CN107536787A - A kind of adlay cleawhite pack and preparation method thereof - Google Patents

A kind of adlay cleawhite pack and preparation method thereof Download PDF

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Publication number
CN107536787A
CN107536787A CN201610473465.8A CN201610473465A CN107536787A CN 107536787 A CN107536787 A CN 107536787A CN 201610473465 A CN201610473465 A CN 201610473465A CN 107536787 A CN107536787 A CN 107536787A
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China
Prior art keywords
adlay
parts
extract
cleawhite pack
extraction
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CN201610473465.8A
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Chinese (zh)
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周丽
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Individual
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Individual
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Priority to CN201610473465.8A priority Critical patent/CN107536787A/en
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Abstract

The invention discloses a kind of adlay cleawhite pack, it is made up of following weight parts raw material:15 25 parts of adlay water extracts, 0.2 0.6 parts of alcohol of C14 22,5 20 parts of glycerine, 0.05 0.15 parts of butanediols, 10 12 parts of Baical Skullcap root P.Es, 0.1 0.4 parts of citric acids, 40 44 parts of deionized waters, 36 parts of dipotassium glycyrrhizinates, 0.35 0.55 parts of pearl powders, 10 15 parts of ultraviolet absorbers, ultraviolet absorber are the one or more in superfine titanic oxide powder, super fine zinc oxide.Moderate performance of the present invention, it is non-stimulated to skin, whitening can be played on the premise of safe and harmless and repairs adlay cleawhite pack of skin effect and preparation method thereof.

Description

A kind of adlay cleawhite pack and preparation method thereof
Technical field
The invention belongs to facial mask technical field, particularly a kind of adlay cleawhite pack and preparation method thereof.
Background technology
By environmental pollution, stay up late all night, computer radiation etc. influence, the skin condition of people form smoke into smother, it is glossy have one's face covered with, hair Hole plug, blackhead are grown thickly, water oil is unbalance, the coarse skin such as low and deep takes place frequently, and existing facial mask is big to skin irritatin, further Skin state is had a negative impact.
The content of the invention
Goal of the invention:The present invention is intended to provide a kind of moderate performance, non-stimulated to skin, can be on the premise of safe and harmless Play whitening and repair adlay cleawhite pack of skin effect and preparation method thereof.
Technical scheme:A kind of adlay cleawhite pack, contain following material and parts by weight in every 50 grams of facial masks:50-55 part heart of a lotus seeds Benevolence extract, 10-12 parts bletilla striata extract, 0.2-0.6 parts kaolin, 5-7 parts glycerine, 1-3 part polyvinyl alcohol sodium alginate, 0.05-0.15 parts butanediol, 3-7 parts lemon extract, 3-6 parts dipotassium glycyrrhizinate, 0.35-0.55 parts honey, 10-15 part lilies Extract, 40-42 part ethanol distillation water.
Further, the adlay extract is obtained by extraction by the following method:By adlay connect shell be together crushed to 30~ The adlay crude extract of 50 mesh numbers, adlay crude extract are pumped into the rectifying column full of carbon dioxide and extracted, the extraction mode It is to allow carbon dioxide inversely to be contacted with adlay crude extract, the operation of the carbon dioxide is in extracting pressure 25~45Mpa temperature 40~75 DEG C of degree, the carbon dioxide and adlay crude oil are continuous feeds, and the carbon dioxide and the matter of adlay crude oil Velocity ratio is measured more than 8, and extraction time is more than 3 hours and extraction that flow is 100~1000 ls/h, profit after extraction Decolourized with Acidic bentonite, vacuum deodorization, be placed in vacuum boiling water and boil, then heating in vacuum degassing and dehydration, removal cause peroxide The material that change valency rises and peculiar smell and moisture, obtain adlay extract.
The adlay is connected into the adlay crude extract that shell is together crushed to 45 mesh numbers.
The operation of the carbon dioxide is in 75 DEG C of extracting pressure 35Mpa temperature.
The carbon dioxide and the mass velocity ratio of adlay crude oil are more than 10.
The extraction time is 7 hours.
The extraction of 800 ls/h of the flow.
Preferably, following material and parts by weight are contained in every 50 grams of facial masks:52 parts of adlay extracts, 10 parts of bletilla striata extractions Thing, 0.35 part of kaolin, 6 parts of glycerine, 2 parts of polyvinyl alcohol sodium alginates, 0.12 part of butanediol, 4 parts of lemon extracts, 3 parts it is sweet Oxalic acid dipotassium, 0.4 part of honey, 15 parts of Bulbus Lilii extracts, 41 parts of ethanol distillation water.
A kind of preparation method of adlay cleawhite pack, the preparation of facial mask are carried out according to the following steps:
(1) adlay extract, bletilla striata extract, lily extraction are added by proportioning in the reactor containing ethanol distillation water Thing, it is heated to 67-80 DEG C and melts completely to each composition;Then glycerine, kaolin are added, stirring makes it well mixed, homogeneous 10 Minute, rotating speed is controlled at 2780-2880 revs/min;
(2) 50-53 DEG C of addition butanediol, polyvinyl alcohol sodium alginate is cooled to continue to cool after stirring;
(3) it is cooled to 40-42 DEG C of addition lemon extract, dipotassium glycyrrhizinate, honey to continue to stir, mixing time control exists More than 50 minutes;
(4) room temperature is cooled to, is aged 24 hours, can filling be after the assay was approved finished product.
Beneficial effect:The present invention is had using natural plant formula, especially adlays such as adlay, the bletilla striata, lemon, lilies Moist skin, whitening mend wet and other effects very distinguished, applied to there is nature whitening effect again on skin, it is new skin to be improved The function of old metabolism and moisturizing, it is safe and non-stimulating, along with honey, whitening effect can be played a part of, repair impaired skin.This The face pack prescription of adlay cleawhite pack based on natral plant ingredients of invention and preparation method thereof, solving with chemical composition While facial mask is to the problems such as user's health effect, moreover it is possible to play whitening, the effect of anti-inflammatory integrated protection.
Embodiment
Adlay cleawhite pack of the present invention and preparation method thereof, is specifically showed from following four embodiment:
Embodiment one:
A kind of adlay cleawhite pack, contain following material and parts by weight in every 50 grams of facial masks:50 parts of adlay extracts, 10 parts Bletilla striata extract, 0.2 part of kaolin, 5 parts of glycerine, 1 part of polyvinyl alcohol sodium alginate, 0.05 part of butanediol, 3 parts of lemon extractions Thing, 3 parts of dipotassium glycyrrhizinates, 0.35 part of honey, 10 parts of Bulbus Lilii extracts, 40 parts of ethanol distillation water.
The adlay extract is obtained by extraction by the following method:Adlay is connected into the heart of a lotus seed that shell is together crushed to 30~50 mesh numbers Benevolence crude extract, adlay crude extract are pumped into the rectifying column full of carbon dioxide and extracted, and the extraction mode is to allow titanium dioxide Carbon inversely contacts with adlay crude extract, the operation of the carbon dioxide be in 40~75 DEG C of 25~45Mpa of extracting pressure temperature, The carbon dioxide and adlay crude oil are continuous feeds, and the carbon dioxide and the mass velocity ratio of adlay crude oil are 8 More than, and extraction time is more than 3 hours and extraction that flow is 100~1000 ls/h, is taken off after extraction using Acidic bentonite Color, vacuum deodorization, it is placed in vacuum boiling water and boils, then heating in vacuum degassing and dehydration, remove the thing for causing peroxide value to rise Matter and peculiar smell and moisture, obtain adlay extract.
A kind of preparation method of adlay cleawhite pack, the preparation of facial mask are carried out according to the following steps:
(1) adlay extract, bletilla striata extract, lily extraction are added by proportioning in the reactor containing ethanol distillation water Thing, it is heated to 67-80 DEG C and melts completely to each composition;Then glycerine, kaolin are added, stirring makes it well mixed, homogeneous 10 Minute, rotating speed is controlled at 2780-2880 revs/min;
(2) 50-53 DEG C of addition butanediol, polyvinyl alcohol sodium alginate is cooled to continue to cool after stirring;
(3) it is cooled to 40-42 DEG C of addition lemon extract, dipotassium glycyrrhizinate, honey to continue to stir, mixing time control exists More than 50 minutes;
(4) room temperature is cooled to, is aged 24 hours, can filling be after the assay was approved finished product.
Embodiment two:
A kind of adlay cleawhite pack, contain following material and parts by weight in every 50 grams of facial masks:52 parts of adlay extracts, 10 parts Bletilla striata extract, 0.35 part of kaolin, 6 parts of glycerine, 2 parts of polyvinyl alcohol sodium alginates, 0.12 part of butanediol, 4 parts of lemon extractions Thing, 3 parts of dipotassium glycyrrhizinates, 0.4 part of honey, 15 parts of Bulbus Lilii extracts, 41 parts of ethanol distillation water.
A kind of preparation method of adlay cleawhite pack, the preparation of facial mask are carried out according to the following steps:
(1) adlay extract, bletilla striata extract, lily extraction are added by proportioning in the reactor containing ethanol distillation water Thing, it is heated to 67-80 DEG C and melts completely to each composition;Then glycerine, kaolin are added, stirring makes it well mixed, homogeneous 10 Minute, rotating speed is controlled at 2780-2880 revs/min;
(2) 50-53 DEG C of addition butanediol, polyvinyl alcohol sodium alginate is cooled to continue to cool after stirring;
(3) it is cooled to 40-42 DEG C of addition lemon extract, dipotassium glycyrrhizinate, honey to continue to stir, mixing time control exists More than 50 minutes;
(4) room temperature is cooled to, is aged 24 hours, can filling be after the assay was approved finished product.
Embodiment three:
A kind of adlay cleawhite pack, contain following material and parts by weight in every 50 grams of facial masks:53 parts of adlay extracts, 11 parts Bletilla striata extract, 0.3 part of kaolin, 6 parts of glycerine, 2 parts of polyvinyl alcohol sodium alginates, 0.11 part of butanediol, 4 parts of lemon extractions Thing, 5 parts of dipotassium glycyrrhizinates, 0.45 part of honey, 10 parts of Bulbus Lilii extracts, 42 parts of ethanol distillation water.
A kind of preparation method of adlay cleawhite pack, the preparation of facial mask are carried out according to the following steps:
(1) adlay extract, bletilla striata extract, lily extraction are added by proportioning in the reactor containing ethanol distillation water Thing, it is heated to 67-80 DEG C and melts completely to each composition;Then glycerine, kaolin are added, stirring makes it well mixed, homogeneous 10 Minute, rotating speed is controlled at 2780-2880 revs/min;
(2) 50-53 DEG C of addition butanediol, polyvinyl alcohol sodium alginate is cooled to continue to cool after stirring;
(3) it is cooled to 40-42 DEG C of addition lemon extract, dipotassium glycyrrhizinate, honey to continue to stir, mixing time control exists More than 50 minutes;
(4) room temperature is cooled to, is aged 24 hours, can filling be after the assay was approved finished product.
Example IV:
A kind of adlay cleawhite pack, contain following material and parts by weight in every 50 grams of facial masks:55 parts of adlay extracts, 12 parts Bletilla striata extract, 0.6 part of kaolin, 7 parts of glycerine, 3 parts of polyvinyl alcohol sodium alginates, 0.15 part of butanediol, 7 parts of lemon extractions Thing, 6 parts of dipotassium glycyrrhizinates, 0.55 part of honey, 15 parts of Bulbus Lilii extracts, 42 parts of ethanol distillation water.
A kind of preparation method of adlay cleawhite pack, the preparation of facial mask are carried out according to the following steps:
(1) adlay extract, bletilla striata extract, lily extraction are added by proportioning in the reactor containing ethanol distillation water Thing, it is heated to 67-80 DEG C and melts completely to each composition;Then glycerine, kaolin are added, stirring makes it well mixed, homogeneous 10 Minute, rotating speed is controlled at 2780-2880 revs/min;
(2) 50-53 DEG C of addition butanediol, polyvinyl alcohol sodium alginate is cooled to continue to cool after stirring;
(3) it is cooled to 40-42 DEG C of addition lemon extract, dipotassium glycyrrhizinate, honey to continue to stir, mixing time control exists More than 50 minutes;
(4) room temperature is cooled to, is aged 24 hours, can filling be after the assay was approved finished product.
The adlay extract is obtained by extraction by the following method:By adlay connect shell be together crushed to 45 mesh numbers adlay it is thick Extract, adlay crude extract are pumped into the rectifying column full of carbon dioxide and extracted, the extraction mode be allow carbon dioxide with Adlay crude extract inversely contacts, and the operation of the carbon dioxide is in 75 DEG C of extracting pressure 35Mpa temperature, the carbon dioxide And adlay crude oil is continuous feed, and the mass velocity ratio of the carbon dioxide and adlay crude oil is more than 10, and extracts Time is 7 hours and extraction that flow is 800 ls/h, is decolourized after extraction using Acidic bentonite, vacuum deodorization, is placed in vacuum Boiled in boiling water, then heating in vacuum degassing and dehydration, the material and peculiar smell and moisture for causing peroxide value to rise are removed, obtains the heart of a lotus seed Benevolence extract.
Film is packaged in transparence cosmetic bottle by the adlay cleawhite pack of the present invention, is seen within two weeks in 6 DEG C of refrigerator cold-storages Examine no lamination.In Mh in 55 DEG C of insulating box, film emulsifies phenomena such as spoiled without layering.
The made films of embodiment 1-4 are placed in bottle for cosmetics, are stored at room temperature investigation 3 months, no lamination, after Feel unchanged, smell is unchanged.Formed film is soft, and film forming is fast, and film is easier to take off, is compared with rear dermal sensation Softness, there is more comfortable sensation.

Claims (9)

1. a kind of adlay cleawhite pack, it is characterised in that contain following material and parts by weight in every 50 grams of facial masks:50-55 part heart of a lotus seeds Benevolence extract, 10-12 parts bletilla striata extract, 0.2-0.6 parts kaolin, 5-7 parts glycerine, 1-3 part polyvinyl alcohol sodium alginate, 0.05-0.15 parts butanediol, 3-7 parts lemon extract, 3-6 parts dipotassium glycyrrhizinate, 0.35-0.55 parts honey, 10-15 part lilies Extract, 40-42 part ethanol distillation water.
2. adlay cleawhite pack according to claim 1, it is characterised in that the adlay extract extracts by the following method Obtain:Adlay is connected into the adlay crude extract that shell is together crushed to 30~50 mesh numbers, adlay crude extract is pumped into full of dioxy Change and extracted in the rectifying column of carbon, the extraction mode is to allow carbon dioxide inversely to be contacted with adlay crude extract, the titanium dioxide The operation of carbon is that the carbon dioxide and adlay crude oil are continuous feeds in 40~75 DEG C of 25~45Mpa of extracting pressure temperature, And the mass velocity ratio of the carbon dioxide and adlay crude oil is more than 8, and extraction time is more than 3 hours and flow is 100~1000 ls/h of extraction, decolourized after extraction using Acidic bentonite, vacuum deodorization, be placed in vacuum boiling water and boil, then Heating in vacuum deaerates and dehydration, removes the material and peculiar smell and moisture for causing peroxide value to rise, obtains adlay extract.
3. adlay cleawhite pack according to claim 2, it is characterised in that the adlay is connected into shell and is together crushed to 45 mesh Several adlay crude extracts.
4. adlay cleawhite pack according to claim 2, it is characterised in that the operation of the carbon dioxide is pressed in extraction 75 DEG C of power 35Mpa temperature.
5. adlay cleawhite pack according to claim 2, it is characterised in that the carbon dioxide and the quality of adlay crude oil Velocity ratio is more than 10.
6. adlay cleawhite pack according to claim 2, it is characterised in that the extraction time is 7 hours.
7. adlay cleawhite pack according to claim 2, it is characterised in that the extraction of 800 ls/h of the flow.
8. adlay cleawhite pack according to claim 1, it is characterised in that containing following material and again in every 50 grams of facial masks Measure part:52 parts of adlay extracts, 10 parts of bletilla striata extracts, 0.35 part of kaolin, 6 parts of glycerine, 2 parts of polyvinyl alcohol alginic acids Sodium, 0.12 part of butanediol, 4 parts of lemon extracts, 3 parts of dipotassium glycyrrhizinates, 0.4 part of honey, 15 parts of Bulbus Lilii extracts, 41 parts of ethanol Distilled water.
A kind of 9. preparation method of adlay cleawhite pack as claimed in claim 1, it is characterised in that the preparation of facial mask press with Lower step is carried out:
(1)Adlay extract, bletilla striata extract, Bulbus Lilii extract are added by proportioning in the reactor containing ethanol distillation water, It is heated to 67-80 DEG C and melts completely to each composition;Then glycerine, kaolin are added, stirring makes it well mixed, and homogeneous 10 divides Clock, rotating speed are controlled at 2780-2880 revs/min;
(2)50-53 DEG C of addition butanediol, polyvinyl alcohol sodium alginate is cooled to continue to cool after stirring;
(3)It is cooled to 40-42 DEG C of addition lemon extract, dipotassium glycyrrhizinate, honey to continue to stir, mixing time is controlled 50 More than minute;
(4)Room temperature is cooled to, is aged 24 hours, can filling be after the assay was approved finished product.
CN201610473465.8A 2016-06-24 2016-06-24 A kind of adlay cleawhite pack and preparation method thereof Pending CN107536787A (en)

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112263536A (en) * 2020-11-27 2021-01-26 陈珲 Exfoliating and whitening mask
CN112641698A (en) * 2020-12-21 2021-04-13 王玉成 Coix seed extract facial mask and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112263536A (en) * 2020-11-27 2021-01-26 陈珲 Exfoliating and whitening mask
CN112641698A (en) * 2020-12-21 2021-04-13 王玉成 Coix seed extract facial mask and preparation method thereof

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Application publication date: 20180105