CN107982072A - The water-based eye-liner and preparation method of a kind of graphene-containing - Google Patents
The water-based eye-liner and preparation method of a kind of graphene-containing Download PDFInfo
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- CN107982072A CN107982072A CN201711333697.4A CN201711333697A CN107982072A CN 107982072 A CN107982072 A CN 107982072A CN 201711333697 A CN201711333697 A CN 201711333697A CN 107982072 A CN107982072 A CN 107982072A
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- Prior art keywords
- graphene
- water
- liner
- eye
- based eye
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/10—Preparations containing skin colorants, e.g. pigments for eyes, e.g. eyeliner, mascara
Abstract
Water-based eye-liner the invention discloses a kind of graphene-containing and preparation method thereof, the eye-liner are by deionized water, graphene slurry, film forming agent, colouring agent, suspending agent, moisturizer, preservative composition, its preparation method：Deionized water is heated to 85 95 DEG C, after keeping the temperature 4 6min；Graphene is starched, colouring agent, suspending agent, moisturizer are added in deionized water and are uniformly mixed, with 6000 10000rpm, 3 5min of homogeneous；Stirring is cooled to 45 50 DEG C, adds film forming agent and is uniformly mixed；Stirring is cooled to 35 40 DEG C, adds preservative, with 600 1000rpm, discharges after stirring 4 6min.This informer's cosmetics is in mucus shape, has the advantages of water-proofing time is longer, argenteous luster effect, skin surface adhesiveness is good.
Description
Technical field
The present invention relates to cosmetic field, and in particular to a kind of eye-liner and preparation method thereof.
Background technology
Informer's cosmetics are to be applied to eyelid lower edge, vertically eyelashes root, and the beauty and make-up drawn is retouched from canthus to eye tail
Product.Informer's cosmetics can protrude and strengthen the glamour of eyes, and commercially available informer's cosmetics can be divided into solid-state and liquid from the appearance
Two classes, can be divided into water-based and two kinds of oiliness from formulation, wherein water-based eye-liner is informer's makeup that applicability is most wide on the market
One of product, have the characteristics that easy to use.
Japan Patent JP2016041674A discloses a kind of eye-liner, and the eye-liner is by acrylic acid esters co-polymer breast
20-40 parts of liquid, 0-1 parts of suspending agent, 1-10 parts of moisturizer, 5-20 parts of colouring agent, Preservative qs, deionized water surplus composition.
French Patent (FRP) FR2832058A1 discloses a kind of film forming polymer, and the film forming polymer is used for eye-liner, and eye-liner composition is
15-40 parts of Acrylate copolymerical emulsion, 0.1-2 parts of suspending agent, 1-20 parts of colouring agent, 10-30 parts of moisturizer, preservative is fitted
Amount, deionized water surplus.According to two above patent：Traditional water-based eye-liner film-formation result depends on esters of acrylic acid
Copolymer emulsion, the membrane formation mechanism of Acrylate copolymerical emulsion are the water evaporations in lotion, and acrylic acid esters co-polymer divides
Sub constantly formation epithelium close to each other, is water soluble polymer yet with acrylic acid esters co-polymer, meets in daily life
It can again be dissolved in the water during to sweat, tear or rainwater, destroy epithelium, so it is the water-based eye-liner of tradition that water-proofing time is short
One of drawback.
Graphene is stripped out from graphite material, the two-dimensional sheet for the only one layer of atomic thickness being made of carbon atom
Structural material, includes 3,000,000 layer graphenes in the graphite of thick 1mm, is to have now been found that most thin, most tough material.Shi Lifang etc.
People has found that graphene oxide can improve the adhesion property of nano silver wire, and the synergistic effect of the two can show laminated film
The characteristics of transparency is high, anti-Escherichia coli performance is good, and develop a kind of LB embrane methods to prepare graphene oxide-silver micro wire compound
Transparent Antibiotic Membrane.Using the laminated structure feature of graphene, tested by adding graphene in informer's formula of liquid, as a result
It was found that graphene can effectively improve the water resistance of eye-liner, extend the adornment effect time, have for developing water-based eye-liner
Important value.
The content of the invention
For the problems of above-mentioned prior art, it is an object of the present invention to provide a kind of water of graphene-containing
Property informer's formula of liquid；The second purpose is to provide a kind of preparation method of the graphene eye-liner, when preparing a kind of waterproof with this
Between longer water-based eye-liner.
In order to achieve the above object, this programme adopts the following technical scheme that.
For purpose 1：A kind of water-based eye-liner of graphene-containing is provided, the eye-liner includes the group of following parts by weight
Point：
Graphene starches 5-30 parts；
10-35 parts of film forming agent；
0-20 parts of colouring agent；
1-10 parts of moisturizer；
0.1-3 parts of suspending agent；
0.05-1 parts of preservative；
Deionized water surplus.
In the water-based eye-liner preferred solution of above-mentioned graphene-containing, the graphene slurry composition is graphene 0.1-5%, is gathered
Glyceral methacrylate 5-25%, propane diols 5-25%, wherein deionized water 60-90%, graphene are appearance dark gray powder,
Slice plane size is 5-15 μm, lamellar spacing average out to 2-3nm, pH value 6-7, metal ion total content ＜ 20ppm.
In the water-based eye-liner preferred solution of above-mentioned graphene-containing, the film forming agent is acrylic acid esters co-polymer, gathers
Mixture more than one or both of vinylpyrrolidone, vinyl pyrrolidone/vinyl acetate copolymer.
In the water-based eye-liner preferred solution of above-mentioned graphene-containing, the colouring agent is carbon black, in iron oxide black
One or more kinds of mixtures, the wherein composition of carbon black are carbon black 25-35%, hydroxyethyl cellulose 0-1%, acrylate
Analog copolymer 0-5%, Phenoxyethanol 0-1%, pungent glycol 0-10%, deionized water 40-70%.Wherein iron oxide black is appearance black powder
End, 325 mesh screen residues are less than 0.50%, relative color strength 95.0-105.0, aberration △ E ＜ 1%, Fe3O4Content ＞ 96% is dry to lose
Weight ＜ 1%, soluble matter is less than 0.5% in water, and insoluble matter ＜ 0.3% in acid, heavy metal and content of microorganisms meet 2015 cosmetics peace
Full technical specification.
In the water-based eye-liner preferred solution of above-mentioned graphene-containing, the moisturizer is propane diols, glycerine, 1,3- fourths two
Mixture more than one or both of alcohol, sorbierite, mannitol.
In the water-based eye-liner preferred solution of above-mentioned graphene-containing, the suspending agent is Magnesiumaluminumsilicate, bentonite, silicon
Mixture more than one or both of stone, hectorite, xanthans.
In the water-based eye-liner preferred solution of above-mentioned graphene-containing, the preservative for Phenoxyethanol, pentanediol, oneself two
The mixture of one or both of alcohol, methyl hydroxybenzoate.
For purpose 2：A kind of preparation method of the water-based eye-liner of graphene-containing is provided, this method comprises the following steps：
（1）Deionized water is heated to 85-95 DEG C, keeps the temperature 4-6min；
（2）Graphene is starched, colouring agent, suspending agent, moisturizer be added in deionized water be uniformly mixed, with 6000-
10000rpm, homogeneous 3-5min；
（3）Material stirring is cooled to 45-50 DEG C, film forming agent is added and stirs evenly；
（4）Material stirring is cooled to 35-40 DEG C, adds preservative with 600-1000rpm, after stirring 4-6min, discharging；
（5）Gained mixed material is carried out filling.
Informer's cosmetics that this programme is formed accordingly are in mucus shape, have the advantages that water-proofing time is longer.
Embodiment
In order to make the technical means, the creative features, the aims and the efficiencies achieved by the present invention easy to understand, tie below
Instantiation is closed, the present invention is further explained.It is to be understood that these embodiments are merely to illustrate the present invention rather than limit this hair
Bright scope.
Unless otherwise defined or described herein, all professional and scientific terms used herein and the skilled people of art technology
Meaning known to member is identical.In addition any method similar or impartial to described content and material all can be applied to the present invention
In method.
Embodiment
The water-based following of eye-liner specific formula of this example
。
Graphene slurry in the present embodiment, wherein graphene slurry composition is graphene 5%, polyglycerolmethacrylate
10%, propane diols 10%, deionized water 75%.
Film forming agent in the present embodiment is polyvinylpyrrolidone, acrylic acid esters co-polymer.
Colouring agent in the present embodiment is carbon black, and the wherein composition of carbon black is carbon black 35%, hydroxyethyl cellulose
0.5%, acrylic acid esters co-polymer 1%, Phenoxyethanol 0.5%, pungent glycol 1%, deionized water 62%.
Moisturizer in the present embodiment is 1,3-BDO.
Suspending agent in the present embodiment is bentonite.
Preservative in the present embodiment is Phenoxyethanol.
Based on above-mentioned each raw material, the water-based eye-liner of the graphene-containing in embodiment is prepared by following steps：
（1）Deionized water is heated to 90 DEG C, keeps the temperature 5min；
（2）Graphene is starched, colouring agent, suspending agent, moisturizer be added in deionized water be uniformly mixed, with 8000rpm/s's
Speed homogeneous 4min obtains mixed material；
（3）Mixed material stirring is cooled to 50 DEG C, film forming agent is added and stirs evenly；
（4）Mixed material stirring is cooled to 40 DEG C, after adding preservative with the speed stirring 5min of 800rpm/s, discharging；
（5）Gained mixed material is carried out filling.
Waterproofing tests.
The eye-liner of different formulations prepared by above example is used for the female consumer of 10 20-30 Sui, small by 4
When, 8 it is small when, 16 it is small when, 24 it is small when, test influence of the different graphene additive amounts to eye-liner water resistance respectively.Commented
After estimating, 1-5 points are provided, and the scoring to 10 female consumers calculates average mark.Wherein standards of grading are：5：It is outstanding, 4：It is good
It is good, 3：It is medium, 2：It is poor, 1：It is very poor.Average score is the average value of 10 tester's every batch of test results, comprehensive grading four
The average value of wheel test average score.
Water-proofing time test evaluation table：
。
The above results show that the water-based eye-liner of the graphene-containing obtained by embodiment is water-based with the increase of graphene amount
The waterproof effect and water-proofing time of eye-liner have a certain upgrade, and with the extension of real testing time, graphene is to eye-liner
Waterproof effect castering action is more notable.For the contrast test of two kinds of film forming agents, graphene prevents polyvinylpyrrolidone
The lifting of water effect is more obvious, and for common acrylic acid esters co-polymer film forming agent, graphene is more suitable for poly-
Eye-liner of the vinylpyrrolidone as film forming agent.
In addition, this programme has also been observed that following beneficial effect in testing：The water of the graphene-containing formed according to this programme
Property eye-liner can show silvery white reflecting feel coated in skin surface, more embody the unique charm of this product.
Therefore, graphene-containing eye-liner scheme provided by the invention not only improves technical problem existing for existing product,
The usage time of eye-liner is effectively extended, there is great market value.
Basic principle, main feature and the advantages of the present invention of the present invention has been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (8)
1. the water-based eye-liner of a kind of graphene-containing, it is characterised in that the eye-liner includes the component of following mass parts：
Graphene starches 5-30 parts；
10-35 parts of film forming agent；
0-20 parts of colouring agent；
1-10 parts of moisturizer；
0.1-3 parts of suspending agent；
0.05-1 parts of preservative；
Deionized water surplus.
A kind of 2. water-based eye-liner of graphene-containing according to claim 1, it is characterised in that the graphene slurry composition
For graphene 0.1-5%, polyglycerolmethacrylate 5-25%, propane diols 5-25%, wherein deionized water 60-90%, graphene
For appearance dark gray powder, slice plane size is 5-15 μm, lamellar spacing average out to 2-3nm, pH value 6-7, metal ion
Total content ＜ 20ppm.
3. the water-based eye-liner of a kind of graphene-containing according to claim 1, it is characterised in that the film forming agent is third
Mixture more than one or both of olefin(e) acid lipin polymer, polyvinylpyrrolidone, polyvinylpyrrolidone derivative.
4. the water-based eye-liner of a kind of graphene-containing according to claim 1, it is characterised in that the colouring agent is charcoal
Mixture more than one or both of black wash, iron oxide black, the wherein composition of carbon black are carbon black 25-35%, and ethoxy is fine
Element 0-1%, acrylic acid esters co-polymer 0-5%, Phenoxyethanol 0-1%, pungent glycol 0-10%, deionized water 40-70% are tieed up,
Wherein iron oxide black is appearance black powder, and 325 mesh screen residues are less than 0.50%, relative color strength 95.0-105.0, aberration
△ E ＜ 1%, Fe3O4Content ＞ 96%, loss on drying ＜ 1%, soluble matter is less than 0.5% in water, insoluble matter ＜ 0.3% in acid, heavy metal
Meet 2015 cosmetics safety technical specifications with content of microorganisms.
5. the water-based eye-liner of a kind of graphene-containing according to claim 1, it is characterised in that the moisturizer is third
Mixture more than one or both of glycol, glycerine, 1,3 butylene glycol, sorbierite, mannitol.
6. the water-based eye-liner of a kind of graphene-containing according to claim 1, it is characterised in that the suspending agent is silicon
Mixture more than one or both of sour magnalium, bentonite, silica, hectorite, xanthans.
7. the water-based eye-liner of a kind of graphene-containing according to claim 1, it is characterised in that the preservative is benzene
Mixture more than one or both of oxyethanol, pentanediol, hexylene glycol, methyl hydroxybenzoate.
8. the preparation method of the water-based eye-liner of a kind of graphene-containing, it is characterised in that the preparation method comprises the following steps：
（1）Deionized water is heated to 85-95 DEG C, keeps the temperature 4-6min；
（2）Graphene is starched, colouring agent, suspending agent, moisturizer be added in deionized water be uniformly mixed, with 6000-
10000rpm, homogeneous 3-5min；
（3）Material stirring is cooled to 45-50 DEG C, film forming agent is added and stirs evenly；
（4）Material stirring is cooled to 35-40 DEG C, adds preservative with 600-1000rpm, after stirring 4-6min, discharging；
（5）Gained mixed material is carried out filling.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711333697.4A CN107982072A (en) | 2017-12-14 | 2017-12-14 | The water-based eye-liner and preparation method of a kind of graphene-containing |
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| CN201711333697.4A CN107982072A (en) | 2017-12-14 | 2017-12-14 | The water-based eye-liner and preparation method of a kind of graphene-containing |
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| CN201711333697.4A Pending CN107982072A (en) | 2017-12-14 | 2017-12-14 | The water-based eye-liner and preparation method of a kind of graphene-containing |
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Cited By (4)
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| CN108852864A (en) * | 2018-07-04 | 2018-11-23 | 齐鲁工业大学 | A kind of graphene-silk-fibroin composite material and preparation method and application |
| IT201800005481A1 (en) * | 2018-05-17 | 2019-11-17 | Non-permanent compositions based on graphene for the coloring and strengthening treatment of the hair | |
| IT201800006990A1 (en) * | 2018-07-06 | 2020-01-06 | Multi-active compositions in long-lasting antiaging make-up containing graphene | |
| CN111870563A (en) * | 2020-08-17 | 2020-11-03 | 宁波爱诗化妆品有限公司 | Pearlescent eyeliner liquid and preparation method thereof |
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Application publication date: 20180504 |