CN107625667A - A kind of basic aqua containing rhamnolipid and preparation method thereof and application - Google Patents
A kind of basic aqua containing rhamnolipid and preparation method thereof and application Download PDFInfo
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- CN107625667A CN107625667A CN201710820675.4A CN201710820675A CN107625667A CN 107625667 A CN107625667 A CN 107625667A CN 201710820675 A CN201710820675 A CN 201710820675A CN 107625667 A CN107625667 A CN 107625667A
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- rhamnolipid
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Abstract
The invention belongs to cosmetic field.A kind of formula and preparation method of the basic aqua as moisturizing nursing materials are provided, this aqua includes natural plant grease, rhamnolipid, natural and mineral water.Rhamnolipid can improve amount retained of the emollient on skin, and help its film forming on skin, promote the emollient of emollient, strengthen sensory effects, the formula uses pure natural components, Nonpoisonous, non-environmental-pollution, it is practical suitable for the basic aqua of moisturizing moisturizing serial cosmetics.
Description
Technical field
The invention belongs to cosmetic field, and in particular to a kind of aqua for basic components containing rhamnolipid, this
Invention further relates to the preparation method and purposes of this aqua.
Background technology
Cosmetics are modern life people's indispensable requisites, especially numerous women.Whether moisturising product is also
The basic standard that daily nursing product should all reach safety nuisance free, as the improvement of people's living standards, to health and
Natural nuisance-free is increasingly paid attention to.
Common moisturising product according to composition difference can be divided into mineral grease, Synthetic Oil, animal fat, vegetable fat and
Organic silicon, one layer of hydrophobic film can be formed in skin surface, suppress moisture of skin evaporation, make skin emolliency glossy.
Emollient is the basic aqua used in skin care item, and it determines the skin sense type of skin care item formula.It is excellent to distinguish emollient
Bad leading indicator is the amount retained and glossiness after use.
Mineral grease, Synthetic Oil and organic silicon etc. are made up mostly using petroleum base as source of chemical industry synthesis mode,
Skin texture can be destroyed, causes immunity degradation, makes skin sensitivity, some has stronger carcinogenicity.Emollient at present
Composition be oriented in natural, natural component, such as animal fat and vegetable fat, but animal fat quality is unstable, easily becomes sour.
Rhamnolipid possesses good surface-active, is also equipped with good cell permeability, and it has good from biology
The good degradable characteristic of nonhazardous.These features make it can be widely applied in various daily chemical products.Rhamnolipid can pass through
Disperse to spread material with wettability.Using help retain moisture, lubrication, produce foam, be used as a kind of cleaning agent.It can be with
The stable system of mixture is kept, the viscosity of product is controlled, the grease in pore can also be emulsified, reduce the generation of acne.
The content of the invention
For the present invention in order to what is proposed the shortcomings that overcoming above-mentioned prior art to exist, its technical problem solved is to provide one
Kind is used for the basic aqua for preparing all kinds of moisturizing cosmetics, utilizes the days such as rhamnolipid, natural plant grease, natural
Right innocuous substance overcomes the excitant and carcinogenicity of mineral grease, Synthetic Oil, animal fat.
The invention provides a kind of basic aqua, rhamnolipid and vegetable fat are included.
Preferably, the purity of the rhamnolipid is 98%-99.9%.
Preferably, also rosemary, cloves, flower are included comprising Vc, dimension E or natural, wherein native oxidant
The extract of green pepper, sweet osmanthus, ginger, shield-fern etc., Tea Polyphenols, astaxanthin, propolis etc..Vc, dimension E or natural contain
Measure as 0.1-1g/L.
Preferably, the content of the rhamnolipid is 50-500mg/L.
Preferred scheme, the content of the rhamnolipid is 100-500mg/L.
Preferred scheme, the content of the rhamnolipid is 300-500mg/L.
The content of vegetable fat is 8-10g/L.
The preferred mineral water of water used in aqua, wherein containing the human body beneficial mineral matter such as strontium, zinc, selenium.
Preferably, the vegetable fat includes the mustard oil of deep-sea two, modified sher butter, granada seed oil, european cranberry oil, Hu
One or more in Radish seed oil, pot marigold oil, purple yu-lan (Magnolia liliflora) oil, candlenut tree seed oil, cucumber seed oil etc..
Present invention also offers a kind of method prepared containing rhamnolipid and vegetable fat, comprise the following steps：
A, the container for containing gauge water is positioned on magnetic stirring apparatus, adjustment of rotational speed 100-500rpm；B, while stirring
Rhamnolipid is added, until system is homogeneous, is further continued for stirring 10-20 minutes；C, obtained solution is passed through into 0.22um microporous barriers
Filtered, obtain the base soln of rhamnolipid；D, the vegetable fat of respective quality, adjustment of rotational speed 100-500rpm are added
Stirring is homogeneous to system, in lasting stirring 10-20 minutes；E, Vc, dimension E or natural are added, is stirred equal to system
One.
The basic aqua can be as the basic components for being used for configuring various moisturizing skin protection cosmetics.
Beneficial effects of the present invention：
1st, the grease that the present invention uses is natural plant grease, overcomes the easy corruption and mineral synthetic oil fat of animal fat
Unsafe factor, it is pure natural nuisanceless.
2nd, for the present invention with rhamnolipid as surface active ingredient, rhamnolipid can improve emollient on skin
Amount retained, and its film forming on skin is helped, promote the emollient of emollient, strengthen sensory effects.
3rd, the basic aqua for preparing of the present invention be transparent or semitransparent system, and particle diameter is small, stability height, and be long placed in will not
It is layered.
4th, basic aqua prepared by the present invention can be universally used in the basic aqua of moisturizing moisturizing serial cosmetics, practical.
Specific embodiment
Basic aqua embodiment is introduced below in conjunction with specific embodiment.
Embodiment 1：
A, the container for containing gauge water is positioned on magnetic stirring apparatus, adjustment of rotational speed 100rpm；
B, rhamnolipid is added while stirring, until system is homogeneous, is further continued for stirring 20 minutes；
C, obtained solution is filtered by 0.22um microporous barriers, obtains the base soln of rhamnolipid；
D, add respective quality vegetable fat, adjustment of rotational speed be 100rpm stir it is homogeneous to system, it is lasting stirring 20
Minute；
E, Vc, dimension E or natural are added, is stirred homogeneous to system.
The content of the rhamnolipid of this embodiment is 50mg/L, and vegetable fat content is 8g/L.Natural contains
Measure as 0.1g/L.
Embodiment 2：
A, the container for containing gauge water is positioned on magnetic stirring apparatus, adjustment of rotational speed 100rpm；B, add while stirring
Rhamnolipid, until system is homogeneous, it is further continued for stirring 20 minutes；C, obtained solution was carried out by 0.22um microporous barriers
Filter, obtains the base soln of rhamnolipid；D, the vegetable fat of respective quality is added, adjustment of rotational speed is that 100rpm is stirred to system
It is homogeneous, in lasting stirring 20 minutes；E, Vc, dimension E or natural are added, is stirred homogeneous to system.
The content of the rhamnolipid of this embodiment is 100mg/L, and vegetable fat content is 8g/L.Natural contains
Measure as 0.3g/L.
Embodiment 3：
A, the container for containing gauge water is positioned on magnetic stirring apparatus, adjustment of rotational speed 200rpm；B, add while stirring
Rhamnolipid, until system is homogeneous, it is further continued for stirring 15 minutes；C, obtained solution was carried out by 0.22um microporous barriers
Filter, obtains the base soln of rhamnolipid；D, the vegetable fat of respective quality is added, adjustment of rotational speed is that 200rpm is stirred to system
It is homogeneous, in lasting stirring 15 minutes；E, Vc, dimension E or natural are added, is stirred homogeneous to system.
The content of the rhamnolipid of this embodiment is 250mg/L, and vegetable fat content is 9g/L.Natural contains
Measure as 0.5g/L.
Embodiment 4：
The making step of this embodiment is formulation content with embodiment 3, difference, and the content of rhamnolipid is 350mg/
L, vegetable fat content are 9g/L.Natural anti-oxidation agent content is 0.6g/L.
Embodiment 5：
A, the container for containing gauge water is positioned on magnetic stirring apparatus, adjustment of rotational speed 500rpm；B, add while stirring
Rhamnolipid, until system is homogeneous, it is further continued for stirring 10 minutes；C, obtained solution was carried out by 0.22um microporous barriers
Filter, obtains the base soln of rhamnolipid；D, the vegetable fat of respective quality is added, adjustment of rotational speed is that 500rpm is stirred to system
It is homogeneous, in lasting stirring 10 minutes；E, Vc, dimension E or natural are added, is stirred homogeneous to system.
The content of the rhamnolipid of this embodiment is 500mg/L, and vegetable fat content is 10g/L.Natural
Content is 1g/L.
Described above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
Member, under the premise without departing from the principles of the invention, can also make some improvement and supplement, and these are improved and supplement also should be regarded as
Protection scope of the present invention.
Emollient test experiments
1st, test sample is made
(1) 100ml mineral waters are added in 200ml cleaning beakers, are placed on magnetic stirring apparatus, adjustment rotating speed 100-
500rpm, rhamnolipid 50-500mg is respectively added slowly to while stirring, until system is homogeneous, be further continued for stirring 10-20min,
Liquid is obtained into the basic components containing rhamnolipid with 0.22 μm of filtering with microporous membrane afterwards；
(2) mustard oil of deep-sea two, modified sher butter, granada seed oil, european cranberry are separately added into 50ml cleaning beakers
Oil, carrot seed oil, pot marigold oil, purple yu-lan (Magnolia liliflora) oil, candlenut tree seed oil, cucumber seed oil 10g, are placed on magnetic stirring apparatus, adjust rotating speed
100-500rpm, basic components of the 1ml containing rhamnolipid are respectively added slowly to while stirring, until system is homogeneous, be further continued for stirring
Mix 10-20min, stand after 3-5d still without layering, record rhamnolipid addition in basic components.Obtain following 9 groups of experiment systems
Agent.
2nd, emollient contrast test
The vegetable fat of natural origin is prepared according to rhamnolipid addition in above-mentioned steps, test sample is made and (compiles
Number 1-9), separately take the vegetable fat for the natural origin for not adding rhamnolipid to do control sample (numbering CK1-9).Both hands are cleaned to dry
After dry, take 100 μ l samples to be applied to the back of the hand 3cm × 3cm regions, smeared with 1 circle/s speed and experience spreadability；Experience after 10s
Heavy feeling and smooth feeling；Respectively smear terminate after, terminate after 5min and 10min experience the amount retained and skin gloss of sample
Degree.Above-mentioned each index is scored and records characteristic sample, and application SPSS19.0 softwares carry out variance analysis.Weight
Multiple above step, evaluation index and points-scoring system see the table below.
9 kinds of test samples and each index average value of control sample and ANOVA variance analyses
Note：* P is represented<0.05；T0 represents that smearing terminates；t5Represent to smear and terminate 5min；t10Represent to smear and terminate 10min.
Conclusion (of pressure testing)：Basic components containing rhamnolipid can improve amount retained of the emollient on skin, and help
Its film forming on skin, promote the emollient of emollient, strengthen sensory effects.
Claims (10)
- A kind of 1. basic aqua, it is characterised in that：Include rhamnolipid and vegetable fat.
- 2. basic aqua according to claim 1, it is characterised in that：The purity of the rhamnolipid is 98%-99.9%.
- 3. basic aqua according to claim 1 or 2, it is characterised in that：Include Vc, dimension E or natural.
- 4. basic aqua according to claim 3, it is characterised in that：Vc, dimension E or the content of natural are 0.1-1g/L。
- 5. basic aqua as claimed in any of claims 1 to 4, it is characterised in that：The content of rhamnolipid is 50- 500mg/L。
- 6. basic aqua according to claim 5, it is characterised in that：The content of rhamnolipid is 100-500mg/L.
- 7. basic aqua according to claim 6, it is characterised in that：The content of rhamnolipid is 300-500mg/L.
- 8. the basic aqua according to claim 1 to 7 any one, it is characterised in that：The content of vegetable fat is 8- 10g/L。
- A kind of 9. preparation method of basic aqua, it is characterised in that：Comprise the following steps：A, the container for containing gauge water is positioned over On magnetic stirring apparatus, adjustment of rotational speed 100-500rpm；B, rhamnolipid is added while stirring, until system is homogeneous, is further continued for Stir 10-20 minutes；C, obtained solution is filtered by 0.22um microporous barriers, obtains the base soln of rhamnolipid； D, add respective quality vegetable fat, adjustment of rotational speed be 100-500rpm stir it is homogeneous to system, lasting stirring 10-20 divide Clock；E, Vc, dimension E or natural are added, is stirred homogeneous to system.
- 10. basic aqua as claimed in any of claims 1 to 8, it is characterised in that：The basic aqua can conduct For configuring the basic components of various moisturizing skin protection cosmetics.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2020087146A1 (en) * | 2018-10-29 | 2020-05-07 | Phytoplenus Bioativos S.A. | Formulation based on medicinal plant, or part or extract thereof, use of the formulation and product including said formulation |
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| US11883453B2 (en) | 2018-10-29 | 2024-01-30 | Phytoplenus Bioativos S.A. | Formulation based on medicinal plant, or part or extract thereof, use of the formulation and product including said formulation |
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Application publication date: 20180126 |