CN108721157A - A kind of preparation method of the anti-oxidant gel facial mask of Exocarpium Citri Grandis - Google Patents
A kind of preparation method of the anti-oxidant gel facial mask of Exocarpium Citri Grandis Download PDFInfo
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/736—Chitin; Chitosan; Derivatives thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
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Abstract
The invention discloses a kind of preparation methods of the anti-oxidant gel facial mask of Exocarpium Citri Grandis, including:A, the preparation of Exocarpium Citri Grandis:The fresh Citrus grandis of medium well is picked, cleans, dry, moisture is dried at a temperature of 90 DEG C, pretreatment obtains Exocarpium Citri Grandis;B, flavones is extracted:Exocarpium Citri Grandis softens, and is sliced, and smashes, and microwave wave Assisted Ethanol extracts flavones, obtains flavone extractive;C, gel facial mask is prepared:Take acrylamide dimethyltaurine ammonium/VP copolymers(Ice crystal forming agent AVC), glycerine, carboxymethyl chitosan, hyaluronic acid, flavone extractive, shaddock essential oil and Phenoxyethanol, micro- heating stirring make to be uniformly mixed, and obtains the facial mask.The facial mask have amber glittering and translucent appearance and shaddock faint scent, it is of low cost, make it is simple, smear it is convenient, and with good moisturizing, antibacterial and antioxidant effect, meets the needs of Exocarpium Citri Grandis products diversification again simultaneously, meet the relevant regulations about gel facial mask in QB/T2872-2007, therefore there is stronger exploitation prospect.
Description
Technical field
The present invention relates to daily cosmetics preparing technical field, the preparation of specifically a kind of anti-oxidant gel facial mask of Exocarpium Citri Grandis
Method.
Background technology
State Intellectual Property Office discloses publication number CN104434651A in 2015-03-25, and patent name is a kind of disposable
The patent document of beauty face-whitening-nourishing sleep mask and preparation method thereof, patent document is using 1% carbomer gel, 1% gel shape
At agent, STABILEZE QM solution, 5% sodium alginate gel, 1% ice crystal forming agent AVC solution, amino acid humectant, water-soluble
Property jojoba oil, glycerine, trehalose, watermiscible vitamin E, vitamin C, forget-me-not extracting solution, Flos Lonicerae extractive solution, cucumber squeeze
It is prepared by raw material compounding to take liquid, efficient antiseptic Glydant, 30% triethanolamine solution, distilled water.Sleep prepared by the present invention
Facial mask is disposable, compensates for the defect that massage cream frequent cannot use, and effectively releives battle-weary and promotes sleep quality.
State Intellectual Property Office discloses publication number CN105310945A in 2016-02-10, and patent name is a kind of skin
The patent document of face pack cream and preparation method thereof is repaired, patent document is using plant creams emulsifier, house oil, Purple Perilla Seed Oil 1
Part, BHT, root bark of tree peony powder, angle sand alkane, ceramide, VB5, ice crystal forming agent, natural epidermal growth factor, distilled water, glycerine, 1.3
Butanediol, rice bran hydrosol, natural antibacterial agent compounding are made.After entire technical recipe is emulsified, the frost worked it out is mainly
To the repair to skin, increase the nutrition of skin adipose membrane and moist degree, to slowly improve the glossy degree of skin, equilibrium oil
While fat, reach softening skin, the effect of repair cell.
Exocarpium Citri Grandis is the prematurity of rutaceae Citrus grandis or shaddock or maturescent dry outer epidermal layer, is clinically used for controlling
Treatment cough due to wind-cold evil, the abundant expectoration circulation of vital energy in the wrong direction, dyspepsia heating and the bored equal diseases of evil of vomitting ruffian, are Guangdong famous and expensive special local product medicinal materials.Flavones is Exocarpium Citri Grandis
One of principle active component has the effects that anti-oxidant, anti-aging, adjusts metabolism, removes fatigue and improve immunity.
Aurantiin and a small amount of Rhoifolin, Poncirus glycosides and neohesperidin are mainly contained in Exocarpium Citri Grandis flavone component.At present to Exocarpium Citri Grandis
Exploitation is mainly in medicine materical crude slice, beverage, health liquor, health protection tea, oral solution, tablet and capsule etc..From the special of published gel facial mask
From the point of view of profit, the complicated component of facial mask, high expensive;The carbomer added in facial mask needs to be adjusted to triethanolamine in acidity
Neutrality, operation are comparatively laborious.Therefore, patent of the present invention is in view of the above-mentioned problems, provide a kind of anti-oxidant gel facial mask of Exocarpium Citri Grandis
Preparation method, it is not only of low cost, make simple, while having good anti-oxidant, moisturizing concurrently, the multiple functions such as antibacterial.
Invention content
The purpose of the present invention is to provide a kind of preparation method of the anti-oxidant gel facial mask of Exocarpium Citri Grandis, this method can be effective
Using the antioxygenic property of Exocarpium Citri Grandis extract, while developing with good antioxidant effect skin-protection product, the product odour
Fragrance has amber glittering and translucent appearance, and it is convenient to smear.The application range of Exocarpium Citri Grandis has also been expanded simultaneously.
To achieve the above object, the present invention provides the following technical solutions:
The preparation method of the anti-oxidant gel facial mask of Exocarpium Citri Grandis, includes the following steps:
A, the preparation of Exocarpium Citri Grandis:The fresh Citrus grandis of medium well is picked, cleans, dry, moisture is dried at a temperature of 90 DEG C, is pre-processed
Obtain Exocarpium Citri Grandis;
B, flavones is extracted:Exocarpium Citri Grandis softens 8~10min, and slice to 3~5mm is smashed to 80~100 mesh, and Microwave-Assisted Ethanol carries
The flavones, extraction conditions is taken to be:The volumetric concentration of 250~400W of microwave power, 2~8min of extraction time, ethyl alcohol are 40~50%,
40 DEG C of Extracting temperature, solid-liquid ratio 1:30, obtain flavone extractive;
C, gel facial mask is prepared:Take ice crystal forming agent 6.0g, 1.0~5.0g of glycerine, 2.0~4.0 g of carboxymethyl chitosan, flavones
0.5~3.5ml of extracting solution, 1.5~2.0 ml of hyaluronic acid, are added ice crystal forming agent, glycerine and carboxymethyl chitosan quality it
0.05~0.5% benzene oxygen of the shaddock essential oil and ice crystal forming agent of the 1~3% of sum, glycerine and carboxymethyl chitosan quality sum
Ethyl alcohol, micro- heating stirring make to be uniformly mixed, and obtain the anti-oxidant gel facial mask of Exocarpium Citri Grandis;The anti-oxidant gel facial mask of Exocarpium Citri Grandis is taken out,
It is sealed with the dry plastic tank of cleaning.
As a further solution of the present invention:In the step A, medium well Citrus grandis in 5~June is picked.
As a further solution of the present invention:In the step B, Exocarpium Citri Grandis softening is by the way of steaming.
As a further solution of the present invention:In the step B, ultrasonic power 400W, extraction time 5min.
As a further solution of the present invention:In the step B, the volumetric concentration of ethyl alcohol is 50%.
As a further solution of the present invention:In the step C, ice crystal forming agent 6.0g, glycerine 5.0g, carboxylic first are taken
Base enclosure glycan 2.0 g, flavone extractive 0.5ml.
As a further solution of the present invention:In the step C, ice crystal forming agent, glycerine and carboxymethyl chitosan is added
0.5% benzene oxygen second of the shaddock essential oil and ice crystal forming agent of the 1% of sugared quality sum, glycerine and carboxymethyl chitosan quality sum
Alcohol.
As a further solution of the present invention:In the step C, the temperature of micro- heating stirring is 45~50 DEG C.
Compared with prior art, the beneficial effects of the invention are as follows:
Exocarpium Citri Grandis aurantiin has good antioxidant effect, and there is no obtain as the Exocarpium Citri Grandis extract of natural
It is utilized to effective.The present invention develops the mask product with antioxidant activity, and new direction is pointed out for Exocarpium Citri Grandis resource application.
In the present invention, the raw material of use is the Citrus grandis of medium well, because of the naringin content of the Citrus grandis of medium well
Higher than ripe Citrus grandis.It is to allow flavones more to leach to increase specific surface area that Exocarpium Citri Grandis slice, which crushes,.It is auxiliary using microwave
It is the effect using broken microwave cell wall to help extraction, and the flavones in cell is made more to discharge.Ethyl alcohol can be effective as solvent
Extracting flavone there are a large amount of water-soluble substances to dissolve out when ethyl alcohol volumetric concentration is less than 50%, cause to filter it is difficult, it is advantageous to
50% ethyl alcohol has the characteristics that volatile as solvent in conjunction with ethyl alcohol, can recycle ethyl alcohol recycling, and filtered after extracting
Filter residue can be used as fertilizer.
The anti-oxidant gel facial mask of Exocarpium Citri Grandis that the present invention makes, neutral condensate can be quickly formed due to containing ice crystal forming agent
Glue assigns the glittering and translucent appearance of facial mask and good sticking nature;Carboxymethyl chitosan can be effectively antibacterial;Glycerine and hyalomitome
Acid can effectively keep facial mask to moisten, and give skin of face moisturizing moisturizing;And Exocarpium Citri Grandis extract(Flavone extractive)With good
Antioxidant effect, to delay skin of face aging;Shaddock essential oil can assign the fresh fragrance of Exocarpium Citri Grandis facial mask Citrus grandis;Benzene oxygen
Ethyl alcohol can prevent Exocarpium Citri Grandis facial mask moldy metamorphism.
Using above-mentioned technical proposal, the anti-oxidant gel facial mask of Exocarpium Citri Grandis obtained has the novel aroma, at low cost of shaddock
It is honest and clean, make it is simple, smear convenient, and there is good antibacterial, moisture-keeping function, antioxidant effect is notable, while satisfactionization tangerine again
The demand of red products diversification meets the relevant regulations about gel facial mask in QB/T2872-2007, therefore is opened with stronger
Send out Utilization prospects.
Specific implementation mode
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, the preparation method of the anti-oxidant gel facial mask of Exocarpium Citri Grandis includes the following steps:
A, the preparation of Exocarpium Citri Grandis:The fresh Citrus grandis of medium well is picked, cleans, dry, moisture is dried at a temperature of 90 DEG C, is pre-processed
Obtain Exocarpium Citri Grandis;
B, flavones is extracted:Exocarpium Citri Grandis softens 8~10min, and slice to 3~5mm is smashed to 80~100 mesh, and Microwave-Assisted Ethanol carries
The flavones, extraction conditions is taken to be:The volumetric concentration of ultrasonic power 400W, extraction time 5min, ethyl alcohol are 50%, 40 DEG C of Extracting temperature,
Solid-liquid ratio is 1:30, obtain flavone extractive;
C, gel facial mask is prepared:Take ice crystal forming agent 6.0g, glycerine 1.0g, carboxymethyl chitosan 4.0g, flavone extractive
Ice crystal forming agent is added in 0.5ml, and the 1% shaddock essential oil and ice crystal forming agent of glycerine and carboxymethyl chitosan quality sum are sweet
0.05% Phenoxyethanol of oil and carboxymethyl chitosan quality sum, micro- heating stirring make to be uniformly mixed, and obtain Exocarpium Citri Grandis antioxygen
Change gel facial mask;The anti-oxidant gel facial mask of Exocarpium Citri Grandis is taken out, is sealed with the dry plastic tank of cleaning.
Embodiment 2
In the embodiment of the present invention, the preparation method of the anti-oxidant gel facial mask of Exocarpium Citri Grandis includes the following steps:
A, the preparation of Exocarpium Citri Grandis:The fresh Citrus grandis of medium well is picked, cleans, dry, moisture is dried at a temperature of 90 DEG C, is pre-processed
Obtain Exocarpium Citri Grandis;
B, flavones is extracted:Exocarpium Citri Grandis softens 8~10min, and slice to 3~5mm is smashed to 80~100 mesh, and Microwave-Assisted Ethanol carries
The flavones, extraction conditions is taken to be:The volumetric concentration of ultrasonic power 300W, extraction time 10min, ethyl alcohol are 50%, Extracting temperature 40
DEG C, solid-liquid ratio 1:30, obtain flavone extractive;
C, gel facial mask is prepared:Take ice crystal forming agent 6.0g, glycerine 5.0g, carboxymethyl chitosan 3.0g, flavone extractive
Ice crystal forming agent is added in 3.5ml, and the 2% shaddock essential oil and ice crystal forming agent of glycerine and carboxymethyl chitosan quality sum are sweet
0.15% Phenoxyethanol of oil and carboxymethyl chitosan quality sum, micro- heating stirring make to be uniformly mixed, and obtain Exocarpium Citri Grandis antioxygen
Change gel facial mask;The anti-oxidant gel facial mask of Exocarpium Citri Grandis is taken out, is sealed with the dry plastic tank of cleaning.
Embodiment 3
In the embodiment of the present invention, the preparation method of the anti-oxidant gel facial mask of Exocarpium Citri Grandis includes the following steps:
A, the preparation of Exocarpium Citri Grandis:The fresh Citrus grandis of medium well is picked, cleans, dry, moisture is dried at a temperature of 90 DEG C, is pre-processed
Obtain Exocarpium Citri Grandis;
B, flavones is extracted:Exocarpium Citri Grandis softens 8~10min, and slice to 3~5mm is smashed to 80~100 mesh, and Microwave-Assisted Ethanol carries
The flavones, extraction conditions is taken to be:The volumetric concentration of microwave power 150W, extraction time 2min, ethyl alcohol are 40%, 40 DEG C of Extracting temperature,
Solid-liquid ratio is 1:30, obtain flavone extractive;
C, gel facial mask is prepared:Take ice crystal forming agent 6.0g, glycerine 3.0g, carboxymethyl chitosan 2.0g, flavone extractive
Ice crystal forming agent is added in 2.5ml, and the 3% shaddock essential oil and ice crystal forming agent of glycerine and carboxymethyl chitosan quality sum are sweet
0.5% Phenoxyethanol of oil and carboxymethyl chitosan quality sum, micro- heating stirring make to be uniformly mixed, and obtain Exocarpium Citri Grandis antioxygen
Change gel facial mask;The anti-oxidant gel facial mask of Exocarpium Citri Grandis is taken out, is sealed with the dry plastic tank of cleaning.
The anti-oxidant gel facial mask of Exocarpium Citri Grandis produced by the present invention have shaddock novel aroma, it is of low cost, make it is simple,
It is convenient to smear, and has good antibacterial, moisture-keeping function, and antioxidant effect is notable, while meeting Exocarpium Citri Grandis products diversification again
Demand, meet the relevant regulations about gel facial mask in QB/T2872-2007, therefore there is stronger exploitation prospect.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Profit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiment being appreciated that.
Claims (8)
1. the preparation method of the anti-oxidant gel facial mask of Exocarpium Citri Grandis, which is characterized in that include the following steps:
A, the preparation of Exocarpium Citri Grandis:The fresh Citrus grandis of medium well is picked, cleans, dry, moisture is dried at a temperature of 90 DEG C, is pre-processed
Obtain Exocarpium Citri Grandis;
B, flavones is extracted:Exocarpium Citri Grandis softens 8~10min, and slice to 3~5mm is smashed to 80~100 mesh, and Microwave-Assisted Ethanol carries
The flavones, extraction conditions is taken to be:The volumetric concentration of 250~400W of microwave power, 2~8min of extraction time, ethyl alcohol are 40~50%,
40 DEG C of Extracting temperature, solid-liquid ratio 1:30, obtain flavone extractive;
C, gel facial mask is prepared:Take ice crystal forming agent 6.0g, 1.0~5.0g of glycerine, carboxymethyl chitosan 2.0~4.0 g are transparent
Ice crystal forming agent, glycerine and carboxymethyl chitosan quality sum is added in matter 0.5~2.0ml of acid, 0.5~3.5ml of flavone extractive
1~3% shaddock essential oil and ice crystal forming agent, 0.05~0.5% benzene oxygen second of glycerine and carboxymethyl chitosan quality sum
Alcohol, micro- heating stirring make to be uniformly mixed, and obtain the anti-oxidant gel facial mask of Exocarpium Citri Grandis;The anti-oxidant gel facial mask of Exocarpium Citri Grandis is taken out, is used
The dry plastic tank of cleaning is sealed.
2. the preparation method of the anti-oxidant gel facial mask of Exocarpium Citri Grandis according to claim 1, which is characterized in that the step
In A, medium well Citrus grandis in 5~June is picked.
3. the preparation method of the anti-oxidant gel facial mask of Exocarpium Citri Grandis according to claim 1, which is characterized in that the step
In B, Exocarpium Citri Grandis softening is by the way of steaming.
4. the preparation method of the anti-oxidant gel facial mask of Exocarpium Citri Grandis according to claim 1, which is characterized in that the step
In B, ultrasonic power 400W, extraction time 5min.
5. the preparation method of the anti-oxidant gel facial mask of Exocarpium Citri Grandis according to claim 1, which is characterized in that the step
In B, the volumetric concentration of ethyl alcohol is 50%.
6. the preparation method of the anti-oxidant gel facial mask of Exocarpium Citri Grandis according to claim 1, which is characterized in that the step
In C, ice crystal forming agent 6.0g, glycerine 5.0g, 2.0 grams, hyaluronic acid 2.0ml of carboxymethyl chitosan, flavone extractive are taken
0.5ml。
7. the preparation method of the anti-oxidant gel facial mask of Exocarpium Citri Grandis according to claim 1, which is characterized in that the step
In C, be added ice crystal forming agent, glycerine and carboxymethyl chitosan quality sum 1% shaddock essential oil and ice crystal forming agent, glycerine
With the Phenoxyethanol of carboxymethyl chitosan quality sum 0.5%.
8. the preparation method of the anti-oxidant gel facial mask of Exocarpium Citri Grandis according to claim 1, which is characterized in that the step C
In, the temperature of micro- heating stirring is 45~50 DEG C.
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106389247A (en) * | 2016-09-14 | 2017-02-15 | 广东石油化工学院 | Preparation method of exocarpium citri grandis anti-oxidant pasty facial mask |
CN109602669A (en) * | 2019-02-22 | 2019-04-12 | 冯涛 | A kind of skin-care gel and preparation method thereof |
CN110200879A (en) * | 2019-07-19 | 2019-09-06 | 广西轻工业科学技术研究院有限公司 | A kind of mulberries red wine gel facial mask and preparation method thereof rich in silkworm chrysalis polypeptide |
WO2023096505A1 (en) * | 2021-11-23 | 2023-06-01 | Bio Natural Solutions S.A.C. | Method for obtaining a composition and a colloidal suspension of flavonoids from peels of fruits of the family rutaceae and the genus citrus, and the composition and colloidal suspension thus obtained |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105310945A (en) * | 2015-12-15 | 2016-02-10 | 钟苏 | Skin repair mask cream and preparation method thereof |
CN106389247A (en) * | 2016-09-14 | 2017-02-15 | 广东石油化工学院 | Preparation method of exocarpium citri grandis anti-oxidant pasty facial mask |
-
2017
- 2017-04-21 CN CN201710264049.1A patent/CN108721157A/en active Pending
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105310945A (en) * | 2015-12-15 | 2016-02-10 | 钟苏 | Skin repair mask cream and preparation method thereof |
CN106389247A (en) * | 2016-09-14 | 2017-02-15 | 广东石油化工学院 | Preparation method of exocarpium citri grandis anti-oxidant pasty facial mask |
Non-Patent Citations (1)
Title |
---|
何志成主编: "《化工原理》", 31 August 2015, 中国医药科技出版社 * |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106389247A (en) * | 2016-09-14 | 2017-02-15 | 广东石油化工学院 | Preparation method of exocarpium citri grandis anti-oxidant pasty facial mask |
CN109602669A (en) * | 2019-02-22 | 2019-04-12 | 冯涛 | A kind of skin-care gel and preparation method thereof |
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