CN103642607B - Sterilization and disinfection laundry detergent - Google Patents
Sterilization and disinfection laundry detergent Download PDFInfo
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- CN103642607B CN103642607B CN201310613125.7A CN201310613125A CN103642607B CN 103642607 B CN103642607 B CN 103642607B CN 201310613125 A CN201310613125 A CN 201310613125A CN 103642607 B CN103642607 B CN 103642607B
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Abstract
The invention belongs to the technical field of laundry detergents, and discloses a sterilization and disinfection laundry detergent which is prepared from the following components in percentage by weight: 1-40% of anionic surfactant, 1-30% of nonionic surfactant, 0-10% of ampholytic surfactant, 0-1% of cationic surfactant, 0-1% of high-molecular thickener, 0-5% of electrolyte, 0.1-10% of bamboo leaf/mulberry leaf extract, 0.1-0.3% of essence, 0.01-0.2% of Kathon and the balance of water. In the sterilization and disinfection laundry detergent provided by the invention, the extract of bamboo leaves and mulberry leaves is used as the sterilization and disinfection liquid, the formula is reasonable without irrigation, and the decontamination effect is remarkable; the sterilization and disinfection laundry detergent has good sterilization and disinfection functions and is safe, environment-friendly and pollution-free.
Description
Technical field
The invention belongs to washing liquid technical field, relate to a kind of sterilization and disinfection washing liquid, be specifically related to a kind of sterilization and disinfection washing liquid containing plant milk extract.
Background technology
At present, the washing liquid on the market particularly washing liquid of disinfection is with the addition of chemostefilant as sterilant mostly, and these disinfectants have strong impulse to human body skin, easily remain on clothes, cause certain injury to human body.Advocate today of natural green environmental protection, people more and more wish to adopt natural sterilant to replace chemicals.
Summary of the invention
The object of the present invention is to provide a kind of take plant milk extract as the washing liquid of sterilant, and natural green, sterilizing power are strong.
The technical solution used in the present invention is as follows:
A kind of sterilization and disinfection washing liquid, is prepared from by the component of following weight per-cent:
Preferably, sterilization and disinfection washing liquid of the present invention is prepared from by the component of following weight per-cent:
The preparation method one of described leaf of bamboo Folium Mori extract is as follows:
Get the leaf of bamboo respectively, mulberry leaf are raw material, after drying is pulverized, under the condition of 25 ~ 100 DEG C, the mass volume ratio of the leaf of bamboo, mulberry leaf and water is 1:20 ~ 1:50, leaches 2 ~ 4 times, each 2 ~ 3 hours, merges leaching liquid; Chloroform extraction, the volume ratio of chloroform and leaching liquid is 1.5 ~ 4:1, and take out chloroform layer and concentrate, obtain the extract of the leaf of bamboo, mulberry leaf respectively, Folium Bambosae extract and Folium Mori extract mix according to mass ratio 1:1.
Or described mulberry leaf, Folium Bambosae extract preparation method two as follows:
Get the leaf of bamboo respectively, mulberry leaf are raw material, after drying is pulverized, under the condition of 20 ~ 80 DEG C, the mass volume ratio of the leaf of bamboo, mulberry leaf and concentration >=95% ethanol is 1:20 ~ 1:50, reflux 2 ~ 4 times, each 2 ~ 3 hours, merging filtrate, be concentrated into without alcohol taste, chloroform extraction, the volume ratio of chloroform and leaching liquid is 1.5 ~ 4:1, takes out chloroform layer and concentrates, obtain the leaf of bamboo, Folium Mori extract respectively, Folium Bambosae extract and Folium Mori extract mix according to mass ratio 1:1.
Described anion surfactant is one or more mixtures in fatty alcohol polyoxyethylene ether sulfate, aliphatic alcohol sulfate, alkylbenzene sulfonate.Preferred fat polyoxyethylenated alcohol sodium sulfate, sodium lauryl sulphate, Sodium dodecylbenzene sulfonate.
Described nonionogenic tenside is one or more mixtures in fatty alcohol-polyoxyethylene ether, fatty diglycollic amide or APG.Preferred fat polyoxyethylenated alcohol-3 (AEO-3), fatty alcohol-polyoxyethylene ether-7 (AEO-7), fatty alcohol-polyoxyethylene ether-9 (AEO-9), APG, lauric acid amide of ethanol.
Described amphoterics is one or more mixtures in betaines tensio-active agent, imidazolines tensio-active agent.Preferred AMONYL 380LC, cocamidopropyl propyl amide hydroxy sulfo lycine, cocamidopropyl propyl amide amine oxide, coco imidoazolinium.
Described cats product is monoalkyl quaternary ammonium salts or dialkyl quaternary ammonium salt.Preferred mountain Yu base trimethyl ammonium chloride, octadecyl trimethyl ammonium chloride, palmityl trimethyl ammonium chloride, distearyl dimethyl ammonium chloride, two mountains Yu base trimethyl ammonium chloride.
Described macromolecule thickener is one or more mixtures in cellulose thickener, guar gum and derivative thereof.Preferred cationic Natvosol, Natvosol, guar hydroxypropyltrimonium ammonium chloride.
Described ionogen is sodium-chlor, Repone K, sodium acetate, sodium sulfate or potassium sulfate.
Beneficial effect of the present invention:
The leaf of bamboo and mulberry leaf are leaves of common green plants, flavones etc. in the leaf of bamboo and mulberry leaf has certain germicidal action, adopt the leaf of bamboo, Folium Mori extract as the sterilant of washing liquid, there is good germicidal action, to streptococcus aureus and intestinal bacteria etc., there is certain lethality especially; The present invention fills a prescription rationally, does not have pungency, and clean effect is remarkable, and have good sterilization and sterilizing function, safety and environmental protection is pollution-free.
Embodiment
Below in conjunction with embodiment, further detailed description is done to the present invention, but embodiments of the present invention are not limited thereto.
Embodiment 1:
A kind of sterilization and disinfection washing liquid, is prepared from by the component of following weight per-cent:
In the present embodiment, the preparation method of described leaf of bamboo Folium Mori extract is as follows: get the leaf of bamboo respectively, mulberry leaf are raw material, after drying is pulverized, under the condition of 25 DEG C, the mass volume ratio of the leaf of bamboo, mulberry leaf and water is: 1:20, leaches 3 times, each 2 hours, merge leaching liquid; Chloroform extraction, the volume ratio of chloroform and leaching liquid is 1.5:1, and take out chloroform layer and concentrate, obtain the extract of the leaf of bamboo, mulberry leaf respectively, Folium Bambosae extract and Folium Mori extract mix according to mass ratio 1:1.
Polyoxyethylenated alcohol sodium sulfate is anion surfactant, fatty alcohol-polyoxyethylene ether-7 and fatty alcohol-polyoxyethylene ether-9 are nonionogenic tenside, AMONYL 380LC is amphoterics, palmityl trimethyl ammonium chloride is cats product, cationic hydroxyethyl cellulose is macromolecule thickener, and Repone K is ionogen.
Embodiment 2:
A kind of sterilization and disinfection washing liquid, is prepared from by the component of following weight per-cent:
In the present embodiment, the preparation method of described leaf of bamboo Folium Mori extract is with embodiment 1.
Polyoxyethylenated alcohol sodium sulfate is anion surfactant, fatty alcohol-polyoxyethylene ether-7 and fatty alcohol-polyoxyethylene ether-9 are nonionogenic tenside, octadecyl trimethyl ammonium chloride is cats product, hydroxypropylguar gum trimethyl ammonium chloride is macromolecule thickener, and sodium-chlor is ionogen.
Embodiment 3:
A kind of sterilization and disinfection washing liquid, is prepared from by the component of following weight per-cent:
In the present embodiment, described mulberry leaf, the preparation method of Folium Bambosae extract are as follows: get the leaf of bamboo respectively, mulberry leaf are raw material, after drying is pulverized, under the condition of 80 DEG C, the mass volume ratio of the leaf of bamboo, mulberry leaf and 95% ethanol is 1:20, reflux 2 times, each 3 hours, merging filtrate, is concentrated into without alcohol taste, chloroform extraction, the volume ratio of chloroform and leaching liquid is 4:1, taking-up chloroform layer concentrates, and obtain the leaf of bamboo, Folium Mori extract respectively, Folium Bambosae extract and Folium Mori extract mix according to mass ratio 1:1.
Polyoxyethylenated alcohol sodium sulfate is anion surfactant, fatty alcohol-polyoxyethylene ether-7, fatty alcohol-polyoxyethylene ether-9 and lauric acid amide of ethanol are nonionogenic tenside, mountain Yu base trimethyl ammonium chloride is cats product, Natvosol is macromolecule thickener, and sodium-chlor is ionogen.
Embodiment 4:
A kind of sterilization and disinfection washing liquid, is prepared from by the component of following weight per-cent:
In the present embodiment, the preparation method of described leaf of bamboo Folium Mori extract is with embodiment 3.
Polyoxyethylenated alcohol sodium sulfate, Sodium dodecylbenzene sulfonate are anion surfactant, APG is nonionogenic tenside, coco imidoazolinium, cocamidopropyl propyl amide amine oxide are amphoterics, two mountains Yu base trimethyl ammonium chloride is cats product, Natvosol is macromolecule thickener, and sodium-chlor is ionogen.
Embodiment 5:
A kind of sterilization and disinfection washing liquid, is prepared from by the component of following weight per-cent:
In the present embodiment, the preparation method of described leaf of bamboo Folium Mori extract is as follows: get the leaf of bamboo respectively, mulberry leaf are raw material, after drying is pulverized, under the condition of 75 DEG C, the mass volume ratio of the leaf of bamboo, mulberry leaf and water is: 1:35, leaches 4 times, each 2 hours, merge leaching liquid; Chloroform extraction, the volume ratio of chloroform and leaching liquid is 2.5:1, and take out chloroform layer and concentrate, obtain the extract of the leaf of bamboo, mulberry leaf respectively, Folium Bambosae extract and Folium Mori extract mix according to mass ratio 1:1.
Sodium alkyl sulfate is anion surfactant, fatty alcohol-polyoxyethylene ether-7, fatty alcohol-polyoxyethylene ether-9 are nonionogenic tenside, AMONYL 380LC is amphoterics, palmityl trimethyl ammonium chloride is cats product, cationic hydroxyethyl cellulose is macromolecule thickener, and sodium sulfate is ionogen.
Embodiment 6:
A kind of sterilization and disinfection washing liquid, is prepared from by the component of following weight per-cent:
In the present embodiment, the preparation method of described leaf of bamboo Folium Mori extract is with embodiment 5.
Polyoxyethylenated alcohol sodium sulfate is anion surfactant, and fatty alcohol-polyoxyethylene ether-7, fatty alcohol-polyoxyethylene ether-9 are nonionogenic tenside, and Repone K is ionogen.
Embodiment 7:
A kind of sterilization and disinfection washing liquid, is prepared from by the component of following weight per-cent:
In the present embodiment, described mulberry leaf, the preparation method of Folium Bambosae extract are as follows: get the leaf of bamboo respectively, mulberry leaf are raw material, after drying is pulverized, under the condition of 80 DEG C, the mass volume ratio of the leaf of bamboo, mulberry leaf and 95% ethanol is 1:30, reflux 3 times, each 3 hours, merging filtrate, is concentrated into without alcohol taste, chloroform extraction, the volume ratio of chloroform and leaching liquid is 3:1, taking-up chloroform layer concentrates, and obtains the extract of the leaf of bamboo, mulberry leaf respectively, and Folium Bambosae extract and Folium Mori extract mix according to mass ratio 1:1.
Sodium alkyl sulfate is anion surfactant, fatty alcohol-polyoxyethylene ether-7, fatty alcohol-polyoxyethylene ether-9 are nonionogenic tenside, AMONYL 380LC is amphoterics, distearyl dimethyl ammonium chloride is cats product, and cationic hydroxyethyl cellulose is macromolecule thickener.
Embodiment 8:
A kind of sterilization and disinfection washing liquid, is prepared from by the component of following weight per-cent:
In the present embodiment, the preparation method of described leaf of bamboo Folium Mori extract is with embodiment 7.
Sodium alkyl sulfate is anion surfactant, fatty alcohol-polyoxyethylene ether-7, fatty alcohol-polyoxyethylene ether-9 are nonionogenic tenside, AMONYL 380LC is amphoterics, two mountains Yu base trimethyl ammonium chloride is cats product, cationic hydroxyethyl cellulose is macromolecule thickener, and Repone K is ionogen.
The sterilization and disinfection washing liquid obtained to embodiment 1-8 carries out the test of study on the stability, detergency test and sterilizing ability.
Study on the stability: the sterilization and disinfection washing liquid sample of Example 1-8, be placed in 40 DEG C ± 2 DEG C constant temperature 24 hours, then be put in-5 DEG C ± 2 DEG C constant temperature 24 hours, 40 DEG C ± 2 DEG C and-5 DEG C ± 2 DEG C circulation placements 7 times, observe all not stratified of embodiment 1-8, produce without precipitation.
Detergency test:
The detergency test of sterilization and disinfection washing liquid sample carries out with reference to GB/T13174-2008.Experimental result shows that embodiment 1-8 all samples to the detersive power of carbon ink water soiled cotton, albumen soiled cotton, sebum soiled cotton, edible oil soiled cotton and starch based soiled cotton all >=1.0.
Sterilizing ability is tested:
1), collecting cells experimental bacteria streptococcus aureus, intestinal bacteria, Pseudomonas aeruginosa, Candida albicans are provided by Biological Engineering College of Southern Yangtze University.Various bacterium is carried out Zengjing Granule, the single bacterium colony of separation and Culture, get type species and be inoculated in nutrient agar inclined-plane, cultivate 24 hours, fresh slant culture Tryptones physiological saline is washed down, mixes dilution and be prepared into bacteria suspension.
2), neutralizing agent qualification test test organisms streptococcus aureus and Candida albicans, test points 6 groups, carries out neutralizing agent qualification test by bacteria suspension quantitative bacteric idal experiment program.Experimental result, when the 6th group of not long bacterium, the 3rd, 4,5 group of growth bacterium amount is 1 × 10
7-5 × 10
7(take Candida albicans as test organisms, bacterium amount controls 1 × 10 cfu/ml
6-5 × 10
6cfu/ml) bacterium number specific inaccuracy is no more than 15% between and between 3 groups of groups, and the 2nd group of growth bacterium number, more than 100cfu/ml, when the 1st group of not long bacterium or bacterium number are much smaller than the 2nd group, shows that neutralizing agent used and working concentration thereof are suitable for.Test repetition 3 times.Determine that neutralizing agent is the PBS solution of Sulfothiorine of 3g/L Yelkin TTS, 3g/L tween 80,5g/L.
3), quantitative bacteric idal experiment is with reference to GB15982-2002, 5mL washing liquid sample is added in 0.1mL experimental bacteria suspension, mixing, act on 2 respectively, 5, 10, drawing 0.5mL with suction pipe after 20min drops into containing the corresponding neutralizing agent of 4.5mL in vitro, draw 0.5mL respectively, be placed in two plates, pour into the nutrient agars of 40 ~ 50 DEG C (bacterium) or sabouraud's agar (yeast) 15mL, rotate plate, make it full and uniform, after agar solidification, upset is dull and stereotyped, cultivate 48 hours (bacteriums) or 72 hours (yeast) for 35 ± 2 DEG C, do viable bacteria enumeration.Test repetition 3 times, calculate sterilizing rate: X3=(A-B)/B × 100%, wherein A is control sample average colony number, and B is specimen sample average colony number.Test-results shows that the sterilization and disinfection washing liquid of embodiment 1-8 to the sterilizing rate of streptococcus aureus, intestinal bacteria, Pseudomonas aeruginosa and Candida albicans all >=90%.
Claims (3)
1. a sterilization and disinfection washing liquid, is characterized in that being prepared from by the component of following weight per-cent:
Described anion surfactant is one or more mixtures in fatty alcohol polyoxyethylene ether sulfate, aliphatic alcohol sulfate, alkylbenzene sulfonate;
Described nonionogenic tenside is one or more mixtures in fatty alcohol-polyoxyethylene ether, fatty diglycollic amide or APG;
Described amphoterics is one or more mixtures in betaines tensio-active agent, imidazolines tensio-active agent;
Described cats product is monoalkyl quaternary ammonium salts or dialkyl quaternary ammonium salt;
Described macromolecule thickener is one or more mixtures in cellulose thickener, guar gum and derivative thereof;
Described ionogen is sodium-chlor, Repone K, sodium acetate, sodium sulfate or potassium sulfate.
2. sterilization and disinfection washing liquid according to claim 1, is characterized in that being prepared from by the component of following weight per-cent:
3. a kind of sterilization and disinfection washing liquid according to claim 1 and 2, is characterized in that described leaf of bamboo Folium Mori extract is prepared by following method:
Get the leaf of bamboo respectively, mulberry leaf are raw material, after drying is pulverized, under the condition of 25 ~ 100 DEG C, the mass volume ratio of the leaf of bamboo, mulberry leaf and water is: 1:20 ~ 1:50, leaches 2 ~ 4 times, each 2 ~ 3 hours, merges leaching liquid; Chloroform extraction, the volume ratio of chloroform and leaching liquid is 1.5 ~ 4:1, and take out chloroform layer and concentrate, obtain the extract of the leaf of bamboo, mulberry leaf respectively, Folium Bambosae extract and Folium Mori extract mix according to mass ratio 1:1;
Or get the leaf of bamboo respectively, mulberry leaf are raw material, drying pulverize after, under the condition of 20 ~ 80 DEG C, the mass volume ratio of the leaf of bamboo, mulberry leaf and concentration >=95% ethanol is 1:20 ~ 1:50, reflux 2 ~ 4 times, each 2 ~ 3 hours, merging filtrate, be concentrated into without alcohol taste, chloroform extraction, the volume ratio of chloroform and leaching liquid is 1.5 ~ 4:1, takes out chloroform layer and concentrates, obtain the leaf of bamboo, Folium Mori extract respectively, Folium Bambosae extract and Folium Mori extract mix according to mass ratio 1:1.
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| CN201310613125.7A CN103642607B (en) | 2013-11-26 | 2013-11-26 | Sterilization and disinfection laundry detergent |
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| CN201310613125.7A CN103642607B (en) | 2013-11-26 | 2013-11-26 | Sterilization and disinfection laundry detergent |
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| CN104365663A (en) * | 2014-11-19 | 2015-02-25 | 苏州佑君环境科技有限公司 | Easily-biodegradable disinfectant and preparation method thereof |
| CN104532626A (en) * | 2014-12-17 | 2015-04-22 | 黄涛 | Pure natural antifading agent |
| CN105112174B (en) * | 2015-09-10 | 2018-01-23 | 辽宁石化职业技术学院 | A kind of fungus and mildew resistance liquid detergent |
| CN105400608A (en) * | 2015-11-27 | 2016-03-16 | 北京市创新精细化工有限责任公司 | Antibacterial laundry detergent |
| CN105543003B (en) * | 2015-12-31 | 2018-02-09 | 广东鹏锦实业有限公司 | Antibacterial softener |
| CN107236627A (en) * | 2017-06-05 | 2017-10-10 | 丁惠良 | Mosquito proof liquid detergent |
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| CN107619723A (en) * | 2017-09-20 | 2018-01-23 | 北京军秀咨询有限公司 | A kind of sterilizing liquid detergent |
| JP2019081891A (en) * | 2017-10-30 | 2019-05-30 | 花王株式会社 | Sterilizing detergent composition |
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| CN111925874A (en) * | 2020-09-10 | 2020-11-13 | 巢湖市圣洁洗涤服务有限公司 | Cleaning solution for sterilizing and disinfecting hotel bed sheet and quilt cover and preparation method thereof |
| CN116731552A (en) * | 2023-07-28 | 2023-09-12 | 中山市富日印刷材料有限公司 | Improved water-based ink cleaning agent and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1294908A (en) * | 2000-09-30 | 2001-05-16 | 李凤友 | Mulberry leaf shampoo and its preparation |
| CN1667110A (en) * | 2004-03-09 | 2005-09-14 | 王旭 | Plant type environmental protection washing powder |
| CN101879133A (en) * | 2009-05-05 | 2010-11-10 | 刘敦友 | Shampoo with functions of treating alopecia and leukotrichia, removing dandruff and relieving itch |
| CN101606896A (en) * | 2009-07-02 | 2009-12-23 | 烟台新时代健康产业日化有限公司 | New use of bamboo leaf extract, its preparation method, skin-care bath composition containing the same and its preparation method |
| CN103301056B (en) * | 2013-06-21 | 2016-04-20 | 李洋 | A kind of pure natural plant Anti-hair loss hair washing medicinal liquid and preparation method thereof |
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