CN110591834A - Laundry detergent containing okra extract and raspberry enzyme and preparation method of laundry detergent - Google Patents
Laundry detergent containing okra extract and raspberry enzyme and preparation method of laundry detergent Download PDFInfo
- Publication number
- CN110591834A CN110591834A CN201910900137.5A CN201910900137A CN110591834A CN 110591834 A CN110591834 A CN 110591834A CN 201910900137 A CN201910900137 A CN 201910900137A CN 110591834 A CN110591834 A CN 110591834A
- Authority
- CN
- China
- Prior art keywords
- parts
- laundry detergent
- extract
- raspberry
- okra
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- 239000003599 detergent Substances 0.000 title claims abstract description 112
- 235000011034 Rubus glaucus Nutrition 0.000 title claims abstract description 70
- 235000009122 Rubus idaeus Nutrition 0.000 title claims abstract description 70
- 102000004190 Enzymes Human genes 0.000 title claims abstract description 59
- 108090000790 Enzymes Proteins 0.000 title claims abstract description 59
- 229940069825 okra extract Drugs 0.000 title claims abstract description 54
- 238000002360 preparation method Methods 0.000 title claims abstract description 36
- 240000007651 Rubus glaucus Species 0.000 title description 48
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 63
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 47
- -1 polyoxyethylene Polymers 0.000 claims abstract description 44
- 239000001397 quillaja saponaria molina bark Substances 0.000 claims abstract description 41
- 229930182490 saponin Natural products 0.000 claims abstract description 41
- 150000007949 saponins Chemical class 0.000 claims abstract description 41
- 239000000284 extract Substances 0.000 claims abstract description 36
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims abstract description 32
- 239000008367 deionised water Substances 0.000 claims abstract description 29
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 29
- 241000196324 Embryophyta Species 0.000 claims abstract description 26
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 23
- 229930195729 fatty acid Natural products 0.000 claims abstract description 23
- 239000000194 fatty acid Substances 0.000 claims abstract description 23
- 239000002994 raw material Substances 0.000 claims abstract description 23
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims abstract description 22
- 240000009087 Crescentia cujete Species 0.000 claims abstract description 21
- 235000005983 Crescentia cujete Nutrition 0.000 claims abstract description 21
- 235000009797 Lagenaria vulgaris Nutrition 0.000 claims abstract description 21
- 244000269722 Thea sinensis Species 0.000 claims abstract description 21
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims abstract description 16
- 235000017557 sodium bicarbonate Nutrition 0.000 claims abstract description 16
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- 238000003756 stirring Methods 0.000 claims description 18
- 241001075517 Abelmoschus Species 0.000 claims description 13
- 241000580955 Sapindus mukorossi Species 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 13
- 238000004140 cleaning Methods 0.000 claims description 10
- 238000001816 cooling Methods 0.000 claims description 9
- 238000001914 filtration Methods 0.000 claims description 9
- 239000000706 filtrate Substances 0.000 claims description 8
- 238000004321 preservation Methods 0.000 claims description 8
- 239000011265 semifinished product Substances 0.000 claims description 8
- 239000010902 straw Substances 0.000 claims description 8
- 238000009210 therapy by ultrasound Methods 0.000 claims description 8
- 238000009849 vacuum degassing Methods 0.000 claims description 8
- 235000009051 Ambrosia paniculata var. peruviana Nutrition 0.000 claims description 7
- 235000003097 Artemisia absinthium Nutrition 0.000 claims description 7
- 240000001851 Artemisia dracunculus Species 0.000 claims description 7
- 235000017731 Artemisia dracunculus ssp. dracunculus Nutrition 0.000 claims description 7
- 235000003261 Artemisia vulgaris Nutrition 0.000 claims description 7
- 235000004347 Perilla Nutrition 0.000 claims description 7
- 244000124853 Perilla frutescens Species 0.000 claims description 7
- 239000001138 artemisia absinthium Substances 0.000 claims description 7
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 6
- 150000004665 fatty acids Chemical class 0.000 claims description 5
- 241000205585 Aquilegia canadensis Species 0.000 claims description 4
- 235000007516 Chrysanthemum Nutrition 0.000 claims description 4
- 244000189548 Chrysanthemum x morifolium Species 0.000 claims description 4
- 241000220317 Rosa Species 0.000 claims description 4
- 229930006000 Sucrose Natural products 0.000 claims description 4
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 4
- 238000000605 extraction Methods 0.000 claims description 4
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 4
- 238000000227 grinding Methods 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 238000005360 mashing Methods 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 4
- 238000010992 reflux Methods 0.000 claims description 4
- 238000005303 weighing Methods 0.000 claims description 4
- 235000006679 Mentha X verticillata Nutrition 0.000 claims description 3
- 235000002899 Mentha suaveolens Nutrition 0.000 claims description 3
- 235000001636 Mentha x rotundifolia Nutrition 0.000 claims description 3
- 238000005406 washing Methods 0.000 abstract description 28
- 239000003945 anionic surfactant Substances 0.000 abstract description 9
- 239000000126 substance Substances 0.000 abstract description 9
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 7
- 239000003795 chemical substances by application Substances 0.000 abstract description 6
- 239000000686 essence Substances 0.000 abstract description 5
- 235000013305 food Nutrition 0.000 abstract description 5
- 239000006260 foam Substances 0.000 abstract description 4
- 239000000049 pigment Substances 0.000 abstract description 4
- 210000002700 urine Anatomy 0.000 abstract description 4
- 230000002087 whitening effect Effects 0.000 abstract description 3
- 210000003296 saliva Anatomy 0.000 abstract description 2
- 229940088598 enzyme Drugs 0.000 description 39
- 235000013616 tea Nutrition 0.000 description 15
- 230000000694 effects Effects 0.000 description 13
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 12
- 230000007794 irritation Effects 0.000 description 10
- 238000012360 testing method Methods 0.000 description 9
- 230000000052 comparative effect Effects 0.000 description 8
- 241000282414 Homo sapiens Species 0.000 description 6
- 230000008569 process Effects 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 230000003385 bacteriostatic effect Effects 0.000 description 5
- 238000005202 decontamination Methods 0.000 description 5
- 230000003588 decontaminative effect Effects 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 4
- 239000003921 oil Substances 0.000 description 4
- 235000019198 oils Nutrition 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 239000004744 fabric Substances 0.000 description 3
- 230000036541 health Effects 0.000 description 3
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 229910052938 sodium sulfate Inorganic materials 0.000 description 3
- 235000011152 sodium sulphate Nutrition 0.000 description 3
- 230000000638 stimulation Effects 0.000 description 3
- 238000010998 test method Methods 0.000 description 3
- 229940100555 2-methyl-4-isothiazolin-3-one Drugs 0.000 description 2
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 description 2
- 206010054786 Skin burning sensation Diseases 0.000 description 2
- 239000012752 auxiliary agent Substances 0.000 description 2
- 239000003899 bactericide agent Substances 0.000 description 2
- 235000019864 coconut oil Nutrition 0.000 description 2
- 239000003240 coconut oil Substances 0.000 description 2
- 239000000645 desinfectant Substances 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 239000002085 irritant Substances 0.000 description 2
- 231100000021 irritant Toxicity 0.000 description 2
- BEGLCMHJXHIJLR-UHFFFAOYSA-N methylisothiazolinone Chemical group CN1SC=CC1=O BEGLCMHJXHIJLR-UHFFFAOYSA-N 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 238000011056 performance test Methods 0.000 description 2
- 239000000419 plant extract Substances 0.000 description 2
- 230000001681 protective effect Effects 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- 229940057950 sodium laureth sulfate Drugs 0.000 description 2
- SXHLENDCVBIJFO-UHFFFAOYSA-M sodium;2-[2-(2-dodecoxyethoxy)ethoxy]ethyl sulfate Chemical compound [Na+].CCCCCCCCCCCCOCCOCCOCCOS([O-])(=O)=O SXHLENDCVBIJFO-UHFFFAOYSA-M 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 1
- 241001116389 Aloe Species 0.000 description 1
- 241000143060 Americamysis bahia Species 0.000 description 1
- 244000125300 Argania sideroxylon Species 0.000 description 1
- 235000016108 Argania sideroxylon Nutrition 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 235000007866 Chamaemelum nobile Nutrition 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 240000000560 Citrus x paradisi Species 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 description 1
- 241000628997 Flos Species 0.000 description 1
- 208000011092 Hand injury Diseases 0.000 description 1
- 244000042664 Matricaria chamomilla Species 0.000 description 1
- 235000007232 Matricaria chamomilla Nutrition 0.000 description 1
- 108091005804 Peptidases Proteins 0.000 description 1
- 239000004365 Protease Substances 0.000 description 1
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 description 1
- 206010040880 Skin irritation Diseases 0.000 description 1
- 150000004996 alkyl benzenes Chemical class 0.000 description 1
- 235000011399 aloe vera Nutrition 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229940077388 benzenesulfonate Drugs 0.000 description 1
- 239000007844 bleaching agent Substances 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 description 1
- 229940073507 cocamidopropyl betaine Drugs 0.000 description 1
- 235000020379 cucumber juice Nutrition 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 description 1
- 229940043237 diethanolamine Drugs 0.000 description 1
- UZBQIPPOMKBLAS-UHFFFAOYSA-N diethylazanide Chemical compound CC[N-]CC UZBQIPPOMKBLAS-UHFFFAOYSA-N 0.000 description 1
- 229940079919 digestives enzyme preparation Drugs 0.000 description 1
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- GVGUFUZHNYFZLC-UHFFFAOYSA-N dodecyl benzenesulfonate;sodium Chemical compound [Na].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 GVGUFUZHNYFZLC-UHFFFAOYSA-N 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000007850 fluorescent dye Substances 0.000 description 1
- 229940075529 glyceryl stearate Drugs 0.000 description 1
- 229930182470 glycoside Natural products 0.000 description 1
- 229940094952 green tea extract Drugs 0.000 description 1
- 235000020688 green tea extract Nutrition 0.000 description 1
- 239000008236 heating water Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 210000004877 mucosa Anatomy 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 231100000572 poisoning Toxicity 0.000 description 1
- 230000000607 poisoning effect Effects 0.000 description 1
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 description 1
- 229920005646 polycarboxylate Polymers 0.000 description 1
- 229940051841 polyoxyethylene ether Drugs 0.000 description 1
- 229920000056 polyoxyethylene ether Polymers 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 210000002345 respiratory system Anatomy 0.000 description 1
- 210000002374 sebum Anatomy 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 230000036556 skin irritation Effects 0.000 description 1
- 231100000475 skin irritation Toxicity 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 description 1
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000010677 tea tree oil Substances 0.000 description 1
- 229940111630 tea tree oil Drugs 0.000 description 1
- 229940098465 tincture Drugs 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/825—Mixtures of compounds all of which are non-ionic
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/10—Carbonates ; Bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2086—Hydroxy carboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/74—Carboxylates or sulfonates esters of polyoxyalkylene glycols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D2111/00—Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
- C11D2111/10—Objects to be cleaned
- C11D2111/12—Soft surfaces, e.g. textile
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a laundry detergent containing okra extract and raspberry enzyme, which is prepared from the following raw materials: plant ash extract, okra extract, raspberry enzyme, soapberry saponin, tea saponin, baking soda, polyoxyethylene fatty acid ester, citric acid, calabash, natural essence and deionized water. The laundry detergent does not contain chemically synthesized or strong-irritation anionic surfactant, enzyme preparation, whitening agent, fluorescent agent, essence, pigment and other potentially harmful auxiliaries, the pH value of the prepared laundry detergent is 6.5-7.3, the foam is fine and rich, the dirt-removing capacity is high, the antibacterial effect is good, the laundry detergent has the characteristics of nature, cleanness and mildness, no harmful chemically synthesized substance residue exists, the urine stain, the saliva stain and the food oil stain of infant clothes can be effectively removed, the laundry detergent is particularly suitable for washing infant clothes, the skin cannot be tense or burnt after the laundry detergent is used up, the safety is high, the water body cannot be polluted due to emission, and the laundry detergent is green and environment-friendly.
Description
Technical Field
The invention belongs to the technical field of detergents, and particularly relates to a laundry detergent containing an okra extract and raspberry enzyme and a preparation method thereof.
Background
The laundry detergent replaces anhydrous sodium sulphate serving as a filling agent in the washing powder with water which is rich in resources and low in price, solves the problem of dust pollution caused by the washing powder in the using process, has a simple preparation process and mild performance, and becomes the first choice of household washing products. The laundry detergent becomes a daily washing product, has the advantages of simple use, quick dissolution, high detergency, easy rinsing and the like, and is more and more popular with consumers. In order to ensure that no stimulation or hand injury occurs in the use process, the use amount of some effective components with strong decontamination capability in the laundry detergent is reduced, so that the disadvantage of weak decontamination effect of the laundry detergent is caused.
At present, anionic surfactants such as LAS, AES, FAS, AOS, MES and the like are still added into the laundry detergent on the market, and part of the laundry detergent with natural product flags is a conceptual product.
With the increasing awareness of health, the cleaning of clothes cannot meet the mere cleaning effect, and the sterilization and disinfection of clothes while cleaning becomes the first choice of consumers. The skin of the infant is fragile and sensitive, the body resistance is low, the infant is easily infected by bacteria in the environment, the clothes are the first barrier for protecting the infant from the environment, and if the laundry detergent with the potential safety hazard is used for a long time, the infant must be damaged. Common washing powder and laundry detergent may remain on clothes and cause irritation and damage to the skin of a baby, so when selecting the laundry detergent for the baby, on the premise of ensuring the cleaning function of the laundry detergent, attention needs to be paid to selecting products which have no irritation to the skin of the baby and have a certain protection effect. Most of the currently marketed baby washing products are poor in washing effect for reducing the toxicity of residues or similar to the components of adult washing products in concentration, but cannot improve the washing effect and reduce the irritation to the skin of the baby, for example:
1. patent application CN201711043583.6 discloses an organic bacteriostatic laundry detergent for infants and a preparation method thereof, wherein the preparation method comprises the following steps: (1) heating water to 65-85 ℃, sequentially adding sodium laureth sulfate, sodium alkyl benzene sulfonate, fatty alcohol-polyoxyethylene ether, sodium polyacrylate and organic acid, and uniformly stirring and mixing to obtain a mixture; (2) cooling the mixture to 45-55 deg.C, sequentially adding herba Avenae Fatuae kernel extract, folium Canarii albi extract, flos Matricariae Chamomillae/leaf/stem extract, sodium chloride, disodium EDTA, potassium hydroxide, essence, and bactericide, stirring, and mixing. The organic bacteriostatic laundry detergent for infants prepared by the invention is reasonably adjusted in a formula system through a large amount of researches, and is mild in performance, safe and free of stimulation; various plant extracts are added into the laundry detergent, so that the laundry effect is promoted, the decontamination capability is strong, and the bacteriostatic effect is good; no chemical residue is caused in the using process, and the washing machine is particularly suitable for washing infant clothes. However, the raw materials of the patent contain anionic surfactant (LAS), which is irritating to the skin of infants and is not environment-friendly, and the bactericide is methyl isothiazolinone which is taken as a formaldehyde donor and can release formaldehyde to pollute the environment.
2. Patent application CN201710001431.3 discloses an infant laundry detergent and a preparation method thereof, and the infant laundry detergent comprises water, sodium laureth sulfate, polyoxyethylene cetyl stearyl diether, cocamidopropyl betaine, coconut oil fatty acid diethylamide, soapberry extract, folium artemisiae argyi extract, argania spinosa kernel extract, enzyme, sodium chloride, disodium edetate, citric acid and the like. The infant laundry detergent disclosed by the invention can be used for effectively removing dirt, softening clothes and effectively sterilizing, does not hurt hands, does not have residues and is easy to rinse. However, the raw materials of the patent contain anionic surfactant, so that the infant skin is stimulated and the infant skin is not environment-friendly.
3. Patent application CN201310738241.1 discloses an infant laundry detergent and a preparation method thereof, which mainly comprises amino acid type surfactant, amine oxide, coconut oil fatty acid diethanolamide, alkyl glycoside and fatty alcohol sodium sulfate. The components are mixed, dissolved and the like to form the laundry detergent. The components and the proportions of the components are matched with each other, and a layer of mild skin-friendly protective film is formed on the surface of fabric fibers of clothes washed and dried by using the laundry detergent, so that the friction among the fabric fibers can be reduced; the formed protective film is combined with water in the air, so that the clothes have certain wettability, the generation of static electricity is reduced, and the washed clothes are more flexible. Therefore, the laundry detergent prepared by the invention has good softness of washed clothes, has good affinity to the skin of infants, and can effectively wash off stubborn stains of the clothes of infants. However, the raw materials of the patent contain anionic surfactant (FAS), which is irritating to the skin of infants and not environment-friendly, and the preservative selects methylisothiazolinone as a formaldehyde donor, which can release formaldehyde and pollute the environment.
4. Patent application CN201210455837.6 discloses an antibacterial laundry detergent for infants, which is characterized in that: the paint comprises the following components in percentage by weight: 18-25% of sodium dodecyl benzene sulfonate, 8-15% of cocoyl diethanol amine, 2-6% of polycarboxylate, 3-10% of tea tree oil, 2-6% of grapefruit, 8-10% of aloe tincture, 3-7% of chamomile, 1-5% of protease, 25-40% of sodium sulfate and the balance of water. The invention has the advantages that: the antibacterial property is good, and the washed clothes are soft and fragrant and have a protection effect on the skin of the infant. However, the main raw material of the patent is an anionic surfactant (LAS), and the enzyme preparation is added, so that laundry detergent remains when clothes are washed, and potential safety hazards exist when skin of an infant contacts the clothes.
5. Patent application CN201210203845.1 discloses a laundry detergent for infants, which comprises the following components by mass percent: 8-13% of glycerol, 6-14% of hexadecanol, 25-33% of glyceryl stearate, 1-10% of cucumber juice extract, 3-12% of green tea extract, 20-29% of cleaning component and the balance of deionized water. The infant laundry detergent disclosed by the invention has a natural plant antibacterial formula, is mild, does not hurt hands, and has a softening effect on clothes. However, the raw material of the patent contains 6 to 14 percent of hexadecanol, and the hexadecanol can stimulate eyes, skin mucosa and upper respiratory tract and can cause water body pollution.
The prior laundry detergent is commonly added with a disinfectant containing chlorine, oxygen or alcohol, and the adopted surfactant and the disinfectant have unpleasant pungent odor; it is irritant and corrosive to fabric and skin; the stability is poor; the compatibility with other raw materials is poor; the environment is not friendly, and the health of the baby is easily damaged; most of the chemical substances are mixed, the alkalinity is high, the irritation to the skin of a human body is high, the skin can be burnt after the chemical substances are used, some chemical substances can permeate into a machine body through pores and possibly generate serious health hidden dangers to human organs, water for cleaning clothes is discharged to cause poisoning in water organisms, river fishes and shrimps are in danger of death, aquatic plants are polluted, the ecological balance is destroyed, and the sustainable development of the society is seriously influenced. In order to develop sustainability of human beings, resources, safety, influence on environment and washing functions must be comprehensively considered in the development process of detergents. With the improvement of the requirements on the quality of life, the requirements on the baby detergent are continuously improved, and the market demand of the baby detergent is gradually increased, so that the development of the green environment-friendly baby detergent which is safer and has no stimulation and ensures good washing effect is very necessary.
Disclosure of Invention
The invention provides a laundry detergent containing an okra extract and raspberry enzyme and a preparation method thereof to solve the technical problems. The laundry detergent is added with the raw materials of okra extract and raspberry enzyme, the compatibility is scientific and reasonable, the laundry detergent does not contain chemically synthesized or strongly irritant anionic surfactant, enzyme preparation, whitening agent, fluorescent agent, essence, pigment and other potentially harmful auxiliary agents, the pH value of the prepared laundry detergent is 6.5-7.3, the foam is fine and rich, the dirt-removing capacity is strong, the bacteriostatic effect is good, the laundry detergent has the characteristics of nature, cleanness and mildness, no harmful chemically synthesized substance residue is left, the washed clothes are clean, soft and skin-friendly after being dried in the air, the excrement stain, the oral water stain and the food oil stain of the baby clothes can be effectively removed, the laundry detergent is particularly suitable for washing the baby clothes, does not hurt hands, does not produce irritation to human skin, does not have tight feeling or burning feeling to the skin after being used, the safety is high, the discharge does not cause pollution to water, and is green, environment-friendly and the preparation process is simple, the operation is simple and convenient, and the production cost of the laundry detergent is greatly reduced.
In order to achieve the above purpose, the invention adopts the following technical scheme:
a laundry detergent containing okra extract and raspberry enzyme is prepared from the following raw materials in parts by weight: 82-92 parts of plant ash extract, 90-100 parts of okra extract, 90-100 parts of raspberry enzyme, 63-73 parts of soapnut saponin, 63-73 parts of tea saponin, 25-35 parts of baking soda, 30-40 parts of polyoxyethylene fatty acid, 45-55 parts of citric acid, 45-55 parts of calabash fruit, 20-30 parts of natural essence and 40-60 parts of deionized water.
Further, the laundry detergent containing the okra extract and the raspberry enzyme is prepared from the following raw materials in parts by weight: 84-90 parts of plant ash extract, 93-97 parts of okra extract, 93-97 parts of raspberry enzyme, 65-70 parts of soapnut saponin, 65-70 parts of tea saponin, 27-33 parts of baking soda, 32-37 parts of polyoxyethylene fatty acid ester, 47-52 parts of citric acid, 48-53 parts of calabash fruit, 23-28 parts of natural essence and 45-55 parts of deionized water.
Further, the laundry detergent containing the okra extract and the raspberry enzyme is prepared from the following raw materials in parts by weight: 87 parts of plant ash extract, 95 parts of okra extract, 95 parts of raspberry enzyme, 68 parts of soapberry saponin, 68 parts of tea saponin, 30 parts of baking soda, 35 parts of polyoxyethylene fatty acid ester, 50 parts of citric acid, 50 parts of calabash fruit, 25 parts of natural essence and 50 parts of deionized water.
Further, the preparation method of the plant ash extract comprises the following steps: burning mildew-free and sun-dried straws, adding deionized water with the weight 2-3 times of the total weight of the straws, performing reflux extraction for 4-5 hours, filtering and collecting filtrate to obtain the plant ash extract.
Further, the preparation method of the okra extract comprises the following steps: placing the okra tender pods and the okra flowers into water with the temperature of 93-97 ℃ for treatment for 5-7 s, taking out the okra tender pods and the okra flowers, cooling to room temperature, adding deionized water, grinding into juice, concentrating and drying at the low temperature of 16-20 ℃ to obtain the okra extract.
Further, the preparation method of the raspberry enzyme comprises the following steps: cleaning and mashing fresh raspberry, adding wormwood 0.3-0.6 times of the mass of the raspberry, white spirit 0.4-0.5 times of the mass of the raspberry and white sugar 0.05-0.1 times of the mass of the raspberry, stirring uniformly, standing and fermenting for 13-15 days, filtering and collecting filtrate to obtain the raspberry enzyme.
Further, the natural essence is one or more of rose essential oil, honeysuckle essential oil, chrysanthemum essential oil, mint essential oil, wormwood essential oil and perilla extract.
In the present application, the preparation method of the perilla extract comprises: adding 2-2.5 times of the weight of the perilla and 75% of ethanol solution into the perilla, performing reflux extraction for 2-3 hours, and filtering and removing residues to obtain the perilla extract.
Further, a preparation method of the laundry detergent containing the okra extract and the raspberry enzyme comprises the following steps:
(1) weighing soapnut saponin, tea saponin, polyoxyethylene fatty acid ester, citric acid, calabash fruit and deionized water in parts by weight, adding the deionized water into a reaction kettle, heating to 65-70 ℃, adding the polyoxyethylene fatty acid ester, the citric acid and the calabash fruit, uniformly stirring, cooling to 37-42 ℃, adjusting the pH value of the solution to 6.8-7.2, adding the soapnut saponin and the tea saponin, and stirring for reacting for 60-70 min to obtain a mixed material;
(2) adding plant ash extract, okra extract, raspberry enzyme, baking soda and natural essence into the mixture obtained in the step (1), performing ultrasonic treatment, stirring, and performing heat preservation treatment at 35-40 ℃ for 155-165 min to obtain a semi-finished product of the laundry detergent;
(3) and (3) performing vacuum degassing on the semi-finished product of the laundry detergent subjected to heat preservation treatment in the step (2), and performing split charging treatment to obtain the laundry detergent.
Further, in the step (2), the ultrasonic treatment is carried out at 0.15-0.3 kHz for 10-15 min.
Further, in the step (3), the negative pressure of the vacuum degassing is controlled to be 3.5-4 MPa.
Due to the adoption of the technical scheme, the invention has the following beneficial effects:
(1) the laundry detergent is scientific and reasonable in compatibility due to the fact that the raw materials of the okra extract and the raspberry enzyme are added, and the laundry detergent does not contain chemically synthesized or strong-irritation anionic surfactant, enzyme preparations, whitening agents, fluorescent agents, essence, pigments and other potentially harmful auxiliaries, is natural, clean and mild, does not hurt hands, and does not cause tight feeling or burning feeling on the skin after washing clothes.
(2) The laundry detergent adopts natural essence to carry fragrance, the fragrance is natural and fresh, the laundry detergent is added with various plant extracts to promote a laundry effect, the foam is fine and rich, the dirt-removing capacity is strong, the antibacterial effect is good, no harmful chemical synthetic substance is left, the washed clothes are clean, soft and skin-friendly after being dried, the urine stain, the mouth water stain and the food oil stain of the baby clothes can be effectively removed, and the laundry detergent is particularly suitable for washing the baby clothes.
(3) The laundry detergent is prepared from natural raw materials, emission does not pollute water, the laundry detergent is green and environment-friendly, the raw material source is wide, the preparation process is simple, the operation is simple and convenient, the production cost of the laundry detergent is greatly reduced, the pH value of the prepared laundry detergent is 6.5-7.3, irritation to human skin is avoided, the skin does not have tightness or burning feeling after use, and the safety is high.
Detailed Description
The following is a detailed description of the embodiments of the present invention, but the present invention is not limited to these embodiments, and any modifications or substitutions in the basic spirit of the embodiments are included in the scope of the present invention as claimed in the claims.
Example 1
A laundry detergent containing okra extract and raspberry enzyme is prepared from the following raw materials in parts by weight: 82-92 parts of plant ash extract, 90-100 parts of okra extract, 90-100 parts of raspberry enzyme, 63-73 parts of soapnut saponin, 63-73 parts of tea saponin, 25-35 parts of baking soda, 30-40 parts of polyoxyethylene fatty acid, 45-55 parts of citric acid, 45-55 parts of calabash fruit, 20-30 parts of natural essence and 40-60 parts of deionized water.
Further, the preparation method of the plant ash extract comprises the following steps: burning mildew-free and sun-dried straws, adding deionized water with the weight 2-3 times of the total weight of the straws, performing reflux extraction for 4-5 hours, filtering and collecting filtrate to obtain the plant ash extract; the preparation method of the okra extract comprises the following steps: placing the okra tender pods and the okra flowers into water with the temperature of 93-97 ℃ for treatment for 5-7 s, taking out the okra tender pods and the okra flowers, cooling to room temperature, adding deionized water, grinding into juice, concentrating and drying at the low temperature of 16-20 ℃ to obtain an okra extract; the preparation method of the raspberry enzyme comprises the following steps: cleaning and mashing fresh raspberry, adding wormwood 0.3-0.6 times of the mass of the raspberry, white spirit 0.4-0.5 times of the mass of the raspberry and white sugar 0.05-0.1 times of the mass of the raspberry, uniformly stirring, standing and fermenting for 13-15 days, filtering and collecting filtrate to obtain raspberry enzyme; the natural essence is one or more of rose essential oil, honeysuckle essential oil, chrysanthemum essential oil, mint essential oil, wormwood essential oil and perilla extract.
A preparation method of a laundry detergent containing okra extract and raspberry enzyme comprises the following steps:
(1) weighing soapnut saponin, tea saponin, polyoxyethylene fatty acid ester, citric acid, calabash fruit and deionized water in parts by weight, adding the deionized water into a reaction kettle, heating to 65-70 ℃, adding the polyoxyethylene fatty acid ester, the citric acid and the calabash fruit, uniformly stirring, cooling to 37-42 ℃, adjusting the pH value of the solution to 6.8-7.2, adding the soapnut saponin and the tea saponin, and stirring for reacting for 60-70 min to obtain a mixed material;
(2) adding plant ash extract, okra extract, raspberry enzyme, baking soda and natural essence into the mixture obtained in the step (1), performing ultrasonic treatment, stirring, and performing heat preservation treatment at 35-40 ℃ for 155-165 min to obtain a semi-finished product of the laundry detergent; the ultrasonic treatment is carried out at 0.15-0.3 kHz for 10-15 min;
(3) vacuum degassing is carried out on the semi-finished product of the laundry detergent subjected to heat preservation treatment in the step (2), and split charging treatment is carried out to obtain the laundry detergent; and the negative pressure of the vacuum degassing is controlled to be 3.5-4 Mpa.
Example 2
The difference from the embodiment 1 is that: a laundry detergent containing okra extract and raspberry enzyme is prepared from the following raw materials in parts by weight: 84 parts of plant ash extract, 93 parts of okra extract, 93 parts of raspberry enzyme, 65 parts of soapberry saponin, 65 parts of tea saponin, 27 parts of baking soda, 32 parts of polyoxyethylene fatty acid ester, 47 parts of citric acid, 48 parts of calabash fruit, 23 parts of natural essence and 45 parts of deionized water, and other conditions are unchanged.
Example 3
The difference from the embodiment 1 is that: a laundry detergent containing okra extract and raspberry enzyme is prepared from the following raw materials in parts by weight: 90 parts of plant ash extract, 97 parts of okra extract, 97 parts of raspberry enzyme, 70 parts of soapberry saponin, 70 parts of tea saponin, 33 parts of baking soda, 37 parts of polyoxyethylene fatty acid ester, 52 parts of citric acid, 53 parts of calabash, 28 parts of natural essence and 55 parts of deionized water, and the other conditions are unchanged.
Example 4
The difference from the embodiment 1 is that: a laundry detergent containing okra extract and raspberry enzyme is prepared from the following raw materials in parts by weight: 87 parts of plant ash extract, 95 parts of okra extract, 95 parts of raspberry enzyme, 68 parts of soapberry saponin, 68 parts of tea saponin, 30 parts of baking soda, 35 parts of polyoxyethylene fatty acid ester, 50 parts of citric acid, 50 parts of calabash fruit, 25 parts of natural essence and 50 parts of deionized water, and other conditions are unchanged.
Example 5
The difference from the embodiment 1 is that: a preparation method of a laundry detergent containing okra extract and raspberry enzyme comprises the following steps:
(1) weighing soapnut saponin, tea saponin, polyoxyethylene fatty acid ester, citric acid, calabash fruit and deionized water in parts by weight, adding deionized water into a reaction kettle, heating to 68 ℃, adding polyoxyethylene fatty acid ester, citric acid and calabash fruit, uniformly stirring, cooling to 40 ℃, adjusting the pH value of the solution to 7.0, adding soapnut saponin and tea saponin, and stirring for reacting for 65min to obtain a mixed material;
(2) adding plant ash extract, okra extract, raspberry enzyme, baking soda and natural essence into the mixture obtained in the step (1), performing ultrasonic treatment, stirring, and performing heat preservation treatment at 37 ℃ for 160min to obtain a semi-finished product of the laundry detergent; the ultrasonic treatment is carried out at 0.22kHz for 13 min;
(3) vacuum degassing is carried out on the semi-finished product of the laundry detergent subjected to heat preservation treatment in the step (2), and then split charging is carried out to obtain the laundry detergent; the negative pressure of the vacuum degassing is controlled to be 3.7 Mpa; other conditions were unchanged.
Example 6
The difference from the embodiment 1 is that: the preparation method of the plant ash extract comprises the following steps: burning mildew-free and sun-dried straws, adding deionized water with the weight 2.5 times of the total weight of the straws, reflux-extracting for 4.5h, filtering, and collecting filtrate to obtain the plant ash extract; the preparation method of the okra extract comprises the following steps: treating tender okra pods and flowers in 95 deg.C water for 6s, cooling to room temperature, adding deionized water, grinding into juice, concentrating at 18 deg.C, and drying to obtain okra extract.
Example 7
The difference from the embodiment 1 is that: the preparation method of the raspberry enzyme comprises the following steps: cleaning fresh raspberry, mashing, adding folium Artemisiae Argyi with a weight of 0.45 times of that of raspberry, Chinese liquor with a weight of 0.45 times of that of raspberry and white sugar with a weight of 0.4 times of that of raspberry, stirring uniformly, standing for fermentation for 14 days, filtering, and collecting filtrate to obtain the raspberry enzyme, wherein other conditions are unchanged.
Example 8
The difference from the embodiment 1 is that: the natural essence is rose essential oil, honeysuckle essential oil, chrysanthemum essential oil and wormwood essential oil, and other conditions are unchanged.
Comparative example 1
The difference from the embodiment 1 is that: the formula of the laundry detergent is not added with okra extract and raspberry enzyme, and other conditions are not changed.
Comparative example 2
The difference from the embodiment 1 is that: the special laundry detergent for the infants is prepared from the following raw materials in parts by weight: 70 parts of plant ash extract, 120 parts of okra extract, 200 parts of raspberry enzyme, 45 parts of soapberry saponin, 30 parts of tea saponin, 45 parts of baking soda, 10 parts of polyoxyethylene fatty acid ester, 25 parts of citric acid, 75 parts of calabash fruit, 50 parts of natural essence and 30 parts of deionized water, and other conditions are unchanged.
Comparative example 3
The difference from the embodiment 1 is that: the formula of the laundry detergent is not added with polyoxyethylene fatty acid ester, tea saponin, calabash and natural essence, and other conditions are not changed.
Comparative example 4
The preparation of the laundry detergent was carried out according to the examples in patent application CN 201711043583.6.
Comparative example 5
The preparation of the laundry detergent was carried out according to the examples in patent application CN 201710001431.3.
To further illustrate that the present invention can achieve the technical effects, the following experiments were performed:
firstly, washing performance test
The test method comprises the following steps: the laundry liquids prepared by the methods of examples 1 to 8 and comparative examples 1 to 5 were respectively subjected to a washing performance test according to the method specified in GB/T13174-2008 "measurement of detergency and circular washing performance of a detergent for clothing", and the test results are shown in table 1 below.
TABLE 1
The test data in table 1 show that the okra extract and the raspberry enzyme added to the laundry detergent disclosed by the invention have good decontamination capability, good emulsification capability on protein dirt and sebum dirt, and good decontamination effect, so that the laundry detergent can effectively remove urine stains, saliva stains, food oil stains and the like of infant clothes.
Second, softness test
The test method comprises the following steps: circularly washing: the method comprises the following steps of (1) randomly and averagely dividing 130 test towels (pure cotton) into 13 groups, respectively putting the groups into a drum-type washing machine, respectively adding the laundry detergents prepared by the methods of examples 1-8 and comparative examples 1-5, starting the washing machine, automatically finishing the washing process under the same conditions (fast washing for 30 minutes), continuously carrying out the washing process for 20 times, taking out the towels, putting the towels on a clothes hanger, naturally airing the towels, and testing the towels for use;
secondly, sensory testing: the standard towels and groups of test towels were laid flat on the palm of the tester's hand (10 people total, a, B, C, D, E, F, G, H, K, L respectively), rubbed on both cheeks with appropriate force or felt their softness simultaneously with the hand, and their softness performance was scored against the standard towels (10 softest, 1 hardest). The results of the experiment are shown in table 2 below.
TABLE 2
As can be seen from the test data in Table 2, the laundry detergent of the present invention has a better laundry softening effect, and the washed laundry is clean, soft and skin-friendly after being dried.
Third, skin irritation test
The test method comprises the following steps: the 130 testers were randomly divided into 13 groups, each group of the volunteers washed the clothes for 15min with the aqueous solution mixed with 0.3% of the laundry detergent prepared by the methods of examples 1 to 8 and comparative examples 1 to 5, the scores of the irritation, tightness and burning of each group of the laundry detergent in the process of washing the clothes were collected, the score of the zero irritation, zero tightness, zero burning skin was 10, the score of the very irritation, very tightness and very burning skin was 1, the average score was taken as the result score, and the experimental results are shown in table 3 below.
TABLE 3
As can be seen from the experimental data in Table 3, the laundry detergent is mild, has no irritation to hands, and does not cause tight feeling or burning feeling to the skin during and after the laundry process.
To sum up, the laundry detergent is added with the raw materials of the okra extract and the raspberry enzyme, the compatibility is scientific and reasonable, the laundry detergent does not contain chemically synthesized or strong-irritation anionic surfactant, enzyme preparation, whitening agent, fluorescent agent, essence, pigment and other potentially harmful auxiliary agents, the pH value of the prepared laundry detergent is 6.5-7.3, the foam is fine and rich, the dirt-removing capacity is strong, the bacteriostatic effect is good, the laundry detergent has the characteristics of nature, cleanness and mildness, no harmful chemically synthesized substance residue exists, the washed clothes are clean, soft and skin-friendly after being dried, the urine stain, the mouth water stain and the food oil stain of the baby clothes can be effectively removed, the laundry detergent is particularly suitable for washing the baby clothes, does not hurt hands, does not irritate human skin, does not have tight feeling or burning feeling on the skin after being used, the safety is high, and the water body cannot be polluted due to discharge, and the laundry detergent is green, the preparation method is environment-friendly, simple in preparation process and simple and convenient to operate, and greatly reduces the production cost of the laundry detergent.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.
Claims (10)
1. The laundry detergent containing the okra extract and the raspberry enzyme is characterized by being prepared from the following raw materials in parts by weight: 82-92 parts of plant ash extract, 90-100 parts of okra extract, 90-100 parts of raspberry enzyme, 63-73 parts of soapnut saponin, 63-73 parts of tea saponin, 25-35 parts of baking soda, 30-40 parts of polyoxyethylene fatty acid, 45-55 parts of citric acid, 45-55 parts of calabash fruit, 20-30 parts of natural essence and 40-60 parts of deionized water.
2. The laundry detergent containing okra extract and raspberry enzyme according to claim 1, is prepared from the following raw materials in parts by weight: 84-90 parts of plant ash extract, 93-97 parts of okra extract, 93-97 parts of raspberry enzyme, 65-70 parts of soapnut saponin, 65-70 parts of tea saponin, 27-33 parts of baking soda, 32-37 parts of polyoxyethylene fatty acid ester, 47-52 parts of citric acid, 48-53 parts of calabash fruit, 23-28 parts of natural essence and 45-55 parts of deionized water.
3. The laundry detergent containing okra extract and raspberry enzyme according to claim 1, is prepared from the following raw materials in parts by weight: 87 parts of plant ash extract, 95 parts of okra extract, 95 parts of raspberry enzyme, 68 parts of soapberry saponin, 68 parts of tea saponin, 30 parts of baking soda, 35 parts of polyoxyethylene fatty acid ester, 50 parts of citric acid, 50 parts of calabash fruit, 25 parts of natural essence and 50 parts of deionized water.
4. The laundry detergent containing okra extract and raspberry enzyme according to any one of claims 1-3, wherein: the preparation method of the plant ash extract comprises the following steps: burning mildew-free and sun-dried straws, adding deionized water with the weight 2-3 times of the total weight of the straws, performing reflux extraction for 4-5 hours, filtering and collecting filtrate to obtain the plant ash extract.
5. The laundry detergent containing okra extract and raspberry enzyme according to any one of claims 1-3, wherein: the preparation method of the okra extract comprises the following steps: placing the okra tender pods and the okra flowers into water with the temperature of 93-97 ℃ for treatment for 5-7 s, taking out the okra tender pods and the okra flowers, cooling to room temperature, adding deionized water, grinding into juice, concentrating and drying at the low temperature of 16-20 ℃ to obtain the okra extract.
6. The laundry detergent containing okra extract and raspberry enzyme according to any one of claims 1-3, wherein: the preparation method of the raspberry enzyme comprises the following steps: cleaning and mashing fresh raspberry, adding wormwood 0.3-0.6 times of the mass of the raspberry, white spirit 0.4-0.5 times of the mass of the raspberry and white sugar 0.05-0.1 times of the mass of the raspberry, stirring uniformly, standing and fermenting for 13-15 days, filtering and collecting filtrate to obtain the raspberry enzyme.
7. The laundry detergent containing okra extract and raspberry enzyme according to any one of claims 1-3, wherein: the natural essence is one or more of rose essential oil, honeysuckle essential oil, chrysanthemum essential oil, mint essential oil, wormwood essential oil and perilla extract.
8. A preparation method of a laundry detergent containing an okra extract and raspberry enzyme is characterized by comprising the following steps:
(1) weighing soapnut saponin, tea saponin, polyoxyethylene fatty acid ester, citric acid, calabash fruit and deionized water in parts by weight, adding the deionized water into a reaction kettle, heating to 65-70 ℃, adding the polyoxyethylene fatty acid ester, the citric acid and the calabash fruit, uniformly stirring, cooling to 37-42 ℃, adjusting the pH value of the solution to 6.8-7.2, adding the soapnut saponin and the tea saponin, and stirring for reacting for 60-70 min to obtain a mixed material;
(2) adding plant ash extract, okra extract, raspberry enzyme, baking soda and natural essence into the mixture obtained in the step (1), performing ultrasonic treatment, stirring, and performing heat preservation treatment at 35-40 ℃ for 155-165 min to obtain a semi-finished product of the laundry detergent;
(3) and (3) performing vacuum degassing on the semi-finished product of the laundry detergent subjected to heat preservation treatment in the step (2), and performing split charging treatment to obtain the laundry detergent.
9. The method for preparing a laundry detergent containing okra extract and raspberry enzyme according to claim 8, wherein the laundry detergent comprises: in the step (2), the ultrasonic treatment is carried out for 0.15-0.3 kHz and the time is 10-15 min.
10. The method for preparing a laundry detergent containing okra extract and raspberry enzyme according to claim 8, wherein the laundry detergent comprises: in the step (3), the negative pressure of the vacuum degassing is controlled to be 3.5-4 Mpa.
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| CN113549499A (en) * | 2021-06-24 | 2021-10-26 | 苏潮辉 | Sapindus saponin laundry detergent and preparation method thereof |
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2019
- 2019-09-23 CN CN201910900137.5A patent/CN110591834A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113549499A (en) * | 2021-06-24 | 2021-10-26 | 苏潮辉 | Sapindus saponin laundry detergent and preparation method thereof |
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