CN107184504A - A kind of natural lip gloss of fragrance type and preparation method thereof - Google Patents
A kind of natural lip gloss of fragrance type and preparation method thereof Download PDFInfo
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- CN107184504A CN107184504A CN201710315128.0A CN201710315128A CN107184504A CN 107184504 A CN107184504 A CN 107184504A CN 201710315128 A CN201710315128 A CN 201710315128A CN 107184504 A CN107184504 A CN 107184504A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The present invention relates to cosmetic field, natural lip gloss of a kind of fragrance type and preparation method thereof is disclosed.In terms of every 100g, lip gloss formula is as follows:The 12g of beeswax 8, the 9g of candelila wax 5, the 7g of Chiba rose wax 3, the 22g of aloe resin 18, the 12g of chamomile fat 8, the 10g of saualane 6, the 25g of coconut oil 21, the 6g of Sweet Almond Oil 2, the 10g of grape-kernel oil 7, Asian puccoon the immersion 6g of olive oil 2, the 6g of marine alga wet gel 4, the 2g of bletilla striata extract 1;In addition, in the above-mentioned formulas of every 100g, being separately added with the 6mL of plants essential oil 1.The lip gloss of the present invention uses natural component, does not contain preservative, artificial color and artificial flavors, mildness is good, and small, nonhazardous is stimulated to human body skin.In addition lip gloss gas permeability of the invention, lubricity are good, and with permanent natural fragrance.
Description
Technical field
The present invention relates to cosmetic field, more particularly to a kind of natural lip gloss of fragrance type and preparation method thereof.
Background technology
Dry changeable in autumn and winter, lip is particularly easy to drying, and lip is easily broken, bleeding.The master of lip gloss
It is to pin lip moisture to act on, and prevents lip water shortage and ftractures.The main component of lip gloss be vaseline, wax and other
Oil substances.The species of lip gloss is multifarious on the market at present, and the feature of lip gloss is also enriched, such as has
Different color, which plays beautification function, distribute fragrance plays fragrant atmosphere effect etc..In order that lip gloss has above-mentioned functions, many profit lips
Various chemical compositions, such as artificial color, artificial flavors, preservative etc. are added with cream.And because lip gloss is to be applied to mouth
Lip, its particularity for smearing position determines that it must have human safety.Found by research, apply a lip gloss,
Probably there is 70% to fall into branch's " being eaten ".Therefore the lip gloss containing a large amount of chemical compositions can bring some pairs to make to human body
With.
Although in addition, existing lip gloss can play water lock function, after its main matter is wax and grease, smearing
A tunic is formed on lip, this tunic is more greasy, its gas permeability is poor, be unfavorable for skin of lip and breathed, can influenceed
The secreting function of skin of lip sebaceous glands, in the course of time, can cause lip skin more and more dry, thus lip gloss is caused according to
Rely.
The content of the invention
In order to solve the above-mentioned technical problem, the invention provides natural lip gloss of a kind of fragrance type and preparation method thereof.This
The lip gloss of invention uses natural component, does not contain preservative, artificial color and artificial flavors, and mildness is good, to human body skin
Stimulate small, nonhazardous.In addition lip gloss gas permeability of the invention, lubricity are good, and with permanent natural fragrance.
The present invention concrete technical scheme be:A kind of natural lip gloss of fragrance type, in terms of every 100g, is formulated as follows:Beeswax
8-12g, candelila wax 5-9g, Chiba rose wax 3-7g, aloe resin 18-22g, chamomile fat 8-12g, saualane 6-10g, coconut
Oily 21-25g, Sweet Almond Oil 2-6g, grape-kernel oil 7-10g, Asian puccoon immersion olive oil 2-6g, marine alga wet gel 4-6g, the bletilla striata carry
Take thing 1-2g;In addition, in the above-mentioned formulas of every 100g, being separately added with plants essential oil 1-6mL.
It is of the invention all to use natural component, it is safe.Using the coconut palm itself with bacteria resistance function in inventive formulation
Seed oil, saualane, Asian puccoon immersion oil and plants essential oil, without addition preservative, artificial color and spices in addition.Wherein, spiny dogfish
Alkane, which has, presses down mycostatic property, and with the function of lubrication, makes the sense of touch non-greasy of product;Coconut oil also has antibacterial work(
Effect;Asian puccoon has effects that anti-inflammatory, antibacterial, and Asian puccoon per se with pigment, and the depth of lipstick color can be used to regulation;Plant
Essential oil has certain biocidal efficacies in itself, and its unique fragrance can assign natural fragrance for lipstick.
The lipstick formula of the present invention defines particularly the ratio between oil, fat, wax three, makes lotion neither too hard, nor too soft, has
It while soft and moist sense, will not feel greasy, lotion is easy to fracture.The composition of wax uses beeswax, candelila wax, Chiba
Oleoptene compounding is formed:Wherein the heat-resistant stability of candelila wax preferably, and with preferable glossiness, is resistant to lipstick
The change of temperature and the appearance slided with silk;Chiba rose wax comes from the natural wax component contained by Chiba rose, can slowly release
Contained rose fragrance is put, increases light fragrance to lipstick.
Marine alga wet gel and bletilla striata extract are also added with the lipstick of the present invention, wherein marine alga wet gel is natural seaweed
Extract, with stickiness, good film-forming property, gas permeability are good after smearing, with water conservation, crease-resistant, inhibiting bacteria and diminishing inflammation effect, and its is right in addition
The sense of touch of skin is refrigerant smooth, can alleviate the greasy feeling of wax and grease to skin.Bletilla striata extract is more gentle to skin, parent
Skin is good, good to percutaneous permeability, it is easy to film forming, can play moisturizing, prevent allergic effect.
Preferably, the plants essential oil is selected from least one of Rosa Damascana, sweet orange oil, lemon grass (Cymbopogon citratus) essential oil.
Preferably, the plants essential oil is 9.99wt% Rosa Damascana, the consumption of the Rosa Damascana is 1mL/
100g。
Because Asian puccoon is per se with pigment, the depth of lipstick color can be used to regulation, when lipstick is rose lipstick, rose
Rare lipstick is pink, therefore Asian puccoon immersion oil content is slightly more.
Preferably, the plants essential oil is sweet orange oil and lemon grass (Cymbopogon citratus) essential oil, the consumption of the sweet orange oil is 5mL/
100g, the consumption of the lemon grass (Cymbopogon citratus) essential oil is 1mL/100g.
Grapefruit lipstick is composited with sweet orange oil and lemon grass (Cymbopogon citratus) essential oil, it is shown grapefruit sweet tea and pure and fresh sensation.
When lipstick be grapefruit lipstick when, grapefruit lipstick for it is pink with it is orange between, therefore Asian puccoon soak oil content it is lower slightly, the essential oil of yellow contains
Amount is slightly more.
Preferably, oil, fat, the ratio of wax are controlled 48: 29-31: 21-23 in the formula.
The content of oil, fat, wax three are further limited to aforementioned proportion, soft or hard the most moderate, the tool of lotion by the present invention
It while having soft and moist sense, will not feel greasy, lotion is easy to fracture.
Preferably, the marine alga wet gel is by pretreatment:It is 55- by the solid content control of marine alga wet gel
75wt%, the sodium bicarbonate that quality is marine alga wet gel 1-3% is added under 5-15 DEG C, 100-200r/min stirring condition makes it
It is uniformly dispersed;Then under 400-600r/min stirring condition, 65-75 DEG C is warming up to 4-6 DEG C/min speed, is then dropped
Obtain mixing alveolate marine alga wet gel after to room temperature;Finally marine alga wet gel is replaced under the conditions of vacuum decompression with absolute ethyl alcohol
Gas in bubble, the marine alga wet gel pre-processed.
In order to further improve the gas permeability after lipstick is smeared, the present invention is pre-processed to marine alga wet gel, located in advance
During reason, appropriate sodium bicarbonate is first added under certain temperature and stir speed (S.S.), sodium bicarbonate is dissolved in after water, is gradually heated up, and together
Shi Tigao stir speed (S.S.)s, after temperature rises to more than 20 DEG C, sodium bicarbonate starts to decompose, generation sodium carbonate and carbon dioxide, in play
Under strong stirring, the carbon dioxide of generation and the air of portion of external are wrapped in marine alga wet gel, form substantial amounts of capillary
Bubble, stir speed (S.S.) needs strict control, could form the bubble of " capillary ".Then marine alga wet gel is positioned over vacuum decompression
Under the conditions of, due to the inside and outside pressure difference of bubble, bubbles burst, gas is escaped, now using absolute ethyl alcohol to the gas in bubble
Enter line replacement, to fill the space in bubble.The reason for using absolute ethyl alcohol is:1st, marine alga gel is not dissolved in ethanol, and second
Alcohol wellability is good, therefore ethanol can be quickly penetrated into inside bubble and is locked in bubble.2nd, ethanol is to skin nonhazardous,
Security is good, and cheap.3rd, ethanol is volatile, and when lipstick is not smeared, ethanol is locked in bubble, when lipstick is smeared
Afterwards, become big suddenly with the contact surface of air, rapid volatilization, ethanol volatilization, after being partly absorbed by the skin, also with bactericidal properties and profit
Skin is acted on, and heat absorption brings refrigerant sense during ethanol volatilization, alleviates greasy feeling.Released in space after ethanol volatilization simultaneously in bubble
Put, therefore lipstick is smeared and leaves a large amount of capillary porosities in film layer after film forming, adds the gas permeability of film layer, is conducive to Skin Cell
Breathing, the greasy feeling that film layer is brought can be made up.
Preferably, the coconut oil, Sweet Almond Oil, grape-kernel oil, Asian puccoon soak olive oil respectively through modification:
Oily substance is added to thermal dehydration in autoclave, catalyst is first added, then is passed through hydrogen, in hydrogen pressure 0.5-
0.7MPa, 100-110 DEG C, react filtering and impurity removing after 20-40min, reaction under 600-800r/min stirring conditions, obtain modified
Oily substance.
During the preservation of lipstick, oily substance fusing point is relatively low, at relatively high temperatures, the knot of wax and grease in lipstick
Poor with joint efforts, grease is readily permeable to lipstick surface after long-time, sweating phenomenon occurs, and sweating phenomenon has had a strong impact on lipstick
Use, lose the lotion ductility after grease and be affected, lotion is more stiff, it is difficult after showing as not easy to apply and smearing
Film forming.In addition, vegetable fat after storage for a long period easily occur aoxidize, become sour, it is smelly, influence lipstick normally use.This
Invention be directed to above-mentioned technical problem, processing is modified to oily substance, the present invention modification after, oily substance melt
Point has obtained appropriate raising, and its oxidation resistance is also improved, therefore lipstick is difficult sweating during long-term live forever
With it is rotten.Need strictly to control modification degree in modifying process, if modified excessive, oily substance fusing point is too high, in liquid
Oily substance can change into softer pasty masses at normal temperatures, can also influence the quality of lipstick, therefore the strict control of the present invention
Modified condition processed, simply carries out slight modification to it.
A kind of preparation method of the natural lip gloss of fragrance type, comprises the following steps:
(1) by beeswax, candelila wax, Chiba rose wax, aloe resin, chamomile fat, saualane, coconut oil, Sweet Almond Oil, grape
Seed oil and Asian puccoon immersion olive oil progress are mixed and heated to 70-80 DEG C and stirred, and obtain oil-based liquid;
(2) marine alga wet gel, bletilla striata extract and plants essential oil be mixed and stirred for uniformly, obtaining mixing wet gel;
(3) oil-based liquid is cooled, in cooling, adds mixing wet gel, stir;Liquid is finally transferred to mould
Cooled and solidified in tool, the natural lip gloss of fragrance type is made after shaping.
It is well known that plants essential oil highly volatile, after long-term preservation process, the sweet of lipstick can gradually weaken, this
Invention is specially mixed plants essential oil with marine alga wet gel in preparation process, and plants essential oil is wet solidifying by marine alga after mixing
Glue is wrapped up, therefore plants essential oil is not volatile, can just be waved rapidly after becoming greatly suddenly with the contact area of air only after smearing
Hair.
Preferably, in step (3), when being cooled to 55-60 DEG C, addition mixing wet gel.
It is compared with the prior art, the beneficial effects of the invention are as follows:The lip gloss of the present invention uses natural component, does not contain anti-
Rotten agent, artificial color and artificial flavors, mildness are good, and small, nonhazardous is stimulated to human body skin.In addition lip gloss of the invention is saturating
Gas, lubricity are good, and with permanent natural fragrance.
Embodiment
With reference to embodiment, the invention will be further described.
Embodiment 1
A kind of natural lip gloss of fragrance type (rose lip gloss), is formulated as follows:Beeswax 9.5g, candelila wax 6.5g, Chiba rose
Wax 4.5g, aloe resin 19g, chamomile fat 9g, saualane 7.5g, coconut oil 22g, Sweet Almond Oil 3.4g, grape-kernel oil 7g, Asian puccoon
Soak olive oil 5g, marine alga wet gel 5g, bletilla striata extract 1.5g, 9.99wt% Rosa Damascana 1mL.
The preparation method of the above-mentioned natural lip gloss of fragrance type, comprises the following steps:
(1) by beeswax, candelila wax, Chiba rose wax, aloe resin, chamomile fat, saualane, coconut oil, Sweet Almond Oil, grape
Seed oil and Asian puccoon immersion olive oil progress are mixed and heated to 75 DEG C and stirred, and obtain oil-based liquid;
(2) marine alga wet gel, bletilla striata extract and plants essential oil be mixed and stirred for uniformly, obtaining mixing wet gel;
(3) oil-based liquid is cooled, when being cooled to 58 DEG C, adds mixing wet gel, stir;Finally liquid is turned
Move in mould and cooled and solidified, the natural lip gloss of fragrance type is made after shaping.
Embodiment 2
A kind of natural lip gloss of fragrance type (rose lip gloss), is formulated as follows:Beeswax 9.5g, candelila wax 6.5g, Chiba rose
Wax 4.5g, aloe resin 19g, chamomile fat 9g, saualane 7.5g, coconut oil 22g, Sweet Almond Oil 3.4g, grape-kernel oil 7g, Asian puccoon
Soak olive oil 5g, marine alga wet gel 5g, bletilla striata extract 1.5g, 9.99wt% Rosa Damascana 1mL.
The marine alga wet gel is by pretreatment:Be 65wt% by the control of the solid content of marine alga wet gel, 10 DEG C,
Quality is added under 150r/min stirring condition makes it be uniformly dispersed for the sodium bicarbonate of marine alga wet gel 2%;Then in 500r/
Under min stirring condition, 70 DEG C are warming up to 5 DEG C/min speed, be then down to after room temperature obtain mix alveolate marine alga it is wet
Gel;It is last to replace the gas in marine alga wet gel bubble, the sea pre-processed with absolute ethyl alcohol under the conditions of vacuum decompression
Algae wet gel.
The coconut oil, Sweet Almond Oil, grape-kernel oil, Asian puccoon soak olive oil respectively through modification:By oils thing
Matter is added to thermal dehydration in autoclave, first adds metallic catalyst, then is passed through hydrogen, in hydrogen pressure 0.6MPa, 105
DEG C, react filtering and impurity removing after 30min, reaction under 700r/min stirring conditions, obtain modified oily substance.
The preparation method of the above-mentioned natural lip gloss of fragrance type, comprises the following steps:
(1) by beeswax, candelila wax, Chiba rose wax, aloe resin, chamomile fat, saualane, coconut oil, Sweet Almond Oil, grape
Seed oil and Asian puccoon immersion olive oil progress are mixed and heated to 75 DEG C and stirred, and obtain oil-based liquid;
(2) marine alga wet gel, bletilla striata extract and plants essential oil be mixed and stirred for uniformly, obtaining mixing wet gel;
(3) oil-based liquid is cooled, when being cooled to 58 DEG C, adds mixing wet gel, stir;Finally liquid is turned
Move in mould and cooled and solidified, the natural lip gloss of fragrance type is made after shaping.
Embodiment 3
A kind of natural lip gloss of fragrance type (grapefruit lip gloss), is formulated as follows:Beeswax 9.5g, candelila wax 6.5g, Chiba rose
Wax 4.5g, aloe resin 19g, chamomile fat 9g, saualane 7.5g, coconut oil 22g, Sweet Almond Oil 4g, grape-kernel oil 8.5g, Asian puccoon
Soak olive oil 3g, marine alga wet gel 5g, bletilla striata extract 1.5g, sweet orange oil 5mL, lemon grass (Cymbopogon citratus) essential oil 1mL.
The preparation method of the above-mentioned natural lip gloss of fragrance type, comprises the following steps:
(1) by beeswax, candelila wax, Chiba rose wax, aloe resin, chamomile fat, saualane, coconut oil, Sweet Almond Oil, grape
Seed oil and Asian puccoon immersion olive oil progress are mixed and heated to 75 DEG C and stirred, and obtain oil-based liquid;
(2) marine alga wet gel, bletilla striata extract and plants essential oil be mixed and stirred for uniformly, obtaining mixing wet gel;
(3) oil-based liquid is cooled, when being cooled to 58 DEG C, adds mixing wet gel, stir;Finally liquid is turned
Move in mould and cooled and solidified, the natural lip gloss of fragrance type is made after shaping.
Embodiment 4
A kind of natural lip gloss of fragrance type (grapefruit lip gloss), is formulated as follows:Beeswax 9.5g, candelila wax 6.5g, Chiba rose
Wax 4.5g, aloe resin 19g, chamomile fat 9g, saualane 7.5g, coconut oil 22g, Sweet Almond Oil 4g, grape-kernel oil 8.5g, Asian puccoon
Soak olive oil 3g, marine alga wet gel 5g, bletilla striata extract 1.5g, sweet orange oil 5mL, lemon grass (Cymbopogon citratus) essential oil 1mL.
The marine alga wet gel is by pretreatment:It is 55wt% by the solid content control of marine alga wet gel, in 5 DEG C, 200r/
Quality is added under min stirring condition makes it be uniformly dispersed for the sodium bicarbonate of marine alga wet gel 1%;Then stirring in 600r/min
Under the conditions of mixing, 65 DEG C are warming up to 4 DEG C/min speed, is then down to after room temperature and obtains mixing alveolate marine alga wet gel;Most
Gas in replacing marine alga wet gel bubble with absolute ethyl alcohol under the conditions of vacuum decompression afterwards, the marine alga pre-processed is wet solidifying
Glue.
The coconut oil, Sweet Almond Oil, grape-kernel oil, Asian puccoon soak olive oil respectively through modification:By oils thing
Matter is added to thermal dehydration in autoclave, first adds metallic catalyst, then is passed through hydrogen, in hydrogen pressure 0.5MPa, 110
DEG C, react filtering and impurity removing after 20min, reaction under 600r/min stirring conditions, obtain modified oily substance.
The preparation method of the above-mentioned natural lip gloss of fragrance type, comprises the following steps:
(1) by beeswax, candelila wax, Chiba rose wax, aloe resin, chamomile fat, saualane, coconut oil, Sweet Almond Oil, grape
Seed oil and Asian puccoon immersion olive oil progress are mixed and heated to 75 DEG C and stirred, and obtain oil-based liquid;
(2) marine alga wet gel, bletilla striata extract and plants essential oil be mixed and stirred for uniformly, obtaining mixing wet gel;
(3) oil-based liquid is cooled, when being cooled to 35 DEG C, adds mixing wet gel, stir;Finally liquid is turned
Move in mould and cooled and solidified, the natural lip gloss of fragrance type is made after shaping.
Embodiment 5
A kind of natural lip gloss of fragrance type (rose lip gloss), is formulated as follows:Beeswax 8g, candelila wax 7.5g, Chiba rose wax
7g, aloe resin 18g, chamomile fat 10g, saualane 6g, coconut oil 21g, Sweet Almond Oil 5g, grape-kernel oil 7g, Asian puccoon immersion olive
Olive oil 4.5g, marine alga wet gel 4g, bletilla striata extract 2g, 9.99wt% Rosa Damascana 1mL.
The marine alga wet gel is by pretreatment:Be 75wt% by the control of the solid content of marine alga wet gel, 15 DEG C,
Quality is added under 1000r/min stirring condition makes it be uniformly dispersed for the sodium bicarbonate of marine alga wet gel 3%;Then in 400r/
Under min stirring condition, 75 DEG C are warming up to 6 DEG C/min speed, be then down to after room temperature obtain mix alveolate marine alga it is wet
Gel;It is last to replace the gas in marine alga wet gel bubble, the sea pre-processed with absolute ethyl alcohol under the conditions of vacuum decompression
Algae wet gel.
The coconut oil, Sweet Almond Oil, grape-kernel oil, Asian puccoon soak olive oil respectively through modification:By oils thing
Matter is added to thermal dehydration in autoclave, first adds metallic catalyst, then is passed through hydrogen, in hydrogen pressure 0.7MPa, 100
DEG C, react filtering and impurity removing after 40min, reaction under 800r/min stirring conditions, obtain modified oily substance.
The preparation method of the above-mentioned natural lip gloss of fragrance type, comprises the following steps:
(1) by beeswax, candelila wax, Chiba rose wax, aloe resin, chamomile fat, saualane, coconut oil, Sweet Almond Oil, grape
Seed oil and Asian puccoon immersion olive oil progress are mixed and heated to 70 DEG C and stirred, and obtain oil-based liquid;
(2) marine alga wet gel, bletilla striata extract and plants essential oil be mixed and stirred for uniformly, obtaining mixing wet gel;
(3) oil-based liquid is cooled, when being cooled to 55 DEG C, adds mixing wet gel, stir;Finally liquid is turned
Move in mould and cooled and solidified, the natural lip gloss of fragrance type is made after shaping.
Embodiment 6
A kind of natural lip gloss of fragrance type (grapefruit lip gloss), is formulated as follows:Beeswax 10.5g, candelila wax 5g, Chiba rose wax
6g, aloe resin 20g, chamomile fat 8g, saualane 9.5g, coconut oil 23.5g, Sweet Almond Oil 2g, grape-kernel oil 8.5g, Asian puccoon leaching
Steep olive oil 2g, marine alga wet gel 6g, bletilla striata extract 1g, sweet orange oil 5mL, lemon grass (Cymbopogon citratus) essential oil 1mL.
The marine alga wet gel is by pretreatment:Be 75wt% by the control of the solid content of marine alga wet gel, 15 DEG C,
Quality is added under 1000r/min stirring condition makes it be uniformly dispersed for the sodium bicarbonate of marine alga wet gel 3%;Then in 400r/
Under min stirring condition, 75 DEG C are warming up to 6 DEG C/min speed, be then down to after room temperature obtain mix alveolate marine alga it is wet
Gel;It is last to replace the gas in marine alga wet gel bubble, the sea pre-processed with absolute ethyl alcohol under the conditions of vacuum decompression
Algae wet gel.
The coconut oil, Sweet Almond Oil, grape-kernel oil, Asian puccoon soak olive oil respectively through modification:By oils thing
Matter is added to thermal dehydration in autoclave, first adds metallic catalyst, then is passed through hydrogen, in hydrogen pressure 0.7MPa, 100
DEG C, react filtering and impurity removing after 40min, reaction under 800r/min stirring conditions, obtain modified oily substance.
The preparation method of the above-mentioned natural lip gloss of fragrance type, comprises the following steps:
(1) by beeswax, candelila wax, Chiba rose wax, aloe resin, chamomile fat, saualane, coconut oil, Sweet Almond Oil, grape
Seed oil and Asian puccoon immersion olive oil progress are mixed and heated to 80 DEG C and stirred, and obtain oil-based liquid;
(2) marine alga wet gel, bletilla striata extract and plants essential oil be mixed and stirred for uniformly, obtaining mixing wet gel;
(3) oil-based liquid is cooled, when being cooled to 60 DEG C, adds mixing wet gel, stir;Finally liquid is turned
Move in mould and cooled and solidified, the natural lip gloss of fragrance type is made after shaping.
The commercially available lip gloss (comparative example 1 and comparative example 2) for being not added with preservative of lip gloss and two to embodiment 1-4
Tested:
First, sensory evaluation:
Lip gloss sensory evaluation index summary sheet
Scoring event is:
Subitem | Embodiment 1 | Embodiment 2 | Comparative example 1 | Comparative example 2 |
a1 | 8.0 | 8.0 | 8.2 | 8.1 |
a2 | 8.2 | 8.1 | 8.3 | 7.5 |
a3 | 8.4 | 8.3 | 8.2 | 8.5 |
a4 | 8.0 | 8.0 | 8.1 | 7.9 |
a5 | 8.8 | 8.7 | 8.3 | 8.2 |
a6 | 8.6 | 8.5 | 8.0 | 7.8 |
a7 | 8.9 | 9.0 | 7.8 | 8.0 |
a8 | 8.0 | 8.1 | 8.1 | 8.0 |
a9 | 7.9 | 8.0 | 8.0 | 7.6 |
a10 | 8.7 | 9.0 | 7.8 | 7.9 |
a11 | 8.2 | 8.2 | 8.3 | 8.2 |
From the foregoing, it will be observed that the product of the present invention is in a5(moistening degree), a6(spreadability), a7(thick and heavy sense-air permeability), a9(greasy feeling)
Aspect has obvious advantage.
2nd, storage stability evaluation:
Observed, do not gone out after embodiment 1-4, comparative example 1-2 lip gloss are placed into 24h, taking-up under 45 ± 1 DEG C of environment
Existing sweating situation and situation of becoming sour.
Embodiment 1-4, comparative example 1-2 lip gloss are placed 30 days under 45 ± 1 DEG C of environment, observed after taking-up,
Situation of becoming sour does not occur sweating situation and in embodiment 1-4 lip gloss, and slight sweating situation occurs in comparative example 1-2 lip gloss,
Do not occur the situation of becoming sour.
Embodiment 1-4, comparative example 1-2 lip gloss are placed 180 days under 45 ± 1 DEG C of environment, observed after taking-up,
Situation of becoming sour do not occur sweating situation and in embodiment 2 and embodiment 4;There is slight sweating situation and light in embodiment 1 and embodiment 3
Slightly sour to lose situation, there is serious sweating situation and serious situation of becoming sour in comparative example 1 and comparative example 2.
Raw materials used in the present invention, equipment, is the conventional raw material, equipment of this area unless otherwise noted;In the present invention
Method therefor, is the conventional method of this area unless otherwise noted.
It is described above, only it is presently preferred embodiments of the present invention, not the present invention is imposed any restrictions, it is every according to the present invention
Any simple modification, change and equivalent transformation that technical spirit is made to above example, still fall within the technology of the present invention side
The protection domain of case.
Claims (9)
1. a kind of natural lip gloss of fragrance type, it is characterised in that:In terms of every 100g, it is formulated as follows:Beeswax 8-12g, candelila wax
5-9g, Chiba rose wax 3-7g, aloe resin 18-22g, chamomile fat 8-12g, saualane 6-10g, coconut oil 21-25g, sweet tea apricot
Benevolence oil 2-6g, grape-kernel oil 7-10g, Asian puccoon immersion olive oil 2-6g, marine alga wet gel 4-6g, bletilla striata extract 1-2g;In addition,
In the above-mentioned formulas of every 100g, plants essential oil 1-6mL is separately added with.
2. a kind of natural lip gloss of fragrance type as claimed in claim 1, it is characterised in that the plants essential oil is selected from rhodamine toner
At least one of oil, sweet orange oil, lemon grass (Cymbopogon citratus) essential oil.
3. a kind of natural lip gloss of fragrance type as claimed in claim 2, it is characterised in that the plants essential oil is 9.99wt%
Rosa Damascana, the consumption of the Rosa Damascana is 1 mL/100g.
4. a kind of natural lip gloss of fragrance type as claimed in claim 2, it is characterised in that the plants essential oil is sweet orange oil
With lemon grass (Cymbopogon citratus) essential oil, the consumption of the sweet orange oil is 5 mL/100g, and the consumption of the lemon grass (Cymbopogon citratus) essential oil is 1 mL/100g.
5. a kind of natural lip gloss of fragrance type as claimed in claim 1, it is characterised in that the ratio of oil, fat, wax in the formula
Example control is 48:29-31:21-23.
6. a kind of natural lip gloss of fragrance type as claimed in claim 1, it is characterised in that the marine alga wet gel is by pre- place
Reason:It is 55-75wt% by the solid content control of marine alga wet gel, matter is added under 5-15 DEG C, 100-200r/min stirring condition
The sodium bicarbonate measured as marine alga wet gel 1-3% makes it be uniformly dispersed;Then under 400-600r/min stirring condition, with 4-6
DEG C/min speed is warming up to 65-75 DEG C, then it is down to after room temperature and obtains mixing alveolate marine alga wet gel;Finally subtract in vacuum
Under the conditions of pressure the gas in marine alga wet gel bubble, the marine alga wet gel pre-processed are replaced with absolute ethyl alcohol.
7. a kind of natural lip gloss of fragrance type as claimed in claim 1, it is characterised in that the coconut oil, Sweet Almond Oil, Portugal
Grape seed oil, Asian puccoon soak olive oil respectively through modification:Oily substance is added to thermal dehydration in autoclave, first
Catalyst is added, then is passed through hydrogen, it is anti-under 0.5-0.7MPa, 100-110 DEG C of hydrogen pressure, 600-800r/min stirring conditions
Filtering and impurity removing after 20-40min, reaction is answered, modified oily substance is obtained.
8. a kind of preparation method of the natural lip gloss of fragrance type as described in one of claim 1-7, it is characterised in that including with
Lower step:
(1)By beeswax, candelila wax, Chiba rose wax, aloe resin, chamomile fat, saualane, coconut oil, Sweet Almond Oil, grape
Seed oil and Asian puccoon immersion olive oil progress are mixed and heated to 70-80 DEG C and stirred, and obtain oil-based liquid;
(2)Marine alga wet gel, bletilla striata extract and plants essential oil be mixed and stirred for uniformly, to obtain mixing wet gel;
(3)Oil-based liquid is cooled, in cooling, mixing wet gel is added, stirs;Liquid is finally transferred to mould
Cooled and solidified in tool, the natural lip gloss of fragrance type is made after shaping.
9. a kind of preparation method of the natural lip gloss of fragrance type as claimed in claim 8, it is characterised in that step(3)In, drop
When temperature is to 55-60 DEG C, addition mixing wet gel.
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CN107693434A (en) * | 2017-11-16 | 2018-02-16 | 武汉生物工程学院 | A kind of purple returns Chinese medicine lipstick and preparation method thereof |
CN110025554A (en) * | 2019-05-31 | 2019-07-19 | 长春师范大学 | Pure natural moist lip gloss of one kind and preparation method thereof |
CN112043665A (en) * | 2020-10-08 | 2020-12-08 | 福建省梦娇兰日用化学品有限公司 | Lithospermum oil-containing baby lip balm and preparation method thereof |
CN112870116A (en) * | 2021-03-22 | 2021-06-01 | 皖南医学院 | Lip balm for moistening, preserving moisture and repairing lips, preparation method of lip balm, lip balm for moistening, preserving moisture and repairing lips and preparation method of lip balm |
CN113576974A (en) * | 2021-08-17 | 2021-11-02 | 广州环亚化妆品科技有限公司 | Lithospermum extract and lip care composition |
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CN113576974A (en) * | 2021-08-17 | 2021-11-02 | 广州环亚化妆品科技有限公司 | Lithospermum extract and lip care composition |
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