CN105030617B - A kind of nano montmorillonite deep layer cleaning moisture-keeping cosmetics and preparation method thereof - Google Patents
A kind of nano montmorillonite deep layer cleaning moisture-keeping cosmetics and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of nano montmorillonite deep layer cleaning moisture-keeping cosmetics and preparation method thereof, including 30 80 parts of nano montmorillonite, 5 10 parts of vitamin C, 27 parts of hyaluronic acid, 3 10 parts of cetostearyl alcohol, 28 parts of rose 30wt% ethanol water extract, 2 10 parts of tulip supercritical carbon dioxide extracting thing, 27 parts of shrub althea flower ethanol extract, 28 parts of folium eucalypti rattan ethyl acetate extract, 35 parts of silver tip pekoe ethanol extract, 25 parts of brier ethanol extract, 0.5 2 parts of orange oil, 0.3 2 parts of raspberry ketone, 0.4 2 parts of citronellyl acetate, 0.5 2 parts of heliotropin, 20 50 parts of deionized water.Preparation method includes the steps such as solvent extraction, supercritical carbon dioxide extracting, concentration, separation, mixing, and cosmetics are prepared.The cosmetics of the present invention can significantly improve the clean level and moistening effect of skin.
Description
Technical field
The invention belongs to cosmetic field, is related to a kind of deep layer cleaning moisture-keeping cosmetics and preparation method thereof, particularly relates to
A kind of and nano montmorillonite deep layer cleaning moisture-keeping cosmetics and preparation method thereof.
Background technology
Montmorillonite effectively can remove and adsorb the grease of the color make-up remained in skin lines, dirt impurity and surplus, and inhale
Attached superfluous grease, exfoliating, accelerates coming off for old dead cell, restrains enlarged pores, desalinates melanocyte, improves the colour of skin.Can
For cosmetics inorganic gel (thickening, suspending, emulsification), facemask powder（Whitening）, the emulsion containing powder, the bed material of skin cream（Go
Dirt, removing toxic substances, antipruritic, beauty, moisturizing）.Montmorillonite such as with glycerine hybrid energy water conservation skin care, increase skin it is elastic, ventilative
Property, make skin brightening, can also decontamination, removing toxic substances, antipruritic, beauty, moisturizing.Montmorillonite is added in cosmetics skin cream can be reduced accordingly
The dosage of organic gel, stimulation of the organic gel to human body skin is alleviated, reduced again because using the household chemicals containing organic gel
Environmental pollution caused by and.Particularly its unique suction-operated, the harmful bacteria of adsorbable skin surface.Nanoscale montmorillonite
The main trend of the household chemicals back to natures such as the current cosmetics of positive adaptation.By the way that nanoscale montmorillonite is planted with natural again
Thing extraction elite is combined, and can effectively improve existing cosmetics its problem of clean effect is poor, moistening effect is poor.
The content of the invention
Technical problems to be solved：The purpose of the present invention is that openly one kind can be clean with deep layer and has good moisturizing work(
Nano montmorillonite deep layer cleaning moisture-keeping cosmetics of effect and preparation method thereof, overcome deep clean, the moisturizing work(of existing cosmetics
The problem of poor is imitated, improves its clean level to skin, performance of keeping humidity.
Technical scheme：The invention discloses a kind of nano montmorillonite deep layer cleaning moisture-keeping cosmetics, described toiletry bag
Include the composition of following weight parts：
Nano montmorillonite 30-80 parts,
Vitamin C 5-10 parts,
Hyaluronic acid 2-7 parts,
Cetostearyl alcohol 3-10 parts,
Rose 30wt% ethanol water extract 2-8 parts,
Tulip supercritical carbon dioxide extracting thing 2-10 parts,
Shrub althea flower ethanol extract 2-7 parts,
Folium eucalypti rattan ethyl acetate extract 2-8 parts,
Silver tip pekoe ethanol extract 3-5 parts,
Brier ethanol extract 2-5 parts,
Orange oil 0.5-2 parts,
Raspberry ketone 0.3-2 parts,
Citronellyl acetate 0.4-2 parts,
Heliotropin 0.5-2 parts,
Deionized water 20-50 parts.
As preferable technical scheme, a kind of described nano montmorillonite deep layer cleaning moisture-keeping cosmetics, described cosmetic
Product include the composition of following weight parts：
Nano montmorillonite 40-70 parts,
Vitamin C 3-8 parts,
Hyaluronic acid 3-5 parts,
Cetostearyl alcohol 4-8 parts,
Rose 30wt% ethanol water extract 3-6 parts,
Tulip supercritical carbon dioxide extracting thing 3-8 parts,
Shrub althea flower ethanol extract 3-5 parts,
Folium eucalypti rattan ethyl acetate extract 3-6 parts,
Silver tip pekoe ethanol extract 4-5 parts,
Brier ethanol extract 2-4 parts,
Orange oil 0.7-1 parts,
Raspberry ketone 0.5-1 parts,
Citronellyl acetate 0.6-1.2 parts,
Heliotropin 0.8-1.4 parts,
Deionized water 30-40 parts.
A kind of preparation method of described nano montmorillonite deep layer cleaning moisture-keeping cosmetics, comprises the following steps：
Step 1：By rose crushed after being dried, heating extraction is stirred with 30wt% ethanol waters, is centrifuged after extraction
Separation, then by supernatant concentration, obtain rose 30wt% ethanol water extracts；
Step 2：By tulip crushed after being dried, then supercritical carbon dioxide extracting is carried out, one-level extraction is collected after extraction
Thing and two level extract, merge, be tulip supercritical carbon dioxide extracting thing；
Step 3：Carried shrub althea flower crushed after being dried, then with absolute ethyl alcohol and stirring hot dipping, hot dipping centrifuges after carrying, then enters
Row is concentrated in vacuo, and is prepared as shrub althea flower ethanol extract；
Step 4：Carried folium eucalypti rattan crushed after being dried, then with ethyl acetate stirring hot dipping, hot dipping centrifuges after carrying, then enters
Row is concentrated in vacuo, and is prepared as folium eucalypti rattan ethyl acetate extract；
Step 5：Carried silver tip pekoe and brier crushed after being dried, then with absolute ethyl alcohol and stirring hot dipping, hot dipping carry after from
The heart separates, then is concentrated in vacuo, and is prepared as silver tip pekoe ethanol extract and brier ethanol extract；
Step 6：Take nano montmorillonite 30-80 parts, vitamin C 5-10 parts, hyaluronic acid 2-7 parts, spermaceti respectively by weight
Stearyl alcohol 3-10 parts, rose 30wt% ethanol water extract 2-8 parts, tulip supercritical carbon dioxide extracting thing 2-10 parts, wood
Rose of Sharon flower ethanol extract 2-7 parts, folium eucalypti rattan ethyl acetate extract 2-8 parts, silver tip pekoe ethanol extract 3-5 parts, brier second
Alcohol extracting thing 2-5 parts, orange oil 0.5-2 parts, raspberry ketone 0.3-2 parts, citronellyl acetate 0.4-2 parts, heliotropin 0.5-2
Part, deionized water 20-50 parts, above-mentioned composition is mixed to uniform, is nano montmorillonite deep layer cleaning moisture-keeping cosmetics.
As preferable technical scheme, a kind of preparation method of described nano montmorillonite deep layer cleaning moisture-keeping cosmetics,
Extraction temperature is 60 DEG C in described step 1, and extraction feed liquid weight ratio is 1:5, extraction time 3h.
As preferable technical scheme, a kind of preparation method of described nano montmorillonite deep layer cleaning moisture-keeping cosmetics,
Supercritical extract pressure is 25MPa in described step 2, and one-level separating still pressure is 9.5MPa, and the auxiliary pressure of the second-order separation is
7MPa, extraction time 3h, extraction temperature are 55 DEG C.
As preferable technical scheme, a kind of preparation method of described nano montmorillonite deep layer cleaning moisture-keeping cosmetics,
Extraction temperature is 50 DEG C in described step 3, step 4 and step 5, and extraction feed liquid weight ratio is 1:8, extraction time is
3h。
A kind of preparation method of nano montmorillonite deep layer cleaning moisture-keeping cosmetics described in any of the above, described drying side
Formula includes the one or more in vacuum drying, heated-air drying, microwave drying.
A kind of preparation method of nano montmorillonite deep layer cleaning moisture-keeping cosmetics described in any of the above, described centrifugation point
It is 2000-8000rpm from rotating speed.
Beneficial effect：The nano montmorillonite contained in the preparation method of the present invention carries out deep clean with very to skin
The effect of good, the natural plant extracts contained in addition such as rose 30wt% ethanol water extract, the overcritical dioxy of tulip
Changing carbon extract, shrub althea flower ethanol extract, folium eucalypti rattan ethyl acetate extract has very good moisture-keeping efficacy, above-mentioned
It is common to improve that conventional montmorillonitization cosmetic its clean effect is relatively low, moisture-keeping efficacy is poor lacks after composition is mixed
Fall into, improve clean skin, the effect of moisturizing of montmorillonitization cosmetic.
Embodiment
Embodiment 1
Step 1：By rose crushed after being dried, heating extraction is stirred with 30wt% ethanol waters, extraction temperature is
60 DEG C, extraction feed liquid weight ratio is 1:5, extraction time 3h, centrifuged after extraction, then by supernatant concentration, obtain rose
Flower 30wt% ethanol water extracts；Step 2：By tulip crushed after being dried, then supercritical carbon dioxide extracting is carried out, it is overcritical
Extracting pressure is 25MPa, and one-level separating still pressure is 9.5MPa, and the auxiliary pressure of the second-order separation is 7MPa, extraction time 3h, is extracted
Temperature is 55 DEG C, and one-level extract and two level extract are collected after extraction, merges, is tulip supercritical carbon dioxide extracting
Thing；Step 3：Carried shrub althea flower crushed after being dried, then with absolute ethyl alcohol and stirring hot dipping, hot dipping centrifuges after carrying, then carries out true
Sky concentration, is prepared as shrub althea flower ethanol extract；Step 4：Hot dipping is stirred folium eucalypti rattan crushed after being dried, then with ethyl acetate
Carry, hot dipping centrifuges after carrying, then is concentrated in vacuo, and is prepared as folium eucalypti rattan ethyl acetate extract；Step 5：Pekoe silver
Pin and brier crushed after being dried, then carried with absolute ethyl alcohol and stirring hot dipping, hot dipping centrifuges after carrying, then is concentrated in vacuo,
It is prepared as silver tip pekoe ethanol extract and brier ethanol extract；Extraction temperature is 50 in step 3, step 4 and step 5
DEG C, extraction feed liquid weight ratio is 1:8, extraction time is 3h.Step 6：Take 80 parts of nano montmorillonite, dimension life respectively by weight
Plain C5 parts, 7 parts of hyaluronic acid, 3 parts of cetostearyl alcohol, 2 parts of rose 30wt% ethanol water extract, the overcritical dioxy of tulip
Change 10 parts of carbon extract, 2 parts of shrub althea flower ethanol extract, 8 parts of folium eucalypti rattan ethyl acetate extract, silver tip pekoe ethanol extract 5
Part, 2 parts of brier ethanol extract, 2 parts of orange oil, 0.3 part of raspberry ketone, 0.4 part of citronellyl acetate, 2 parts of heliotropin, go
50 parts of ionized water, above-mentioned composition is mixed to uniform, is nano montmorillonite deep layer cleaning moisture-keeping cosmetics.
Embodiment 2
Step 1：By rose crushed after being dried, heating extraction is stirred with 30wt% ethanol waters, extraction temperature is
60 DEG C, extraction feed liquid weight ratio is 1:5, extraction time 3h, centrifuged after extraction, then by supernatant concentration, obtain rose
Flower 30wt% ethanol water extracts；Step 2：By tulip crushed after being dried, then supercritical carbon dioxide extracting is carried out, it is overcritical
Extracting pressure is 25MPa, and one-level separating still pressure is 9.5MPa, and the auxiliary pressure of the second-order separation is 7MPa, extraction time 3h, is extracted
Temperature is 55 DEG C, and one-level extract and two level extract are collected after extraction, merges, is tulip supercritical carbon dioxide extracting
Thing；Step 3：Carried shrub althea flower crushed after being dried, then with absolute ethyl alcohol and stirring hot dipping, hot dipping centrifuges after carrying, then carries out true
Sky concentration, is prepared as shrub althea flower ethanol extract；Step 4：Hot dipping is stirred folium eucalypti rattan crushed after being dried, then with ethyl acetate
Carry, hot dipping centrifuges after carrying, then is concentrated in vacuo, and is prepared as folium eucalypti rattan ethyl acetate extract；Step 5：Pekoe silver
Pin and brier crushed after being dried, then carried with absolute ethyl alcohol and stirring hot dipping, hot dipping centrifuges after carrying, then is concentrated in vacuo,
It is prepared as silver tip pekoe ethanol extract and brier ethanol extract；Extraction temperature is 50 in step 3, step 4 and step 5
DEG C, extraction feed liquid weight ratio is 1:8, extraction time is 3h.Step 6：Take 30 parts of nano montmorillonite, dimension life respectively by weight
Plain C10 parts, 2 parts of hyaluronic acid, 10 parts of cetostearyl alcohol, 8 parts of rose 30wt% ethanol water extract, tulip overcritical two
2 parts of carbonoxide extract, 7 parts of shrub althea flower ethanol extract, 2 parts of folium eucalypti rattan ethyl acetate extract, silver tip pekoe ethanol extract 3
Part, 5 parts of brier ethanol extract, 0.5 part of orange oil, 2 parts of raspberry ketone, 2 parts of citronellyl acetate, 0.5 part of heliotropin, go
20 parts of ionized water, above-mentioned composition is mixed to uniform, is nano montmorillonite deep layer cleaning moisture-keeping cosmetics.
Embodiment 3
Step 1：By rose crushed after being dried, heating extraction is stirred with 30wt% ethanol waters, extraction temperature is
60 DEG C, extraction feed liquid weight ratio is 1:5, extraction time 3h, centrifuged after extraction, then by supernatant concentration, obtain rose
Flower 30wt% ethanol water extracts；Step 2：By tulip crushed after being dried, then supercritical carbon dioxide extracting is carried out, it is overcritical
Extracting pressure is 25MPa, and one-level separating still pressure is 9.5MPa, and the auxiliary pressure of the second-order separation is 7MPa, extraction time 3h, is extracted
Temperature is 55 DEG C, and one-level extract and two level extract are collected after extraction, merges, is tulip supercritical carbon dioxide extracting
Thing；Step 3：Carried shrub althea flower crushed after being dried, then with absolute ethyl alcohol and stirring hot dipping, hot dipping centrifuges after carrying, then carries out true
Sky concentration, is prepared as shrub althea flower ethanol extract；Step 4：Hot dipping is stirred folium eucalypti rattan crushed after being dried, then with ethyl acetate
Carry, hot dipping centrifuges after carrying, then is concentrated in vacuo, and is prepared as folium eucalypti rattan ethyl acetate extract；Step 5：Pekoe silver
Pin and brier crushed after being dried, then carried with absolute ethyl alcohol and stirring hot dipping, hot dipping centrifuges after carrying, then is concentrated in vacuo,
It is prepared as silver tip pekoe ethanol extract and brier ethanol extract；Extraction temperature is 50 in step 3, step 4 and step 5
DEG C, extraction feed liquid weight ratio is 1:8, extraction time is 3h.Step 6：Take 70 parts of nano montmorillonite, dimension life respectively by weight
Plain C8 parts, 3 parts of hyaluronic acid, 8 parts of cetostearyl alcohol, 6 parts of rose 30wt% ethanol water extract, the overcritical dioxy of tulip
Change 8 parts of carbon extract, 3 parts of shrub althea flower ethanol extract, 3 parts of folium eucalypti rattan ethyl acetate extract, silver tip pekoe ethanol extract 2
Part, 4 parts of brier ethanol extract, 1 part of orange oil, 0.5 part of raspberry ketone, 0.6 part of citronellyl acetate, 1.4 parts of heliotropin,
40 parts of deionized water, above-mentioned composition is mixed to uniform, is nano montmorillonite deep layer cleaning moisture-keeping cosmetics.
Embodiment 4
Step 1：By rose crushed after being dried, heating extraction is stirred with 30wt% ethanol waters, extraction temperature is
60 DEG C, extraction feed liquid weight ratio is 1:5, extraction time 3h, centrifuged after extraction, then by supernatant concentration, obtain rose
Flower 30wt% ethanol water extracts；Step 2：By tulip crushed after being dried, then supercritical carbon dioxide extracting is carried out, it is overcritical
Extracting pressure is 25MPa, and one-level separating still pressure is 9.5MPa, and the auxiliary pressure of the second-order separation is 7MPa, extraction time 3h, is extracted
Temperature is 55 DEG C, and one-level extract and two level extract are collected after extraction, merges, is tulip supercritical carbon dioxide extracting
Thing；Step 3：Carried shrub althea flower crushed after being dried, then with absolute ethyl alcohol and stirring hot dipping, hot dipping centrifuges after carrying, then carries out true
Sky concentration, is prepared as shrub althea flower ethanol extract；Step 4：Hot dipping is stirred folium eucalypti rattan crushed after being dried, then with ethyl acetate
Carry, hot dipping centrifuges after carrying, then is concentrated in vacuo, and is prepared as folium eucalypti rattan ethyl acetate extract；Step 5：Pekoe silver
Pin and brier crushed after being dried, then carried with absolute ethyl alcohol and stirring hot dipping, hot dipping centrifuges after carrying, then is concentrated in vacuo,
It is prepared as silver tip pekoe ethanol extract and brier ethanol extract；Extraction temperature is 50 in step 3, step 4 and step 5
DEG C, extraction feed liquid weight ratio is 1:8, extraction time is 3h.Step 6：Take 40 parts of nano montmorillonite, dimension life respectively by weight
Plain C3 parts, 5 parts of hyaluronic acid, 4 parts of cetostearyl alcohol, 3 parts of rose 30wt% ethanol water extract, the overcritical dioxy of tulip
Change 3 parts of carbon extract, 5 parts of shrub althea flower ethanol extract, 6 parts of folium eucalypti rattan ethyl acetate extract, silver tip pekoe ethanol extract 4
Part, 5 parts of brier ethanol extract, 0.7 part of orange oil, 1 part of raspberry ketone, 1.2 parts of citronellyl acetate, 0.8 part of heliotropin,
30 parts of deionized water, above-mentioned composition is mixed to uniform, is nano montmorillonite deep layer cleaning moisture-keeping cosmetics.
Comparative example 1
Step 1：By rose crushed after being dried, heating extraction is stirred with 30wt% ethanol waters, extraction temperature is
60 DEG C, extraction feed liquid weight ratio is 1:5, extraction time 3h, centrifuged after extraction, then by supernatant concentration, obtain rose
Flower 30wt% ethanol water extracts；Step 2：By tulip crushed after being dried, then supercritical carbon dioxide extracting is carried out, it is overcritical
Extracting pressure is 25MPa, and one-level separating still pressure is 9.5MPa, and the auxiliary pressure of the second-order separation is 7MPa, extraction time 3h, is extracted
Temperature is 55 DEG C, and one-level extract and two level extract are collected after extraction, merges, is tulip supercritical carbon dioxide extracting
Thing；Step 3：Carried shrub althea flower crushed after being dried, then with absolute ethyl alcohol and stirring hot dipping, hot dipping centrifuges after carrying, then carries out true
Sky concentration, is prepared as shrub althea flower ethanol extract；Step 4：Hot dipping is stirred folium eucalypti rattan crushed after being dried, then with ethyl acetate
Carry, hot dipping centrifuges after carrying, then is concentrated in vacuo, and is prepared as folium eucalypti rattan ethyl acetate extract；Step 5：Pekoe silver
Pin and brier crushed after being dried, then carried with absolute ethyl alcohol and stirring hot dipping, hot dipping centrifuges after carrying, then is concentrated in vacuo,
It is prepared as silver tip pekoe ethanol extract and brier ethanol extract；Extraction temperature is 50 in step 3, step 4 and step 5
DEG C, extraction feed liquid weight ratio is 1:8, extraction time is 3h.Step 6：Take 5 parts of vitamin C, hyaluronic acid respectively by weight
7 parts, 3 parts of cetostearyl alcohol, 2 parts of rose 30wt% ethanol water extract, 10 parts of tulip supercritical carbon dioxide extracting thing,
2 parts of shrub althea flower ethanol extract, 8 parts of folium eucalypti rattan ethyl acetate extract, 5 parts of silver tip pekoe ethanol extract, brier ethanol carry
2 parts of thing, 2 parts of orange oil, 0.3 part of raspberry ketone, 0.4 part of citronellyl acetate, 2 parts of heliotropin, 50 parts of deionized water are taken, will be upper
The composition stated is mixed to uniform, is deep layer cleaning moisture-keeping cosmetics.
Comparative example 2
Step 1：Carried shrub althea flower crushed after being dried, then with absolute ethyl alcohol and stirring hot dipping, hot dipping centrifuges after carrying, then enters
Row is concentrated in vacuo, and is prepared as shrub althea flower ethanol extract；Step 2：Heat is stirred folium eucalypti rattan crushed after being dried, then with ethyl acetate
Extraction, hot dipping centrifuges after carrying, then is concentrated in vacuo, and is prepared as folium eucalypti rattan ethyl acetate extract；Step 3：Pekoe
Acupuncture needle and brier crushed after being dried, then carried with absolute ethyl alcohol and stirring hot dipping, hot dipping centrifuges after carrying, then to carry out vacuum dense
Contracting, is prepared as silver tip pekoe ethanol extract and brier ethanol extract；Extraction temperature is equal in step 1, step 2 and step 3
For 50 DEG C, extraction feed liquid weight ratio is 1:8, extraction time is 3h.Step 4：Take respectively by weight 80 parts of nano montmorillonite,
5 parts of vitamin C, 7 parts of hyaluronic acid, 3 parts of cetostearyl alcohol, 2 parts of shrub althea flower ethanol extract, folium eucalypti rattan ethyl acetate extract
8 parts, 5 parts of silver tip pekoe ethanol extract, 2 parts of brier ethanol extract, 2 parts of orange oil, 0.3 part of raspberry ketone, acetic acid lemongrass
0.4 part of ester, 2 parts of heliotropin, 50 parts of deionized water, above-mentioned composition is mixed to uniform, be that nano montmorillonite deep layer is clean
Moisture-keeping cosmetics.
Comparative example 3
Step 1：By rose crushed after being dried, heating extraction is stirred with 30wt% ethanol waters, extraction temperature is
60 DEG C, extraction feed liquid weight ratio is 1:5, extraction time 3h, centrifuged after extraction, then by supernatant concentration, obtain rose
Flower 30wt% ethanol water extracts；Step 2：By tulip crushed after being dried, then supercritical carbon dioxide extracting is carried out, it is overcritical
Extracting pressure is 25MPa, and one-level separating still pressure is 9.5MPa, and the auxiliary pressure of the second-order separation is 7MPa, extraction time 3h, is extracted
Temperature is 55 DEG C, and one-level extract and two level extract are collected after extraction, merges, is tulip supercritical carbon dioxide extracting
Thing；Step 3：Carried silver tip pekoe and brier crushed after being dried, then with absolute ethyl alcohol and stirring hot dipping, centrifugation point after hot dipping carries
From, then be concentrated in vacuo, it is prepared as silver tip pekoe ethanol extract and brier ethanol extract；Extraction temperature in step 3
It it is 50 DEG C, extraction feed liquid weight ratio is 1:8, extraction time is 3h.Step 4：Take nano montmorillonite 80 respectively by weight
Part, 5 parts of vitamin C, 7 parts of hyaluronic acid, 3 parts of cetostearyl alcohol, 2 parts of rose 30wt% ethanol water extract, tulip surpass and faced
10 parts of boundary's carbon dioxide abstraction thing, 5 parts of silver tip pekoe ethanol extract, 2 parts of brier ethanol extract, 2 parts of orange oil, raspberry
0.3 part of ketone, 0.4 part of citronellyl acetate, 2 parts of heliotropin, 50 parts of deionized water, above-mentioned composition is mixed to uniform, to receive
Rice montmorillonite deep layer cleaning moisture-keeping cosmetics.
The deep layer of embodiments of the invention and the cosmetics of comparative example is tried out respectively by 200 triers randomly selected
Clean and moisture-keeping efficacy, it is 20 days to try out the time, daily to carry out facial application with cosmetics of the invention, and the daily application time is
30min.Specific effect, the skin cleaning situation of trier and the moistening effect of skin are observed, improvement situation, which is divided into, to be significantly improved
Be effectively improved, situation is as follows：
It is as follows that the cosmetics of comparative example improve situation：
As can be seen that the survey for passing through the nano montmorillonite depth cleaning moisture-keeping cosmetics effect to preparation from above-mentioned two table
Examination, nano montmorillonite depth cleaning moisture-keeping cosmetics of the invention have to improving the greasy degree of skin, improving the elastic of skin
Play the role of very good, its is average to significantly improve rate 90% or so, far above the improvement rate of comparative example.Comparative example 1,2,3
In due to being not added with nano montmorillonite, rose 30wt% ethanol water extract, tulip supercritical carbon dioxide extracting thing, wood
Rose of Sharon flower ethanol extract, folium eucalypti rattan ethyl acetate extract, its improvement rate to skin are all greatly reduced, and nanometer of the invention is covered
De- stone depth cleaning moisture-keeping cosmetics achieve unexpected technique effect.
Claims (1)
1. a kind of nano montmorillonite deep layer cleaning moisture-keeping cosmetics, it is characterised in that described cosmetics include following weight parts
Composition：
Nano montmorillonite 40-70 parts,
Vitamin C 3-8 parts,
Hyaluronic acid 3-5 parts,
Cetostearyl alcohol 4-8 parts,
Rose 30wt% ethanol water extract 3-6 parts,
Tulip supercritical carbon dioxide extracting thing 3-8 parts,
Shrub althea flower ethanol extract 3-5 parts,
Folium eucalypti rattan ethyl acetate extract 3-6 parts,
Silver tip pekoe ethanol extract 4-5 parts,
Brier ethanol extract 2-4 parts,
Orange oil 0.7-1 parts,
Raspberry ketone 0.5-1 parts,
Citronellyl acetate 0.6-1.2 parts,
Heliotropin 0.8-1.4 parts,
Deionized water 30-40 parts；
A kind of described nano montmorillonite deep layer cleaning moisture-keeping cosmetics are prepared by following preparation methods：
Step 1：By rose crushed after being dried, heating extraction is stirred with 30wt% ethanol waters, centrifugation point after extraction
From, then by supernatant concentration, obtain rose 30wt% ethanol water extracts；
Step 2：By tulip crushed after being dried, then carry out supercritical carbon dioxide extracting, after extraction collect one-level extract and
Two level extract, merge, be tulip supercritical carbon dioxide extracting thing；
Step 3：Carried shrub althea flower crushed after being dried, then with absolute ethyl alcohol and stirring hot dipping, hot dipping centrifuges after carrying, then carries out true
Sky concentration, is prepared as shrub althea flower ethanol extract；
Step 4：Carried folium eucalypti rattan crushed after being dried, then with ethyl acetate stirring hot dipping, hot dipping centrifuges after carrying, then carries out true
Sky concentration, is prepared as folium eucalypti rattan ethyl acetate extract；
Step 5：Carried silver tip pekoe and brier crushed after being dried, then with absolute ethyl alcohol and stirring hot dipping, centrifugation point after hot dipping carries
From, then be concentrated in vacuo, it is prepared as silver tip pekoe ethanol extract and brier ethanol extract；
Step 6：Take nano montmorillonite 40-70 parts, vitamin C 3-8 parts, hyaluronic acid 3-5 parts, cetostearyl alcohol respectively by weight
4-8 parts, rose 30wt% ethanol water extract 3-6 parts, tulip supercritical carbon dioxide extracting thing 3-8 parts, shrub althea flower ethanol
Extract 3-5 parts, folium eucalypti rattan ethyl acetate extract 3-6 parts, silver tip pekoe ethanol extract 4-5 parts, brier ethanol extract
2-4 parts, orange oil 0.7-1 parts, raspberry ketone 0.5-1 parts, citronellyl acetate 0.6-1.2 parts, heliotropin 0.8-1.4 parts, go
Ionized water 30-40 parts, above-mentioned composition is mixed to uniform, is nano montmorillonite deep layer cleaning moisture-keeping cosmetics；
Extraction temperature is 60 DEG C in described step 1, and extraction feed liquid weight ratio is 1:5, extraction time 3h；
Supercritical extract pressure is 25MPa in described step 2, and one-level separating still pressure is 9.5MPa, the second-order separation kettle pressure
For 7MPa, extraction time 3h, extraction temperature is 55 DEG C；
Extraction temperature is 50 DEG C in described step 3, step 4 and step 5, and extraction feed liquid weight ratio is 1:8, extraction time
It is 3h；
Described drying mode includes the one or more in vacuum drying, heated-air drying, microwave drying；
Described centrifugation rotating speed is 2000-8000rpm.
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| CN101416932A (en) * | 2007-10-22 | 2009-04-29 | 武汉启明科技有限责任公司 | Nano montmorillonite mask and production method thereof |
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| CN104586712A (en) * | 2013-10-31 | 2015-05-06 | 马文 | Whitening hand cream |
| CN103550424B (en) * | 2013-11-07 | 2015-05-13 | 扬州大学 | Face cleaning product with acne treating effect and preparation method of face cleaning product |
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