CN107536768A - A kind of adlay whitening sun protection facial treatment milk and preparation method thereof - Google Patents
A kind of adlay whitening sun protection facial treatment milk and preparation method thereof Download PDFInfo
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- CN107536768A CN107536768A CN201610474380.1A CN201610474380A CN107536768A CN 107536768 A CN107536768 A CN 107536768A CN 201610474380 A CN201610474380 A CN 201610474380A CN 107536768 A CN107536768 A CN 107536768A
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Abstract
The invention discloses a kind of adlay whitening sun protection facial treatment milk and preparation method thereof, it is made up of following weight parts raw material：20 35 parts of adlay water extracts, 0.2 0.6 parts of hamamelis extracts, 5 20 parts of ursin, 0.05 0.15 parts of butanediols, 1 10 parts of Radix et Caulis Opuntiae Dillenii extracts, 0.1 0.4 parts of citric acids, 60 80 parts of deionized waters, 36 parts of dipotassium glycyrrhizinates, 0.1 0.3 parts of Sodium Hyaluronates, 0.5 1.5 parts of ultraviolet absorbers, ultraviolet absorber are the one or more in superfine titanic oxide powder, super fine zinc oxide.The adlay whitening sun protection facial treatment milk moderate performance of the present invention, it is non-stimulated to skin, whitening, resistance ultraviolet, the effect of anti-inflammatory integrated protection can be played on the premise of safe and harmless.
Description
Technical field
The invention belongs to facial treatment milk technical field, particularly a kind of adlay whitening sun protection facial treatment milk and its preparation
Method.
Background technology
Influenceed by environmental pollution, all night of staying up late, computer radiation etc., the skin condition of people is form smoke into smother, glossy
Have one's face covered with, clogging of pores, blackhead are grown thickly, water oil is unbalance, the coarse skin such as low and deep takes place frequently, existing purifying
The facial treatment milk of length of schooling agent, it is big to skin irritatin, further skin state is had a negative impact.
The content of the invention
Goal of the invention：The present invention is intended to provide a kind of moderate performance, non-stimulated to skin, can be safe and harmless
Under the premise of play whitening, resistance ultraviolet, facial treatment milk and preparation method thereof of anti-inflammatory integrated protection effect.
Technical scheme：A kind of adlay whitening sun protection facial treatment milk, is made up of following weight parts raw material：20-35 parts
Adlay water extract, 0.2-0.6 part hamamelis extract, 5-20 parts ursin, 0.05-0.15 parts fourth two
Alcohol, 1-10 parts Radix et Caulis Opuntiae Dillenii extract, 0.1-0.4 parts citric acid, 60-80 parts deionized water, 3-6 part glycyrrhizic acids
Dipotassium, 0.1-0.3 parts Sodium Hyaluronate, 0.5-1.5 part ultraviolet absorbers, ultraviolet absorber are ultra-fine titanium dioxide
One or more in titanium valve, super fine zinc oxide.
Further, it is made up of following weight parts raw material：25-30 part adlays water extract, 0.3-0.5 parts north
U.S. hamamelis extract, 10-20 parts ursin, 0.05-0.15 parts butanediol, 4-9 parts Radix et Caulis Opuntiae Dillenii extract,
0.2-0.4 parts citric acid, 65-70 parts deionized water, 3-5 parts dipotassium glycyrrhizinate, 0.1-0.3 parts Sodium Hyaluronate,
0.5-1.5 part ultraviolet absorbers, ultraviolet absorber are superfine titanic oxide powder and super fine zinc oxide.
The adlay extract is obtained by extraction by the following method：Adlay is connected into shell and is together crushed to 30~50 mesh
Several adlay crude extracts, adlay crude extract are pumped into the rectifying column full of carbon dioxide and extracted, the extraction
Mode is to allow carbon dioxide inversely to be contacted with adlay crude extract, and the operation of the carbon dioxide is in extracting pressure
40~75 DEG C of 25~45Mpa temperature, the carbon dioxide and adlay crude oil are continuous feeds, and described
The mass velocity ratio of carbon dioxide and adlay crude oil is more than 8, and extraction time is more than 3 hours and flow is
100~1000 ls/h of extraction, decolourized after extraction using Acidic bentonite, vacuum deodorization, be placed in vacuum boiling water
In boil, then heating in vacuum degassing and dehydration remove material and peculiar smell and the moisture for causing peroxide value to rise,
Obtain adlay extract.
A kind of preparation method of adlay whitening sun protection facial treatment milk, the preparation of facial treatment milk are carried out according to the following steps：
(1) adlay water extract is added by proportioning in the reactor containing deionized water, hamamelis carries
Thing and ursin are taken, is slowly stirred uniformly and is warming up to 60-70 DEG C；Then ultraviolet absorber is added, stirring makes
It is well mixed；
(2) it is cooled to 50-60 DEG C and adds after butanediol stirs and continues to cool；
(3) 40-45 DEG C of addition Radix et Caulis Opuntiae Dillenii extract, citric acid, dipotassium glycyrrhizinate is cooled to continue to stir；
(4) 38 DEG C are cooled to, adds Sodium Hyaluronate, after stirring, 48 hours is stood, discharges and produce
Facial treatment milk.
The step (1) is warming up to 67 DEG C.
Beneficial effect：The present invention is using the natural plant formulas such as adlay, hamamelis, cactus, safe nothing
Stimulate, along with citric acid, dipotassium glycyrrhizinate, ultraviolet absorber comprehensive function so that the present invention can play
Effect whitening, beat back melanin, to anti-ultraviolet effect, and it is safe and non-stimulating.
Embodiment
Adlay whitening sun protection facial treatment milk of the present invention and preparation method thereof, specifically from following embodiment
Showed：
Embodiment one：
A kind of adlay whitening sun protection facial treatment milk, is made up of following weight parts raw material：20 parts of adlay water extracts,
0.2-0.6 part hamamelis extract, 5 parts of ursin, 0.05 part of butanediol, 1 part of Radix et Caulis Opuntiae Dillenii extract,
0.1 part of citric acid, 60 parts of deionized waters, 3 parts of dipotassium glycyrrhizinates, 0.1 part of Sodium Hyaluronate, 0.5 part it is ultraviolet
Absorbent, ultraviolet absorber are superfine titanic oxide powder.
The adlay extract is obtained by extraction by the following method：Adlay is connected into shell and is together crushed to 30~50 mesh
Several adlay crude extracts, adlay crude extract are pumped into the rectifying column full of carbon dioxide and extracted, the extraction
Mode is to allow carbon dioxide inversely to be contacted with adlay crude extract, and the operation of the carbon dioxide is in extracting pressure
40~75 DEG C of 25~45Mpa temperature, the carbon dioxide and adlay crude oil are continuous feeds, and described
The mass velocity ratio of carbon dioxide and adlay crude oil is more than 8, and extraction time is more than 3 hours and flow is
100~1000 ls/h of extraction, decolourized after extraction using Acidic bentonite, vacuum deodorization, be placed in vacuum boiling water
In boil, then heating in vacuum degassing and dehydration remove material and peculiar smell and the moisture for causing peroxide value to rise,
Obtain adlay extract.
The preparation of facial treatment milk is carried out according to the following steps：
(1) adlay water extract is added by proportioning in the reactor containing deionized water, hamamelis carries
Thing and ursin are taken, is slowly stirred uniformly and is warming up to 70 DEG C；Then superfine titanic oxide powder, stirring are added
Make it well mixed；
(2) it is cooled to 50-60 DEG C and adds after butanediol stirs and continues to cool；
(3) 40-45 DEG C of addition Radix et Caulis Opuntiae Dillenii extract, citric acid, dipotassium glycyrrhizinate is cooled to continue to stir；
(4) 38 DEG C are cooled to, adds Sodium Hyaluronate, after stirring, discharges and produces facial treatment milk.
Embodiment two：
A kind of adlay whitening sun protection facial treatment milk, is made up of following weight parts raw material：25 parts of adlay water extracts,
0.4 part of hamamelis extract, 10 parts of ursin, 0.1 part of butanediol, 5 parts of Radix et Caulis Opuntiae Dillenii extracts, 0.3
Part citric acid, 70 parts of deionized waters, 4 parts of dipotassium glycyrrhizinates, 0.23 part of Sodium Hyaluronate, 0.85 part of ultraviolet suction
Agent is received, ultraviolet absorber is super fine zinc oxide.
The adlay extract is obtained by extraction by the following method：Adlay is connected into shell and is together crushed to 30~50 mesh
Several adlay crude extracts, adlay crude extract are pumped into the rectifying column full of carbon dioxide and extracted, the extraction
Mode is to allow carbon dioxide inversely to be contacted with adlay crude extract, and the operation of the carbon dioxide is in extracting pressure
40~75 DEG C of 25~45Mpa temperature, the carbon dioxide and adlay crude oil are continuous feeds, and described
The mass velocity ratio of carbon dioxide and adlay crude oil is more than 8, and extraction time is more than 3 hours and flow is
100~1000 ls/h of extraction, decolourized after extraction using Acidic bentonite, vacuum deodorization, be placed in vacuum boiling water
In boil, then heating in vacuum degassing and dehydration remove material and peculiar smell and the moisture for causing peroxide value to rise,
Obtain adlay extract.
The preparation of facial treatment milk is carried out according to the following steps：
(1) adlay water extract is added by proportioning in the reactor containing deionized water, hamamelis carries
Thing and ursin are taken, is slowly stirred uniformly and is warming up to 65 DEG C；Then super fine zinc oxide is added, stirring makes it
It is well mixed；
(2) 55 DEG C are cooled to and is added after butanediol stirs and continues to cool；
(3) 42 DEG C of addition Radix et Caulis Opuntiae Dillenii extracts, citric acid, dipotassium glycyrrhizinates are cooled to continue to stir；
(4) 38 DEG C are cooled to, adds Sodium Hyaluronate, after stirring, discharges and produces facial treatment milk.
Embodiment three：
A kind of adlay whitening sun protection facial treatment milk, is made up of following weight parts raw material：25-30 part adlay water extractions
Take thing, 0.3-0.5 part hamamelis extract, 10-20 parts ursin, 0.05-0.15 parts butanediol, 4-9
Part Radix et Caulis Opuntiae Dillenii extract, 0.2-0.4 parts citric acid, 65-70 parts deionized water, 3-5 parts dipotassium glycyrrhizinate, 0.1-0.3
Part Sodium Hyaluronate, 0.5-1.5 part ultraviolet absorbers, ultraviolet absorber is superfine titanic oxide powder and ultra-fine oxidation
Zinc.
The preparation of facial treatment milk is carried out according to the following steps：
(1) adlay water extract is added by proportioning in the reactor containing deionized water, hamamelis carries
Thing and ursin are taken, is slowly stirred uniformly and is warming up to 67 DEG C；Then superfine titanic oxide powder and ultra-fine is added
Zinc oxide, stirring make it well mixed；
(2) 50 DEG C are cooled to and is added after butanediol stirs and continues to cool；
(3) 40 DEG C of addition Radix et Caulis Opuntiae Dillenii extracts, citric acid, dipotassium glycyrrhizinates are cooled to continue to stir；
(4) 38 DEG C are cooled to, adds Sodium Hyaluronate, after stirring, discharges and produces facial treatment milk.
Example IV：
A kind of adlay whitening sun protection facial treatment milk, is made up of following weight parts raw material：35 parts of adlay water extracts,
0.6 part of hamamelis extract, 20 parts of ursin, 0.15 part of butanediol, 10 parts of Radix et Caulis Opuntiae Dillenii extracts,
0.4 part of citric acid, 80 parts of deionized waters, 6 parts of dipotassium glycyrrhizinates, 0.3 part of Sodium Hyaluronate, 1.5 parts it is ultraviolet
Absorbent, ultraviolet absorber are superfine titanic oxide powder and super fine zinc oxide.
The adlay extract is obtained by extraction by the following method：Adlay is connected into shell and is together crushed to 30~50 mesh
Several adlay crude extracts, adlay crude extract are pumped into the rectifying column full of carbon dioxide and extracted, the extraction
Mode is to allow carbon dioxide inversely to be contacted with adlay crude extract, and the operation of the carbon dioxide is in extracting pressure
40~75 DEG C of 25~45Mpa temperature, the carbon dioxide and adlay crude oil are continuous feeds, and described
The mass velocity ratio of carbon dioxide and adlay crude oil is more than 8, and extraction time is more than 3 hours and flow is
100~1000 ls/h of extraction, decolourized after extraction using Acidic bentonite, vacuum deodorization, be placed in vacuum boiling water
In boil, then heating in vacuum degassing and dehydration remove material and peculiar smell and the moisture for causing peroxide value to rise,
Obtain adlay extract.
The preparation of facial treatment milk is carried out according to the following steps：
(1) adlay water extract is added by proportioning in the reactor containing deionized water, hamamelis carries
Thing and ursin are taken, is slowly stirred uniformly and is warming up to 60 DEG C；Then superfine titanic oxide powder and ultra-fine is added
Zinc oxide, stirring make it well mixed；
(2) 50 DEG C are cooled to and is added after butanediol stirs and continues to cool；
(3) 40 DEG C of addition Radix et Caulis Opuntiae Dillenii extracts, citric acid, dipotassium glycyrrhizinates are cooled to continue to stir；
(4) 38 DEG C are cooled to, adds Sodium Hyaluronate, after stirring, discharges and produces facial treatment milk.
Claims (6)
1. a kind of adlay whitening sun protection facial treatment milk, it is characterised in that be made up of following weight parts raw material：20-35 part adlays water extract, 0.2-0.6 part hamamelis extract, 5-20 parts ursin, 0.05-0.15 parts butanediol, 1-10 parts Radix et Caulis Opuntiae Dillenii extract, 0.1-0.4 parts citric acid, 60-80 parts deionized water, 3-6 parts dipotassium glycyrrhizinate, 0.1-0.3 parts Sodium Hyaluronate, 0.5-1.5 part ultraviolet absorbers, ultraviolet absorber are the one or more in superfine titanic oxide powder, super fine zinc oxide.
2. a kind of adlay whitening sun protection facial treatment milk, it is characterised in that be made up of following weight parts raw material：25-30 part adlays water extract, 0.3-0.5 part hamamelis extract, 10-20 parts ursin, 0.05-0.15 parts butanediol, 4-9 parts Radix et Caulis Opuntiae Dillenii extract, 0.2-0.4 parts citric acid, 65-70 parts deionized water, 3-5 parts dipotassium glycyrrhizinate, 0.1-0.3 parts Sodium Hyaluronate, 0.5-1.5 part ultraviolet absorbers, ultraviolet absorber are superfine titanic oxide powder and super fine zinc oxide.
3. a kind of adlay whitening sun protection facial treatment milk as claimed in claim 1, it is characterised in that the adlay extract is obtained by extraction by the following method：Adlay is connected into the adlay crude extract that shell is together crushed to 30~50 mesh numbers, adlay crude extract is pumped into the rectifying column full of carbon dioxide and extracted, the extraction mode is to allow carbon dioxide inversely to be contacted with adlay crude extract, the operation of the carbon dioxide is in 40~75 DEG C of 25~45Mpa of extracting pressure temperature, the carbon dioxide and adlay crude oil are continuous feeds, and the carbon dioxide and the mass velocity ratio of adlay crude oil are more than 8, and extraction time is more than 3 hours and extraction that flow is 100~1000 ls/h, decolourized after extraction using Acidic bentonite, vacuum deodorization, it is placed in vacuum boiling water and boils, heating in vacuum degassing and dehydration again, remove the material and peculiar smell and moisture for causing peroxide value to rise, obtain adlay extract.
4. a kind of adlay whitening sun protection facial treatment milk as claimed in claim 3, it is characterised in that the extraction time is 5 hours.
5. the preparation method of the adlay whitening sun protection facial treatment milk according to claim 1-2 any one, it is characterised in that the preparation of facial treatment milk is carried out according to the following steps：
（1）Adlay water extract, hamamelis extract and ursin are added by proportioning in the reactor containing deionized water, is slowly stirred uniformly and is warming up to 60-70 DEG C；Then ultraviolet absorber is added, stirring makes it well mixed；
（2）It is cooled to 50-60 DEG C and adds after butanediol stirs and continues to cool；
（3）40-45 DEG C of addition Radix et Caulis Opuntiae Dillenii extract, citric acid, dipotassium glycyrrhizinate is cooled to continue to stir；
（4）38 DEG C are cooled to, adds Sodium Hyaluronate, after stirring, 48 hours is stood, discharges and produce facial treatment milk.
6. the preparation method of adlay whitening sun protection facial treatment milk according to claim 4, it is characterised in that the step（1）It is warming up to 67 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610474380.1A CN107536768A (en) | 2016-06-24 | 2016-06-24 | A kind of adlay whitening sun protection facial treatment milk and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610474380.1A CN107536768A (en) | 2016-06-24 | 2016-06-24 | A kind of adlay whitening sun protection facial treatment milk and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN107536768A true CN107536768A (en) | 2018-01-05 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610474380.1A Pending CN107536768A (en) | 2016-06-24 | 2016-06-24 | A kind of adlay whitening sun protection facial treatment milk and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108420779A (en) * | 2018-06-15 | 2018-08-21 | 广州无添加主义化妆品有限公司 | A kind of sunscreen and preparation method thereof |
| CN108743505A (en) * | 2018-08-04 | 2018-11-06 | 芜湖慧宇商贸有限公司 | A kind of preparation method of the after-sun lotion of the extract containing adlay |
-
2016
- 2016-06-24 CN CN201610474380.1A patent/CN107536768A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108420779A (en) * | 2018-06-15 | 2018-08-21 | 广州无添加主义化妆品有限公司 | A kind of sunscreen and preparation method thereof |
| CN108743505A (en) * | 2018-08-04 | 2018-11-06 | 芜湖慧宇商贸有限公司 | A kind of preparation method of the after-sun lotion of the extract containing adlay |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20180105 |
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| WD01 | Invention patent application deemed withdrawn after publication |