CN102552092B - A vine tea mask capsule and a method of preparing the same - Google Patents
A vine tea mask capsule and a method of preparing the same Download PDFInfo
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- CN102552092B CN102552092B CN 201210039472 CN201210039472A CN102552092B CN 102552092 B CN102552092 B CN 102552092B CN 201210039472 CN201210039472 CN 201210039472 CN 201210039472 A CN201210039472 A CN 201210039472A CN 102552092 B CN102552092 B CN 102552092B
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- ampelopsis grossedentata
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Abstract
The invention relates to a method of preparing a vine tea mask capsule. The method comprises the steps of preparing vine tea powder, degreasing, extracting vine tea flavonoid, crystallizing and removing impurities, crushing and disinfecting, preparing mask capsule powder and finally filling the powder into a capsule. The vine tea mask capsule is composed of pure plant components, is antiseptic-free and additive-free, and causes no irritation and harm to skins. When a user is using the capsule, the user opens the capsule, fetches 80ML hot water with 80 DEG C, and slowly and uniformly pours the powder in the capsule into the hot water while stirring. The user stirs the capsule powder to make the power fully dissolved and then pours into a mold plate. When the dissolved powder is cooled to be a mask, the user applies the mask onto the face for 20 to 30 minutes. The vine tea mask is prepared from pure natural konjac gum andxanthan gum, is crystal clear in appearance, and is fast in penetration and fine in absorption. No non-woven fabric needs to be a medium, and most essences are not liable to be absorbed by mask paper. Furthermore, various masks with beauty treatment efficacies can be prepared based on needs of skin whitening, skin dullness removal, rosy cheek improvement, acne clearance, toxin expelling or the like.
Description
Technical field
The present invention relates to a kind of cosmetics and preparation method thereof, be specifically related to a kind of Ampelopsis grossedentata mask capsule and preparation method thereof.
Background technology
Step into gradually aging and diet is unhealthy, Exposure to Sunlight, pressure, environmental pollution etc. along with Chinese society, the anti-aging beauty-care skin care item more and more are subject to people's attention.The data of China spices and essence cosmetics industry association issue show that defying age is the problem that present women is concerned about most.One of main factor of skin aging is that the skin photosensitiveness that caused by ultraviolet radiation is old and feeble, because ultraviolet is after infiltrating skin, can produce harmful free radical, these free radicals can destroy elastic fibers of skin, the stimulation melanin cell increases secretion, thereby cause xerosis cutis lax, accelerate old and feeble.So need to help reduce by replenishing antioxidant the generation of free radical.Present antioxidant has enzyme and non-enzyme two classes, and because of its poor stability, and molecular weight is larger, infiltrates skin and is restricted, and has limited its application in cosmetics.Recently the Molecular antioxidant substances that discovery is extracted from plant has very strong antioxidation, and more easily infiltrates skin, and is more stable.Plant flavonoids has very strong oxidation resistance, has free radical in the skin of removing, promotion skin metabolism, reduces the effects such as pigmentation, moist skin.Because flavones content is high in the Ampelopsis grossedentata, extract simple, can be developed into for safely, natural material in the green cosmetic field that has no side effect.
Application number is 01104418.7 patent of invention " a kind of biological anti-senility cosmetics " (applying date: 2001/02/26), introduced the crease-resistant emulsion of a kind of skin moistening.Though the main defying age composition cucumber extract of these cosmetics, Aloe extraction solution also are biotypes, but added Polyethylene Glycol as o/w type emulsifying agent and stabilizing agent, show that it has side effect to skin although go back no evidence, show when it influentially to gastric secretion and gastric acid output during as the solvent in the pharmaceutical preparation or substrate but have been reported, illustrate that it still has certain toxicity.
Application number is 200810030279.2 patent of invention " interpolation the anti-aging cosmetics " (applying date: 2008/08/20), introduced a kind of biomedical high nutritional type lyophilized powder, it adopts nanotechnology with the technical finesse of effective collagenic protein by lyophilized powder, uses the effective defying age composition of active ingredient transmission.Although this cosmetics absorbance is high, need to add antiseptic, and troublesome poeration, cost is also higher.
Application number is 01135113.6 patent of invention " the natural plant beauty skin-protection mask " (applying date: 2001/11/19), introduced a kind of powder face pack.Although this formula for a product also has the effect of anti-ageing wrinkle removal, its furnishing paste can only be smeared after adding water, and the paste fixed effect is not good enough, and is unfavorable for cleaning, use comparatively trouble.
Application number is patent of invention " a kind of konjac facial mask " (applying date: 2008/11/24), introduced a kind of konjac facial mask of 200810158986.x.Although this product also has certain Antiageing effect, this type of facial film needs Bao Installed cost, and storage life or antiseptical problem are arranged, and price is higher, not environmental protection, and variability is little simultaneously, can't fill a prescription according to the demand adjustment voluntarily, thereby cause using inconvenience.
Summary of the invention
In view of the deficiencies in the prior art, film property after the object of the invention is to utilize the anti-oxidation characteristics of flavone compound in the Ampelopsis grossedentata and Konjac glucomannan and xanthan gum composite, provide a kind of with low cost, safely, Ampelopsis grossedentata mask capsule of having no side effect, can being absorbed fast by skin and preparation method thereof.
The preparation method of a kind of Ampelopsis grossedentata mask capsule of the present invention is characterized in that operating procedure is as follows:
(1) preparation of Ampelopsis grossedentata powder: the chopping of Ampelopsis grossedentata tender leaf is placed in the baking oven, under 50～100 ℃ of conditions, toasted 48～60 hours, take out pulverizing and cross 60～80 mesh sieves, make the Ampelopsis grossedentata powder;
(2) ungrease treatment: the Ampelopsis grossedentata powder that step (1) is made, be that 10-30 ethyl acetate doubly is to carry out ungrease treatment under 50～70 ℃ of reflux states in temperature with quality, the defat response time is 1.6～2 hours, then filter, vacuum drying is 1～2 hour under 70～80 ℃ of conditions, removes ethyl acetate;
(3) extract the vine tea flavone compounds: (W/V) is 1:20～35 by the mass volume ratio of feed liquid, in extraction vessel, add Ampelopsis grossedentata powder and distilled water after step (2) ungrease treatment, reflux is 2～4 hours under 80～90 ℃ of conditions, be cooled to room temperature, with 3000～4000rpm centrifugalize, collect supernatant, be the vine tea flavone crude extract;
(4) crystallization remove impurity: vacuum concentration is to 1/10～1/20 of initial volume under 50 ℃ of conditions of vine tea flavone crude extract that step (3) is made, the deionized water and stirring that adds 1～2 times of concentrated solution volume is even, in boiling water bath, heated 20～30 minutes, leave standstill crystalline deposit, filter, get crystal, drying obtains vine tea flavone;
(5) pulverize and sterilization: the vine tea flavone that step (4) is made is pulverized and is crossed 1000～1200 mesh sieves, in 100～110 ℃ of lower sterilization treatment, can not check pathogenic bacterium to inspection, makes the vine tea flavone powder;
(6) preparation of mask capsule powder: the mask capsule powder comprises following each raw material, and the percentage rate that each raw material accounts for mask capsule powder gross mass is: vine tea flavone powder 20～26%, Konjac glucomannan 15～18%, xanthan gum 15～18%, soybean protein isolate 10～14%, arbutin 5～8%, hyaluronic acid (HA) 5～10%, Radix Scutellariae 4～8%, left-handed VC6～8%, allantoin 4～5%;
(7) incapsulate: incapsulate behind the mask capsule powder mix homogeneously with step (6) preparation.
Described Konjac glucomannan, xanthan gum, soybean protein isolate, hyaluronic acid, Radix Scutellariae, left-handed VC, arbutin, allantoin are cosmetics-stage.
The using method of capsule of the present invention is: every capsules is generally 0.45g.Open capsule during use, get the hot water of 80 ℃ of 80ML, stir on the limit, and the limit is slowly poured the powder in the capsule in the hot water into uniformly.Then be stirred to and pour lamina membranacea into after capsule powders is fully dissolved, cooling forming is facial film, and facial film is applied note in face, stops to get final product in 20-30 minute.
The present invention has the following advantages: 1, the anti-ageing wrinkle removal effect of the present invention significantly and its composition be pure plant component, the various chemical compositions such as preservative free, additive, the non-stimulated and injury to skin.Flavone extract has good defying age, antiinflammatory, antibacterial and the multiple skin-care effect such as brighten in the Ampelopsis grossedentata; Rhizoma amorphophalli glucomannan has antibiotic property, water absorption, non-oxidizability, can prevent the skin dehydration, alleviates old and feeble; Xanthan gum can promote collagen protein synthesis, and pre-anti-aging reduces microgroove, desalination melanin; Soybean protein isolate contains the multiple essential amino acids of human body and trace element, has very high nutritive value and health-care effect; Arbutin can suppress activity, desalination pigment, the whitening of tryrosinase in the skin.2, can prepare multiple beauty functions facial film.Can when dissolving, add the natural components such as milk, red wine, lotus-seed-heart powder, green tea powder according to needs such as self skin whitening, de-etiolation, ruddy, anti-acne toxin expellings, prepare at any time multiple facial film with above-mentioned functions.And dryness, oiliness and Combination skin all should use.
3, quick permeation, good absorbing.Formulated by pure natural Konjac glucomannan and xanthan gum, the facial film profile is glittering and translucent.Do not need non-woven fabrics to do medium, can be because face paper suck most of elite, therefore can real former absorption.Nutritional labeling all condenses in the facial film, with rapid permeability after the contact skin, and solution absorption gradually.
The specific embodiment
The present invention is further elaborated below in conjunction with embodiment.
Embodiment: a kind of preparation method of Ampelopsis grossedentata mask capsule may further comprise the steps:
(1) preparation of Ampelopsis grossedentata powder: the chopping of Ampelopsis grossedentata tender leaf is placed in the baking oven, and baking is 48 hours under 70 ℃ of conditions, takes out pulverizing and crosses 80 mesh sieves, makes the Ampelopsis grossedentata powder;
(2) ungrease treatment: the Ampelopsis grossedentata powder quality that step (1) is made is to carry out ungrease treatment under 60 ℃ of reflux states for its ethyl acetate of 8 times in temperature, the defat response time is 1.7 hours, then filter, vacuum drying is 2 hours under 70 ℃ of conditions, removes ethyl acetate;
(3) extract the vine tea flavone compounds: (W/V) is 1:30 by the mass volume ratio of feed liquid, in extraction vessel, add Ampelopsis grossedentata powder and distilled water after step (2) ungrease treatment, reflux is 3 hours under 90 ℃ of conditions, be cooled to room temperature, with the 4000rpm centrifugalize, collect supernatant, be the vine tea flavone crude extract;
(4) crystallization remove impurity: vacuum concentration is to 1/10 of initial volume under 50 ℃ of conditions of vine tea flavone crude extract that step (3) is made, the deionized water and stirring that adds 2 times of concentrated solution volumes is even, heating is 25 minutes in boiling water bath, leave standstill crystalline deposit, get crystallization after the filtration, the crystal behind the secondary filter is filtered, merged to the deionized water crystallization that filtrate is used equivalent more once, drying obtains vine tea flavone;
(5) pulverize and sterilization: the vine tea flavone that step (4) is made is pulverized and is crossed 1200 mesh sieves, in 100 ℃ of sterilization treatment, can not check pathogenic bacterium to inspection, makes the vine tea flavone powder;
(6) preparation of mask capsule powder: the mask capsule powder comprises following each raw material, and the percentage rate that each raw material accounts for mask capsule powder gross mass is: vine tea flavone powder 26%, Konjac glucomannan 17%, xanthan gum 17%, soybean protein isolate 12%, arbutin 8%, Radix Scutellariae 6%, left-handed VC 5%, hyaluronic acid (HA) 5%, allantoin 4%;
(7) incapsulate: the mask capsule powder with step (6) preparation incapsulates every capsules 0.45g behind the mix homogeneously.
The above only is preferred embodiment of the present invention, and all equalizations of doing according to the present patent application claim change and modify, and all should belong to covering scope of the present invention.
Claims (3)
1. the preparation method of an Ampelopsis grossedentata mask capsule is characterized in that operating procedure is as follows:
(1) preparation of Ampelopsis grossedentata powder: the chopping of Ampelopsis grossedentata tender leaf is placed in the baking oven, under 50～100 ℃ of conditions, toasted 48～60 hours, take out pulverizing and cross 60～80 mesh sieves, make the Ampelopsis grossedentata powder;
(2) ungrease treatment: the Ampelopsis grossedentata powder that step (1) is made, be that 10-30 ethyl acetate doubly is to carry out ungrease treatment under 50～70 ℃ of reflux states in temperature with quality, the defat response time is 1.6～2 hours, then filter, vacuum drying is 1～2 hour under 70～80 ℃ of conditions, removes ethyl acetate;
(3) extract the vine tea flavone compounds: (W/V) is 1:20～35 by the mass volume ratio of feed liquid, in extraction vessel, add Ampelopsis grossedentata powder and distilled water after step (2) ungrease treatment, reflux is 2～4 hours under 80～90 ℃ of conditions, be cooled to room temperature, with 3000～4000rpm centrifugalize, collect supernatant, be the vine tea flavone crude extract;
(4) crystallization remove impurity: vacuum concentration is to 1/10～1/20 of initial volume under 50 ℃ of conditions of vine tea flavone crude extract that step (3) is made, the deionized water and stirring that adds 1～2 times of concentrated solution volume is even, in boiling water bath, heated 20～30 minutes, leave standstill crystalline deposit, filter, get crystal, drying obtains vine tea flavone;
(5) pulverize and sterilization: the vine tea flavone that step (4) is made is pulverized and is crossed 1000～1200 mesh sieves, in 100～110 ℃ of lower sterilization treatment, can not check pathogenic bacterium to inspection, makes the vine tea flavone powder;
(6) preparation of mask capsule powder: the mask capsule powder comprises following each raw material, and the percentage rate that each raw material accounts for mask capsule powder gross mass is: vine tea flavone powder 20～26%, Konjac glucomannan 15～18%, xanthan gum 15～18%, soybean protein isolate 10～14%, arbutin 5～8%, hyaluronic acid 5～10%, Radix Scutellariae 4～8%, left-handed VC6～8%, allantoin 4～5%;
(7) incapsulate: the mask capsule powder with step (6) preparation incapsulates behind the mix homogeneously.
2. the preparation method of an Ampelopsis grossedentata mask capsule is characterized in that operating procedure is as follows:
(1) preparation of Ampelopsis grossedentata powder: the chopping of Ampelopsis grossedentata tender leaf is placed in the baking oven, and baking is 48 hours under 70 ℃ of conditions, takes out pulverizing and crosses 80 mesh sieves, makes the Ampelopsis grossedentata powder;
(2) ungrease treatment: the Ampelopsis grossedentata powder quality that step (1) is made is to carry out ungrease treatment under 60 ℃ of reflux states for its ethyl acetate of 8 times in temperature, the defat response time is 1.7 hours, then filter, vacuum drying is 2 hours under 70 ℃ of conditions, removes ethyl acetate;
(3) extract the vine tea flavone compounds: (W/V) is 1:30 by the mass volume ratio of feed liquid, in extraction vessel, add Ampelopsis grossedentata powder and distilled water after step (2) ungrease treatment, reflux is 3 hours under 90 ℃ of conditions, be cooled to room temperature, with the 4000rpm centrifugalize, collect supernatant, be the vine tea flavone crude extract;
(4) crystallization remove impurity: vacuum concentration is to 1/10 of initial volume under 50 ℃ of conditions of vine tea flavone crude extract that step (3) is made, the deionized water and stirring that adds 2 times of concentrated solution volumes is even, heating is 25 minutes in boiling water bath, leave standstill crystalline deposit, get crystallization after the filtration, the crystal behind the secondary filter is filtered, merged to the deionized water crystallization that filtrate is used equivalent more once, drying obtains vine tea flavone;
(5) pulverize and sterilization: the vine tea flavone that step (4) is made is pulverized and is crossed 1200 mesh sieves, in 100 ℃ of sterilization treatment, can not check pathogenic bacterium to inspection, makes the vine tea flavone powder;
(6) preparation of mask capsule powder: the mask capsule powder comprises following each raw material, and the percentage rate that each raw material accounts for mask capsule powder gross mass is: vine tea flavone powder 26%, Konjac glucomannan 17%, xanthan gum 17%, soybean protein isolate 12%, arbutin 8%, Radix Scutellariae 6%, left-handed VC 5%, hyaluronic acid 5%, allantoin 4%;
(7) incapsulate: the mask capsule powder with step (6) preparation incapsulates every capsules 0.45g behind the mix homogeneously.
3. by the Ampelopsis grossedentata mask capsule of the method for claim 1 or 2 preparation.
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Cited By (1)
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| US9827188B2 (en) | 2015-08-14 | 2017-11-28 | Johnson & Johnson Consumer Inc. | Compositions comprising ampelopsis grossedentata and albizia julibrissin extracts |
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| CN104706551A (en) * | 2013-12-13 | 2015-06-17 | 江南大学 | Facial cleanser containing ampelopsin grossedentata extract |
| CN103976899A (en) * | 2014-05-21 | 2014-08-13 | 广州佩尔美容器械制造有限公司 | Method for quickly preparing film and device thereof |
| CN104873428A (en) * | 2015-05-22 | 2015-09-02 | 周维新 | After-sun repair mask capsule |
| CN104873430A (en) * | 2015-05-22 | 2015-09-02 | 杨知雨 | Anti-inflammation mask capsule |
| CN104873422A (en) * | 2015-05-22 | 2015-09-02 | 周维新 | Whitening mask capsule |
| CN104873423A (en) * | 2015-05-22 | 2015-09-02 | 周维新 | Anti-wrinkle mask capsule |
| CN105213248A (en) * | 2015-08-07 | 2016-01-06 | 袁朝宁 | A kind of ecosystem fruit-vegetable facial mask pastes |
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| CN107519083A (en) * | 2017-08-28 | 2017-12-29 | 李冉冉 | Toner containing natural plant extracts |
| CN108938533B (en) * | 2018-07-31 | 2021-06-04 | 北京东方淼森生物科技有限公司 | Anti-aging skin care composition and preparation method and application thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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