CN106821840A - A kind of waterproof mascara and preparation method thereof - Google Patents
A kind of waterproof mascara and preparation method thereof Download PDFInfo
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- CN106821840A CN106821840A CN201611230207.3A CN201611230207A CN106821840A CN 106821840 A CN106821840 A CN 106821840A CN 201611230207 A CN201611230207 A CN 201611230207A CN 106821840 A CN106821840 A CN 106821840A
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- waterproof mascara
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/733—Alginic acid; Salts thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/10—Preparations containing skin colorants, e.g. pigments for eyes, e.g. eyeliner, mascara
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention belongs to cosmetic technical field, and in particular to a kind of waterproof mascara and preparation method thereof.The waterproof mascara that the present invention is provided includes following components and its mass percent：Alginate fibre 12~14%, allantoin 12~14%, beeswax 12~14%, colouring agent 12~14%, NMF 10~14%, vitamin E 7~9%, film forming agent 2~4%, preservative 1~3% and deionized water 14~32%.It is of the invention it is a technical advantage that：Stability more preferably, be difficult dizzy dye, uniform and difficult for drop-off and caking, source wide material sources, safety are adapted to eye and decorate, and security is higher.
Description
Technical field
The invention belongs to cosmetic technical field, and in particular to a kind of waterproof mascara and preparation method thereof.
Background technology
The application target of mascara is to be coated on eyelashes the shortcoming or beautiful to eyes addition to make up eyebrow form,
The functions such as the condition that usual mascara needs to have is stuck up to assign dense, volume, fine length, waterproof, and be difficult by sweat, tear and oil
Part is dropped without powder and is equably smeared while fuzzy, and free of a burden when using, and the possibility of pollution to microorganism is small, washes eye
When need easily wipe.
Chinese patent application CN104666190A discloses a kind of with the water-resistance mascara for increasing effect, by following heavy
Amount part raw material composition：Silk Powder 3-5, petroleum ether 45-55, stearic acid 3-9, beeswax 20-30, palm wax 4-8, wool grease 2-
6th, triethanolamine 0.5-3, natural black pigment 4-9, glycerine 5-10, vitamin E 0.2-2, preservative 0.1-0.3 and aluminum stearate 2-
4.Mascara of the present invention is vegetable wax to be molded, but the soft and moist degree of vegetable wax palm wax is bad, can be molded after makeup, but
It is repeated several times and just occur shape rupture, cause to be peeled away from eyelashes, lasting effects is bad.
Chinese patent CN100398086C discloses a kind of water content waterproof mascara high, and the present invention includes oil
Phase, it contains liquid ester, oil or its mixture, film forming agent, gelatinizing agent, pigment, powder, filler and its mixture, water, surface
Activating agent etc., wherein the grease separation is from silicone oil, mineral oil, Parleam, polyisoprene etc..Mineral oil to eye or
Skin pore easily blocks airtight, and especially eye is more fragile, is easily caused infection.
Therefore this area needs to develop lotion safety and stability, smears uniform and good water-proof effect, and the persistently eyelash of makeup
Hair cream.
The content of the invention
To solve the problems, such as waterproof mascara in the prior art, the present invention provides a kind of waterproof mascara and its preparation
Method.
Waterproof mascara of the present invention, including following components and its mass percent：
Alginate fibre 12~14%, allantoin 12~14%, beeswax 12~14%, colouring agent 12~14%, NMF 10
~14%, vitamin E 7~9%, film forming agent 2~4%, preservative 1~3% and deionized water 14~32%.
Preferably, described waterproof mascara is made up of following components and its mass percent：
Alginate fibre 13%, allantoin 13%, beeswax 13%, colouring agent 13%, NMF 12%, vitamin E 8%, into
Film 3%, preservative 2% and deionized water 23%.
Preferably, described colouring agent is by plant carbon black and fruit of Cherokee rose palm fibre in mass ratio 2:3 compositions.
Preferably, described NMF is by glycerine, sodium alginate and sorbierite in mass ratio 2:3:5 compositions.
Preferably, described film forming agent is acrylic resin.
Further preferably, described preservative is Tea Polyphenols.
In addition, present invention also offers a kind of preparation method of waterproof mascara, comprising the following steps：
S1, will 1.5 times of beeswax and its quality deionized water add material-compound tank in, be mixed and heated to 70-80 DEG C until
It is standby to transparency liquid A；
S2, alginate fibre, allantoin, colouring agent, NMF, vitamin E and remaining deionized water are added into another container
In be heated to 60-70 DEG C and be stirring evenly and then adding into film forming agent, stir to obtain B liquid；
S3, A the and B liquid for obtaining S1 and S2 mixing add emulsion tank, are cooled to room temperature, and the lower addition preservative of stirring is
.
Allantoin CAS：97-59-6；Beeswax CAS：8012-89-3；Plant carbon black CAS：1333-86-4；Jin Ying
Sub- palm fibre No. CAS：327-97-9；Sodium alginate CAS：9005-38-3；Sorbierite CAS：50-70-4；Acrylic resin CAS
Number：9003-01-4；Tea Polyphenols CAS：84650-60-2.
The chief value of alginate fibre is algae component, and the contact with skin in the fibre will not allow the people to have the anti-of allergy
Answer, and can actively discharge the vitamin and mineral matter of marine alga, this fiber includes the main mineral matters, vitamin bag such as calcium and magnesium
Vitamin A, C, E etc. are included, in the research of cosmetics, shows minerals and vitamins A, C, E that algae component has to skin
Skin and hair have the properties such as natural benefit, degradable absorbability, biocompatibility.
Allantoin is a kind of amphoteric compound, can combine many kinds of substance formed double salt, with lucifuge, sterilization and anticorrosion, analgesic,
Antioxidation, can make skin keep moisture content, moisten and soft, be the additive of the cosmetics such as cosmetology, use extensively
In adding for freckle cream, anti-acne toner, shampoo, perfumed soap, toothpaste, shaving lotion, hair nursing agent, astringent, the deodorant lotion of anti-sweat etc.
Plus agent, add the cosmetics of allantoin have protective tissue, it is hydrophilic, absorb water and the effect such as prevent moisture from distributing, add allantoin
Hair-cream, hair cream, shampoo etc. have protective effect to hair, can make hair not bifurcated, constantly fall, recover original elasticity and light
Pool.
Beeswax is four pairs of wax gland secretory substances below worker bee belly, and its main component has acids, free fatty, free fat
Fat alcohol and carbohydrate, beeswax have having been widely used in industrial or agricultural, in cosmetic formulation art, in many cosmetic products
All contain beeswax, such as bathing lotion, lipstick, kermes, it is trees fat liquefaction stone, is amorphous liquid, without fixed interior atoms
Structure and outer shape.
Plant carbon black and fruit of Cherokee rose palm fibre are natural colorant, and product safety is nonirritant to human body.
Glycerine has moistening effect；Sodium alginate hydrophily is strong, can be dissolved in cold water and warm water, is formed very sticky
Uniform solution, there are other analogs to be difficult to flexibility, homogeneity and other good characteristics for obtaining the true solution of formation,
Effect with very strong protecting colloid；Sorbierite also has good moistening effect.
Vitamin E is the general name of tocopherol and tocotrienol, is liposoluble vitamin, is the important composition on cell membrane
Composition, is also the primary anti-oxidant on cell membrane, and vitamin E is widely present in animals and plants food, is polyenoic fatty acid
Antioxidant, is combined into the structure of compound and stabilization film on cell membrane with the polyvalent unsaturated fatty acid of membrane phospholipid, prevents
The enzyme containing sulfenyl is damaged by oxidant in PUFA and cell on biomembrane.
Acrylic resin can form one layer and stick together firmly as the important component that film forming agent is mascara on surface, have
Certain flexibility, extensibility and elasticity, rub resistance, the uniform film of water resistance, make mascara have waterproof effect.
Preservative Tea Polyphenols is the general name of Polyphenols of Tea, including flavanol compound, anthocyanin class, flavonoids, Huang
Ketols and phenolic acid class etc., with antiseptic effect.
Compatibility of the present invention is reasonable, science, and each component cooperates, synergy, and the safe and stable property of formation is good and is difficult to swoon
The waterproof mascara of dye.
Compared with prior art, it is of the invention it is a technical advantage that：Stability more preferably, be difficult dizzy dye, uniform and be difficult
Come off and lump, source wide material sources, safety are adapted to eye decoration, and security is higher.
Specific embodiment
The present invention is described in further details below by specific embodiment, these embodiments are only used for the mesh of illustration
, it is in no way intended to limit protection scope of the present invention.
Alginate fibre producer：The sea blue biological products Co., Ltd in Qingdao.
Embodiment 1-3, comparative example 1-2
Table 1 lists the component and matter of the specific embodiment 1-3 and comparative example 1-2 of waterproof mascara provided by the present invention
Amount percentage.
The embodiment of table 1 and comparative example mascara component and mass percent
Comparative example 1 is with the difference of embodiment 2：Without allantoin, increase the content of alginate fibre.
Comparative example 2 is with the difference of embodiment 2：Without film forming agent, increase the content of beeswax.
The preparation method of the waterproof mascara of embodiment 1：
S1, the deionized water of 1.5 times of beeswax and its quality adds material-compound tank, be mixed and heated to 70 DEG C until obtaining
Prescribed liquid A, it is standby；
S2, alginate fibre, allantoin, colouring agent, NMF, vitamin E and remaining deionized water are added into another container
In be heated to 60 DEG C and be stirring evenly and then adding into film forming agent, stir to obtain B liquid；
S3, A the and B liquid for obtaining S1 and S2 mixing add emulsion tank, are cooled to room temperature, and the lower addition preservative of stirring is
.
The preparation method of the waterproof mascara of embodiment 2：
S1, the deionized water of 1.5 times of beeswax and its quality adds material-compound tank, be mixed and heated to 75 DEG C until obtaining
Prescribed liquid A, it is standby；
S2, alginate fibre, allantoin, colouring agent, NMF, vitamin E and remaining deionized water are added into another container
In be heated to 65 DEG C and be stirring evenly and then adding into film forming agent, stir to obtain B liquid；
S3, A the and B liquid for obtaining S1 and S2 mixing add emulsion tank, are cooled to room temperature, and the lower addition preservative of stirring is
.
The preparation method of the waterproof mascara of embodiment 3：
S1, the deionized water of 1.5 times of beeswax and its quality adds material-compound tank, be mixed and heated to 80 DEG C until obtaining
Prescribed liquid A, it is standby；
S2, alginate fibre, allantoin, colouring agent, NMF, vitamin E and remaining deionized water are added into another container
In be heated to 70 DEG C and be stirring evenly and then adding into film forming agent, stir to obtain B liquid；
S3, A the and B liquid for obtaining S1 and S2 mixing add emulsion tank, are cooled to room temperature, and the lower addition preservative of stirring is
.
The preparation method of comparative example 1-2 mascaras is similar to Example 2.
Properties of product evaluation test
Test example 1：Detection of Stability
In order to compare the stability of mascara prepared by above-described embodiment 1-3 and comparative example 1-2, each composition is according to temperature
Degree condition visually detects the stability in 5 DEG C, 36 DEG C, 45 DEG C and 50 DEG C respectively, and specific method is as follows：
S1, be respectively charged into the plastic containers of 50mL 20mL embodiment 1-3 and comparative example 1-2 mascara
Afterwards, observed 1 month after being placed on thermostat according to each temperature；
S2, evaluated in the following manner, if being separated without content, for very good, if separating layer is below 1mm,
Then it is difference if more than 2mm for general if 1~2mm for good.Testing result is as shown in table 2.
The embodiment of table 2 and comparative example mascara Detection of Stability result
As can be seen from Table 2, embodiment of the present invention 1-3 mascaras are more preferable compared with the stability of comparative example 1-2 mascaras.
Test example 2：Waterproofing tests
Subjects：The mascara prepared using embodiment 1-3 and comparative example 1-2 formulas.
Test method：Cut lock 0.7-1.2cm and be fixed into eyelashes shape, be fabricated to false eyelashes, by mascara application
Above, true usage scenario is simulated, after 3 hours, sprayed water to false eyelashes using spraying, make shower nozzle directly over sample, every 3 is small
When spray once, observe the dizzy dye situation of mascara, it is specific as shown in table 3.
The dizzy dye situation of the mascara of table 3
| Mascara | 3 hours | 6 hours | 9 hours | 12 hours |
| Embodiment 1 | Uniformly, without dizzy dye | Uniformly, without dizzy dye | Uniformly, without dizzy dye | Uniformly, without dizzy dye |
| Embodiment 2 | Uniformly, without dizzy dye | Uniformly, without dizzy dye | Uniformly, without dizzy dye | Uniformly, without dizzy dye |
| Embodiment 3 | Uniformly, without dizzy dye | Uniformly, without dizzy dye | Uniformly, without dizzy dye | Uniformly, without dizzy dye |
| Comparative example 1 | Uniformly, without dizzy dye | Uniformly, without dizzy dye | Uniformly, slightly dizzy dye | Slightly dizzy dye, fall off |
| Comparative example 2 | Uniformly, without dizzy dye | Uniformly, without dizzy dye | Slightly dizzy dye, lump, fall off | Slightly dizzy dye, lump, fall off |
From table 3 it is observed that embodiment of the present invention 1-3 is difficult dizzy dye, uniformly, and not compared to for comparative example 1-2
Easy to fall off and caking, is adapted to eye decoration, and security is higher.
The above is only the preferred embodiment of the present invention, it is noted that it is right that above-mentioned preferred embodiment is not construed as
Limitation of the invention, protection scope of the present invention should be defined by claim limited range.For the art
For those of ordinary skill, without departing from the spirit and scope of the present invention, some improvements and modifications can also be made, these change
Enter and retouch and also should be regarded as protection scope of the present invention.
Claims (7)
1. a kind of waterproof mascara, it is characterised in that including following components and its mass percent：
Alginate fibre 12~14%, allantoin 12~14%, beeswax 12~14%, colouring agent 12~14%, NMF 10~
14%th, vitamin E 7~9%, film forming agent 2~4%, preservative 1~3% and deionized water 14~32%.
2. waterproof mascara according to claim 1, it is characterised in that be made up of following components and its mass percent：
Alginate fibre 13%, allantoin 13%, beeswax 13%, colouring agent 13%, NMF 12%, vitamin E 8%, film forming agent
3%th, preservative 2% and deionized water 23%.
3. waterproof mascara according to claim 1 and 2, it is characterised in that described colouring agent is by plant carbon black and gold
Cherry palm fibre in mass ratio 2:3 compositions.
4. waterproof mascara according to claim 1 and 2, it is characterised in that described NMF is by glycerine, sodium alginate
With sorbierite in mass ratio 2:3:5 compositions.
5. waterproof mascara according to claim 1 and 2, it is characterised in that described film forming agent is acrylic resin.
6. waterproof mascara according to claim 1 and 2, it is characterised in that described preservative is Tea Polyphenols.
7. the preparation method of the waterproof mascara according to claim any one of 1-6, it is characterised in that including following step
Suddenly：
S1, the deionized water of 1.5 times of beeswax and its quality adds material-compound tank, be mixed and heated to 70-80 DEG C until obtaining
Prescribed liquid A, it is standby；
S2, alginate fibre, allantoin, colouring agent, NMF, vitamin E and remaining deionized water are added in another container plus
Heat is to 60-70 DEG C and is stirring evenly and then adding into film forming agent, and stir to obtain B liquid；
S3, A the and B liquid for obtaining S1 and S2 mixing add emulsion tank, are cooled to room temperature, and stirring is lower to add preservative to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611230207.3A CN106821840A (en) | 2016-12-27 | 2016-12-27 | A kind of waterproof mascara and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611230207.3A CN106821840A (en) | 2016-12-27 | 2016-12-27 | A kind of waterproof mascara and preparation method thereof |
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| CN106821840A true CN106821840A (en) | 2017-06-13 |
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| CN201611230207.3A Withdrawn CN106821840A (en) | 2016-12-27 | 2016-12-27 | A kind of waterproof mascara and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107982072A (en) * | 2017-12-14 | 2018-05-04 | 广州联锴粉体科技有限公司 | The water-based eye-liner and preparation method of a kind of graphene-containing |
| CN109431931A (en) * | 2018-11-26 | 2019-03-08 | 陈晓霞 | A kind of water-resistance mascara formulation with growth effect |
| CN113116746A (en) * | 2019-12-31 | 2021-07-16 | 新生活化妆品科技(上海)有限公司 | Composition for preparing mascara, mascara and method for lengthening hair |
| CN114845779A (en) * | 2019-12-26 | 2022-08-02 | 欧莱雅 | Mascara based on polyphenols and film-forming polymers and method for making up eyelashes |
-
2016
- 2016-12-27 CN CN201611230207.3A patent/CN106821840A/en not_active Withdrawn
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107982072A (en) * | 2017-12-14 | 2018-05-04 | 广州联锴粉体科技有限公司 | The water-based eye-liner and preparation method of a kind of graphene-containing |
| CN109431931A (en) * | 2018-11-26 | 2019-03-08 | 陈晓霞 | A kind of water-resistance mascara formulation with growth effect |
| CN114845779A (en) * | 2019-12-26 | 2022-08-02 | 欧莱雅 | Mascara based on polyphenols and film-forming polymers and method for making up eyelashes |
| CN113116746A (en) * | 2019-12-31 | 2021-07-16 | 新生活化妆品科技(上海)有限公司 | Composition for preparing mascara, mascara and method for lengthening hair |
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Application publication date: 20170613 |