CN103690404A - Baby bath agent containing marine bioactive substances as well as compositions and preparation method of baby bath agent - Google Patents

Baby bath agent containing marine bioactive substances as well as compositions and preparation method of baby bath agent Download PDF

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CN103690404A
CN103690404A CN201310719933.1A CN201310719933A CN103690404A CN 103690404 A CN103690404 A CN 103690404A CN 201310719933 A CN201310719933 A CN 201310719933A CN 103690404 A CN103690404 A CN 103690404A
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bath agent
baby bath
stirring
percent
mixed liquor
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CN103690404B (en
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王鑫
李艳妮
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Qingdao Hifun Marine Biological Technology Co Ltd
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Qingdao Hifun Marine Biological Technology Co Ltd
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Abstract

The invention discloses a baby bath agent containing marine bioactive substances as well as compositions and a preparation method of the baby bath agent. The baby bath agent comprises the following components in parts by percent: 2.0-4.0 percent of a marine biological antibacterial agent, 5.0-10.0 percent of algal polysaccharides, 1.0-2.0 percent of chitin, 9.0-15.0 percent of alkyl glycoside, 4.0-8.0 percent of cocamidopropyl betaine, 11.0-16.0 percent of alcohol carboxylate, 1.0-15 percent of sodium chloride, 0.5-2.0 percent of citric acid, 0.5-2.0 percent of edible essence and the balance of purified water. The preparation method comprises the following steps: adding the alkyl glycoside, cocamidopropyl betaine and alcohol carboxylate into the purified water, stirring, emulsifying and obtaining a mixed solution A; adding the marine biological antibacterial agent, algal polysaccharides and chitin into the mixed solution A, uniformly stirring and mixing, thereby obtaining a mixed solution B; adding the sodium chloride, citric acid and edible essence, uniformly stirring and mixing, thereby obtaining the baby bath agent containing marine bioactive substances. The baby bath agent containing marine bioactive substances does not contain a preservative and does not have adverse stimulation to the baby's skin.

Description

The baby bath agent that contains marine bioactivity material and compositions, preparation method
Technical field
The present invention relates to the preparation of taking a shower, relate in particular to a kind of baby bath agent that contains marine bioactivity material and compositions, preparation method.
Background technology
At present, the kind of existing baby bath articles for use is a lot, and main adding ingredient is: surfactant and antiseptic.Infant skin has skin thin, and lipid is few, and skin resistance is poor, the feature that metabolism is fast, and bath article as strong in frequent thigmic stimulus, can cause pessimal stimulation to baby's body skin, cause xerosis cutis, dermatitis, eczema or allergic phenomena.
Summary of the invention
Provide hereinafter about brief overview of the present invention, to the basic comprehension about some aspect of the present invention is provided.Should be appreciated that this general introduction is not about exhaustive general introduction of the present invention.It is not that intention is determined key of the present invention or pith, and nor is it intended to limit the scope of the present invention.Its object is only that the form of simplifying provides some concept, usings this as the preorder in greater detail of discussing after a while.
The object of the embodiment of the present invention is the defect for above-mentioned prior art, provides a kind of not containing antiseptic, the baby bath agent that contains marine bioactivity material to infant skin without pessimal stimulation.
Another object of the present invention is to provide a kind of preparation method of the baby bath agent that contains marine bioactivity material.
To achieve these goals, the technical scheme that the present invention takes is:
The invention provides a kind of compositions for the baby bath agent that contains marine bioactivity material, comprise the component of following weight percentage:
Figure BDA0000444681280000011
Figure BDA0000444681280000021
The present invention also provides a kind of method of using above-mentioned compositions to prepare the baby bath agent that contains marine bioactivity material, comprises the following steps:
Step S10: to the alkyl polyglucoside, cocamido propyl betaine and the alcohol ether carboxylate that add proportional quantity in pure water, stir, carry out emulsifying, obtain mixed liquor A;
Step S20: marine organisms bacteria remover, Sargassum polysaccharides and chitin to adding proportional quantity in mixed liquor A, be uniformly mixed, obtain mixed liquid B;
Step S30: to the sodium chloride, citric acid and the edible essence that add proportional quantity in mixed liquid B, mix homogeneously obtains the baby bath agent that contains marine bioactivity material.
The present invention also provides a kind of baby bath agent that contains marine bioactivity material of preparing according to above-mentioned method.
Compared with prior art, the invention has the beneficial effects as follows:
The baby bath agent that contains marine bioactivity material of the present invention, owing to containing marine organisms bacteria remover composition, therefore, and after use, effectively degerming, and then the interpolation of alternative antiseptic there is antibacterial action.
The Sargassum polysaccharides containing and chitin are known marine bioactivity material, as natural immunostimulant, not only can the immunity of enhancing body and the ability of resist the disease, and can reduce the generation of body patience, promote the growth of animal, the complexation of Sargassum polysaccharides and mineral element, not only can improve the utilization rate of mineral element, reduce residually, can also produce cooperative effect.Simultaneously; Sargassum polysaccharides is a kind of good emollient; its active matter mass-energy is combined with skin protein and is formed the gel of moisture retention; and it can also form protecting film on the surface of skin by hydration; prevent moisture evaporation; there is obvious moisture-keeping function, therefore, can well protect the tender and lovely skin of baby.
The preparation method of the baby bath agent that contains marine bioactivity material of the present invention, because order by merging and the mixing condition of each material are comparatively reasonable, make each component mix homogeneously of the baby bath agent that contains marine bioactivity material making by preparation method of the present invention, good stability.
The specific embodiment
For making object, technical scheme and the advantage of the embodiment of the present invention clearer, below the technical scheme in the embodiment of the present invention is clearly and completely described, obviously, described embodiment is the present invention's part embodiment, rather than whole embodiment.Element and the feature described in one embodiment of the invention can combine with element and feature shown in one or more embodiment.It should be noted that for purposes of clarity, in explanation, omitted expression and the description of unrelated to the invention, parts known to persons of ordinary skill in the art and processing.Embodiment based in the present invention, those of ordinary skills, not paying the every other embodiment obtaining under creative work prerequisite, belong to the scope of protection of the invention.
The invention provides a kind of compositions for the baby bath agent that contains marine bioactivity material, comprise the component of following weight percentage:
Figure BDA0000444681280000031
Edible essence of the present invention can be selected edible strawberry essence, edible apple essence or edible Fructus Citri Limoniae essence.
The baby bath agent that contains marine bioactivity material of the present invention, owing to containing marine organisms bacteria remover composition, therefore, and the interpolation of instead of chemical antiseptic completely, the Sargassum polysaccharides containing and chitin can effectively moisten infant skin.
The selected surfactant of baby bath agent that contains marine bioactivity material of the present invention is all environment-friendly type, the novel surfactant non-stimulated to skin, and therefore, bath shampoo of the present invention is non-stimulated to infant skin.
In the present embodiment, in order to obtain better antibacterial and antiseptic effect, optional, for the compositions of the baby bath agent that contains marine bioactivity material, comprise the component of following weight percentage:
Figure BDA0000444681280000041
Preferred technical scheme: for the compositions of the baby bath agent that contains marine bioactivity material, comprise the component of following weight percentage:
Figure BDA0000444681280000042
Figure BDA0000444681280000051
Each component of the present invention, containing antiseptic, is not applicable to baby, and to infant skin, without pessimal stimulation, scientific formulation is reasonable.
In the present embodiment, in order to obtain better sterilization bacteria-eliminating efficacy, optional, described marine organisms bacteria remover by weight percent meter proportioning is as follows:
In the present embodiment, in order to make the mixed effect of each component better, described hydromining pure water.
It is the cecropin described in CN101104637B that described cecropin can adopt notification number, can certainly adopt other cecropin.
The present invention also provides a kind of method of using above-mentioned compositions to prepare the baby bath agent that contains marine bioactivity material, comprises the following steps:
Step S10: to the alkyl polyglucoside, cocamido propyl betaine and the alcohol ether carboxylate that add proportional quantity in pure water, stir, carry out emulsifying, obtain mixed liquor A;
Step S20: marine organisms bacteria remover, Sargassum polysaccharides and chitin to adding proportional quantity in mixed liquor A, be uniformly mixed, obtain mixed liquid B;
Step S30: to the sodium chloride, citric acid and the edible essence that add proportional quantity in mixed liquid B, mix homogeneously obtains the baby bath agent that contains marine bioactivity material.
The preparation method of the baby bath agent that contains marine bioactivity material of the present embodiment, because order by merging and the mixing condition of each material are reasonable, make each component mix homogeneously of the baby bath agent that contains marine bioactivity material making by preparation method of the present invention, good stability.
Preferably, described marine organisms bacteria remover is prepared as follows:
Step S101: carboxymethyl chitosan and Sargassum polysaccharides to adding proportional quantity in the water of 30~35 ℃, stir and within 10~20 minutes, obtain the first mixed liquor;
Step S102: the cecropin toward adding proportional quantity in the first mixed liquor, stirs and within 3~7 minutes, obtains the second mixed liquor;
Step S103: the N-acetylmuramide lycanohydrlase toward adding proportional quantity in the second mixed liquor, stirs and within 3~7 minutes, obtains described degerming marine organisms bacteria remover.
In the present embodiment, in order to make each component obtain better mixed effect, in described step S10: the temperature of described pure water is 40-50 ℃, the time of stirring is 30-40 minute, and the speed of stirring is 80-90 rev/min.
In the present embodiment, in order to make each component obtain better mixed effect, in described step S20: the temperature of stirring is 25-35 ℃, the time of stirring is 15-20 minute, and the speed of stirring is 70-80 rev/min; In described step S30: the time of stirring is 10-15 minute, the speed of stirring is 70-80 rev/min.
In the present embodiment, in order to obtain portable shampoo, after step S30, also comprise step S40: after the baby bath agent that contains marine bioactivity material is cooling, carry out subpackage.
The present invention also provides a kind of baby bath agent that contains marine bioactivity material of preparing according to above-mentioned method.
Below by specific embodiment, the present invention is further illustrated:
Embodiment 1
The present embodiment provides a kind of baby bath agent that contains marine bioactivity material, and percent meter proportioning is as follows by weight:
Figure BDA0000444681280000061
Figure BDA0000444681280000071
The edible essence that the embodiment of the present invention is added can be selected the essence adding in shampoo in prior art or bath gel.Preferably edible apple essence.
Marine organisms bacteria remover in the present embodiment by weight percent meter proportioning is: carboxymethyl chitosan 1.5%; Sargassum polysaccharides 3.0%; Cecropin 7.0%; N-acetylmuramide lycanohydrlase 2.0%; Water 86.5%.
Marine organisms bacteria remover is prepared as follows:
Step S101: carboxymethyl chitosan and Sargassum polysaccharides to adding proportional quantity in the water of 32 ℃, stir and within 15 minutes, obtain the first mixed liquor;
Step S102: the cecropin toward adding proportional quantity in the first mixed liquor, stirs and within 6 minutes, obtains the second mixed liquor;
Step S103: the N-acetylmuramide lycanohydrlase toward adding proportional quantity in the second mixed liquor, stirs and within 5 minutes, obtains described degerming marine organisms bacteria remover.
The preparation method of the baby bath agent that contains marine bioactivity material of the present embodiment is carried out as follows:
Step S10: to the alkyl polyglucoside, cocamido propyl betaine, the alcohol ether carboxylate AEC that add proportional quantity in the pure water of 45 ℃, take speed as 85 revs/min.Stir 35 minutes, carry out emulsifying and obtain mixed liquor A;
Step S20: to the marine organisms bacteria remover, Sargassum polysaccharides and the chitin that add proportional quantity in mixed liquor A, at 35 ℃, take speed as 75 revs/min.Stir 15 minutes, mix homogeneously obtains mixed liquid B;
Step S30: to the sodium chloride, citrin and the edible apple essence that add proportional quantity in mixed liquid B, take speed as 75 revs/min.Stir 15 minutes, mix homogeneously obtains the baby bath agent that contains marine bioactivity material.
Through experiment, the effectively decontamination of baby bath agent that contains marine bioactivity material of the present embodiment, antibacterial, and after using, non-stimulated to skin, skin-moisturizing, skin is good.
Embodiment 2
The present embodiment provides a kind of baby bath agent that contains marine bioactivity material, and percent meter proportioning is as follows by weight:
Figure BDA0000444681280000081
Marine organisms bacteria remover in the present embodiment by weight percent meter proportioning is: carboxymethyl chitosan 2.0%; Sargassum polysaccharides 4.0%; Cecropin 8.0%; N-acetylmuramide lycanohydrlase 3.5%; Water 82.5%.It is the cecropin described in CN101104637B that the present embodiment adopts Chinese notification number.
Marine organisms bacteria remover is prepared as follows:
Step S101: carboxymethyl chitosan and Sargassum polysaccharides to adding proportional quantity in the water of 30 ℃, stir and within 10 minutes, obtain the first mixed liquor;
Step S102: the cecropin toward adding proportional quantity in the first mixed liquor, stirs and within 7 minutes, obtains the second mixed liquor;
Step S103: the N-acetylmuramide lycanohydrlase toward adding proportional quantity in the second mixed liquor, stirs and within 3 minutes, obtains described degerming marine organisms bacteria remover.
The preparation method of the baby bath agent that contains marine bioactivity material of the present embodiment is carried out as follows:
Step S10: to the alkyl polyglucoside, cocamido propyl betaine, the alcohol ether carboxylate AEC that add proportional quantity in the pure water of 40 ℃, take speed as 80 revs/min, stir 40 minutes, carry out emulsifying and obtain mixed liquor A;
Step S20: to the marine organisms bacteria remover, Sargassum polysaccharides and the chitin that add proportional quantity in mixed liquor A, at 28 ℃, take speed as 80 revs/min, stir 13 minutes, mix homogeneously obtains mixed liquid B;
Step S30: to the sodium chloride, citrin and the edible strawberry essence that add proportional quantity in mixed liquid B, take speed as 70 revs/min, stir 14 minutes, mix homogeneously obtains the baby bath agent that contains marine bioactivity material.
Through test, the baby bath agent that contains marine bioactivity material of the present embodiment, smooth with rear skin.
Embodiment 3
The present embodiment provides a kind of baby bath agent that contains marine bioactivity material, and percent meter proportioning is as follows by weight:
Figure BDA0000444681280000091
Marine organisms bacteria remover in the present embodiment by weight percent meter proportioning is: carboxymethyl chitosan 1.0%; Sargassum polysaccharides 2.0%; Cecropin 6.0%; N-acetylmuramide lycanohydrlase 1.5%; Water 89.5%.
Marine organisms bacteria remover is prepared as follows:
Step S101: carboxymethyl chitosan and Sargassum polysaccharides to adding proportional quantity in the water of 35 ℃, stir and within 20 minutes, obtain the first mixed liquor;
Step S102: the cecropin toward adding proportional quantity in the first mixed liquor, stirs and within 3 minutes, obtains the second mixed liquor;
Step S103: the N-acetylmuramide lycanohydrlase toward adding proportional quantity in the second mixed liquor, stirs and within 7 minutes, obtains described degerming marine organisms bacteria remover.
The preparation method of the baby bath agent that contains marine bioactivity material of the present embodiment is carried out as follows:
Step S10: to the alkyl polyglucoside, cocamido propyl betaine, the alcohol ether carboxylate AEC that add proportional quantity in the pure water of 50 ℃, take speed as 90 revs/min, stir 30 minutes, carry out emulsifying and obtain mixed liquor A;
Step S20: to the marine organisms bacteria remover, Sargassum polysaccharides and the chitin that add proportional quantity in mixed liquor A, at 25 ℃, take speed as 70 revs/min, stir 20 minutes, mix homogeneously obtains mixed liquid B;
Step S30: to the sodium chloride, citrin and the edible Fructus Citri Limoniae essence that add proportional quantity in mixed liquid B, take speed as 80 revs/min, stir 10 minutes, mix homogeneously obtains the baby bath agent that contains marine bioactivity material.
Through experiment, the effectively decontamination of baby bath agent that contains marine bioactivity material of the present embodiment, antibacterial, and after using, non-stimulated to infant skin, moistening effect is good.
Pharmacodynamics research of the present invention:
From zoopery aspect, verify antibacterial action of the present invention:
1, material
Animal mice, regular grade, male and female half and half, body weight 18-22g, rat, male, body weight 180-220g.
2, carry out external susceptibility minimum inhibitory concentration MIC determination test:
Test strain: fungus, Candida albicans, staphylococcus aureus, Escherichia coli.
Method: each test strain is made to bacteria suspension with normal saline, and to be diluted to turbidity be the above bacteria suspension of 2.0McF, use again 100 times of normal saline dilutions, rev/min Ii640 culture fluid is released 10 times, test group (bath shampoo in the embodiment of the present invention 1) and matched group (baby Jinsui River bath gel) doubling dilution, in 96 well culture plates, cultivate 72-96h, slightly concussion, 490nm place carries out photoelectric colorimetry.
Table 1
Figure BDA0000444681280000101
2.3 conclusion
Referring to table 1, through external susceptibility MIC test, can find out: the present invention all has stronger antibacterial action to fungus, Candida albicans, staphylococcus aureus, Escherichia coli.
More than test shows: the present invention has antibacterial action, the interpolation of alternative antiseptic.
In the various embodiments described above of the present invention, the sequence number of embodiment is only convenient to describe, and does not represent the quality of embodiment.Description to each embodiment all emphasizes particularly on different fields, and there is no the part of detailed description in certain embodiment, can be referring to the associated description of other embodiment.
In the embodiment such as apparatus and method of the present invention, obviously, each parts or each step reconfigure after can decomposing, combine and/or decomposing.These decomposition and/or reconfigure and should be considered as equivalents of the present invention.Simultaneously, in the above in the description of the specific embodiment of the invention, the feature of describing and/or illustrating for a kind of embodiment can be used in same or similar mode in one or more other embodiment, combined with the feature in other embodiment, or substitute the feature in other embodiment.
Should emphasize, term " comprises/comprises " existence that refers to feature, key element, step or assembly while using herein, but does not get rid of the existence of one or more further feature, key element, step or assembly or add.
Finally it should be noted that: although described above the present invention and advantage thereof in detail, be to be understood that in the situation that do not exceed the spirit and scope of the present invention that limited by appended claim and can carry out various changes, alternative and conversion.And scope of the present invention is not limited only to the specific embodiment of the described process of description, equipment, means, method and step.One of ordinary skilled in the art will readily appreciate that from disclosure of the present invention, can use carry out with the essentially identical function of corresponding embodiment described herein or obtain process, equipment, means, method or step result essentially identical with it, that existing and will be developed future according to the present invention.Therefore, appended claim is intended to comprise such process, equipment, means, method or step in their scope.

Claims (10)

1. for a compositions for the baby bath agent that contains marine bioactivity material, it is characterized in that, comprise the component of following weight percentage:
Figure FDA0000444681270000011
2. the compositions for the baby bath agent that contains marine bioactivity material according to claim 1, is characterized in that, comprises the component of following weight percentage:
3. the compositions for the baby bath agent that contains marine bioactivity material according to claim 1, is characterized in that, comprises the component of following weight percentage:
Figure FDA0000444681270000013
Figure FDA0000444681270000021
4. according to the compositions for the baby bath agent that contains marine bioactivity material described in claim 1-3 any one, it is characterized in that, described marine organisms bacteria remover by weight percent meter proportioning is as follows:
Figure FDA0000444681270000022
5. a method for the baby bath agent that the compositions preparation described in right to use requirement 1-4 any one contains marine bioactivity material, is characterized in that, comprises the following steps:
Step S10: to the alkyl polyglucoside, cocamido propyl betaine and the alcohol ether carboxylate that add proportional quantity in pure water, stir, carry out emulsifying, obtain mixed liquor A;
Step S20: marine organisms bacteria remover, Sargassum polysaccharides and chitin to adding proportional quantity in mixed liquor A, be uniformly mixed, obtain mixed liquid B;
Step S30: sodium chloride, citric acid and edible essence to adding proportional quantity in mixed liquid B, be uniformly mixed, obtain the baby bath agent that contains marine bioactivity material.
6. method according to claim 5, is characterized in that, described marine organisms bacteria remover is prepared as follows:
Step S101: carboxymethyl chitosan and Sargassum polysaccharides to adding proportional quantity in the water of 30~35 ℃, stir and within 10~20 minutes, obtain the first mixed liquor;
Step S102: the cecropin toward adding proportional quantity in the first mixed liquor, stirs and within 3~7 minutes, obtains the second mixed liquor;
Step S103: the N-acetylmuramide lycanohydrlase toward adding proportional quantity in the second mixed liquor, stirs and within 3~7 minutes, obtains described degerming marine organisms bacteria remover.
7. according to the method described in claim 5 or 6, it is characterized in that, in described step S10: the temperature of described pure water is 40-50 ℃, the time of stirring is 30-40 minute, and the speed of stirring is 80-90 rev/min.
8. according to the method described in claim 5 or 6, it is characterized in that, in described step S20: the temperature of stirring is 25-35 ℃, the time of stirring is 15-20 minute, and the speed of stirring is 70-80 rev/min; Or/and; In described step S30: the time of stirring is 10-15 minute, the speed of stirring is 70-80 rev/min.
9. according to the method described in claim 5 or 6, it is characterized in that, after step S30, also comprise step S40: after the baby bath agent that contains marine bioactivity material is cooling, carry out subpackage.
10. a baby bath agent that contains marine bioactivity material of preparing according to the method described in claim 5-9 any one.
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106176380A (en) * 2016-08-11 2016-12-07 王君 A kind of enzyme natural ecological bath lotion
CN111743817A (en) * 2020-08-20 2020-10-09 广州荃智美肤生物科技研究院有限公司 Children washing and protecting composition containing algal polysaccharide

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103027857A (en) * 2012-12-25 2013-04-10 青岛海芬海洋生物科技有限公司 Shampoo containing marine biological degerming components and preparation method of shampoo

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103027857A (en) * 2012-12-25 2013-04-10 青岛海芬海洋生物科技有限公司 Shampoo containing marine biological degerming components and preparation method of shampoo

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106176380A (en) * 2016-08-11 2016-12-07 王君 A kind of enzyme natural ecological bath lotion
CN111743817A (en) * 2020-08-20 2020-10-09 广州荃智美肤生物科技研究院有限公司 Children washing and protecting composition containing algal polysaccharide

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