CN107184504B - Fragrant natural lip balm and preparation method thereof - Google Patents
Fragrant natural lip balm and preparation method thereof Download PDFInfo
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- CN107184504B CN107184504B CN201710315128.0A CN201710315128A CN107184504B CN 107184504 B CN107184504 B CN 107184504B CN 201710315128 A CN201710315128 A CN 201710315128A CN 107184504 B CN107184504 B CN 107184504B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
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- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention relates to the field of cosmetics and discloses a fragrant natural lip balm and a preparation method thereof. The lip balm formulation is as follows per 100 g: 8-12g of beewax, 5-9g of candelilla wax, 3-7g of rose wax, 18-22g of aloe grease, 8-12g of chamomile grease, 6-10g of squalane, 21-25g of coconut oil, 2-6g of sweet almond oil, 7-10g of grape seed oil, 2-6g of lithospermum-soaked olive oil, 4-6g of seaweed wet gel and 1-2g of bletilla striata extract; in addition, 1-6mL of vegetable essential oil is additionally added in each 100g of the formula. The lip balm disclosed by the invention adopts natural components, does not contain preservatives, artificial pigments and artificial perfumes, is good in mildness, has small irritation to human skin, and is non-toxic. In addition, the lip balm has good air permeability and lubricity and has long-lasting natural fragrance.
Description
Technical Field
The invention relates to the field of cosmetics, in particular to a fragrant natural lip balm and a preparation method thereof.
Background
In autumn and winter, the weather is dry and changeable, the lips are particularly easy to dry, and the lips are easy to crack and bleed. The lip balm has the main function of locking the moisture of the lips and preventing the lips from cracking due to water shortage. The main components of the lip balm are vaseline, wax and other oil and fat substances. The existing lip balm in the market is of the type of five-flower eight, and the functionality of the lip balm is also rich, for example, the lip balm has different colors and plays a role in beautifying, gives off fragrance and plays a role in fragrance, and the like. In order to provide the above-mentioned functions to lip gloss, many lip gloss contains various chemical components such as artificial colors, artificial perfumes, preservatives, and the like. Since the lip balm is applied to the lips, the safety of the human body is determined by the specificity of the applied part. It has been found that, with a single application of lip balm, approximately 70% of the ingredients are "eaten". Therefore, lip gloss containing a large amount of chemical components may cause some side effects to the human body.
In addition, although current lip gloss can play the lock water function, its main material is wax and grease, forms a rete on the lip after paining, and this rete is comparatively greasy, and its gas permeability is relatively poor, is unfavorable for lip skin to breathe, can influence the secretory function of lip skin sebaceous gland, and in the long term, can lead to lip skin to be dry more and more to cause the dependency to the lip gloss.
Disclosure of Invention
In order to solve the technical problems, the invention provides a fragrant natural lip balm and a preparation method thereof. The lip balm disclosed by the invention adopts natural components, does not contain preservatives, artificial pigments and artificial perfumes, is good in mildness, has small irritation to human skin, and is non-toxic. In addition, the lip balm has good air permeability and lubricity and has long-lasting natural fragrance.
The specific technical scheme of the invention is as follows: a fragrant natural lip balm comprises the following formula (per 100 g): 8-12g of beewax, 5-9g of candelilla wax, 3-7g of rose wax, 18-22g of aloe grease, 8-12g of chamomile grease, 6-10g of squalane, 21-25g of coconut oil, 2-6g of sweet almond oil, 7-10g of grape seed oil, 2-6g of lithospermum-soaked olive oil, 4-6g of seaweed wet gel and 1-2g of bletilla striata extract; in addition, 1-6mL of vegetable essential oil is additionally added in each 100g of the formula.
The invention adopts all natural components, and has high safety. The coconut oil, squalane, lithospermum soaking oil and plant essential oil which have bacteriostatic functions are adopted in the formula of the invention, and no preservative, artificial pigment and spice are required to be added. Wherein, squalane has the property of inhibiting mould, has the function of lubrication, and ensures that the touch of the product is not greasy; coconut oil also has antibacterial effect; the lithospermum has the effects of diminishing inflammation and resisting bacteria, and the lithospermum has pigments, and the color depth of the lipstick can be adjusted by the pigments; the plant essential oil has certain sterilization effect, and the unique fragrance of the plant essential oil can endow the lipstick with natural fragrance.
The formula of the lipstick particularly limits the proportion of the oil, the grease and the wax, so that the lipstick is moderate in softness and hardness, has soft and moist feeling, does not feel greasy, and does not easily break. The wax is prepared by compounding beeswax, candelilla wax and rose wax: the candelilla wax has good heat resistance and stability and good glossiness, so that the lipstick can resist temperature change and has a silky appearance; the rose thousand-leaf wax is derived from natural waxy components contained in the rose thousand-leaf, can slowly release the contained rose fragrance, and adds light fragrance to the lipstick.
The lipstick provided by the invention is also added with the seaweed wet gel and the bletilla striata extract, wherein the seaweed wet gel is a natural seaweed extract, has viscosity, good film-forming property after being smeared and good air permeability, has the functions of water retention, wrinkle resistance, bacteriostasis and inflammation diminishing, and is cool and smooth in touch to the skin and capable of relieving greasy feeling of wax and grease to the skin. The bletilla striata extract is mild to skin, good in skin friendliness and good in skin permeability, is easy to form a film, and can achieve the effects of moistening skin and preventing skin allergy.
Preferably, the plant essential oil is at least one selected from rose essential oil, sweet orange essential oil and lemon grass essential oil.
Preferably, the plant essential oil is 9.99wt% of rose essential oil, and the dosage of the rose essential oil is 1mL/100 g.
Because the lithospermum has pigment, the color depth of the lipstick can be adjusted by the pigment, and when the lipstick is a rose lipstick, the rose lipstick is pink, so the lithospermum has a little more soaking oil content.
Preferably, the plant essential oil is sweet orange essential oil and lemongrass essential oil, the dosage of the sweet orange essential oil is 5mL/100g, and the dosage of the lemongrass essential oil is 1mL/100 g.
The grapefruit lipstick is compounded by sweet orange essential oil and lemon grass essential oil, so that the grapefruit lipstick shows a sweet and fresh feeling. When the lipstick is grapefruit lipstick, the grapefruit lipstick is pink or orange, so the lithospermum soaking oil content is slightly low, and the yellow essential oil content is slightly more.
Preferably, the ratio of oil, fat and wax in the formula is controlled to be 48:29-31: 21-23.
The invention further limits the contents of the oil, the grease and the wax to the proportion, so that the paste is the most moderate in hardness, has soft and moist feeling, cannot feel greasy, and cannot be easily broken.
Preferably, the seaweed wet gel is pre-treated: controlling the solid content of the seaweed wet gel to be 55-75wt%, and adding baking soda with the mass of 1-3% of the seaweed wet gel under the stirring condition of 100-200r/min at 5-15 ℃ to uniformly disperse the seaweed wet gel; then heating to 65-75 ℃ at the speed of 4-6 ℃/min under the stirring condition of 400-600r/min, and then cooling to room temperature to obtain the seaweed wet gel mixed with bubbles; and finally, replacing gas in bubbles of the seaweed wet gel with absolute ethyl alcohol under the vacuum decompression condition to obtain the pretreated seaweed wet gel.
In order to further improve the air permeability of the lipstick after being applied, the seaweed wet gel is pretreated, in the pretreatment process, a proper amount of baking soda is added at a certain temperature and stirring speed, the baking soda is gradually heated after being dissolved in water, the stirring speed is improved, the baking soda begins to decompose after the temperature is increased to be higher than 20 ℃, sodium carbonate and carbon dioxide are generated, the generated carbon dioxide and part of external air are wrapped in the seaweed wet gel under violent stirring to form a large amount of capillary bubbles, and the stirring speed needs to be strictly controlled so as to form the capillary bubbles. And then placing the seaweed wet gel under a vacuum decompression condition, wherein the bubbles are broken due to the pressure difference between the inside and the outside of the bubbles, and the gas escapes, and at the moment, the gas in the bubbles is replaced by absolute ethyl alcohol so as to fill the space in the bubbles. The reason why absolute ethyl alcohol is used is that: 1. the seaweed gel is insoluble in ethanol, and the ethanol has good wettability, so that the ethanol can quickly permeate into the air bubbles and be locked in the air bubbles. 2. The ethanol has no toxicity to skin, good safety and low cost. 3. The ethanol is volatile, when the lipstick is not applied, the ethanol is locked in the bubbles, when the lipstick is applied, the contact surface with the air is suddenly enlarged, the ethanol is rapidly volatilized, the ethanol is volatilized, after part of the ethanol is absorbed by the skin, the lipstick also has the bactericidal effect and the skin moistening effect, and when the ethanol is volatilized, heat is absorbed to bring a cool feeling and relieve a greasy feeling. Meanwhile, after the ethanol volatilizes, the space in the bubbles is released, so that a large number of capillary pores are left in the film layer after the lipstick is smeared to form a film, the air permeability of the film layer is increased, the breathing of skin cells is facilitated, and the greasy feeling brought by the film layer can be compensated.
Preferably, the coconut oil, the sweet almond oil, the grape seed oil and the lithospermum immersed olive oil are respectively subjected to modification treatment: adding the oil substances into a high-pressure reaction kettle, heating for dehydration, adding a catalyst, introducing hydrogen, reacting for 20-40min under the conditions of hydrogen pressure of 0.5-0.7MPa, 100-110 ℃ and 600-800r/min stirring, and filtering to remove impurities after the reaction to obtain the modified oil substances.
In the process of storing the lipstick, the melting point of oil substances is low, the binding force between wax and grease in the lipstick is poor at a high temperature, the grease is easy to permeate to the surface of the lipstick after a long time, the sweating phenomenon occurs, the sweating phenomenon seriously influences the use of the lipstick, the ductility of the lipstick after losing the grease is influenced, the lipstick is dry and hard, and the lipstick is not easy to paint and form a film after being painted. In addition, vegetable oil and fat are easy to oxidize, rancidity and smell after being stored for a long time, and the normal use of the lipstick is influenced. Aiming at the technical problems, the oil substances are modified, and after the modification treatment, the melting point of the oil substances is properly improved, and the oxidation resistance of the oil substances is also improved, so that the lipstick is not easy to sweat and deteriorate in the long-term storage process. The modification degree needs to be strictly controlled in the modification process, if the modification is excessive, the melting point of the oil substance is too high, the liquid oil substance can be changed into a softer paste substance at normal temperature, and the quality of the lipstick can also be influenced, so that the modification condition is strictly controlled, and only the modification is slightly carried out.
A preparation method of a fragrant natural lip balm comprises the following steps:
(1) mixing Cera flava, candelilla wax, flos Rosae Laevigatae wax, Aloe resin, flos Matricariae Chamomillae fat, squalane, oleum Cocois, sweet almond oil, grape seed oil and radix Arnebiae in oleum Olivarum, heating to 70-80 deg.C, and stirring to obtain oily liquid;
(2) mixing the seaweed wet gel, the bletilla striata extract and the plant essential oil, and uniformly stirring to obtain a mixed wet gel;
(3) cooling the oily liquid, adding the mixed wet gel during cooling, and uniformly stirring; and finally, transferring the liquid into a mold for cooling and solidifying, and forming to obtain the fragrant natural lip balm.
As is well known, the plant essential oil is very easy to volatilize, the fragrant smell of the lipstick is gradually weakened after the lipstick is stored for a long time, and the plant essential oil is specially mixed with the seaweed wet gel in the preparation process, and the plant essential oil is wrapped by the seaweed wet gel after being mixed, so that the plant essential oil is not easy to volatilize, and can be quickly volatilized only after the contact area between the plant essential oil and the air is suddenly increased after the plant essential oil is smeared.
Preferably, in step (3), the wet gel is added and mixed when the temperature is reduced to 55-60 ℃.
Compared with the prior art, the invention has the beneficial effects that: the lip balm disclosed by the invention adopts natural components, does not contain preservatives, artificial pigments and artificial perfumes, is good in mildness, has small irritation to human skin, and is non-toxic. In addition, the lip balm has good air permeability and lubricity and has long-lasting natural fragrance.
Detailed Description
The present invention will be further described with reference to the following examples.
Example 1
A fragrant natural lip balm (rose lip balm) has the following formula: 9.5g of beeswax, 6.5g of candelilla wax, 4.5g of rose wax, 19g of aloe vera grease, 9g of chamomile grease, 7.5g of squalane, 22g of coconut oil, 3.4g of sweet almond oil, 7g of grape seed oil, 5g of lithospermum immersed olive oil, 5g of seaweed wet gel, 1.5g of bletilla striata extract and 1mL of 9.99wt% rose essential oil.
The preparation method of the aromatic natural lip balm comprises the following steps:
(1) mixing beeswax, candelilla wax, rose wax, aloe resin, chamomile resin, squalane, coconut oil, sweet almond oil, grape seed oil and lithospermum erythrorhizon soaked in olive oil, heating to 75 ℃, and stirring uniformly to obtain oily liquid;
(2) mixing the seaweed wet gel, the bletilla striata extract and the plant essential oil, and uniformly stirring to obtain a mixed wet gel;
(3) cooling the oily liquid, adding the mixed wet gel when the temperature is reduced to 58 ℃, and uniformly stirring; and finally, transferring the liquid into a mold for cooling and solidifying, and forming to obtain the fragrant natural lip balm.
Example 2
A fragrant natural lip balm (rose lip balm) has the following formula: 9.5g of beeswax, 6.5g of candelilla wax, 4.5g of rose wax, 19g of aloe vera grease, 9g of chamomile grease, 7.5g of squalane, 22g of coconut oil, 3.4g of sweet almond oil, 7g of grape seed oil, 5g of lithospermum immersed olive oil, 5g of seaweed wet gel, 1.5g of bletilla striata extract and 1mL of 9.99wt% rose essential oil.
The seaweed wet gel is pretreated: controlling the solid content of the seaweed wet gel to be 65 wt%, and adding baking soda with the mass of 2% of the seaweed wet gel under the stirring condition of 10 ℃ and 150r/min to uniformly disperse the seaweed wet gel; then heating to 70 ℃ at the speed of 5 ℃/min under the stirring condition of 500r/min, and then cooling to room temperature to obtain the seaweed wet gel mixed with air bubbles; and finally, replacing gas in bubbles of the seaweed wet gel with absolute ethyl alcohol under the vacuum decompression condition to obtain the pretreated seaweed wet gel.
The coconut oil, the sweet almond oil, the grape seed oil and the lithospermum soaked olive oil are respectively subjected to modification treatment: adding the oil substances into a high-pressure reaction kettle, heating for dehydration, adding a metal catalyst, introducing hydrogen, reacting for 30min under the conditions of hydrogen pressure of 0.6MPa, 105 ℃ and 700r/min stirring, and filtering to remove impurities after the reaction to obtain the modified oil substances.
The preparation method of the aromatic natural lip balm comprises the following steps:
(1) mixing beeswax, candelilla wax, rose wax, aloe resin, chamomile resin, squalane, coconut oil, sweet almond oil, grape seed oil and lithospermum erythrorhizon soaked in olive oil, heating to 75 ℃, and stirring uniformly to obtain oily liquid;
(2) mixing the seaweed wet gel, the bletilla striata extract and the plant essential oil, and uniformly stirring to obtain a mixed wet gel;
(3) cooling the oily liquid, adding the mixed wet gel when the temperature is reduced to 58 ℃, and uniformly stirring; and finally, transferring the liquid into a mold for cooling and solidifying, and forming to obtain the fragrant natural lip balm.
Example 3
A fragrant natural lip balm (grapefruit lip balm) has the following formula: 9.5g of beeswax, 6.5g of candelilla wax, 4.5g of rose wax, 19g of aloe vera fat, 9g of chamomile fat, 7.5g of squalane, 22g of coconut oil, 4g of sweet almond oil, 8.5g of grape seed oil, 3g of lithospermum immersed olive oil, 5g of seaweed wet gel, 1.5g of bletilla striata extract, 5mL of sweet orange essential oil and 1mL of lemon grass essential oil.
The preparation method of the aromatic natural lip balm comprises the following steps:
(1) mixing beeswax, candelilla wax, rose wax, aloe resin, chamomile resin, squalane, coconut oil, sweet almond oil, grape seed oil and lithospermum erythrorhizon soaked in olive oil, heating to 75 ℃, and stirring uniformly to obtain oily liquid;
(2) mixing the seaweed wet gel, the bletilla striata extract and the plant essential oil, and uniformly stirring to obtain a mixed wet gel;
(3) cooling the oily liquid, adding the mixed wet gel when the temperature is reduced to 58 ℃, and uniformly stirring; and finally, transferring the liquid into a mold for cooling and solidifying, and forming to obtain the fragrant natural lip balm.
Example 4
A fragrant natural lip balm (grapefruit lip balm) has the following formula: 9.5g of beeswax, 6.5g of candelilla wax, 4.5g of rose wax, 19g of aloe vera fat, 9g of chamomile fat, 7.5g of squalane, 22g of coconut oil, 4g of sweet almond oil, 8.5g of grape seed oil, 3g of lithospermum immersed olive oil, 5g of seaweed wet gel, 1.5g of bletilla striata extract, 5mL of sweet orange essential oil and 1mL of lemon grass essential oil.
The seaweed wet gel is pretreated: controlling the solid content of the seaweed wet gel to be 55 wt%, and adding baking soda with the mass of 1% of the seaweed wet gel under the stirring condition of 5 ℃ and 200r/min to uniformly disperse the seaweed wet gel; then heating to 65 ℃ at the speed of 4 ℃/min under the stirring condition of 600r/min, and then cooling to room temperature to obtain the seaweed wet gel mixed with bubbles; and finally, replacing gas in bubbles of the seaweed wet gel with absolute ethyl alcohol under the vacuum decompression condition to obtain the pretreated seaweed wet gel.
The coconut oil, the sweet almond oil, the grape seed oil and the lithospermum soaked olive oil are respectively subjected to modification treatment: adding the oil substances into a high-pressure reaction kettle, heating for dehydration, adding a metal catalyst, introducing hydrogen, reacting for 20min under the conditions of hydrogen pressure of 0.5MPa, 110 ℃ and 600r/min stirring, and filtering to remove impurities after the reaction to obtain the modified oil substances.
The preparation method of the aromatic natural lip balm comprises the following steps:
(1) mixing beeswax, candelilla wax, rose wax, aloe resin, chamomile resin, squalane, coconut oil, sweet almond oil, grape seed oil and lithospermum erythrorhizon soaked in olive oil, heating to 75 ℃, and stirring uniformly to obtain oily liquid;
(2) mixing the seaweed wet gel, the bletilla striata extract and the plant essential oil, and uniformly stirring to obtain a mixed wet gel;
(3) cooling the oily liquid, adding the mixed wet gel when the temperature is reduced to 35 ℃, and uniformly stirring; and finally, transferring the liquid into a mold for cooling and solidifying, and forming to obtain the fragrant natural lip balm.
Example 5
A fragrant natural lip balm (rose lip balm) has the following formula: 8g of beeswax, 7.5g of candelilla wax, 7g of rose thousand leaf wax, 18g of aloe vera fat, 10g of chamomile fat, 6g of squalane, 21g of coconut oil, 5g of sweet almond oil, 7g of grape seed oil, 4.5g of lithospermum-soaked olive oil, 4g of seaweed wet gel, 2g of bletilla striata extract and 1mL of 9.99wt% rose essential oil.
The seaweed wet gel is pretreated: controlling the solid content of the seaweed wet gel to be 75wt%, and adding baking soda with the mass of 3% of the seaweed wet gel under the stirring condition of 15 ℃ and 1000r/min to uniformly disperse the seaweed wet gel; then heating to 75 ℃ at the speed of 6 ℃/min under the stirring condition of 400r/min, and then cooling to room temperature to obtain the seaweed wet gel mixed with bubbles; and finally, replacing gas in bubbles of the seaweed wet gel with absolute ethyl alcohol under the vacuum decompression condition to obtain the pretreated seaweed wet gel.
The coconut oil, the sweet almond oil, the grape seed oil and the lithospermum soaked olive oil are respectively subjected to modification treatment: adding the oil substances into a high-pressure reaction kettle, heating for dehydration, adding a metal catalyst, introducing hydrogen, reacting for 40min under the conditions of 0.7MPa of hydrogen pressure, 100 ℃ and 800r/min of stirring, and filtering to remove impurities after the reaction to obtain the modified oil substances.
The preparation method of the aromatic natural lip balm comprises the following steps:
(1) mixing beeswax, candelilla wax, rose wax, aloe resin, chamomile resin, squalane, coconut oil, sweet almond oil, grape seed oil and lithospermum erythrorhizon soaked in olive oil, heating to 70 ℃, and stirring uniformly to obtain oily liquid;
(2) mixing the seaweed wet gel, the bletilla striata extract and the plant essential oil, and uniformly stirring to obtain a mixed wet gel;
(3) cooling the oily liquid, adding the mixed wet gel when the temperature is reduced to 55 ℃, and uniformly stirring; and finally, transferring the liquid into a mold for cooling and solidifying, and forming to obtain the fragrant natural lip balm.
Example 6
A fragrant natural lip balm (grapefruit lip balm) has the following formula: 10.5g of beeswax, 5g of candelilla wax, 6g of Chinese artichoke wax, 20g of aloe vera fat, 8g of chamomile fat, 9.5g of squalane, 23.5g of coconut oil, 2g of sweet almond oil, 8.5g of grape seed oil, 2g of lithospermum-soaked olive oil, 6g of seaweed wet gel, 1g of bletilla striata extract, 5mL of sweet orange essential oil and 1mL of lemongrass essential oil.
The seaweed wet gel is pretreated: controlling the solid content of the seaweed wet gel to be 75wt%, and adding baking soda with the mass of 3% of the seaweed wet gel under the stirring condition of 15 ℃ and 1000r/min to uniformly disperse the seaweed wet gel; then heating to 75 ℃ at the speed of 6 ℃/min under the stirring condition of 400r/min, and then cooling to room temperature to obtain the seaweed wet gel mixed with bubbles; and finally, replacing gas in bubbles of the seaweed wet gel with absolute ethyl alcohol under the vacuum decompression condition to obtain the pretreated seaweed wet gel.
The coconut oil, the sweet almond oil, the grape seed oil and the lithospermum soaked olive oil are respectively subjected to modification treatment: adding the oil substances into a high-pressure reaction kettle, heating for dehydration, adding a metal catalyst, introducing hydrogen, reacting for 40min under the conditions of 0.7MPa of hydrogen pressure, 100 ℃ and 800r/min of stirring, and filtering to remove impurities after the reaction to obtain the modified oil substances.
The preparation method of the aromatic natural lip balm comprises the following steps:
(1) mixing beeswax, candelilla wax, rose wax, aloe resin, chamomile resin, squalane, coconut oil, sweet almond oil, grape seed oil and lithospermum erythrorhizon soaked in olive oil, heating to 80 ℃, and stirring uniformly to obtain oily liquid;
(2) mixing the seaweed wet gel, the bletilla striata extract and the plant essential oil, and uniformly stirring to obtain a mixed wet gel;
(3) cooling the oily liquid, adding the mixed wet gel when the temperature is reduced to 60 ℃, and uniformly stirring; and finally, transferring the liquid into a mold for cooling and solidifying, and forming to obtain the fragrant natural lip balm.
The lip balms of examples 1-4 were compared to two commercially available lip balms without preservatives (comparative example 1 and comparative example 2)
The test was carried out:
firstly, sensory evaluation:
lip balm sensory evaluation index summary sheet
The scoring conditions are:
| itemizing | Example 1 | Example 2 | Comparative example 1 | Comparative example 2 |
| a1 | 8.0 | 8.0 | 8.2 | 8.1 |
| a2 | 8.2 | 8.1 | 8.3 | 7.5 |
| a3 | 8.4 | 8.3 | 8.2 | 8.5 |
| a4 | 8.0 | 8.0 | 8.1 | 7.9 |
| a5 | 8.8 | 8.7 | 8.3 | 8.2 |
| a6 | 8.6 | 8.5 | 8.0 | 7.8 |
| a7 | 8.9 | 9.0 | 7.8 | 8.0 |
| a8 | 8.0 | 8.1 | 8.1 | 8.0 |
| a9 | 7.9 | 8.0 | 8.0 | 7.6 |
| a10 | 8.7 | 9.0 | 7.8 | 7.9 |
| a11 | 8.2 | 8.2 | 8.3 | 8.2 |
From the above, the product of the present invention is represented by5(degree of moistening) a6(spreadability) a7(Thick feeling-air permeability), a9Has obvious advantages in (greasy feeling) aspect.
Secondly, evaluating the storage stability:
the lip balms of the examples 1 to 4 and the comparative examples 1 to 2 were left at 45. + -. 1 ℃ for 24 hours, and were observed after being taken out, and neither sweating nor rancidity occurred.
When the lip balms of examples 1 to 4 and comparative examples 1 to 2 were left at 45. + -. 1 ℃ for 30 days and were observed after taking out, the lip balms of examples 1 to 4 did not show sweating and rancidity, and the lip balms of comparative examples 1 to 2 showed slight sweating and rancidity.
The lip balms of the examples 1-4 and the comparative examples 1-2 are placed at 45 +/-1 ℃ for 180 days, and observed after being taken out, and the sweating condition and the rancidity condition do not appear in the examples 2 and 4; examples 1 and 3 exhibited mild sweating and mild rancidity, and comparative examples 1 and 2 exhibited severe sweating and severe rancidity.
The raw materials and equipment used in the invention are common raw materials and equipment in the field if not specified; the methods used in the present invention are conventional in the art unless otherwise specified.
The above description is only a preferred embodiment of the present invention, and is not intended to limit the present invention, and all simple modifications, alterations and equivalents of the above embodiments according to the technical spirit of the present invention are still within the protection scope of the technical solution of the present invention.
Claims (5)
1. A fragrant natural lip balm is characterized in that: the formulation, on a per 100g basis, is as follows: 8-12g of beewax, 5-9g of candelilla wax, 3-7g of rose wax, 18-22g of aloe grease, 8-12g of chamomile grease, 6-10g of squalane, 21-25g of coconut oil, 2-6g of sweet almond oil, 7-10g of grape seed oil, 2-6g of lithospermum-soaked olive oil, 4-6g of seaweed wet gel and 1-2g of bletilla striata extract; in addition, 1-6mL of vegetable essential oil is additionally added in each 100g of the formula; the proportion of oil, fat and wax in the formula is controlled to be 48:29-31: 21-23;
the seaweed wet gel is pretreated: controlling the solid content of the seaweed wet gel to be 55-75wt%, and adding baking soda with the mass of 1-3% of the seaweed wet gel under the stirring condition of 100-200r/min at 5-15 ℃ to uniformly disperse the seaweed wet gel; then heating to 65-75 ℃ at the speed of 4-6 ℃/min under the stirring condition of 400-600r/min, and then cooling to room temperature to obtain the seaweed wet gel mixed with bubbles; finally, replacing gas in bubbles of the seaweed wet gel with absolute ethyl alcohol under the vacuum decompression condition to obtain pretreated seaweed wet gel;
the coconut oil, the sweet almond oil, the grape seed oil and the lithospermum soaked olive oil are respectively subjected to modification treatment: adding the oil substances into a high-pressure reaction kettle, heating for dehydration, adding a catalyst, introducing hydrogen, reacting for 20-40min under the conditions of hydrogen pressure of 0.5-0.7MPa, 100-110 ℃ and 600-800r/min stirring, and filtering to remove impurities after the reaction to obtain modified oil substances;
the preparation method of the aromatic natural lip balm comprises the following steps:
(1) mixing Cera flava, candelilla wax, flos Rosae Laevigatae wax, Aloe resin, flos Matricariae Chamomillae fat, squalane, oleum Cocois, sweet almond oil, grape seed oil and radix Arnebiae in oleum Olivarum, heating to 70-80 deg.C, and stirring to obtain oily liquid;
(2) mixing the seaweed wet gel, the bletilla striata extract and the plant essential oil, and uniformly stirring to obtain a mixed wet gel;
(3) cooling the oily liquid, adding the mixed wet gel during cooling, and uniformly stirring; and finally, transferring the liquid into a mold for cooling and solidifying, and forming to obtain the fragrant natural lip balm.
2. The aromatic natural lip balm according to claim 1, wherein the plant essential oil is at least one selected from the group consisting of rose essential oil, sweet orange essential oil, and lemongrass essential oil.
3. The fragrant natural lip balm according to claim 2, wherein the plant essential oil is 9.99wt% of rose essential oil, and the amount of the rose essential oil is 1mL/100 g.
4. The fragrant natural lip balm according to claim 2, wherein the plant essential oils are sweet orange essential oil and lemongrass essential oil, the sweet orange essential oil is used in an amount of 5mL/100g, and the lemongrass essential oil is used in an amount of 1mL/100 g.
5. The fragrant natural lip balm according to claim 1, wherein the wet gel is added and mixed at the time of cooling to 55 to 60 ℃ in the step (3).
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| CN107693434A (en) * | 2017-11-16 | 2018-02-16 | 武汉生物工程学院 | A kind of purple returns Chinese medicine lipstick and preparation method thereof |
| CN110025554A (en) * | 2019-05-31 | 2019-07-19 | 长春师范大学 | Pure natural moist lip gloss of one kind and preparation method thereof |
| CN112043665A (en) * | 2020-10-08 | 2020-12-08 | 福建省梦娇兰日用化学品有限公司 | Lithospermum oil-containing baby lip balm and preparation method thereof |
| CN112870116B (en) * | 2021-03-22 | 2022-12-30 | 皖南医学院 | Lip balm for moistening, preserving moisture and repairing lips, preparation method of lip balm, lip balm for moistening, preserving moisture and repairing lips and preparation method of lip balm |
| CN113576974B (en) * | 2021-08-17 | 2022-08-30 | 广州环亚化妆品科技股份有限公司 | Lithospermum extract and lip care composition |
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