CN109125177A - A kind of petal water and preparation method thereof of anti-ageing firm skin - Google Patents
A kind of petal water and preparation method thereof of anti-ageing firm skin Download PDFInfo
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- CN109125177A CN109125177A CN201811149768.XA CN201811149768A CN109125177A CN 109125177 A CN109125177 A CN 109125177A CN 201811149768 A CN201811149768 A CN 201811149768A CN 109125177 A CN109125177 A CN 109125177A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/347—Phenols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4913—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9717—Rhodophycota or Rhodophyta [red algae], e.g. Porphyra
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9741—Pteridophyta [ferns]
- A61K8/9749—Filicopsida or Pteridopsida
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
Abstract
The present invention relates to technical field of skin care; more particularly to a kind of petal water and preparation method thereof of anti-ageing firm skin, which includes the raw material of following parts by weight: 10-16 parts of petal liquid of pretreatment, 3-12 parts of acetylation hexapeptide, 8-16 parts of two peptide, 2-8 parts of coffee polyphenols, auxiliary anti-ageing active material 12-24 parts, 8-14 parts of moisturizer, 5-10 parts of reparative factor, 0.1-5.0 parts of anti-sensitizer of releiving, 55-75 parts of solvent.Petal water raw material of the present invention is mildly safe, does not damage skin, can block myoneural transmission speed, inhibit the generation of expression line and fine wrinkles, the generation for promoting collagen, elastic fibers and hyaluronic acid simultaneously improves the water content and elasticity of skin, and effectively removes skin free radical, the activity of tyrosinase can effectively be inhibited, inhibit the calm of pigment to generate, repair epidermal cell, collagenous fibres is accelerated to update, reach anti-aging, the effect of firm skin.
Description
Technical field
The present invention relates to technical field of skin care, and in particular to a kind of petal water of anti-ageing firm skin and its preparation side
Method.
Background technique
With the living habit that social work pressure is big, environmental problem is serious, irregular, very big pressure all is caused to skin
Power, and ultraviolet light, air pollution, there is a great harm for skin, so the problem of aging, is more more serious than previous, and typical skin
Skin senile symptom is wrinkle occur, and cutis laxa is sagging, and skin is intensely dark, and color spot generates, and skin elasticity decline is dried
Skin, furfur etc..Thus cosmetics are increasingly becoming the necessity of people's daily life, but with the improvement of living standards, people couple
The requirement of cosmetics is also higher and higher.
Currently, anti-ageing compact skin-protection product in the market, use chemically strong anti-ageing reagent, free radical scavenger,
Moisturizer, skin cause serious damage, so that the self-protection defence capability of skin accumulation rubbish, weakening skin significantly, and
And it is easy that skin is made to generate telangiectasia erythema, papule, skin of face atrophy, acne rosacea fash and pigmentation etc. now
As destroying the normal ecological balance of skin.Therefore, need to develop a day that can fundamentally improve Skin Cell at this stage
The anti-ageing skin care item of right bioactivity.
Summary of the invention
In order to overcome shortcoming and defect existing in the prior art, the purpose of the present invention is to provide a kind of anti-ageing compact skins
The petal water of skin, the mild safety of the petal water raw material do not damage skin, can block myoneural transmission speed, inhibit expression line and
The generation of fine wrinkles, while promoting the generation of collagen, elastic fibers and hyaluronic acid, improve the water content and bullet of skin
Property, and skin free radical is effectively removed, it can effectively inhibit the activity of tyrosinase, the calm of pigment is inhibited to generate, repair epidermis
Cell accelerates collagenous fibres to update, reaches anti-aging, the effect of firm skin.
Another object of the present invention is to provide a kind of petal water and preparation method thereof of brilliant white skin, preparation method letters
Single easily operated, high production efficiency, production cost is low, can be used for being mass produced, each technique of strict control and parameter, and is made
The petal water of anti-ageing firm skin the generation of microgroove can be effectively suppressed, while promoting collagen, elastic fibers and hyalomitome
The generation of acid improves the water content and elasticity of skin, and effectively removes skin free radical, inhibits the activity and inhibition of tyrosinase
The calm of pigment generates, and repairs epidermal cell, accelerates collagenous fibres to update, reaches anti-aging, the effect of firm skin.
The purpose of the invention is achieved by the following technical solution: a kind of petal water of anti-ageing firm skin, including weighs as follows
Measure the raw material of part:
Petal water of the invention is made by using above-mentioned raw materials, and acetylation hexapeptide used is by blocking myoneural transmitting
Speed inhibits the generation of expression line and fine wrinkles, has the function that anti-aging, and in every part of petal water acetylation hexapeptide use
Amount is strict controlled in 8-12 parts of ranges, cannot effectively achieve the effect that myoneural is blocked to transmit completely if dosage is too low；
Two peptide can promote the generation of collagen, elastic fibers and hyaluronic acid, improve the water content of skin, increase skin thickness with
And microgroove is reduced, it is matched with acetylation hexapeptide, and control the mixed proportion of the two, promotes collagen egg while inhibiting microgroove
White and hyaluronic acid generation, has the function that anti-ageing compact；Further, coffee polyphenols can remove interior free yl, suppression
Oxygenerating reaction progress, but also have antiallergic, the external barrier action of skin can be improved, achieve the effect that it is anti-ageing, on
Collaboration anti-aging and firm skin can effectively be cooperated by stating substance.
Preferably, every part of anti-ageing active material of auxiliary includes the raw material of following parts by weight:
5-15 parts of lycium ruthenicum
0.1-1.0 parts of vitamin E
8-16 parts of resveratrol.
The lycium ruthenicum that the anti-ageing active material of auxiliary described in raw material of the present invention uses contains a large amount of polysaccharide, B- carrotene
Can be anti-oxidant well with anthocyanidin, along with trace elements of selenium contained by fructus lycii and vitamin E play synergistic effect, eliminate people
Body free radical has the function of significant anti-aging, in addition, its vitamin A contained can cooperate with vitamin E be added to maintain
The growth and differentiation of epithelial tissue prevent dry skin and follicular keratosis, and petal water obtained is made to play beautifying face and moistering lotion, moisten flesh
The effect of skin；And resveratrol can be repaired, be rised in value by the expression of intracellular antioxidant activity and activation SIRT1 gene
Epidermal cell is wanted the dosage in every part of petal water of strict control in 8-16 parts of ranges, is activated if dosage is too low when being added
The expression of SIRT1 gene comes that remediation efficiency is low, will lead to that adherent growth is overstocked to influence epidermal cell instead if dosage is excessively high
Repair rate.
Preferably, every part of moisturizer includes the raw material of following parts by weight:
6-14 parts of PCA natural moisturizing factor
2-8 parts of Chondrus crispus extract
0.01-1.0 parts of cetanol.
Moisturizer described in raw material of the present invention can assist PCA natural moisturizing factor and whale using Chondrus crispus extract
Ceryl alcohol improves skin moisturizing content, and cetanol water imbibition is strong, when being contacted with water or waterborne liquid, shape after absorbing water after being sufficiently stirred
At w/o type matrix, each water conservation ingredient can be made sufficiently to merge the moistening effect for further increasing made petal water.
Preferably, every part of reparative factor includes the raw material of following parts by weight:
0.1-2.0 parts of EGF reparative factor
3-8 parts of natural vigour element
2-10 parts of allantoin.
The EGF reparative factor that reparative factor described in raw material of the present invention uses can be with effective stimulus epithelical cell growth factor
Receptor tyrosin phosphorylation promotes skin progenitor cell constantly differentiation again so that the differentiation of epidermal cell, growth rate be promoted to accelerate
Neonatal cell, reduces the content of melanocyte and coloured corpuscle in skin, and then is finally reached and repairs skin, promotes cell
Metabolism and anti-ageing compact effect；And natural vigour element used is the separation and Extraction from leguminous plant, containing abundant natural
Glucoside, can be by effectively inhibiting the activity of 5- lipoxygenase, and the white alkene of blocking peptide achievees the effect that anti-inflammatory, antiallergy and anti-irritant,
So that skin histology is kept good physiological equilibrium and vigor, but want the dosage of strict control natural vigour element in every part of petal water,
Keep it in 3-8 parts of ranges, cannot effectively inhibit the activity of 5- lipoxygenase if dosage is too low, if but dosage it is excessively high
Skin histology physiological equilibrium is caused to be lacked of proper care；The allantoin of addition can be formed because it is a kind of amphoteric compound in conjunction with many kinds of substance
Double salt plays sterilization and anticorrosion and antioxidation, while skin can also be made to keep moisture, promotes tissue growth, cell new old generation
Thank, the effects of cutin-softening layer albumen so that petal water achieve the effect that it is anti-ageing compact.
Preferably, every part of solution is what 40-60:5-15 was formed with weight ratio by deionized water, 1,3-PD
Mixture.
Solvent 1,3-PD employed in petal water of the present invention is mild safely, and stimulation discomfort etc. will not be caused to skin
Phenomenon can sufficiently dissolve other compositions used in this technology, and have preferable moisture-keeping function, promote each raw material of petal water mutual
The water conservation water lock effect of petal water is improved on the basis of molten.
Preferably, the pretreatment petal liquid is at least one of roseleaf, peony petal, lily petal.It is described
Pretreatment petal liquid comprises the following steps: with deionized water ready petal raw material is clean, dry powder after moisture
Broken addition deionized water keeps the temperature 60-100 minutes under conditions of temperature is 40-55 DEG C；Then power is the item in 500W-800W
Microwave Extraction 5-10min under part, after standing 20-40min, then Microwave Extraction 5-10min under the conditions of power is 500W-800W,
Stop, filtered fluid is obtained by filtration as pretreatment petal liquid in standing, and the petal raw material and the solid-liquid ratio of deionized water stated is 3:35-
45。
Pretreatment petal liquid described in raw material of the present invention is prepared by the above method, needs strict control to keep the temperature in the preparation
Time and temperature, if the excessively high activity for being highly vulnerable to breakage effective component in petal of temperature, reduces its effect, if temperature be difficult in the past by
Essential ingredient in Petal extracts, and cooperation is 500W-800W's in power while controlling soaking time and temperature
Under the conditions of microwave the intersolubility of the macromolecular essence liquid particles in Petal and dissolution can be enhanced, and carry out microwave twice and mention
It takes, the extraction extracting rate of essential ingredient can be improved, improve the concentration of active constituent, in addition above-mentioned petal fragrant, add in petal
The fresh scent that petal water can be improved in water increases the artistic feeling of product, while there is certain inhibition to make Uric Acid enzyme
With can be effectively suppressed containing grease or sweat rouge excessive secretion, improve the salubrious feeling of petal water.
Preferably, which further includes 0.001-0.1 parts of essence, and the essence is natural flowery type essence.
The perfume (or spice) that diverse fragrant flavour can be added according to the people of different demands is added in bouquet type composition described in raw material of the present invention
Essence increases the fragrant of petal water, plays the role of certain refreshing oneself and relieves fatigue.
It is furthermore preferred that the essential oil is narra essential oil, Pogostemon cablin essential, needle juniper essential oil, Salvia japonica essential oil, Yilan essence
At least one in oil, Geranium Essential, Bergamot, polyphenol powde essential oil, yulan essential oil, lily of the valley essential oil and Rosemary Oil
Kind.
The perfume (or spice) that diverse fragrant flavour can be added according to the people of different demands is added in bouquet type composition described in raw material of the present invention
Essence increases the fragrant of petal water, can promote the pore convergence of skin, it is anti-to improve skin quality fragility, melanin deposition, whelk
The skin problems such as multiple, skin aging, enable skin pure and fresh smooth, play the role of certain refreshing oneself and relieve fatigue.
Another object of the present invention is achieved through the following technical solutions: a kind of preparation side of the petal water of anti-ageing firm skin
Method includes the following steps:
1) according to parts by weight successively by Chondrus crispus extract, lycium ruthenicum, resveratrol, EGF reparative factor and spermaceti
Alcohol is added into solvent, and is warming up to 75-85 DEG C, stirs 30-50min with 800-1200r/min revolving speed, and component A is made, standby
With；
2) according to parts by weight by acetylation hexapeptide, two peptide, coffee polyphenols, vitamin E, PCA natural moisturizing factor, natural
Huolisu and allantoin are stood after 10-30min is mixed, and obtain component B, spare；
3) the component A that step 1) obtains and the component B that step 2) obtains are mixed evenly, stirring rate 800-
1200r/min, mixing time 30-45min, is then cooled to 35-45 DEG C, obtains component C, spare；
4) petal liquid will be pre-processed according to parts by weight and essence is added in the resulting component C of step 3), and be stirred
It is even, then sieved and filtered with 100-130 mesh, sterilizing obtains petal water finished product at a high temperature of filtrate is finally moved to 90-110 DEG C.
The preparation step of the petal water of the anti-ageing firm skin of the present invention uses method operating procedure simple as described above, adopting this,
It is easy to control, high production efficiency；And since Chondrus crispus extract viscosity is larger, when dissolution, is slower, thus in advance plus
Enter into solvent stirring and dissolving, improves the solubility of Chondrus crispus extract, and energy is added more preferably in resveratrol and cetanol
Chondrus crispus extract is uniformly dissolved with bonding solvent, form more liquid aqueous fluid, and with lycium ruthenicum, EGF
Reparative factor forms anti-ageing compact core frame；And acetylation hexapeptide, two peptide, coffee polyphenols, vitamin in step 2)
E, PCA natural moisturizing factor, natural vigour element, the intersolubility of allantoin are strong, can enhance that by biological general character after dissolution
Synergistic effect between this, activation acetylation hexapeptide, two peptide, PCA natural moisturizing factor, natural vigour element, allantoin etc.
Activity；Component A and component B after mixing evenly, add will pretreatment petal liquid and essence, improve petal water mobility,
Permeability and fragrance improve its comprehensive stability.
Wherein, by strict control whipping temp, by strict control whipping temp in step 1), it can activate and keep second
The activity of the materials such as acylated hexapeptide, two peptide, PCA natural moisturizing factor, natural vigour element, allantoin, and each material can be promoted
Solubility, and temperature be not easy it is excessively high, if excessively high, be easy so that solvent 1,3-PD volatilize, reduce to the mutual of material
Solubility, and excessively high temperature is highly vulnerable to breakage the activity of EGF reparative factor, influences EGF in petal water to the repairing effect of skin,
Insufficient, the especially Chondrus crispus extract that dissolves each other of each ingredient if temperature is too low, the solubility at 75-85 DEG C is good,
It can promote the mutual solubility with unclassified stores；Stirring rate is not easy too fast in step 3), too fast, reduces component A's and component B
It sufficiently dissolves each other effect；It wants strict control is selected to sieve mesh number in step 4), the effect of filtering residue is not had if excessive, if
Mesh number is too small, can filter the effective component of petal water in filter process, reduce the active constituent and anti-ageing compact work of petal water
Strict control sterilising temp is wanted when with, filtrate high-temperature sterilization, temperature is unsuitable excessively high, can inhibit acetylation hexapeptide and two if excessively high
Win peptide molecule activity, the anti-ageing crease-resistant, the effects of promoting collagen to generate for reducing petal water, sterilizing is not achieved if too low
Effect, influences the holding time of petal water.
More preferably, the pretreatment petal liquid is roseleaf, peony petal and lily petal according to weight ratio:
1.2-1.5:0.5-0.8:0.7-1.0 the mixture of composition.
The mixing of petal liquid strict control roseleaf, peony petal and lily petal is pre-processed described in raw material of the present invention
Ratio is improved the infiltration preserving moisture and protecting skin effect of petal water in conjunction with respective effective component, and is played using the fragrance of more persons synthesis
The effect of Titian improves the pure and fresh property of smell of petal water.
The beneficial effects of the present invention are: the raw material of petal water of the invention is green safe, does not damage epidermal tissue, can hinder
Disconnected myoneural transmission speed, inhibits the generation of expression line and fine wrinkles, while promoting collagen, elastic fibers and transparent
The generation of matter acid improves the water content and elasticity of skin, and effectively removes skin free radical, can effectively inhibit junket ammonia from the root
The activity of sour enzyme inhibits the calm of pigment to generate, reaches anti-aging, the effect of firm skin.
Preparation method of the invention is simply easily operated, and high production efficiency, production cost is low, can be used for large-scale production,
Strict control charging sequence and each technological parameter are wanted during the preparation process, can activate the activity of material and make it using biological general character
Synergistic effect between enhancing, and then enhance the anti-aging of petal water obtained, the effect of firm skin.
Specific embodiment
For the ease of the understanding of those skilled in the art, below with reference to embodiment, the present invention is further illustrated, real
The content that the mode of applying refers to not is limitation of the invention.
Embodiment 1
A kind of petal water of anti-ageing firm skin, every part of raw material including following parts by weight:
Every part of anti-ageing active material of auxiliary includes the raw material of following parts by weight:
5 parts of lycium ruthenicum
0.1 part of vitamin E
8 parts of resveratrol.
Every part of moisturizer includes the raw material of following parts by weight:
6 parts of PCA natural moisturizing factor
2 parts of Chondrus crispus extract
0.01 part of cetanol.
Every part of reparative factor includes the raw material of following parts by weight:
0.1 part of EGF reparative factor
3 parts of natural vigour element
2 parts of allantoin.
The mixture that every part of solution is made of deionized water, 1,3- propylene glycol with weight ratio for 40:5.
The pretreatment petal liquid is roseleaf, and the pretreatment petal liquid comprises the following steps:
With deionized water ready petal raw material is clean, dry to crush after moisture deionized water be added in temperature
60 minutes are kept the temperature under conditions of being 40 DEG C；Then power is Microwave Extraction 5min under conditions of 500W, after standing 20min, then
Microwave Extraction 5min under the conditions of power is 500W stops, and filtered fluid is obtained by filtration as pretreatment petal liquid, the petal in standing
Raw material and the solid-liquid ratio of deionized water are 3:35.
A kind of preparation method of the petal water of anti-ageing firm skin, includes the following steps:
1) successively Chondrus crispus extract, lycium ruthenicum, resveratrol, the EGF in the raw material are repaired according to parts by weight
Multifactor and cetanol, which are added, is warming up to 75 DEG C into solvent, stirs 30min with 800r/min revolving speed, and component A is made, spare；
2) according to parts by weight by acetylation hexapeptide, two peptide, coffee polyphenols, vitamin E, PCA natural moisturizing factor, natural
Huolisu and allantoin are stood after 10min is mixed, and obtain component B, spare；
3) the component A that step 1) obtains and the component B that step 2) obtains are mixed evenly, stirring rate 800r/
Then min, mixing time 30min are cooled to 35 DEG C, obtain component C, spare；
4) petal liquid will be pre-processed according to parts by weight and essence is added in the resulting component C of step 3), and be stirred
It is even, then sieved and filtered with 100 meshes, sterilizing obtains petal water finished product at a high temperature of filtrate is finally moved to 100 DEG C.
Embodiment 2
A kind of petal water of anti-ageing firm skin, every part of raw material including following parts by weight:
Every part of anti-ageing active material of auxiliary includes the raw material of following parts by weight:
7.5 parts of lycium ruthenicum
0.25 part of vitamin E
10 parts of resveratrol.
Every part of moisturizer includes the raw material of following parts by weight:
8 parts of PCA natural moisturizing factor
3.5 parts of Chondrus crispus extract
0.25 part of cetanol.
Every part of reparative factor includes the raw material of following parts by weight:
0.5 part of EGF reparative factor
4 parts of natural vigour element
4 parts of allantoin.
The mixture that every part of solution is made of deionized water, 1,3- propylene glycol with weight ratio for 45:7.5.
The pretreatment petal liquid is peony petal, and the pretreatment petal liquid comprises the following steps:
With deionized water ready petal raw material is clean, dry to crush after moisture deionized water be added in temperature
70 minutes are kept the temperature under conditions of being 44 DEG C；Then power is Microwave Extraction 6min under conditions of 575W, after standing 25min, then
Microwave Extraction 6min under the conditions of power is 575W stops, and filtered fluid is obtained by filtration as pretreatment petal liquid, the petal in standing
Raw material and the solid-liquid ratio of deionized water are 3:38.
A kind of preparation method of the petal water of anti-ageing firm skin, includes the following steps:
1) successively Chondrus crispus extract, lycium ruthenicum, resveratrol, the EGF in the raw material are repaired according to parts by weight
Multifactor and cetanol, which are added, is warming up to 78 DEG C into solvent, stirs 35min with 900r/min revolving speed, and component A is made, spare；
2) according to parts by weight that the acetylation hexapeptide in the raw material, two peptide, coffee polyphenols, vitamin E, PCA is natural
Moisturizing factor, natural vigour element and allantoin are stood after 15min is mixed, and obtain component B, spare；
3) the component A that step 1) obtains and the component B that step 2) obtains are mixed evenly, stirring rate 900r/
Then min, mixing time 38min are cooled to 38 DEG C, obtain component C, spare；
4) petal liquid will be pre-processed according to parts by weight and essence is added in the resulting component C of step 3), and be stirred
It is even, then sieved and filtered with 107 meshes, sterilizing obtains petal water finished product at a high temperature of filtrate is finally moved to 105 DEG C.
Embodiment 3
A kind of petal water of anti-ageing firm skin, every part of raw material including following parts by weight:
Every part of anti-ageing active material of auxiliary includes the raw material of following parts by weight:
10 parts of lycium ruthenicum
0.5 part of vitamin E
12 parts of resveratrol.
Every part of moisturizer includes the raw material of following parts by weight:
10 parts of PCA natural moisturizing factor
5 parts of Chondrus crispus extract
0.5 part of cetanol.
Every part of reparative factor includes the raw material of following parts by weight:
1.0 parts of EGF reparative factor
5.5 parts of natural vigour element
6 parts of allantoin.
The mixture that every part of solution is made of deionized water, 1,3- propylene glycol with weight ratio for 50:10.
The pretreatment petal liquid is lily petal, and the pretreatment petal liquid comprises the following steps:
With deionized water ready petal raw material is clean, dry to crush after moisture deionized water be added in temperature
80 minutes are kept the temperature under conditions of being 48 DEG C；Then power is Microwave Extraction 7min under conditions of 650W, after standing 30min, then
Microwave Extraction 7min under the conditions of power is 650W stops, and it is pretreatment petal liquid that filtered fluid, which is obtained by filtration, in standing, described to state flower
Valve raw material and the solid-liquid ratio of deionized water are 3:40.
A kind of preparation method of the petal water of anti-ageing firm skin, includes the following steps:
1) successively Chondrus crispus extract, lycium ruthenicum, resveratrol, the EGF in the raw material are repaired according to parts by weight
Multifactor and cetanol, which are added, is warming up to 80 DEG C into solvent, stirs 40min with 1000r/min revolving speed, and component A is made, spare；
2) according to parts by weight by acetylation hexapeptide, two peptide, coffee polyphenols, vitamin E, PCA natural moisturizing factor, natural
Huolisu and allantoin are stood after 20min is mixed, and obtain component B, spare；
3) the component A that step 1) obtains and the component B that step 2) obtains are mixed evenly, stirring rate 1000r/
Min, mixing time 38min, and it is made to be cooled to 40 DEG C of temperature, component C is obtained, it is spare；
4) petal liquid will be pre-processed according to parts by weight and essence is added in the resulting component C of step 3), and be stirred
It is even, then sieved and filtered with 115 meshes, sterilizing obtains petal water finished product at a high temperature of filtrate is finally moved to 110 DEG C.
Embodiment 4
A kind of petal water of anti-ageing firm skin, every part of raw material including following parts by weight:
Every part of anti-ageing active material of auxiliary includes the raw material of following parts by weight:
12.5 parts of lycium ruthenicum
0.75 part of vitamin E
14 parts of resveratrol.
Every part of moisturizer includes the raw material of following parts by weight:
12 parts of PCA natural moisturizing factor
6.5 parts of Chondrus crispus extract
0.75 part of cetanol.
Every part of reparative factor includes the raw material of following parts by weight:
1.5 parts of EGF reparative factor
7 parts of natural vigour element
8 parts of allantoin.
The mixture that every part of solution is made of deionized water, 1,3- propylene glycol with weight ratio for 55:12.5.
The pretreatment petal liquid is roseleaf, peony petal and lily petal according to weight ratio 1.2:0.5:0.7 group
At mixture, the pretreatment petal liquid comprises the following steps:
With deionized water ready petal raw material is clean, dry to crush after moisture deionized water be added in temperature
90 minutes are kept the temperature under conditions of being 52 DEG C；Then power is Microwave Extraction 9min under conditions of 725W, after standing 35min, then
Microwave Extraction 9min under the conditions of power is 725W stops, and it is pretreatment petal liquid that filtered fluid, which is obtained by filtration, in standing, described to state flower
Valve raw material and the solid-liquid ratio of deionized water are 3:42.
A kind of preparation method of the petal water of anti-ageing firm skin, includes the following steps:
1) according to parts by weight successively by Chondrus crispus extract, lycium ruthenicum, resveratrol, EGF reparative factor and spermaceti
Alcohol, which is added, is warming up to 83 DEG C into solvent, stirs 45min with 1100r/min revolving speed, and component A is made, spare；
2) according to parts by weight that the acetylation hexapeptide in the raw material, two peptide, coffee polyphenols, vitamin E, PCA is natural
Moisturizing factor, natural vigour element, allantoin are stood after 25min is mixed, and obtain component B, spare；
3) the component A that step 1) obtains and the component B that step 2) obtains are mixed evenly, stirring rate 1100r/
Then min, mixing time 42min are cooled to 43 DEG C, obtain component C, spare；
4) petal liquid will be pre-processed according to parts by weight and essence is added in the resulting component C of step 3), and be stirred
It is even, then sieved and filtered with 118 meshes, sterilizing obtains petal water finished product at a high temperature of filtrate is finally moved to 115 DEG C.
Embodiment 5
A kind of petal water of anti-ageing firm skin, every part of raw material including following parts by weight:
Every part of anti-ageing active material of auxiliary includes the raw material of following parts by weight:
15 parts of lycium ruthenicum
1.0 parts of vitamin E
16 parts of resveratrol.
Every part of moisturizer includes the raw material of following parts by weight:
14 parts of PCA natural moisturizing factor
8 parts of Chondrus crispus extract
1.0 parts of cetanol.
Every part of reparative factor includes the raw material of following parts by weight:
2.0 parts of EGF reparative factor
8 parts of natural vigour element
10 parts of allantoin.
The mixture that every part of solution is made of deionized water, 1,3- propylene glycol with weight ratio for 40:15.
The pretreatment petal liquid is roseleaf, peony petal and lily petal according to weight ratio 1.5:0.8:1.0 group
At mixture, the pretreatment petal liquid comprises the following steps:
With deionized water ready petal raw material is clean, dry to crush after moisture deionized water be added in temperature
100 minutes are kept the temperature under conditions of being 55 DEG C；Then power is Microwave Extraction 10min under conditions of 800W, after standing 40min,
Microwave Extraction 10min under the conditions of power is 800W again, stops, and it is pretreatment petal liquid that filtered fluid, which is obtained by filtration, in standing, described
The solid-liquid ratio for stating petal raw material and deionized water is 3:35-45.
A kind of preparation method of the petal water of anti-ageing firm skin, includes the following steps:
1) successively Chondrus crispus extract, lycium ruthenicum, resveratrol, the EGF in the raw material are repaired according to parts by weight
Multifactor and cetanol, which are added, is warming up to 85 DEG C into solvent, stirs 50min with 1200r/min revolving speed, and component A is made, spare；
2) according to parts by weight that the acetylation hexapeptide in the raw material, two peptide, coffee polyphenols, vitamin E, PCA is natural
Moisturizing factor, natural vigour element, allantoin are stood after 30min is mixed, and obtain component B, spare；
3) the component A that step 1) obtains and the component B that step 2) obtains are mixed evenly, stirring rate 1200r/
Then min, mixing time 45min are cooled to 45 DEG C, obtain component C, spare；
4) petal liquid will be pre-processed according to parts by weight and essence is added in the resulting component C of step 3), and be stirred
It is even, then sieved and filtered with 130 meshes, sterilizing obtains petal water finished product at a high temperature of filtrate is finally moved to 120 DEG C.
Comparative example 1
This comparative example and the difference of above-described embodiment 1 are:
A kind of petal water of anti-ageing firm skin, every part of raw material including following parts by weight:
A kind of preparation method of the petal water of anti-ageing firm skin, includes the following steps:
1) successively Chondrus crispus extract, lycium ruthenicum, resveratrol, the EGF in the raw material are repaired according to parts by weight
Multifactor and cetanol, which are added, is warming up to 75 DEG C into solvent, stirs 30min with 800r/min revolving speed, and component A is made, spare；
2) it by two peptide, coffee polyphenols, vitamin E, PCA natural moisturizing factor, natural vigour element and is urinated according to parts by weight
Bursin is stood after 10min is mixed, and obtains component B, spare；
3) the component A that step 1) obtains and the component B that step 2) obtains are mixed evenly, stirring rate 800r/
Then min, mixing time 30min are cooled to 35 DEG C, obtain component C, spare；
4) petal liquid will be pre-processed according to parts by weight and essence is added in the resulting component C of step 3), and be stirred
It is even, then sieved and filtered with 100 meshes, sterilizing obtains petal water finished product at a high temperature of filtrate is finally moved to 100 DEG C.
Comparative example 2
This comparative example and the difference of above-described embodiment 3 are:
A kind of petal water of anti-ageing firm skin, every part of raw material including following parts by weight:
A kind of preparation method of the petal water of anti-ageing firm skin, includes the following steps:
1) successively Chondrus crispus extract, lycium ruthenicum, resveratrol, the EGF in the raw material are repaired according to parts by weight
Multifactor and cetanol, which are added, is warming up to 80 DEG C into solvent, stirs 40min with 1000r/min revolving speed, and component A is made, spare；
2) according to parts by weight that acetylation hexapeptide, coffee polyphenols, vitamin E, PCA natural moisturizing factor, natural vigour is plain
It is stood after 20min is mixed with allantoin, obtains component B, it is spare；
3) the component A that step 1) obtains and the component B that step 2) obtains are mixed evenly, stirring rate 1000r/
Min, mixing time 38min, and it is made to be cooled to 40 DEG C of temperature, component C is obtained, it is spare；
4) petal liquid will be pre-processed according to parts by weight and essence is added in the resulting component C of step 3), and be stirred
It is even, then sieved and filtered with 115 meshes, sterilizing obtains petal water finished product at a high temperature of filtrate is finally moved to 110 DEG C.
Comparative example 3
This comparative example and the difference of above-described embodiment 5 are:
A kind of petal water of anti-ageing firm skin, every part of raw material including following parts by weight:
Every part of moisturizer includes the raw material of following parts by weight:
8 parts of Chondrus crispus extract
1.0 parts of cetanol.
A kind of preparation method of the petal water of anti-ageing firm skin, includes the following steps:
1) successively Chondrus crispus extract, lycium ruthenicum, resveratrol, the EGF in the raw material are repaired according to parts by weight
Multifactor and cetanol, which are added, is warming up to 85 DEG C into solvent, stirs 50min with 1200r/min revolving speed, and component A is made, spare；
2) according to parts by weight by the acetylation hexapeptide in the raw material, two peptide, coffee polyphenols, vitamin E, natural vigour
Element, allantoin are stood after 30min is mixed, and obtain component B, spare；
3) the component A that step 1) obtains and the component B that step 2) obtains are mixed evenly, stirring rate 1200r/
Then min, mixing time 45min are cooled to 45 DEG C, obtain component C, spare；
4) petal liquid will be pre-processed according to parts by weight and essence is added in the resulting component C of step 3), and be stirred
It is even, then sieved and filtered with 130 meshes, sterilizing obtains petal water finished product at a high temperature of filtrate is finally moved to 120 DEG C.
Comparative example 4
This comparative example and the difference of above-described embodiment 5 are:
A kind of petal water of anti-ageing firm skin, every part of raw material including following parts by weight:
Every part of reparative factor includes the raw material of following parts by weight:
2.0 parts of EGF reparative factor
8 parts of natural vigour element.
A kind of preparation method of the petal water of anti-ageing firm skin, includes the following steps:
1) successively Chondrus crispus extract, lycium ruthenicum, resveratrol, the EGF in the raw material are repaired according to parts by weight
Multifactor and cetanol are added to deionized water, 1, are warming up to 85 DEG C in 3 propylene glycol oil mixtures, are stirred with 1200r/min revolving speed
50min is mixed, component A is made, it is spare；
2) according to parts by weight that the acetylation hexapeptide in the raw material, two peptide, coffee polyphenols, vitamin E, PCA is natural
Moisturizing factor and natural vigour element are stood after 30min is mixed, and obtain component B, spare；
3) the component A that the step 1) obtains and the component B that the step 2) obtains are mixed evenly, stirring rate
For 1200r/min, mixing time 45min, being then cooled to temperature is 45 DEG C, obtains component C, spare；
4) petal liquid will be pre-processed according to parts by weight and essence is added in the resulting component C of step 3), and stir mixed
It closes uniformly, then is sieved and filtered with 130 meshes, sterilizing obtains petal water finished product at a high temperature of filtrate is finally moved to 120 DEG C.
It will resist respectively containing petal water made from specific embodiment 1-5 and containing petal water made from comparative example 1-4
Free radical ability, moisture-absorbing moisture-keeping effect and anti-aging ability detection.
(1) detection method
1, antiradical activities
Anti- DPPH free radical ability measurement is carried out to petal water made from embodiment 1-5 and comparative example 1-4.Firstly, accurate
20mgDPPH (1,1- dimethyl benzyl phenylhydrazine) is weighed, is dissolved in 250mL volumetric flask surely with dehydrated alcohol, DPPH concentration is 2 × 10- 4mol/L.It mixes well, after room temperature dark stands 30min, measures absorbance value under 517nm wavelength.Same measurement repeats 3
It is secondary.Experimental measuring and DPPH clearance rate the results are shown in Table 1.
DPPH free radical scavenging activity (%)=[(1-X sample-X blank)/X control] × 100%
X sample: absorbance value of the sample under 517nm wavelength.
X blank: absorbance value of the blank under 517nm wavelength.
X control: to the absorbance value impinged upon under 517nm wavelength.
Petal water experimental measuring and DPPH clearance rate result in table 1 embodiment 1-5 and comparative example 1-4
| Embodiment | DPPH/ml | Sample/ml | Water/ml | DPPH clearance rate % |
| Embodiment 1 | 2.5 | 2.5 | 0 | 92.4 |
| Embodiment 2 | 2.5 | 2.5 | 0 | 93.9 |
| Embodiment 3 | 2.5 | 2.5 | 0 | 95.8 |
| Embodiment 4 | 2.5 | 2.5 | 0 | 90.2 |
| Embodiment 5 | 2.5 | 2.5 | 0 | 88.9 |
| Comparative example 1 | 2.5 | 2.5 | 0 | 58.5 |
| Comparative example 2 | 2.5 | 2.5 | 0 | 57.2 |
| Comparative example 3 | 2.5 | 2.5 | 0 | 75.2 |
| Comparative example 4 | 2.5 | 2.5 | 0 | 65.4 |
| Control | 2.5 | 0 | 2.5 | 0 |
Table 1 the experimental results showed that, comparative example 1-4 preparation petal water antiradical activities significantly lower than the present invention implement
The petal water of example, showing has good synergistic function between the component of product of the present invention, myoneural can be blocked to transmit
Speed, inhibits the generation of expression line and fine wrinkles, while promoting the generation of collagen, elastic fibers and hyaluronic acid, mentions
The water content and elasticity of high skin, and skin free radical is effectively removed, reach anti-aging, the effect of firm skin.
2, moisture-absorbing moisture-keeping effect
Its moisture-absorbing moisture-keeping effect is evaluated by the hydroscopicity and moisturizing rate of skin care item, hydroscopicity and moisturizing rate are higher, say
Bright moisture-absorbing moisture-keeping effect is better.
Saturation (NH will be filled4)2SO4Environment (RH=80%) of the drier inner cavity of aqueous solution as relative humidity 81%,
Saturation K will be filled2SO4Environment (RH=40%) of the drier inner cavity of aqueous solution as relative humidity 43%.It accurately weighs respectively
0.5g is dry, and the petal water (sample) into the embodiment 1-5 and comparative example 1-4 of constant weight is placed in small weighing bottle, is put in respectively
It states in 2 driers.It is to stand for 24 hours in 20 DEG C of isoperibols, weigh the quality of each sample that 2 driers, which are placed in temperature, is counted
Calculate hydroscopicity:
Hydroscopicity=(m2-m1)/m1 × 100%
M1 is the initial mass of sample, m2 be for 24 hours after sample quality.
The dry skin care item into the embodiment 1-5 and comparative example 1-4 of constant weight of 0.5g are accurately weighed, quality 10% is loaded
Deionized water, be placed in small weighing bottle, be put in above-mentioned 2 driers respectively.It is 20 DEG C of perseverances that 2 driers, which are placed in temperature,
It in warm environment, stands for 24 hours, weighs the quality of each sample, calculate moisturizing rate:
Moisturizing rate=m4/m3 × 100%
M3 is the initial biodiversity of sample, and m4 is the biodiversity of rear sample for 24 hours.
3, anti-aging ability measures
It carries out to petal water made from embodiment 1-5 and containing petal water made from comparative example 1-4 using SOD vigor as index
Anti-aging ability measurement.
Kunming kind cleaning grade mouse 50, half male and half female, weight (25 ± 2) g, by Guangdong medical university Experimental Animal Center
It provides, is randomly divided into 5 groups (control group, sample sets), every group 10.Since the one morning 8:30, sample sets are given to fill daily
Stomach embodiment of the present invention 1-5 and the petal water prepared than embodiment 1-4 carry out Experiment intervention, weigh 1 time, fill every 1 day mouse
Stomach amount (10g/kg) is adjusted accordingly according to weight.The physiological saline of control group also stomach-filling equivalent.After continuous one month, mouse is taken
Cerebral cortex cells detect SOD vigor.
(2) testing result
Such as to the testing result of petal water moisture-absorbing moisture-keeping effect and anti-aging ability in embodiment 1-5 and comparative example 1-4
Shown in table 2:
Petal water skin whitening, moisturizing efficacy detection result in 2 embodiment 1-5 of table and in comparative example 1-4
The above results can have it is found that the petal water in 1-5 of the embodiment of the present invention all has good anti-aging ability effect
Effect inhibits tyrosinase activity, while having good hygroscopicity, moisture retention and antiradical activities.Wherein, in embodiment 3
Petal water items effect is best.
Anti-aging ability measurement shows that petal water energy prepared by the present invention significantly improves the SOD vigor of mouse cortex, into
And the ability that body removes free radical is enhanced, mitigate attack of the free radical to biomembrane macromolecular, weakens polyradical pair
Biological membrane damage ensure that the complete of membrane structure and function, delay the generation of Apoptosis, illustrate prepared by the present invention
Petal water has excellent anti-aging effects.The antiradical activities of the petal water of comparative example 1-4 preparation are significantly lower than the present invention
The product of embodiment 1-5 further illustrates there is good synergistic function between the component of product of the present invention, effectively removes
Skin free radical can effectively inhibit the activity of tyrosinase, inhibit the calm of pigment to generate, repair epidermal cell, accelerate collagen
Fiber updates, and reaches anti-aging, the effect of firm skin.
Compared with Example 1, without addition acetylation hexapeptide in the raw material of 1 petal water of comparative example, using described in it
Raw material is made petal water progress antiradical activities, moisture-absorbing moisture-keeping effect and anti-aging ability detection, analysis and finds this petal water
Antiradical activities, moisture-absorbing moisture-keeping effect and the equal relative reduction of anti-aging ability；Illustrate that acetylation is added in raw material in the present invention
Hexapeptide can promote the generation of cell elasticity fiber, and then improve the water-retaining property of skin, increase skin elasticity and moisture content, improve and protect
Wet rate reaches anti-aging, the effect of firm skin, so that skin lightening water moistens, it is smooth flexible.
Compared with Example 3, in the raw material of 2 petal water of comparative example without addition two peptide, utilizing the raw material described in it
Petal water is made and carries out antiradical activities, moisture-absorbing moisture-keeping effect and anti-aging ability detection, analysis finds the anti-of this petal water
Free radical ability, moisture-absorbing moisture-keeping effect and the equal relative reduction of anti-aging ability；Illustrate that the present invention can in raw material addition two peptide energy
Promote collagen, elastic fibers and hyaluronic acid hyperplasia, improve the water content of skin, increase skin thickness and reduces thin
Line can promote collagen, elastic fibers and hyaluronic acid hyperplasia, and then reach anti-aging, the effect of firm skin, so that skin
Skin brilliant white water profit, it is smooth flexible.
Compared with Example 5, PCA natural moisturizing factor is not added in the raw material of 3 petal water of comparative example, to its institute of utilization
The raw material stated is made petal water progress antiradical activities, moisture-absorbing moisture-keeping effect and anti-aging ability detection, analysis and finds this flower
The equal relative reduction of moisture-absorbing moisture-keeping effect and anti-aging ability of valve water；Illustrate that PCA natural moisturizing factor is added in raw material in the present invention
It can improve and petal water moisturizing dilution effect is made, and then reach anti-aging, the effect of firm skin, so that skin lightening water moistens,
It is smooth flexible.
Compared with Example 5, in the raw material of 4 petal water of comparative example without addition allantoin, utilizing the raw material described in it
Petal water is made and carries out antiradical activities, moisture-absorbing moisture-keeping effect and anti-aging ability detection, analysis finds the anti-of this petal water
Free radical ability, moisture-absorbing moisture-keeping effect and the equal relative reduction of anti-aging ability；Illustrate that the present invention is added allantoin in raw material and can mention
The obtained petal moisturizing dilution effect of height, cell metabolism, and promote collagen, elastic fibers and hyaluronic acid hyperplasia, into
And reach anti-aging, the effect of firm skin, so that skin lightening water moistens, it is smooth flexible.
Above-described embodiment is the preferable implementation of the present invention, and in addition to this, the present invention can be realized with other way,
Do not depart under the premise of present inventive concept it is any obviously replace it is within the scope of the present invention.
Claims (10)
1. a kind of petal water of anti-ageing firm skin, it is characterised in that: the raw material including following parts by weight:
2. a kind of petal water of anti-ageing firm skin according to claim 1, it is characterised in that: every part of auxiliary is anti-ageing
Active material includes the raw material of following parts by weight:
5-15 parts of lycium ruthenicum
0.1-1.0 parts of vitamin E
8-16 parts of resveratrol.
3. a kind of petal water of anti-ageing firm skin according to claim 1, it is characterised in that: every part of moisturizer packet
Include the raw material of following parts by weight:
6-14 parts of PCA natural moisturizing factor
2-8 parts of Chondrus crispus extract
0.01-1.0 parts of cetanol.
4. a kind of petal water of anti-ageing firm skin according to claim 1, it is characterised in that: every part of reparative factor
Raw material including following parts by weight:
0.1-2.0 parts of EGF reparative factor
3-8 parts of natural vigour element
Allantoin 2-10.
5. a kind of petal water of anti-ageing firm skin according to claim 1, it is characterised in that: every part of solution be by
The mixture that deionized water and 1,3- propylene glycol are formed with weight ratio for 40-60:5-15.
6. a kind of petal water of anti-ageing firm skin according to claim 1, it is characterised in that: every part of pretreatment flower
Valve liquid is at least one of roseleaf, peony petal, lily petal.
7. a kind of petal water of anti-ageing firm skin according to claim 1, it is characterised in that: every part of pretreatment flower
Valve liquid comprises the following steps:
With deionized water ready petal raw material is clean, dry to crush after moisture and deionized water is added in temperature is
60-100 minutes are kept the temperature under conditions of 40-55 DEG C；Then Microwave Extraction 5-10min under conditions of power is 500W-800W, it is quiet
After setting 20-40min, then Microwave Extraction 5-10min under the conditions of power is 500W-800W, stop, filtered fluid is obtained by filtration in standing
For pretreatment petal liquid, the solid-liquid ratio of the petal raw material and deionized water is 3:35-45.
8. a kind of petal water of anti-ageing firm skin according to claim 1, it is characterised in that: the petal water further includes
0.001-0.1 parts of essence, the essence are natural flowery type essence.
9. a kind of preparation method of such as petal water of the described in any item anti-ageing firm skins of claim 1-8, it is characterised in that:
Include the following steps:
1) successively Chondrus crispus extract, lycium ruthenicum, resveratrol, EGF reparative factor and cetanol are added according to parts by weight
Enter into solvent, component A is made in heating stirring, spare；
2) according to parts by weight by acetylation hexapeptide, two peptide, coffee polyphenols, vitamin E, PCA natural moisturizing factor, natural vigour
Element, allantoin are stood after being mixed evenly, and obtain component B, spare；
3) the component A that step 1) obtains and the component B that step 2) obtains are mixed evenly, are then cooled down, obtain component C,
It is spare；
4) petal liquid will be pre-processed according to parts by weight and essence is added in the resulting component C of step 3), and be uniformly mixed, then
It is filtered with screening, obtains petal water finished product after filtrate high-temperature sterilization.
10. a kind of preparation method of the petal water of anti-ageing firm skin according to claim 9, it is characterised in that: described
In step 1), warming temperature is 75-85 DEG C, stirring rate 800-1200r/min, mixing time 30-50min；The step
It is rapid 2) in, mixing time 10-30min；In the step 3), it is cooled to 35-45 DEG C, stirring rate 800-1200r/min,
Mixing time is 30-45min；In the step 4), filtering sieve used is 100-130 mesh, and sterilising temp is 90-110 DEG C.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110772446A (en) * | 2019-12-19 | 2020-02-11 | 深圳市维琪医药研发有限公司 | Water-in-oil system skin repair polypeptide composition |
| CN113546153A (en) * | 2021-07-30 | 2021-10-26 | 陈翠华 | Anti-aging composition capable of activating cells and preparation method thereof |
| CN113633596A (en) * | 2020-12-22 | 2021-11-12 | 广州德亿化妆品有限公司 | Full-effect repairing anti-allergy jelly cleaning mask and preparation method thereof |
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| CN110772446A (en) * | 2019-12-19 | 2020-02-11 | 深圳市维琪医药研发有限公司 | Water-in-oil system skin repair polypeptide composition |
| CN110772446B (en) * | 2019-12-19 | 2023-08-22 | 深圳市维琪科技股份有限公司 | Skin repair polypeptide composition of water-in-oil system |
| CN113633596A (en) * | 2020-12-22 | 2021-11-12 | 广州德亿化妆品有限公司 | Full-effect repairing anti-allergy jelly cleaning mask and preparation method thereof |
| CN113546153A (en) * | 2021-07-30 | 2021-10-26 | 陈翠华 | Anti-aging composition capable of activating cells and preparation method thereof |
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