CN110755347A - Skin moistening humectant and preparation method and application thereof - Google Patents

Skin moistening humectant and preparation method and application thereof Download PDF

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Publication number
CN110755347A
CN110755347A CN201911093108.9A CN201911093108A CN110755347A CN 110755347 A CN110755347 A CN 110755347A CN 201911093108 A CN201911093108 A CN 201911093108A CN 110755347 A CN110755347 A CN 110755347A
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fenugreek
extract
moisturizing
water
extraction
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王洪伦
何彦峰
胡娜
栾广祥
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Northwest Institute of Plateau Biology of CAS
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Northwest Institute of Plateau Biology of CAS
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

Abstract

The invention discloses a skin moistening agent and a preparation method and application thereof, wherein the skin moistening agent comprises the following components in percentage by weight: 1-2 parts of fenugreek polysaccharide, 0.1-1 part of fenugreek seed oil, 0.1-1 part of chamomile extract and 0.1-1 part of aloe extract. The moisturizing agent disclosed by the invention adopts the fenugreek polysaccharide and the fenugreek seed oil, is matched with the chamomile extract and the aloe extract for use, has a synergistic effect, can greatly improve the moisturizing effect of the product, better ensures the overall skin care effect of the product, is high in safety, and is suitable for various skins; the preparation process is simple and can be used for large-scale industrial production.

Description

Skin moistening humectant and preparation method and application thereof
Technical Field
The invention relates to the field of skin care products, in particular to a skin moisturizing agent and a preparation method thereof.
Background
Skin care products, i.e. products for protecting the skin. With the continuous progress of social economy and the abundance of material life, the skin care product is no longer a thing which is only used by abundant people in the past. Skin care products are now moving into the homes of ordinary people. It plays a great role in improving the spirit and the image of people.
Skin care products are diverse in variety and different in characteristics, but as a basis for skin care, almost all skin care products need to have an effect: and (5) moisturizing. The normal skin stratum corneum water content is 10-20%, the granular layer is 50-60%, the spinous layer is about 65%, the basal layer is about 70%, and the dermal layer water content is 80%. A large amount of water is filled in epidermal cells, and the water of the skin and other tissues together ensure that the skin is moist, full and elastic. If the skin contains insufficient moisture, the cells supporting the skin "deflate" and the skin loses its luster and becomes dull and dull.
The lotion is a common liquid cream skin care product, is particularly suitable for being used in dry seasons, is light in texture, is suitable for any skin type, and is popular among many people. Compared with the moisture-keeping preparation of chemical synthesis, the extract of natural plants is used in the skin care product, which is milder and safer, and has better market prospect, so that the development of more skin care products taking the natural extract as the main effective component is particularly important.
Disclosure of Invention
The invention aims to provide a fenugreek seed oil and fenugreek polysaccharide humectant and a preparation method thereof, which can effectively moisten and protect skin and improve the moisturizing effect of a product.
In order to solve the problems, the invention provides a moisturizing agent, which comprises the following components: fenugreek polysaccharide, fenugreek seed oil, chamomile extract, and aloe extract.
Further, the skin moistening agent comprises the following components in parts by weight: 1-2 parts of fenugreek polysaccharide, 0.1-1 part of fenugreek seed oil, 0.1-1 part of chamomile extract and 0.1-1 part of aloe extract.
Further, the fenugreek polysaccharide is obtained by subcritical water extraction and ultrafiltration membrane interception extraction of fenugreek seeds;
further, performing subcritical water extraction on fenugreek seed powder at 100-200 ℃ and under the pressure of 2-6 MPa to obtain polysaccharide extract; intercepting the polysaccharide extract by using an ultrafiltration membrane to obtain intercepted liquid; removing the solvent from the trapped fluid to obtain the product;
furthermore, the molecular weight cut-off of the ultrafiltration membrane is 20-100K;
further, the conditions for the ultrafiltration membrane interception are as follows: the pressure is 3-10 Kg, and the flow rate is 50-200 mL/min;
further, the ultrafiltration membrane is an organic ultrafiltration membrane.
Further, the fenugreek seed oil is prepared by subjecting fenugreek seeds to supercritical CO extraction2The preparation method comprises the following steps of (1) extracting;
further, the using amount of the compound enzyme is 0.5 percent;
further, the supercritical extraction conditions are as follows: the extraction pressure is 25-30 MPa, the extraction temperature is 35-45 ℃, and the extraction time is 80-120 min
Further, the supercritical extraction conditions are: the extraction pressure is 28.5MPa, the extraction temperature is 41 ℃, and the extraction time is 118 min.
However, the extraction methods of the above-mentioned various extracts are not limited to the above-mentioned methods, and any extraction method disclosed in the art for preparing a cosmetic-grade extract can be applied to the present invention.
The invention also provides a skin care product which comprises the skin moistening agent.
The invention also provides a moisturizing emulsion which comprises sodium ethylene diamine tetracetate, triethanolamine, stearic acid, cetyl alcohol, lanolin, vitamin E, fenugreek polysaccharide, fenugreek seed oil, chamomile extract, aloe extract, essence, preservative and water.
Further, the moisturizing emulsion comprises the following components in percentage by weight: 0.01-0.1% of sodium ethylene diamine tetracetate, 0.1-0.3% of triethanolamine, 0.1-1.0% of stearic acid, 1.0-3.0% of hexadecanol, 1.0-3.0% of lanolin, 0.1-0.5% of vitamin E, 1.0-2.0% of fenugreek polysaccharide, 0.1-1.0% of fenugreek seed oil, 0.1-1.0% of chamomile extract, 0.1-1.0% of aloe extract, 0.1-0.8% of essence, 0.1-1.0% of preservative and the balance of water;
further, the moisturizing emulsion comprises the following components in percentage by weight: 0.05% of sodium ethylene diamine tetracetate, 0.2% of triethanolamine, 0.5% of stearic acid, 2.0% of hexadecanol, 1.5% of lanolin, 0.2% of vitamin E, 1.0% of fenugreek polysaccharide, 0.5% of fenugreek seed oil, 0.5% of chamomile extract, 0.5% of aloe extract, 0.1% of essence, 0.2% of preservative and the balance of water.
The moisturizing emulsion is not particularly limited to the selection of the essence and the preservative, and the existing essence and preservative which can be used for skin care products or external clothing can be suitable for the moisturizing emulsion, for example, the preservative can be selected from methyl paraben, propyl paraben and the like, and the essence can be selected from rose fragrance, jasmine fragrance, lemon fragrance and the like.
The amount of water used in the moisturizing emulsion is not particularly limited, and the amount of water can be properly added according to the concentration degree of the required product.
The invention also provides a preparation method of the moisturizing emulsion, which comprises the following steps:
(1) preparing a water phase material: mixing sodium ethylene diamine tetracetate, triethanolamine, fenugreek polysaccharide, chamomile extract, aloe extract and water, heating and stirring until the mixture is completely dissolved to form a water phase;
(2) preparing an oil phase material: mixing stearic acid, lanolin, cetyl alcohol, vitamin E and fenugreek seed oil, heating and stirring until completely dissolving to form an oil phase;
(3) emulsification forming: and (3) pouring the water phase into the oil phase one by one at the temperature of 70-90 ℃, stirring while adding to form uniform emulsion, cooling to 60-50 ℃, and adding essence and preservative to obtain the emulsion.
In the step (3), the water phase is poured into the oil phase one by one, which means that the water phase is not all poured into the oil phase together at the same time at one time; the water phase can be added into the oil phase in batches with small amount of water phase, or slowly poured into the oil phase at a certain flow rate and constant speed or variable speed within a certain time.
Further, in the step (1), the temperature is raised to 70-90 ℃, preferably 85 ℃;
in the step (2), the heating is carried out to 70-90 ℃, preferably 85 ℃;
in step (3), the temperature of the water phase is 85 ℃ when the water phase is added into the oil phase, and the emulsion is cooled to 60 ℃ when the essence is added.
The invention also provides the application of the moisturizing agent and the moisturizing emulsion in preparing products with moisturizing effects.
Such products include, but are not limited to, skin care products, topical pharmaceuticals, and the like.
The invention has the beneficial effects that:
(1) the fenugreek polysaccharide and the fenugreek seed oil are added into the moisturizing agent, and are matched with the chamomile extract and the aloe extract for use, so that the synergy is realized, the moisturizing effect of the skin care product can be greatly improved, and the overall skin care effect of the product can be better ensured.
(2) The moisturizing emulsion disclosed by the invention is pure in color, fine in texture, safe to use, free of irritation, sensitization and toxic and side effects, good in moisturizing effect and suitable for various skins.
(3) The moisturizing emulsion disclosed by the invention is simple in preparation process and can be produced industrially on a large scale.
Detailed Description
The present invention is further illustrated by the following specific examples and specific tests.
In the present invention, the fenugreek seed oil, fenugreek polysaccharide, chamomile extract, and aloe extract can be obtained by purchasing commercially available products, or by purchasing raw materials and extracting them by the prior art.
Example 1
A moisturizing emulsion is prepared from the following raw materials in parts by weight to prepare a 100mL product:
0.01g of sodium ethylene diamine tetracetate, 0.3g of triethanolamine, 0.1g of stearic acid, 1.0g of hexadecanol, 1.0g of lanoline, 0.1g of vitamin E, 1.0g of fenugreek polysaccharide, 0.1g of fenugreek seed oil, 0.1g of chamomile extract, 0.1g of aloe extract, 0.1g of essence, 0.1g of preservative and the balance of refined water.
The preparation method comprises the following steps:
(1) preparing a water phase material: adding water phase raw materials such as sodium ethylene diamine tetracetate, triethanolamine, semen Trigonellae polysaccharide, flos Matricariae Chamomillae extract, and Aloe extract into water phase pot, adding refined water, heating and stirring to dissolve completely, heating to 70 deg.C, maintaining for 20min, and sterilizing to obtain water phase;
(2) preparing an oil phase material: sequentially adding oil phase raw materials such as stearic acid, lanolin, cetyl alcohol, vitamin E, fenugreek seed oil, etc. into an oil phase pot, mixing, heating and stirring to completely dissolve to 70 deg.C, maintaining for 20min, and sterilizing to form oil phase;
(3) emulsification forming: when the water phase and the oil phase are uniform liquid, slowly pouring the water phase into the oil phase in a trickle shape on a water bath kettle at 70 ℃, continuously stirring in the same direction while adding, stirring for 8 minutes on the water phase kettle after the water phase is poured out to form uniform emulsion, taking down the emulsion from the water bath kettle, cooling to 50 ℃, respectively adding essence and preservative, stirring uniformly and cooling to room temperature to obtain the moisturizing emulsion.
Example 2
A moisturizing emulsion is prepared from the following raw materials in parts by weight to prepare a 100mL product:
0.1g of sodium ethylene diamine tetracetate, 0.1g of triethanolamine, 1.0g of stearic acid, 3.0g of hexadecanol, 3.0g of lanoline, 0.5g of vitamin E, 2.0g of fenugreek polysaccharide, 1.0g of fenugreek seed oil, 1.0g of chamomile extract, 1.0g of aloe extract, 0.8g of essence, 1.0g of preservative and the balance of refined water.
The preparation method comprises the following steps:
(1) preparing a water phase material: adding water phase raw materials such as sodium ethylene diamine tetracetate, triethanolamine, semen Trigonellae polysaccharide, flos Matricariae Chamomillae extract, and Aloe extract into water phase pot, adding refined water, heating and stirring to dissolve completely, heating to 90 deg.C, maintaining for 20min, and sterilizing to obtain water phase;
(2) preparing an oil phase material: sequentially adding oil phase raw materials such as stearic acid, lanolin, cetyl alcohol, vitamin E, fenugreek seed oil, etc. into an oil phase pot, mixing, heating and stirring to dissolve completely to 90 deg.C, maintaining for 20min, and sterilizing to form oil phase;
(3) emulsification forming: when the water phase and the oil phase are uniform liquid, slowly pouring the water phase into the oil phase in a trickle shape on a water bath kettle at the temperature of 90 ℃, continuously stirring in the same direction while adding, stirring for 8 minutes on the water phase kettle after the water phase is poured out to form uniform emulsion, taking down the emulsion from the water bath kettle, cooling to the temperature of 60 ℃, respectively adding essence and preservative, stirring uniformly and cooling to the room temperature to obtain the moisturizing emulsion.
Example 3
A moisturizing emulsion is prepared from the following raw materials in parts by weight to prepare a 100mL product:
0.05g of sodium ethylene diamine tetracetate, 0.2g of triethanolamine, 0.5g of stearic acid, 2.0g of hexadecanol, 1.5g of lanoline, 0.2g of vitamin E, 1.0g of fenugreek polysaccharide, 0.5g of fenugreek seed oil, 0.5g of chamomile extract, 0.5g of aloe extract, 0.1g of essence, 0.2g of preservative and the balance of refined water.
The preparation method comprises the following steps:
(1) preparing a water phase material: adding water phase raw materials such as sodium ethylene diamine tetracetate, triethanolamine, semen Trigonellae polysaccharide, flos Matricariae Chamomillae extract, and Aloe extract into water phase pot, adding refined water, heating and stirring to dissolve completely, heating to 85 deg.C, maintaining for 20min, and sterilizing to obtain water phase;
(2) preparing an oil phase material: sequentially adding oil phase raw materials such as stearic acid, lanolin, cetyl alcohol, vitamin E, fenugreek seed oil, etc. into an oil phase pot, mixing, heating and stirring to dissolve completely to 85 deg.C, maintaining for 20min, and sterilizing to form oil phase;
(3) emulsification forming: when the water phase and the oil phase are uniform liquid, slowly pouring the water phase into the oil phase in a trickle shape on a water bath kettle at 85 ℃, continuously stirring in the same direction while adding, stirring for 8 minutes on the water phase kettle after the water phase is poured out to form uniform emulsion, taking down the emulsion from the water bath kettle, cooling to 60 ℃, respectively adding essence and preservative, stirring uniformly and cooling to room temperature to obtain the moisturizing emulsion.
Comparative example 1
A moisturizing emulsion is prepared from the following raw materials in parts by weight to prepare a 100mL product:
0.05g of sodium ethylene diamine tetracetate, 0.2g of triethanolamine, 0.5g of stearic acid, 2.0g of hexadecanol, 1.5g of lanoline, 0.2g of vitamin E, 0.5g of chamomile extract, 0.5g of aloe extract, 0.1g of essence, 0.2g of preservative and the balance of refined water.
The preparation method comprises the following steps:
(1) preparing a water phase material: adding water phase raw materials such as sodium ethylene diamine tetracetate, triethanolamine, flos Matricariae Chamomillae extract, Aloe extract, etc. into water phase pot, adding refined water, heating and stirring to dissolve completely, heating to 85 deg.C, maintaining for 20min, sterilizing to form water phase;
(2) preparing an oil phase material: sequentially adding oil phase raw materials such as stearic acid, lanolin, cetyl alcohol, vitamin E, etc. into an oil phase pot, mixing, heating and stirring to dissolve completely to 85 deg.C, maintaining for 20min, sterilizing to form oil phase;
(3) emulsification forming: when the water phase and the oil phase are uniform liquid, slowly pouring the water phase into the oil phase in a trickle shape on a water bath kettle at 85 ℃, continuously stirring in the same direction while adding, stirring for 8 minutes on the water phase kettle after the water phase is poured out to form uniform emulsion, taking down the emulsion from the water bath kettle, cooling to 60 ℃, respectively adding essence and preservative, stirring uniformly, and cooling to room temperature to obtain the control moisturizing emulsion.
Test example 1
And (3) carrying out efficacy performance test and quality detection on the moisturizing emulsion prepared in the example 3 and the moisturizing emulsion prepared in the comparative example 1, and carrying out effect comparison:
the application method of the moisturizing emulsion comprises the following steps: after the skin is cleaned, the product is lightly tapped on the face or the neck until the product is completely absorbed, and the using effect is observed and felt.
A total of 100 subjects were divided into two groups, 50 for each of the examples and the control, and the skin of the hands, face and neck was cleansed with warm water every day, the moisturizing lotions of the examples and the control were applied to the skin of the face and neck uniformly every 12 hours for one month, and then the subjects were listened to their feelings. The results are shown in Table 1.
TABLE 1
Figure BDA0002267453140000081
As can be seen from table 1, more than 90% of the test subjects of the moisturizing emulsion of the present invention (example 3) considered that the emulsion had a good skin care effect, good and durable moisturizing performance, and no irritation; the moisture retention effect of the product is considered to be good by only 60% of the test subjects of the emulsion in the comparison example. In conclusion, the fenugreek seed oil and the fenugreek polysaccharide can enhance the skin care effect and play a role in synergy with other components in the emulsion.
And (3) quality detection:
1. sensory detection: the color is milky white, and the fragrance is pleasant and not greasy.
2. Physical and chemical detection: pH4.5-8.5
3. And (3) detecting microorganisms: the total number of bacteria is less than 500/g; fecal coliform bacteria, pseudomonas aeruginosa and staphylococcus aureus are not detected and meet the cosmetic standard.
4. And (3) heavy metal detection: mercury is less than 1ppm, lead is less than 40ppm, arsenic is less than 10ppm, and the mercury, the lead and the arsenic are within the standard range of cosmetics.
And (3) safety testing:
the moisturizing lotion is carried out according to the method specified in QB963-1985, and results show that the moisturizing lotion has no irritation to skin and mucosa of normal human bodies and can be safely used.
In conclusion, the fenugreek seed oil, the fenugreek polysaccharide, the chamomile extract, the aloe extract and other components are used in a compatible manner, so that the skin care effect of the emulsion is obviously enhanced, the effect of the emulsion is obviously superior to that of a moisturizing emulsion with the chamomile extract and the aloe extract, and the synergistic effect is fully exerted. The moisturizing emulsion disclosed by the invention has no toxic or side effect and has excellent moisturizing effect.
The above description is only an embodiment of the present invention, and not intended to limit the scope of the present invention, and all modifications of equivalent structures and equivalent processes, which are made by the present specification, or directly or indirectly applied to other related technical fields, are included in the scope of the present invention.

Claims (10)

1. The skin moistening agent is characterized by comprising the following components: fenugreek polysaccharide, fenugreek seed oil, chamomile extract, and aloe extract.
2. The skin moisturizer according to claim 1, which is characterized by comprising the following components in parts by weight: 1-2 parts of fenugreek polysaccharide, 0.1-1 part of fenugreek seed oil, 0.1-1 part of chamomile extract and 0.1-1 part of aloe extract.
3. The moisturizing agent as claimed in claim 1 or 2, wherein the fenugreek polysaccharide is obtained by subcritical water extraction and ultrafiltration membrane interception extraction of fenugreek seeds;
further, performing subcritical water extraction on fenugreek seed powder at 100-200 ℃ and under the pressure of 2-6 MPa to obtain polysaccharide extract; intercepting the polysaccharide extract by using an ultrafiltration membrane to obtain intercepted liquid; removing the solvent from the trapped fluid to obtain the product;
furthermore, the molecular weight cut-off of the ultrafiltration membrane is 20-100K;
further, the conditions for the ultrafiltration membrane interception are as follows: the pressure is 3-10 Kg, and the flow rate is 50-200 mL/min;
further, the ultrafiltration membrane is an organic ultrafiltration membrane.
4. The moisturizing agent as claimed in claim 1 or 2, wherein the fenugreek seed oil is obtained by subjecting fenugreek seeds to supercritical CO extraction2The preparation method comprises the following steps of (1) extracting;
further, the using amount of the compound enzyme is 0.5 percent;
further, the supercritical extraction conditions are as follows: the extraction pressure is 25-30 MPa, the extraction temperature is 35-45 ℃, and the extraction time is 80-120 min
Further, the supercritical extraction conditions are: the extraction pressure is 28.5MPa, the extraction temperature is 41 ℃, and the extraction time is 118 min.
5. A skin care preparation comprising the skin moisturizing agent according to any one of claims 1 to 4.
6. A moisturizing lotion is characterized by comprising sodium ethylene diamine tetracetate, triethanolamine, stearic acid, cetyl alcohol, lanolin, vitamin E, fenugreek polysaccharide, fenugreek seed oil, chamomile extract, aloe extract, essence, preservative and water.
7. The moisturizing emulsion of claim 6, comprising the following components in percentage by weight: 0.01-0.1% of sodium ethylene diamine tetracetate, 0.1-0.3% of triethanolamine, 0.1-1.0% of stearic acid, 1.0-3.0% of hexadecanol, 1.0-3.0% of lanolin, 0.1-0.5% of vitamin E, 1.0-2.0% of fenugreek polysaccharide, 0.1-1.0% of fenugreek seed oil, 0.1-1.0% of chamomile extract, 0.1-1.0% of aloe extract, 0.1-0.8% of essence, 0.1-1.0% of preservative and the balance of water;
further, the moisturizing emulsion comprises the following components in percentage by weight: 0.05% of sodium ethylene diamine tetracetate, 0.2% of triethanolamine, 0.5% of stearic acid, 2.0% of hexadecanol, 1.5% of lanolin, 0.2% of vitamin E, 1.0% of fenugreek polysaccharide, 0.5% of fenugreek seed oil, 0.5% of chamomile extract, 0.5% of aloe extract, 0.1% of essence, 0.2% of preservative and the balance of water.
8. The method for preparing a moisturizing emulsion according to claim 6 or 7, comprising the following steps:
(1) preparing a water phase material: mixing sodium ethylene diamine tetracetate, triethanolamine, fenugreek polysaccharide, chamomile extract, aloe extract and water, heating and stirring until the mixture is completely dissolved to form a water phase;
(2) preparing an oil phase material: mixing stearic acid, lanolin, cetyl alcohol, vitamin E and fenugreek seed oil, heating and stirring until completely dissolving to form an oil phase;
(3) emulsification forming: and (3) pouring the water phase into the oil phase one by one at the temperature of 70-90 ℃, stirring while adding to form uniform emulsion, cooling to 60-50 ℃, and adding essence and preservative to obtain the emulsion.
9. The method according to claim 8, wherein in the step (1), the temperature is raised to 70-90 ℃, preferably 85 ℃;
in the step (2), the heating is carried out to 70-90 ℃, preferably 85 ℃;
in step (3), the temperature of the water phase is 85 ℃ when the water phase is added into the oil phase, and the emulsion is cooled to 60 ℃ when the essence is added.
10. Use of the emollient moisturizer of any one of claims 1 to 4, the moisturizing emulsion of claim 6 or 7 in the preparation of a product with moisturizing efficacy.
CN201911093108.9A 2019-11-11 2019-11-11 Skin moistening humectant and preparation method and application thereof Pending CN110755347A (en)

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