergent is made.
Embodiment 2
A kind of Soapberry liquid laundry detergent is prepared by the raw material of following parts by weight:
3 parts of dodecyl ether sulfates；3 parts of linear alkyl benzene sulfonic acids；20 parts of lauroylamidopropyl betaines；3 parts of lists
Tristerin；0.2 part of polyquaternium -7；3 parts of sodium citrates；0.5 part of soapberry extract；0.01 portion of preservative；50 parts
Deionized water.
The preparation method of above-mentioned Soapberry liquid laundry detergent the following steps are included:
Step 1: taking out soapberry seed, its pericarp is placed in baking oven, after 80 DEG C of drying, be crushed to 60 mesh；
Step 2: will be mixed by drying, smashed soapberry pericarp powder with the water of 2 times of quality, impregnate 22h, obtain
Soapberry pericarp mixed liquor；
Step 3: the soapberry pericarp mixed liquor boiling 4h after impregnating will be mixed with water, it is mixed that addition is equivalent to soapberry pericarp
The ethyl alcohol of 3 times of quality of liquid, refluxing extraction 2-4h are closed, refluxing extraction temperature is 50 DEG C；
Step 4: after the ethyl alcohol in the extracting solution of refluxing extraction volatilizees completely, obtaining soapberry extract；
Step 5: using obtain 0.5 part of soapberry extract as raw material and 3 parts of dodecyl ether sulfates；3 parts straight
Alkyl group benzene sulfonic acid；20 parts of lauroylamidopropyl betaines；3 parts of glycerin monostearates；0.2 part of polyquaternium -7；3 portions of lemons
Sour sodium；0.01 portion of preservative；50 parts of deionized waters are uniformly mixed, and Soapberry liquid laundry detergent is made.
Embodiment 3
A kind of Soapberry liquid laundry detergent is prepared by the raw material of following parts by weight:
5 parts of dodecyl ether sulfates；5 parts of linear alkyl benzene sulfonic acids；40 parts of lauroylamidopropyl betaines；5 parts of lists
Tristerin；0.5 part of polyquaternium -7；4 parts of sodium citrates；3 parts of soapberry extracts；0.05 portion of preservative；70 parts are gone
Ionized water.
The preparation method of above-mentioned Soapberry liquid laundry detergent the following steps are included:
Step 1: taking out soapberry seed, its pericarp is placed in baking oven, after 100 DEG C of drying, be crushed to 100 mesh；
Step 2: will be mixed by drying, smashed soapberry pericarp powder with the water of 2 times of quality, impregnate 26h, obtain
Soapberry pericarp mixed liquor；
Step 3: the soapberry pericarp mixed liquor boiling 6h after impregnating will be mixed with water, it is mixed that addition is equivalent to soapberry pericarp
The ethyl alcohol of 5 times of quality of liquid, refluxing extraction 4h are closed, refluxing extraction temperature is 70 DEG C；
Step 4: after the ethyl alcohol in the extracting solution of refluxing extraction volatilizees completely, obtaining soapberry extract；
Step 5: using obtain 3 parts of soapberry extracts as raw material and 5 parts of dodecyl ether sulfates；5 parts of straight chains
Alkyl benzene sulphonate；40 parts of lauroylamidopropyl betaines；5 parts of glycerin monostearates；0.5 part of polyquaternium -7；4 parts of citric acids
Sodium；0.05 portion of preservative；70 parts of deionized waters are uniformly mixed, and Soapberry liquid laundry detergent is made.
In conclusion in Soapberry liquid laundry detergent ingredient provided by the invention, with dodecyl ether sulfate, straight chained alkyl
Benzene sulfonic acid, glycerin monostearate, lauroylamidopropyl betaine, part polyquaternium -7 are mixed according to special ratios, and are added
The soapberry extract of specific quantity reduces the irritation of linear alkyl benzene sulfonic acid by reasonably matching, pH value is neutralized to
Neutrality, it is mild skin friendly, by the cooperation of a variety of chemicals, make liquid detergent that there is outstanding emulsification, foam performance, and
Antifoam performance has stronger dirt-removing power and antibacterial ability compared to traditional liquid detergent, and has the characteristics that easily to rinse；This Shen
It is all made of chemicals in addition to soapberry extract in the Soapberry liquid laundry detergent ingredient related to, compares pure natural liquid detergent, greatly
While reducing production cost greatly, its mild skin friendly characteristic ensure that.
The above description is only an embodiment of the present invention, is not intended to limit the scope of the invention, all to utilize this hair
Equivalents made by bright description are applied directly or indirectly in relevant technical field, are similarly included in this hair
In bright scope of patent protection.
Claims (8)
1. a kind of Soapberry liquid laundry detergent, which is characterized in that be prepared by the raw material of following parts by weight:
3-5 parts of dodecyl ether sulfates；3-5 parts of linear alkyl benzene sulfonic acids；20-40 parts of lauroylamidopropyl betaines；3-5
Part glycerin monostearate；0.2-0.5 parts of polyquaterniums -7；3-4 parts of sodium citrates；0.5-3 parts of soapberry extracts；0.01-
0.05 portion of preservative；50-70 parts of deionized waters.
2. Soapberry liquid laundry detergent according to claim 1, which is characterized in that specifically by following parts by weight raw material preparation and
At:
3-5 parts of dodecyl ether sulfates；4 parts of linear alkyl benzene sulfonic acids；30 parts of lauroylamidopropyl betaines；4 parts of lists are hard
Glycerol；0.3 part of polyquaternium -7；3.5 parts of sodium citrates；2 parts of soapberry extracts；0.03 portion of preservative；60 parts are gone
Ionized water.
3. Soapberry liquid laundry detergent according to claim 1, which is characterized in that specifically by following parts by weight raw material preparation and
At:
3 parts of dodecyl ether sulfates；3 parts of linear alkyl benzene sulfonic acids；20 parts of lauroylamidopropyl betaines；3 parts single stearic
Acid glyceride；0.2 part of polyquaternium -7；3 parts of sodium citrates；0.5 part of soapberry extract；0.01 portion of preservative；50 parts go from
Sub- water.
4. Soapberry liquid laundry detergent according to claim 1, which is characterized in that specifically by following parts by weight raw material preparation and
At:
5 parts of dodecyl ether sulfates；5 parts of linear alkyl benzene sulfonic acids；40 parts of lauroylamidopropyl betaines；5 parts single stearic
Acid glyceride；0.5 part of polyquaternium -7；4 parts of sodium citrates；3 parts of soapberry extracts；0.05 portion of preservative；70 parts of deionizations
Water.
5. a kind of preparation method of Soapberry liquid laundry detergent, which comprises the following steps:
Step 1: taking out soapberry seed, its pericarp is placed in baking oven, after 80-100 DEG C of drying, be crushed to 60-100 mesh；
Step 2: will be mixed by drying, smashed soapberry pericarp powder with the water of 2 times of quality, impregnate 22-26h, obtain
Soapberry pericarp mixed liquor；
Step 3: the soapberry pericarp mixed liquor boiling 4-6h after impregnating will be mixed with water, addition is equivalent to the mixing of soapberry pericarp
The ethyl alcohol of 3-5 times of quality of liquid, refluxing extraction 2-4h, refluxing extraction temperature are 50-70 DEG C；
Step 4: after the ethyl alcohol in the extracting solution of refluxing extraction volatilizees completely, obtaining soapberry extract；
Step 5: using obtained 0.5-3 part soapberry extract as raw material and 3-5 parts of dodecyl ether sulfates；3-5 parts
Linear alkyl benzene sulfonic acid；20-40 parts of lauroylamidopropyl betaines；3-5 parts of glycerin monostearates；0.2-0.5 parts of polyquaternary amines
Salt -7；3-4 parts of sodium citrates；0.01-0.05 portions of preservatives；50-70 parts of deionized waters are uniformly mixed, and soapberry laundry is made
Liquid.
6. the preparation method of Soapberry liquid laundry detergent according to claim 5, which is characterized in that specifically includes the following steps:
Step 1: taking out soapberry seed, its pericarp is placed in baking oven, after 80 DEG C of drying, be crushed to 60 mesh；
Step 2: will be mixed by drying, smashed soapberry pericarp powder with the water of 2 times of quality, impregnate 22h, obtain no trouble
Sub- pericarp mixed liquor；
Step 3: the soapberry pericarp mixed liquor boiling 4h after impregnating will be mixed with water, addition is equivalent to soapberry pericarp mixed liquor
The ethyl alcohol of 3 times of quality, refluxing extraction 2-4h, refluxing extraction temperature are 50 DEG C；
Step 4: after the ethyl alcohol in the extracting solution of refluxing extraction volatilizees completely, obtaining soapberry extract；
Step 5: using obtain 0.5 part of soapberry extract as raw material and 3 parts of dodecyl ether sulfates；3 parts of straight chain alkane
Base benzene sulfonic acid；20 parts of lauroylamidopropyl betaines；3 parts of glycerin monostearates；0.2 part of polyquaternium -7；3 parts of citric acids
Sodium；0.01 portion of preservative；50 parts of deionized waters are uniformly mixed, and Soapberry liquid laundry detergent is made.
7. the preparation method of Soapberry liquid laundry detergent according to claim 5, which is characterized in that specifically includes the following steps:
Step 1: taking out soapberry seed, its pericarp is placed in baking oven, after 90 DEG C of drying, be crushed to 80 mesh；
Step 2: will be mixed by drying, smashed soapberry pericarp powder with the water of 2 times of quality, impregnate for 24 hours, obtain no trouble
Sub- pericarp mixed liquor；
Step 3: the soapberry pericarp mixed liquor boiling 5h after impregnating will be mixed with water, addition is equivalent to soapberry pericarp mixed liquor
The ethyl alcohol of 4 times of quality, refluxing extraction 3h, refluxing extraction temperature are 60 DEG C；
Step 4: after the ethyl alcohol in the extracting solution of refluxing extraction volatilizees completely, obtaining soapberry extract；
Step 5: using obtain 2 parts of soapberry extracts as raw material and 3-5 parts of dodecyl ether sulfates；4 parts of straight chain alkane
Base benzene sulfonic acid；30 parts of lauroylamidopropyl betaines；4 parts of glycerin monostearates；0.3 part of polyquaternium -7；3.5 parts of citric acids
Sodium；0.03 portion of preservative；60 parts of deionized waters are uniformly mixed, and Soapberry liquid laundry detergent is made.
8. the preparation method of Soapberry liquid laundry detergent according to claim 5, which is characterized in that specifically includes the following steps:
Step 1: taking out soapberry seed, its pericarp is placed in baking oven, after 100 DEG C of drying, be crushed to 100 mesh；
Step 2: will be mixed by drying, smashed soapberry pericarp powder with the water of 2 times of quality, impregnate 26h, obtain no trouble
Sub- pericarp mixed liquor；
Step 3: the soapberry pericarp mixed liquor boiling 6h after impregnating will be mixed with water, addition is equivalent to soapberry pericarp mixed liquor
The ethyl alcohol of 5 times of quality, refluxing extraction 4h, refluxing extraction temperature are 70 DEG C；
Step 4: after the ethyl alcohol in the extracting solution of refluxing extraction volatilizees completely, obtaining soapberry extract；
Step 5: using obtain 3 parts of soapberry extracts as raw material and 5 parts of dodecyl ether sulfates；5 parts of straight chained alkyls
Benzene sulfonic acid；40 parts of lauroylamidopropyl betaines；5 parts of glycerin monostearates；0.5 part of polyquaternium -7；4 parts of sodium citrates；
0.05 portion of preservative；70 parts of deionized waters are uniformly mixed, and Soapberry liquid laundry detergent is made.
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| CN111748419A (en) * | 2020-06-30 | 2020-10-09 | 广州市金盛生物科技有限公司 | Antibacterial gel special for underwear and preparation method thereof |
| CN111876272A (en) * | 2020-07-28 | 2020-11-03 | 上海时宜品牌管理有限公司 | Laundry detergent |
| CN112877148A (en) * | 2021-01-19 | 2021-06-01 | 北京圣永制药有限公司 | Bacteriostatic laundry detergent containing natural plant components |
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