CN103027857B - Shampoo containing marine biological degerming components and preparation method of shampoo - Google Patents
Shampoo containing marine biological degerming components and preparation method of shampoo Download PDFInfo
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- CN103027857B CN103027857B CN201210575389.3A CN201210575389A CN103027857B CN 103027857 B CN103027857 B CN 103027857B CN 201210575389 A CN201210575389 A CN 201210575389A CN 103027857 B CN103027857 B CN 103027857B
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Abstract
The invention discloses a shampoo containing marine biological degerming components and a preparation method of the shampoo. The shampoo comprises the following components by weight percent: 2.0-4.0% of marine biological degerming agent, 8.0-14.0% of alkyl glycoside, 7.0-10% of cocamidopropyl betaine, 6.0-10.0% of coco fatty acid diethanol amide, 0.5-2.0% of alkyl dimethyl polysiloxane, 1.0-1.5% of sodium chloride, 1.0-1.5% of sodium citrate, 0-5.0% of essence, and the balance of water. The shampoo containing the marine biological degerming components has itch relieving and dandruff removal functions and further has the advantages that the shampoo has no stimulation and corrosion to hairs.
Description
Technical field
The present invention relates to shampoo, relate in particular to a kind of shampoo that contains marine organisms degerming composition and preparation method thereof.
Background technology
Common scalp is uncomfortable, is mainly the dandruff and head pruritus, and the major reason that causes the dandruff is fungal infection, different according to the kind of individual variation and bacterial infection, is divided into:
1, seborrheic dermatitis: seborrheic dermatitis is to cause the topmost reason of the dandruff.Usually appear in Adult Groups, show as on scalp and have thicker oiliness secretions or hair to be dried.
2, tinea capitis: general thicker and tighter being attached on scalp, surface coverage silvery white squama, normal journey speckle shape distributes.
3, chronic eczema: have the germ infection of scalp and hair to cause, show as the destruction of dandruff and hair.Can be with inflammatory reaction when serious.
4, atoipc dermatitis: show as the dry bits of scalp diffusivity.
At present, existing shampoo kind is a lot, functional shampoo is mainly dandruff control shampoo containing and generating and nourishing hair class shampoo, main adding ingredient is: pyridine copper sulfate or other antifungal drugs (having ketoconazole, climbazole, selenium sulfide etc.) and Chinese medicine preparation, antimycotic medicine life-time service can produce drug resistance, and production cost is high.Chinese medicine preparation complex manufacturing, and sterilization, fungistatic effect are weak type.
Summary of the invention
An object of the present invention is to provide a kind of antipruritic and shampoo that contains marine organisms degerming composition anti-dandruff function that has.
Another object of the present invention is to provide a kind of preparation method with the shampoo that contains marine organisms degerming composition of antipruritic and anti-dandruff function.
The shampoo that contains marine organisms degerming composition of the present invention, percent meter proportioning is as follows by weight:
Marine organisms bacteria remover 2.0-4.0%;
Alkyl polyglucoside 8.0-14.0%;
Cocamido propyl betaine 7.0-10.0%;
Cocoanut fatty acid diethanolamide 6.0-10.0%;
Alkyl-dimethyl based polysiloxane 0.5-2.0%;
Sodium chloride 1.0-1.5%;
Sodium citrate 1.0-1.5%;
Essence 0-5.0%;
Surplus is water.
The preparation method of the shampoo that contains marine organisms degerming composition of the present invention, comprises the following steps:
Step S10: alkyl polyglucoside, cocamido propyl betaine, cocoanut fatty acid diethanolamide, alkyl-dimethyl based polysiloxane to adding proportional quantity in the water of 35-40 ℃, carry out emulsifying and obtain mixed liquor A under stirring condition;
Step S20: the marine organisms bacteria remover to adding proportional quantity in mixed liquor A is uniformly mixed to obtain institute's mixed liquid B under 25-35 ℃ of temperature conditions;
Step S30: to the sodium citrate, sodium chloride and the essence that add proportional quantity in mixed liquid B, the shampoo that contains marine organisms degerming composition described in mix homogeneously obtains.
The shampoo that contains marine organisms degerming composition of the present invention, owing to containing marine organisms bacteria remover composition, therefore, after use, effectively degerming, and then there is antipruritic and effect anti-dandruff, and because each component of this shampoo that contains marine organisms degerming composition is nontoxic, non-stimulated, the free from corrosion material of skin, so this shampoo also has non-stimulated, the free from corrosion advantage of hair and hair.
The preparation method of the shampoo that contains marine organisms degerming composition of the present invention, because order by merging and the mixing condition of each material are comparatively reasonable, make each component mix homogeneously of the shampoo that contains marine organisms degerming composition making by preparation method of the present invention, good stability.
The specific embodiment
Embodiment 1
The shampoo that contains marine organisms degerming composition of the present embodiment, percent meter proportioning is as follows by weight: marine organisms bacteria remover 2.0-4.0%;
Alkyl polyglucoside 8.0-14.0%;
Cocamido propyl betaine 7.0-10.0%;
Cocoanut fatty acid diethanolamide 6.0-10.0%;
Alkyl-dimethyl based polysiloxane 0.5-2.0%;
Sodium chloride 1.0-1.5%;
Sodium citrate 1.0-1.5%;
Essence 0-5.0%;
Surplus is water.
The shampoo that contains marine organisms degerming composition of the present embodiment, owing to containing marine organisms bacteria remover composition, therefore, after use, effectively degerming, and then there is antipruritic and effect anti-dandruff, and because each component of this shampoo that contains marine organisms degerming composition is nontoxic, non-stimulated, the free from corrosion material of skin, so this shampoo also has non-stimulated, the free from corrosion advantage of hair and hair.
In the present embodiment, in order to obtain better antipruritic and anti-dandruff effect, the described shampoo that contains marine organisms degerming composition, percent meter proportioning is as follows by weight:
Marine organisms bacteria remover 2.5-3.5%;
Alkyl polyglucoside 9.0-13.0%;
Cocamido propyl betaine 8.0-9.0%;
Cocoanut fatty acid diethanolamide 7.0-9.0%;
Alkyl-dimethyl based polysiloxane 1.0-1.5%;
Sodium chloride 1.1-1.4%;
Sodium citrate 1.1-1.4%;
Essence 0.5-2.0%;
Surplus is water.
In the present embodiment, in order to obtain better antipruritic and anti-dandruff effect, preferred, described marine organisms bacteria remover by weight percent meter proportioning is as follows:
Carboxymethyl chitosan 1.0 ~ 2.0%;
Sargassum polysaccharides 2.0 ~ 4.0%;
Cecropin 6.0 ~ 8.0%;
N-acetylmuramide lycanohydrlase 1.5 ~ 3.5%;
Water 82.5 ~ 89.5%.
In the present embodiment, preferred, described essence is plant essence.
In the present embodiment, in order to make the mixed effect of each component better, described hydromining pure water.
It is the cecropin described in CN101104637B that described cecropin can adopt notification number, can certainly adopt other cecropin.
Described marine organisms bacteria remover can be prepared as follows:
Step S10: to the carboxymethyl chitosan and the Sargassum polysaccharides that add proportional quantity in the water of 30 ~ 35 ℃, be uniformly mixed 10 ~ 20 minutes mixed liquor A;
Step S20: toward the cecropin that adds proportional quantity in mixed liquor A, the time being uniformly mixed be 3 ~ 7 minutes mixed liquid B;
Step S30: toward the N-acetylmuramide lycanohydrlase that adds proportional quantity in mixed liquid B, be uniformly mixed 3 ~ 7 minutes described degerming marine organisms bacteria remover.
Embodiment 2
The present embodiment provides a kind of preparation method for the shampoo that contains marine organisms degerming composition described in embodiment 1, comprises the following steps:
Step S10: alkyl polyglucoside, cocamido propyl betaine, cocoanut fatty acid diethanolamide, alkyl-dimethyl based polysiloxane to adding proportional quantity in the water of 35-40 ℃, carry out emulsifying and obtain mixed liquor A under stirring condition;
Step S20: the marine organisms bacteria remover to adding proportional quantity in mixed liquor A is uniformly mixed to obtain institute's mixed liquid B under 25-35 ℃ of temperature conditions;
Step S30: to the sodium citrate, sodium chloride and the essence that add proportional quantity in mixed liquid B, the shampoo that contains marine organisms degerming composition described in mix homogeneously obtains.
The preparation method of the shampoo that contains marine organisms degerming composition of the present embodiment, because order by merging and the mixing condition of each material are comparatively reasonable, make each component mix homogeneously of the shampoo that contains marine organisms degerming composition making by preparation method of the present invention, good stability.
In the present embodiment, in order to make each component obtain better mixed effect, in described step S10, the temperature of described water is 40 ℃, and under stirring condition, carrying out emulsification times is 15-25 minute.
In the present embodiment, in order to make each component obtain better mixed effect, in described step S20, the time being uniformly mixed is 3-7 minute.
In the present embodiment, in order to make each component obtain better mixed effect, in described step S30, the time being uniformly mixed is 7-12 minute.
In the present embodiment, in order to obtain portable shampoo, after step S30, also comprise step S40: after the shampoo that contains marine organisms degerming composition is cooling, carry out subpackage.
Embodiment 3
The present embodiment provides a kind of shampoo that contains marine organisms degerming composition, and percent meter proportioning is as follows by weight:
Marine organisms bacteria remover 4.0%;
Alkyl polyglucoside 14.0%;
Cocamido propyl betaine 10.0%;
Cocoanut fatty acid diethanolamide 10.0%;
Alkyl-dimethyl based polysiloxane 2.0%;
Sodium chloride 1.5%;
Sodium citrate 1.5%;
Essence 5.0%;
Surplus is water.
Marine organisms bacteria remover in the present embodiment by weight percent meter proportioning is: carboxymethyl chitosan 1.0%; Sargassum polysaccharides 2.0%; Cecropin 6.0%; N-acetylmuramide lycanohydrlase 1.5%; Water 89.5%.
The preparation method of the shampoo that contains marine organisms degerming composition of the present embodiment is carried out as follows:
Step S301: to the alkyl polyglucoside, cocamido propyl betaine, cocoanut fatty acid diethanolamide, the alkyl-dimethyl based polysiloxane that add proportional quantity in the water of 35 ℃, under stirring condition, carry out emulsifying 15 minutes mixed liquor A;
Step S302: to the marine organisms bacteria remover that adds proportional quantity in mixed liquor A, under 25 ℃ of temperature conditions, be uniformly mixed 3 minutes institute's mixed liquid B;
Step S303: to the sodium citrate, sodium chloride and the essence that add proportional quantity in mixed liquid B, mix 7 minutes described in contain marine organisms degerming composition shampoo.
Through experiment, the shampoo that contains marine organisms degerming composition of the present embodiment can be effectively antipruritic, anti-dandruff, and after using, non-stimulated, corrosion-free to head, hair is submissiveer.
Embodiment 4
The present embodiment provides a kind of shampoo that contains marine organisms degerming composition, and percent meter proportioning is as follows by weight: marine organisms bacteria remover 2.0%;
Alkyl polyglucoside 8.0%;
Cocamido propyl betaine 7.0%;
Cocoanut fatty acid diethanolamide 6.0%;
Alkyl-dimethyl based polysiloxane 0.5%;
Sodium chloride 1.0%;
Sodium citrate 1.0%;
Surplus is water.
Marine organisms bacteria remover in the present embodiment by weight percent meter proportioning is: carboxymethyl chitosan 2.0%; Sargassum polysaccharides 4.0%; Cecropin 8.0%; N-acetylmuramide lycanohydrlase 3.5%; Water 82.5%.
The preparation method of the shampoo that contains marine organisms degerming composition of the present embodiment is carried out as follows:
Step S401: to the alkyl polyglucoside, cocamido propyl betaine, cocoanut fatty acid diethanolamide, the alkyl-dimethyl based polysiloxane that add proportional quantity in the water of 35 ℃, under stirring condition, carry out emulsifying 25 minutes mixed liquor A;
Step S402: to the marine organisms bacteria remover that adds proportional quantity in mixed liquor A, under 25 ℃ of temperature conditions, be uniformly mixed 7 minutes institute's mixed liquid B;
Step S403: to the sodium citrate, sodium chloride and the essence that add proportional quantity in mixed liquid B, mix 12 minutes described in contain marine organisms degerming composition shampoo.
Step S404: after the shampoo that contains marine organisms degerming composition is cooling, carry out subpackage.
Through experiment, the shampoo that contains marine organisms degerming composition of the present embodiment can be effectively antipruritic, anti-dandruff, and after using, non-stimulated, corrosion-free to head, hair is submissiveer.
Embodiment 5
The present embodiment provides a kind of shampoo that contains marine organisms degerming composition, and percent meter proportioning is as follows by weight:
Marine organisms bacteria remover 3.5%;
Alkyl polyglucoside 13.0%;
Cocamido propyl betaine 9.0%;
Cocoanut fatty acid diethanolamide 9.0%;
Alkyl-dimethyl based polysiloxane 1.5%;
Sodium chloride 1.4%;
Sodium citrate 1.4%;
Essence 2.0%;
Surplus is water.
Marine organisms bacteria remover in the present embodiment by weight percent meter proportioning is: carboxymethyl chitosan 1.5%; Sargassum polysaccharides 3.0%; Cecropin 7.0%; N-acetylmuramide lycanohydrlase 2.0%; Water 86.5%.
The preparation method of the shampoo that contains marine organisms degerming composition of the present embodiment is carried out as follows:
Step S501: to the alkyl polyglucoside, cocamido propyl betaine, cocoanut fatty acid diethanolamide, the alkyl-dimethyl based polysiloxane that add proportional quantity in the water of 40 ℃, under stirring condition, carry out emulsifying 20 minutes mixed liquor A;
Step S502: to the marine organisms bacteria remover that adds proportional quantity in mixed liquor A, under 35 ℃ of temperature conditions, be uniformly mixed 5 minutes institute's mixed liquid B;
Step S503: to the sodium citrate, sodium chloride and the essence that add proportional quantity in mixed liquid B, mix 10 minutes described in contain marine organisms degerming composition shampoo.
Step S504: after the shampoo that contains marine organisms degerming composition is cooling, carry out subpackage.
Through experiment, the shampoo that contains marine organisms degerming composition of the present embodiment can be effectively antipruritic, anti-dandruff, and after using, non-stimulated, corrosion-free to head, hair is submissiveer.
Embodiment 6
The present embodiment provides a kind of shampoo that contains marine organisms degerming composition, and percent meter proportioning is as follows by weight:
Marine organisms bacteria remover 2.5%;
Alkyl polyglucoside 9.0%;
Cocamido propyl betaine 8.0%;
Cocoanut fatty acid diethanolamide 7.0%;
Alkyl-dimethyl based polysiloxane 1.0%;
Sodium chloride 1.1%;
Sodium citrate 1.1%;
Essence 0.5%;
Surplus is water.
Marine organisms bacteria remover in the present embodiment by weight percent meter proportioning is: carboxymethyl chitosan 1.5%; Sargassum polysaccharides 3.0%; Cecropin 7.0%; N-acetylmuramide lycanohydrlase 2.0%; Water 86.5%.
The preparation method of the shampoo that contains marine organisms degerming composition of the present embodiment is carried out as follows:
Step S601: to the alkyl polyglucoside, cocamido propyl betaine, cocoanut fatty acid diethanolamide, the alkyl-dimethyl based polysiloxane that add proportional quantity in the water of 38 ℃, under stirring condition, carry out emulsifying 20 minutes mixed liquor A;
Step S602: to the marine organisms bacteria remover that adds proportional quantity in mixed liquor A, under 35 ℃ of temperature conditions, be uniformly mixed 5 minutes institute's mixed liquid B;
Step S603: to the sodium citrate, sodium chloride and the essence that add proportional quantity in mixed liquid B, mix 10 minutes described in contain marine organisms degerming composition shampoo.
Step S604: after the shampoo that contains marine organisms degerming composition is cooling, carry out subpackage.
Through experiment, the shampoo that contains marine organisms degerming composition of the present embodiment can be effectively antipruritic, anti-dandruff, and after using, non-stimulated, corrosion-free to head, hair is submissiveer.
Pharmacodynamics research of the present invention:
One, from zoopery aspect checking antipruritic and antibacterial action of the present invention:
1 material
1.1 animal
Mice, regular grade, male and female half and half, body weight 18-22g, rat, male, body weight 180-220g.
1.2 medicines and reagent
Modeling reagent: depilatory cream: carrageenin: histamine phosphate; Dimethylbenzene.
Use medicine: the shampoo in the full example 5 of the invention process
Key instrument
Electronic balance, electric-heated thermostatic water bath, sufficient sole of the foot capacity measurer
2 methods and result
2.1 itching-relieving actions:
Get 20 of mices and be divided at random two groups, 10 every group, male and female half and half, are respectively matched group, test group.24h before experiment, shaves hair to each group right back instep of Cavia porcellus, smears 1 time each 5 seconds with cotton swab.Test the same day, with coarse sandpaper, abrade right back foot and shave hair place, area 1c ㎡.Smear 1 time with cotton swab part, each 5 second 1 time, at wound surface Chu Di 0.01% 0.05ml/ of histamine phosphate only after 10min, start, and after this every 3min0.02%, 0.03% ... progressive concentration is only 0.05ml/ at every turn.Until Cavia porcellus later licks the right back histamine phosphate's total amount (μ g) giving when sufficient, it is itch-threshold.Record the relatively itch-threshold of each group.Result shows: dehumidifying itching-relieving gels group itch-threshold (321 ± 350.8) μ g, and with matrix group (55 ± 47.2) μ g comparison, P < 0.01.Visible product of the present invention has the effect of pruritus due to obvious antagonism histamine phosphate.
2.2 bacteriostasis
Carry out external susceptibility MIC test:
Test strain: fungus, Candida albicans, staphylococcus aureus, Escherichia coli.
Method: each test strain is made to bacteria suspension with normal saline, and to be diluted to turbidity be the above bacteria suspension of 2.0McF, use again 100 times of normal saline dilutions, 10 times of RPMII640 dilutions, test group (shampoo in the embodiment of the present invention 5) and matched group (health king's washing liquid) doubling dilution, in 96 well culture plates, cultivate 72-96h, slightly concussion, 490nm place carries out photoelectric colorimetry.
Table 1
2.3 conclusion
Referring to table 1, the present invention has the inhibitory action (P < 0.05 or P < 0.01) of highly significant to the guinea pig skin pruritus test due to histamine phosphate; Through external susceptibility MIC test, have a look at out: the present invention all has stronger antibacterial action to fungus, Candida albicans, staphylococcus aureus, Escherichia coli.
More than test shows: the present invention has the effect of antipruritic antibacterial, therefore, above each microbial dandruff is also had to the effect of removal.
The main clinical research of the present invention:
The shampoo of getting in the embodiment of the present invention 3, embodiment 4, embodiment 5, embodiment 6 is tested, occupation mode be every two days once, duration is 16 days, the results are shown in Table 2, the visible shampoo that contains marine organisms degerming composition of the present invention has effect antipruritic, anti-dandruff, and non-stimulated, corrosion-free to scalp, after using, hair is submissive.
Table 2
Finally it should be noted that: above embodiment only, in order to technical scheme of the present invention to be described, is not intended to limit; Although the present invention is had been described in detail with reference to previous embodiment, those of ordinary skill in the art is to be understood that: its technical scheme that still can record aforementioned each embodiment is modified, or part technical characterictic is wherein equal to replacement; And these modifications or replacement do not make the essence of appropriate technical solution depart from the spirit and scope of various embodiments of the present invention technical scheme.
Claims (9)
1. a shampoo that contains marine organisms degerming composition, is characterized in that, percent meter proportioning is as follows by weight:
Wherein, percent meter proportioning is as follows by weight for described marine organisms bacteria remover:
2. the shampoo that contains marine organisms degerming composition according to claim 1, is characterized in that, percent meter proportioning is as follows by weight:
3. the shampoo that contains marine organisms degerming composition according to claim 1 and 2, is characterized in that, described essence is plant essence.
4. the shampoo that contains marine organisms degerming composition according to claim 1 and 2, is characterized in that, described water pure water.
5. a preparation method for the shampoo that contains marine organisms degerming composition as described in claim 1-4 any one, is characterized in that, comprises the following steps:
Step S10: alkyl polyglucoside, cocamido propyl betaine, cocoanut fatty acid diethanolamide, alkyl-dimethyl based polysiloxane to adding proportional quantity in the water of 35-40 ℃, carry out emulsifying and obtain mixed liquor A under stirring condition;
Step S20: the marine organisms bacteria remover to adding proportional quantity in mixed liquor A is uniformly mixed to obtain institute's mixed liquid B under 25-35 ℃ of temperature conditions;
Step S30: to the sodium citrate, sodium chloride and the essence that add proportional quantity in mixed liquid B, the shampoo that contains marine organisms degerming composition described in mix homogeneously obtains.
6. the preparation method of the shampoo that contains marine organisms degerming composition according to claim 5, is characterized in that: in described step S10, the temperature of described water is 40 ℃, and under stirring condition, carrying out emulsification times is 15-25 minute.
7. the preparation method of the shampoo that contains marine organisms degerming composition according to claim 5, is characterized in that: in described step S20, the time being uniformly mixed is 3-7 minute.
8. the preparation method of the shampoo that contains marine organisms degerming composition according to claim 5, is characterized in that: in described step S30, the time being uniformly mixed is 7-12 minute.
9. the preparation method of the shampoo that contains marine organisms degerming composition according to claim 5, is characterized in that: after step S30, also comprise step S40: after the shampoo that contains marine organisms degerming composition is cooling, carry out subpackage.
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| CN106726716A (en) * | 2016-11-12 | 2017-05-31 | 然久生物科技(上海)有限公司 | Shampoo and preparation method thereof |
| CN109771367A (en) * | 2019-03-18 | 2019-05-21 | 聂绪明 | A kind of EM bacterium shampoo and its production method |
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