CN103690400A - Natural plant type body wash and preparation method thereof - Google Patents
Natural plant type body wash and preparation method thereof Download PDFInfo
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- CN103690400A CN103690400A CN201310719007.4A CN201310719007A CN103690400A CN 103690400 A CN103690400 A CN 103690400A CN 201310719007 A CN201310719007 A CN 201310719007A CN 103690400 A CN103690400 A CN 103690400A
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Abstract
The invention relates to natural plant type body wash and a preparation method thereof. The body wash is formed by mixing the following components in parts by weight: 70-90 parts of limonene, 1-3 parts of olive oil and multiple environment-friendly nonirritant surfactants according to a ratio of 1:(3-5). The surfactants are prepared from mixed two or three of coconut diethanolamide, sucrose fatty acid ester, alkyl glycoside, fatty acid methyl ester sulfonate, rhamnolipid and octadecyl dimethyl ammonium chloride. The body wash can be prepared by uniformly mixing the main components and the surfactants by using a stirring machine in the stirring speed of 1,000r/min to 2,000r/min, subsequently standing for 60-120 minutes, adding water to emulsify according to a ratio of 1:(1.5-3.0), and uniformly mixing up at normal temperature. The body wash is simple in process, convenient to operate and undemanding in preparation condition, energy consumption can be effectively reduced, beneficial conditions can be provided for production, and the raw materials adopted by the body wash are all recyclable resources with good biodegradability, good stability, nonirritant for skin and excellent effects such as decontamination and sterilization.
Description
Technical field
The present invention relates to a kind of bath gel, particularly a kind of natural plant type bath gel and preparation method thereof.
Background technology
At present, the bath gel that sell in market generally adopts by the synthetic alkali electroless solvent of sodium alkyl benzene sulfonate, sodium sulfate, toluene sodium iodate, sodium tripolyphosphate and carboxymethyl cellulose, the bath gel of being made as key component by this solvent; Wherein contain in a large number the poisonous and hazardous material of human body, easily make Keratoderma, be chapped from the cold; After entering human body hemopoietic system, can affect liver function; In addition, phosphorus-containing compound can cause the eutrophication of water body, therefore when serious infringement people are healthy, the ecological balance of the Nature will endangered, moreover prepare the above-mentioned industrial chemicals multi-source of bath gel in oil accessory, because oil is non-renewable resources, so cost of material will constantly rise, the price of bath gel is occupied high, and make its raw material of preparing face the condition of the constantly deficient exhaustion of resource.
Therefore, provide a kind of circular regeneration aboundresources, technique simple, be widely used, environment friendly and pollution-free natural plant type bath gel and preparation method thereof, be one of these those skilled in the art problem that should address.
Summary of the invention
The object of the invention is to overcome above-mentioned weak point, simple, of many uses, environment friendly and pollution-free natural plant type bath gel of a kind of circular regeneration aboundresources, technique and preparation method thereof is provided.
The technical solution adopted in the present invention is for achieving the above object: a kind of natural plant type bath gel, it is characterized in that: this bath gel in weight portion mainly by 70～90 parts of limonenes, 1～3 part, olive oil, and with the ratio of 1:3～5, evenly mix composition with multiple environmental protection nonirritant surfactant, then add water emulsification in the ratio of 1:1.5～3.0.
Described surfactant adopts wherein two or three mixture of coconut oil diethanol amide, sucrose fatty acid ester, alkyl polyglucoside, MES, rhamnolipid, octadecyl alkyl dimethyl ammonium chloride.
The preparation method of this natural plant type bath gel, implementation step is as follows:
(1), by 70～90 parts of limonene limonenes, 1～3 part, olive oil, evenly mixed preparing forms preliminary mixed system;
(2) preliminary mixed system and surfactant are pressed to 1:3～5 proportioning mixing and stirring, mixing speed is 1000r/min～2000r/min, standing 60min～120min;
(3) mixture of preliminary mixed system and surfactant is added to water emulsification, the proportioning of its mixture and water is 1:1.5～3.0, mix homogeneously under normal temperature condition.
Be below characteristic and the composition principle of each component in the present invention:
One of bath gel main component be from pure natural plant as Fructus Citri tangerinae skin, Fericarpium Citri Limoniae, Pericarpium citri sinensis through the limonene of distillation extraction, it is a kind of organic solvent of plant base environmental protection, there is the very strong decontamination ability of deoiling, not only substituted the particularly organic solvent of benzene series industrial chemicals of oil accessory, effectively guaranteed that product is nontoxic, and promoted the industrialized development of Pericarpium Citri tangerinae deep processing.Most importantly utilize degradable limonene to replace mineral oil solvent, add other functional aid, the bath gel cleaning performance developed by compounded technology is good, the effect of protection skin nonirritant.
Described olive oil has splendid natural health and beauty functions; add olive oil and effectively guarantee that people do not injure skin when taking a shower; the water oil balance that keeps skin surface; in addition; olive oil is specially adapted to pregnant mother and baby's nursing; can directly spread upon on skin; just can effectively strengthen its elasticity; thereby prevention chapped skin; and olive oil is very soft; not only there is the effect of nourishing and protecting the tender and lovely skin of baby, also can not cause any bad stimulation to skin simultaneously.In described natural plant type bath gel, add olive oil, during bathing, bath gel whole body is looped and smeared massage, then pass through the stifling of water vapour, can remove the dirt being invisible to the naked eye in pore, nourish skin, increase gloss and the elasticity of skin, remove tiny wrinkle.
Limonene in described bath gel and olive oil by reaching clean mixing of distinctive emulsifying process, skin moistening is two-in-one, prepared bath gel dissolving power is strong, detergency is good, combine the advantage of two kinds of key components, have good antibacterial, bactericidal property, pure natural formula does not injure skin when removing dirt simultaneously.
The limonene of described bath gel one-component, not only can give out fragrant fragrance, pleasant aroma, make people's spirit and QI cleaning, and potent decontamination, the deep layer that can reach skin is clean, clearly, still inevitably in decontamination, take away a small amount of oils and fats of skin surface.One-component olive oil skin effect is remarkable, directly the smearing massage and can make skin smooth of skin surface, delicate flexible but skin absorbs unnecessary oils and fats cleaning problem later and can not be ignored, when the two effectively combines, limonene reaches clean with olive oil by mixing of distinctive emulsifying process, skin moistening is two-in-one, prepared bath gel dissolving power is strong, detergency is good, the advantage that combines two kinds of key components has good antibacterial simultaneously, bactericidal property, pure natural formula does not injure skin when removing dirt, technique is simple, easy to operate, under normal temperature condition, can carry out, a large amount of energy consumptions that reduce are for producing the sharp condition that provides.Adopting raw material is recyclable regenerative resource, and biodegradability is good, and good stability to skin nonirritant, and has the good effects such as stain removal bactericidal.
Described surfactant adopts wherein two or three mixture of coconut oil diethanol amide, sucrose fatty acid ester, alkyl polyglucoside, MES, rhamnolipid, octadecyl alkyl dimethyl ammonium chloride.
Natural plant type bath gel of the present invention, by fully natural green raw material and obtain product through one step or a few step machining and be prepared from nontoxic, wherein, described MES, to take the anion surfactant that palm stearin is raw material production, anti-hard water and scourability are superior, in price, there is suitable advantage, in addition raw material sources are in the natural biological materials such as animal and plant fat, raw material sources are extensive, renewable, produce conveniently, biological degradability is good, to biological nontoxic, easily by microorganism, decomposed, high to the gentle non-stimulated detergency of skin, reach identical detergency, the consumption of MES is only prepared 30% of gained sodium alkyl benzene sulfonate LAS consumption for take oil as raw material, in addition, MES is specially adapted to configure baby's articles for washing and the subsensitivety goods of low stimulation.
Described coconut oil diethanol amide is a kind of non-ionic surface active agent, itself and anion, cation amphitypy surfactant compatibility are good, there is moistening, thickening, washing, emulsifying, steady bubble, the performance such as soft, can with kinds of surface activating agent compatibility, stability in hard water is good.Coconut oil diethanol amide is applicable to various skin quality simultaneously, can kill antibacterial, fungus, virus and the parasite etc. that cause disease.
Described alkyl polyglucoside is synthetic by Renewable resource natural acid alcohol and glucose, it is the more comprehensive new non-ionic surfactants of a kind of performance, have the characteristic of common nonionic and anion surfactant concurrently, there is high surface, good ecological security and intermiscibility, it is internationally recognized first-selection " green " functional surface activating agent, surface tension is low, without cloud point, wetting power is strong, soil release performance is good, compatibility is good, can with various ion-types, the composite generation potentiation of nonionic surfactant, there is stronger broad spectrum antibiotic activity, sterilizing ability is strong, foaming characteristic is good, foam is abundant fine and smooth, the strong acid of resistance to highly basic, hard water and electrolyte, there is good thickening capabilities, good with skin intermiscibility, significantly improve the mildness of formula, nontoxic, non-stimulated, easily biological-degradable and thorough rapidly, can not cause the pollution to environment, by APG, make bath gel and there is good dissolubility, mildness and degreasing power, anti-hard water and the washing performance of cortex dirt is obviously improved, easily rinsing, good flowing properties, not only can effectively save the energy, also can improve the output of unit interval simultaneously, reduce costs.
Described rhamnolipid is by the anion biosurfactant of microorganisms, shows good dissolution characteristics in alkaline aqueous solution.It has good chemistry and biological nature concurrently, there is oil, water is amphipathic, can material be spread by dispersion and wettability, using help to retain moisture, lubricated, produce foam, as a kind of bath gel, it can keep the stable system of mixture, control the viscosity of product, the oils and fats in all right emulsifying pore, reduces the generation of acne; Can reduce water surface tension; Can be used as wetting agent, emulsifying agent and foaming agent uses.Rhamnolipid biological surface activator can be used in temperature, pH value and salinity under extreme situation, and nontoxic, can biodegradation.
The molecular structure of described octadecyl alkyl dimethyl ammonium chloride determines that it has good physical and chemical performance, make to reduce the capillary ability of aqueous solution and efficiency more outstanding, thereby obtain higher surface activity, compare it with conventional surfactant and be more easily adsorbed on two-phase interface, absorbability is 10～1000 times of conventional surfactant, thereby reducing surface tension, foaming, steady bubble, emulsifying aspect has special good efficient capacity, its cmc is only conventional surfactant 1/10～1/100 in addition, this just means that its zest is little, and there is superpower solubilizing effect and cost advantage, can with various ion-types, the composite generation potentiation of nonionic surfactant, the synergist that can be used as common cation surfactant simultaneously, the efficient emulsifying agent of emulsion polymerisation.
Described sucrose fatty acid ester, a kind of non-ionic surface active agent, the simple substance or the mixture that by sucrose and fatty acid, through esterification, are generated.According to the esterification number of sucrose hydroxyl, can obtain the sucrose fatty acid ester series of products to the different HLB values of hydrophilic (1～16) by lipophile, there is surface activity, as emulsifying agent, can reduce surface tension, have good emulsifying simultaneously, disperse solubilising, lubricated, infiltration, foaming, viscosity regulate, prevent the performances such as aging, antibacterial.Because of non-stimulated to eyes, skin etc., be also widely used in the production of medicine and cosmetics, biological degradability is strong, so residue is pollution-free simultaneously.
The present invention has incomparable advantage in properties of product, in energy-conserving and environment-protective in sum, more focused on the processing of details simultaneously, not only remarkable to skin dirt cleaning effect, can make skin avoid the injury of alkaline bath shampoo simultaneously, moreover and effective Glycerin, the formula of pure natural environment protection meets all age group or even baby's shower washing, accomplish simultaneously nontoxic and cost-saving in a large number, for the expanding production of product provides advantage.
Bath gel of the present invention detects that requirement according to rower QB/T1994-2004 all reaches and higher than standard, and can meet the standard of child form, and indices is as table 1, table 2.
The invention has the beneficial effects as follows: the main component limonene of this bath gel has stronger dissolving power that detergency and bacteriostasis and sterilization effect the experiment proved that limonene reaches 100% to the bacteriostasis rate of antibacterial, fungus.Olive oil can further improve dissolving power, strengthens dissolution with solvents scope; Olive oil balance solvent evaporates speed, olive oil has softness, skin moistening effect simultaneously, makes skin smooth flexible, and nourishes rough skin in the time of cleaning deep skin dirt, makes skin more smooth, fine and smooth, flexible.Alkyl polyglucoside disinfection effect is remarkable, and has flexibility concurrently.Coconut oil diethanol amide is applicable to various skin quality, can kill antibacterial, fungus, virus and the parasite etc. that cause disease.The anti-hard water of MES is good, washability is superior, and MES is specially adapted to configure baby's articles for washing and the subsensitivety goods of low stimulation.The absorbability of octadecyl alkyl dimethyl ammonium chloride is 10～1000 times of traditional activating agent, and cmc is traditional activating agent 1/10～1/100.The effective cleaning component that is micellization state in this type of surfactant solution is in the great majority, but not the surfactant concentration of micellization is lower, thereby can reduce toxicity, abirritate, and on dissolved water insoluble matter, show high efficiency and there is better foaming, dispersion and emulsifiability, when itself and monomer surfactant mix, can produce cooperative effect, nonirritant, gentle decontamination.High-quality fatty acid cane sugar ester odorless, tasteless is nontoxic, and non-stimulated to eyes, skin etc., biological degradability is strong, and residue is pollution-free.Rhamnolipid, except possessing good surface activity, also possesses good cell permeability, and it derives from biology, has good nonhazardous degradable characteristic.This bath gel containing benzene,toluene,xylene, cyclononane etc. to human body poisonous and harmful substance, the also heavy metal such as not leaded, chromium, cadmium, antimony and barium.Non-secondary pollution of the present invention, biological degradability is good; Technique is simple, easy to operate, and production environment condition is loose, without special equipment and the supporting facility that decontaminates, has significant practical value and economic benefit.Adopting raw material is recyclable regenerative resource, and source is abundant and extensive; In twice laid, when turning waste into wealth, reach and remove deep skin dirt, organic chemical industry's bath gel of benzene class thing as an alternative, clean, decontamination, can be used for the shower washing of various skin quality, each age group, remove deep skin dirt, the effect of nourishes rough skin is played in sterilization, antibacterial simultaneously.
The specific embodiment
Below in conjunction with preferred embodiment, to according to the specific embodiment provided by the invention, details are as follows:
Every part of embodiment 1(, by 1kg, adopts surfactant effective active thing content requirement >=50%)
Limonene 70kg, the even mixed preparing of olive oil 1kg are formed to preliminary mixed system, then press 1:3 preparation with emulsifying agent, emulsifying agent adopts respectively octadecyl alkyl dimethyl ammonium chloride, coconut oil diethanol amide mixture 210kg(to divide equally); Mixing and stirring, mixing speed is 1000r/min～2000r/min, standing 60min～120min; Again natural plant solvent and emulsifier mixture are added to water emulsification, the proportioning of its mixture and water is 1:1.5, adds about 420kg water, mix homogeneously under normal temperature condition.
Embodiment 2
By limonene 80kg, olive oil 2kg, natural plant solvent and emulsifying agent that evenly mixed preparing forms mix and form with 1:4; Emulsifying agent adopts respectively sucrose fatty acid ester, MES, alkyl polyglucoside mixture 320kg(to divide equally); Natural plant solvent adds water emulsification after mixing with emulsifying agent, with the proportioning of water be 1:2.0, add about 800kg water mix homogeneously under normal temperature condition.
Other preparation process is equal to embodiment 1.
Embodiment 3
By limonene 90kg, olive oil 3kg, natural plant solvent and emulsifying agent that evenly mixed preparing forms mix and form with 1:5; Emulsifying agent adopts respectively MES, alkyl polyglucoside, rhamnolipid mixture 450kg(substantially to divide equally); Natural plant solvent adds water emulsification after mixing with emulsifying agent, with the proportioning of water be 1:3.0, add about 1350kg water mix homogeneously under normal temperature condition.
Other preparation process is equal to embodiment 1.
Embodiment 4
By limonene 75kg, olive oil 3kg, natural plant solvent and emulsifying agent that evenly mixed preparing forms mix and form with 1:5; Emulsifying agent adopts respectively rhamnolipid mixture, alkyl polyglucoside, coconut oil diethanol amide mixture 390kg(substantially to divide equally); Natural plant solvent adds water emulsification after mixing with emulsifying agent, with the proportioning of water be 1:1.5, add about 585kg water mix homogeneously under normal temperature condition.
Other preparation process is equal to embodiment 1.
Embodiment 5
By limonene 85kg, olive oil 1kg, natural plant solvent and emulsifying agent that evenly mixed preparing forms mix and form with 1:4; Emulsifying agent adopts respectively MES, alkyl polyglucoside, rhamnolipid mixture 344kg(to divide equally); Natural plant solvent adds water emulsification after mixing with emulsifying agent, with the proportioning of water be 1:3.0, add about 1032kg water mix homogeneously under normal temperature condition.
Other preparation process is equal to embodiment 1.
Embodiment 6
By limonene 88kg, olive oil 2kg, natural plant solvent and emulsifying agent that evenly mixed preparing forms mix and form with 1:3; Emulsifying agent adopts respectively MES, alkyl polyglucoside, rhamnolipid mixture 270kg(substantially to divide equally); Natural plant solvent adds water emulsification after mixing with emulsifying agent, with the proportioning of water be 1:2.0, add about 540kg water mix homogeneously under normal temperature condition.
Other preparation process is equal to embodiment 1.
Feature of the present invention and purposes:
(1) the present invention adopts micro-emulsion technology, has solved emulsifying lamination.
(2) require during raw material selection especially strictly, all meet natural non-stimulated standard, biological degradability is good simultaneously, environmental sound.
(3) at the emulsifying of bath gel, moistening, dispersion solubilising, lubricated, infiltration, foaming, viscosity, regulate, prevent, in the performance such as aging, antibacterial, to make full use of the complementary action of each raw material and adjuvant, make its clean and skin effect reach optimized effect.
Using method:
Select bath gel of the present invention, cleaning performance is remarkable; Skin-friendly is good, and deep layer cleaning skin dirt does not injure skin simultaneously, also can be applicable to the daily cleaning nursing of infant, without paying special attention to.
Above-mentioned detailed description of this natural plant type bath gel and preparation method thereof being carried out with reference to embodiment; illustrative rather than determinate; according to component proportion limited range, can enumerate several embodiment; therefore in the variation and the modification that do not depart under general plotting of the present invention, within should belonging to protection scope of the present invention.
Claims (3)
1. a natural plant type bath gel, it is characterized in that: this bath gel in weight portion by 70～90 parts of limonenes, 1～3 part, olive oil, and with the ratio of 1:3～5, evenly mix composition with multiple environmental protection nonirritant surfactant, then add water emulsification in the ratio of 1:1.5～3.0.
2. natural plant type bath gel according to claim 1, is characterized in that described surfactant adopts wherein two or three mixture of coconut oil diethanol amide, sucrose fatty acid ester, alkyl polyglucoside, MES, rhamnolipid, octadecyl alkyl dimethyl ammonium chloride.
3. a preparation method for natural plant type bath gel according to claim 1 and 2, is characterized in that implementation step is as follows:
(1), by 70～90 parts of limonenes, 1～3 part, olive oil, evenly mixed preparing forms preliminary mixed system;
(2) preliminary mixed system and surfactant are pressed to 1:3～5 proportioning mixing and stirring, mixing speed is 1000r/min～2000r/min, standing 60min～120min;
(3) mixture of preliminary mixed system and surfactant is added to water emulsification, the proportioning of its mixture and water is 1:1.5～3.0, mix homogeneously under normal temperature condition.
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| CN201310719007.4A CN103690400A (en) | 2013-12-24 | 2013-12-24 | Natural plant type body wash and preparation method thereof |
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| CN201310719007.4A CN103690400A (en) | 2013-12-24 | 2013-12-24 | Natural plant type body wash and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106726761A (en) * | 2016-12-24 | 2017-05-31 | 叶宗瑞 | A kind of salubrious shower cream and preparation method thereof |
| CN107625667A (en) * | 2017-09-13 | 2018-01-26 | 西安瑞捷生物科技有限公司 | A kind of basic aqua containing rhamnolipid and preparation method thereof and application |
| CN114176077A (en) * | 2021-12-09 | 2022-03-15 | 中化化工科学技术研究总院有限公司 | Barrel-mixed spraying aid containing rhamnolipid and preparation method and application thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102277239A (en) * | 2011-07-20 | 2011-12-14 | 天津鎏虹科技发展有限公司 | Natural plant aqueous cleaning agent and preparation method thereof |
-
2013
- 2013-12-24 CN CN201310719007.4A patent/CN103690400A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102277239A (en) * | 2011-07-20 | 2011-12-14 | 天津鎏虹科技发展有限公司 | Natural plant aqueous cleaning agent and preparation method thereof |
Non-Patent Citations (1)
| Title |
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| 张永奎等: "《现代生物工程与技术概论》", 31 July 2011, article "在生物表面活性剂生产中的应用" * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106726761A (en) * | 2016-12-24 | 2017-05-31 | 叶宗瑞 | A kind of salubrious shower cream and preparation method thereof |
| CN107625667A (en) * | 2017-09-13 | 2018-01-26 | 西安瑞捷生物科技有限公司 | A kind of basic aqua containing rhamnolipid and preparation method thereof and application |
| CN114176077A (en) * | 2021-12-09 | 2022-03-15 | 中化化工科学技术研究总院有限公司 | Barrel-mixed spraying aid containing rhamnolipid and preparation method and application thereof |
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Application publication date: 20140402 |