CN106544179A - A kind of infant coagulates pearl and preparation method and application with laundry - Google Patents
A kind of infant coagulates pearl and preparation method and application with laundry Download PDFInfo
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- CN106544179A CN106544179A CN201610961437.0A CN201610961437A CN106544179A CN 106544179 A CN106544179 A CN 106544179A CN 201610961437 A CN201610961437 A CN 201610961437A CN 106544179 A CN106544179 A CN 106544179A
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- laundry
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- coagulates
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- 238000002360 preparation method Methods 0.000 title claims abstract description 23
- 239000007788 liquid Substances 0.000 claims abstract description 36
- 238000000605 extraction Methods 0.000 claims abstract description 31
- 240000001789 Carlina acaulis Species 0.000 claims abstract description 18
- 235000005882 Carlina acaulis Nutrition 0.000 claims abstract description 18
- 241000628997 Flos Species 0.000 claims abstract description 9
- 125000000217 alkyl group Chemical group 0.000 claims abstract description 9
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229940073507 cocamidopropyl betaine Drugs 0.000 claims abstract description 9
- -1 lauroyl musculamine Chemical compound 0.000 claims abstract description 6
- 239000003845 household chemical Substances 0.000 claims abstract description 4
- 239000000843 powder Substances 0.000 claims description 35
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 28
- 239000000203 mixture Substances 0.000 claims description 28
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 22
- 238000003756 stirring Methods 0.000 claims description 17
- 239000008367 deionised water Substances 0.000 claims description 14
- 229910021641 deionized water Inorganic materials 0.000 claims description 14
- 238000001914 filtration Methods 0.000 claims description 14
- 150000005846 sugar alcohols Polymers 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 8
- 238000004806 packaging method and process Methods 0.000 claims description 8
- 235000013162 Cocos nucifera Nutrition 0.000 claims description 7
- 244000060011 Cocos nucifera Species 0.000 claims description 7
- QXNVGIXVLWOKEQ-UHFFFAOYSA-N Disodium Chemical compound [Na][Na] QXNVGIXVLWOKEQ-UHFFFAOYSA-N 0.000 claims description 7
- 241000196324 Embryophyta Species 0.000 claims description 7
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 claims description 7
- 108091005804 Peptidases Proteins 0.000 claims description 7
- 239000004365 Protease Substances 0.000 claims description 7
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims description 7
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 7
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 7
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 claims description 7
- 229960004756 ethanol Drugs 0.000 claims description 7
- 229930195729 fatty acid Natural products 0.000 claims description 7
- 239000000194 fatty acid Substances 0.000 claims description 7
- 150000004665 fatty acids Chemical class 0.000 claims description 7
- 239000001257 hydrogen Substances 0.000 claims description 7
- 229910052739 hydrogen Inorganic materials 0.000 claims description 7
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 6
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 6
- 229920002565 Polyethylene Glycol 400 Polymers 0.000 claims description 2
- JLFNLZLINWHATN-UHFFFAOYSA-N pentaethylene glycol Chemical compound OCCOCCOCCOCCOCCO JLFNLZLINWHATN-UHFFFAOYSA-N 0.000 claims description 2
- 229940113115 polyethylene glycol 200 Drugs 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 8
- 239000004094 surface-active agent Substances 0.000 abstract description 4
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 3
- 238000005202 decontamination Methods 0.000 abstract description 3
- 230000003588 decontaminative effect Effects 0.000 abstract description 3
- 229940051841 polyoxyethylene ether Drugs 0.000 abstract description 3
- 229920000056 polyoxyethylene ether Polymers 0.000 abstract description 3
- 238000005406 washing Methods 0.000 abstract description 3
- SNRUBQQJIBEYMU-UHFFFAOYSA-N Dodecane Natural products CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 abstract description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract description 2
- 206010040880 Skin irritation Diseases 0.000 abstract description 2
- XEFQLINVKFYRCS-UHFFFAOYSA-N Triclosan Chemical compound OC1=CC(Cl)=CC=C1OC1=CC=C(Cl)C=C1Cl XEFQLINVKFYRCS-UHFFFAOYSA-N 0.000 abstract description 2
- 239000002253 acid Substances 0.000 abstract description 2
- 230000003078 antioxidant effect Effects 0.000 abstract description 2
- 230000003385 bacteriostatic effect Effects 0.000 abstract description 2
- 150000001875 compounds Chemical class 0.000 abstract description 2
- JMGZBMRVDHKMKB-UHFFFAOYSA-L disodium;2-sulfobutanedioate Chemical compound [Na+].[Na+].OS(=O)(=O)C(C([O-])=O)CC([O-])=O JMGZBMRVDHKMKB-UHFFFAOYSA-L 0.000 abstract description 2
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 abstract description 2
- 229930003935 flavonoid Natural products 0.000 abstract description 2
- 150000002215 flavonoids Chemical class 0.000 abstract description 2
- 235000017173 flavonoids Nutrition 0.000 abstract description 2
- 238000005187 foaming Methods 0.000 abstract description 2
- 150000004676 glycans Chemical class 0.000 abstract description 2
- 150000008442 polyphenolic compounds Chemical class 0.000 abstract description 2
- 235000013824 polyphenols Nutrition 0.000 abstract description 2
- 229920001282 polysaccharide Polymers 0.000 abstract description 2
- 239000005017 polysaccharide Substances 0.000 abstract description 2
- 239000003755 preservative agent Substances 0.000 abstract description 2
- 230000002335 preservative effect Effects 0.000 abstract description 2
- 230000036556 skin irritation Effects 0.000 abstract description 2
- 231100000475 skin irritation Toxicity 0.000 abstract description 2
- 229910052708 sodium Inorganic materials 0.000 abstract description 2
- 239000011734 sodium Substances 0.000 abstract description 2
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 abstract description 2
- 235000010234 sodium benzoate Nutrition 0.000 abstract description 2
- 239000004299 sodium benzoate Substances 0.000 abstract description 2
- 150000005856 steroid saponins Chemical class 0.000 abstract description 2
- 229960003500 triclosan Drugs 0.000 abstract description 2
- 230000000845 anti-microbial effect Effects 0.000 abstract 1
- 239000003963 antioxidant agent Substances 0.000 abstract 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 10
- 238000001035 drying Methods 0.000 description 7
- ULUAUXLGCMPNKK-UHFFFAOYSA-N Sulfobutanedioic acid Chemical class OC(=O)CC(C(O)=O)S(O)(=O)=O ULUAUXLGCMPNKK-UHFFFAOYSA-N 0.000 description 6
- BQODPTQLXVVEJG-UHFFFAOYSA-N [O].C=C Chemical group [O].C=C BQODPTQLXVVEJG-UHFFFAOYSA-N 0.000 description 5
- 239000003599 detergent Substances 0.000 description 5
- 235000013350 formula milk Nutrition 0.000 description 4
- 238000004108 freeze drying Methods 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 2
- 210000004247 hand Anatomy 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2065—Polyhydric alcohols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38618—Protease or amylase in liquid compositions only
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/90—Betaines
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D2111/00—Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
- C11D2111/10—Objects to be cleaned
- C11D2111/12—Soft surfaces, e.g. textile
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
Abstract
The present invention discloses solidifying pearl of a kind of infant laundry and preparation method and application, belongs to household chemicals field.The solidifying pearl product of the laundry contains natural botanical extraction liquid, the effect of with antibacterial bacteriostatic；Using surfactant such as alkyl polyglucoside 0814, cocamido propyl betaine CBA 35, Dodecyl Polyoxyethylene Ether sulfosuccinate disodium, lauroyl musculamine acid sodium etc. are used as washing decontamination main body, for green product, low, foaming abundancy can be remained with degradable, detergency ability is good, and moderate performance, it is little to skin irritation, it is specially adapted to infant or child.Contain Radix Ophiopogonis polysaccharide, steroid saponin, polyphenol in the extract for selecting Flos Camelliae Japonicae quintessence oil, Radix Ophiopogonis and Carlina acauliss, the compounds such as flavonoid, it is antimicrobial and antioxidant qualities that they have, and instead of traditional triclosan, the preservative such as Kazon, sodium benzoate so as to infant skin will not be caused damage.
Description
Technical field
The invention belongs to household chemicals field, and in particular to a kind of infant coagulates pearl and preparation method and application with laundry.
Background technology
With expanding economy and growth in the living standard, laundry detergents product from the laundry soap at initial stage excessively to detergent,
It is then the liquid detergent for yielding unusually brilliant results in recent years.Washing market is constantly developed, in April, 2015, and green wave is released new first at home
Generation laundry product --- the solidifying pearl of laundry.The product is considered as the upgrade version of liquid detergent.The solidifying pearl of laundry is subject to European ＆ American Market blue or green
Look at, and the achievement that market attracts people's attention with regard to acquirement once release at home, this is had compared with Important Relations with its excellent properties.The solidifying pearl of laundry
Due to using PVA pouch-packaged, using very simple and convenient, not dirty handss, not hurting hands.Its formula adopts ultra concentration surface activity
Agent, Rhizoma Trillii Tschonoskii, son can wash 6kg or so clothes, with 3 times of cleaning ability；Noresidue, pure and fresh pleasant, soft clothing are rinsed easily
Thing is non-stimulated, degerming antistatic；Simultaneously because its packaging is presented different shapes and examination so as to non-using transparent PVA film
Often there is visual impact.
At present, the patent of the solidifying pearl of the laundry of open report has CN201510436322.5, which discloses a kind of quintessence oil
Solidifying pearl of laundry and preparation method thereof；Patent CN201510437124.0, which disclose a kind of solidifying pearl of multifunctional laundry and its
Preparation method.The formula existing defects of above-mentioned two patent：Water content too high (>=10%) in formula, so high-moisture are washed
The stability of the solidifying pearl of clothing brings very big hidden danger.Patent CN201610216176.X discloses a kind of solidifying pearl of softening laundry and its preparation
Method.The adaption object of the solidifying pearl formulation product of above-mentioned laundry is adult, retrieves current patent it is not yet found that being adapted to child
Or the solidifying pearl product of laundry of infant.In this patent, we have proposed a kind of solidifying pearl product of laundry for being adapted to infant
Formula.
The content of the invention
In order to overcome the deficiencies in the prior art and shortcoming, the primary and foremost purpose of the present invention is to provide a kind of infant laundry
Solidifying pearl, the solidifying pearl product of the laundry contain natural botanical extraction liquid, the effect of with antibacterial bacteriostatic；The surfactant for adopting is for green
Color product, can remain low, foaming abundancy with degradable, and detergency ability is good, and moderate performance, little to skin irritation, especially
It is adapted to infant or child.
Another object of the present invention is to provide the preparation method of the solidifying pearl of above-mentioned infant laundry.
It is still another object of the present invention to provide application of the above-mentioned infant with the solidifying pearl of laundry.
The purpose of the present invention is achieved through the following technical solutions：
A kind of infant coagulates pearl with laundry, comprising component as follows by mass percentage：
Described polyhydric alcohol is ethylene glycol, glycerol, polyethylene glycol 200 or PEG400；
Described natural botanical extraction liquid is the mixture of Radix Ophiopogonis extract and Carlina acauliss extracting solution；
The preparation method of described natural botanical extraction liquid, comprises the steps of：
(1) by dry root Radix Ophiopogonis and the mixing of Carlina acauliss leaf, crush, obtain mixture of powders；
(2) mixture of powders obtained in step (1) is mixed with the ethanol of 3～8 times of volumes, then carries out Soxhlet and take out
Carry；After the completion of extraction, extracting solution is filtered, abandon filtering residue；
(3) extracting solution after step (2) filtration is dried, obtains extract dry powder；
(4) extract dry powder, dehydrated alcohol and deionized water obtained in step (3) are mixed into dissolving, obtains natural
Plant extraction liquid；
The mass ratio of Radix Ophiopogonis and Carlina acauliss described in step (1) is (1～3)：1；
The time of the soxhlet type described in step (2) is 3～8h.
The mode of the drying described in step (3) is preferably vacuum flashing drying or lyophilization；
The mass ratio of extract dry powder, second alcohol and water described in step (4) is 1:0.5:2；
The described infant preparation method of the solidifying pearl of laundry, comprises the steps of：
(1) by deionized water, cocoanut fatty acid diethanolamide, cocamido propyl betaine CAB-35 and lauryl alcohol
Polyoxyethylene ether sulfosuccinic acid esters disodium is mixed in proportion, and stirs until mix homogeneously；
(2) then cool down, sequentially add polyhydric alcohol, alkyl polyglucoside 0814 and N- lauroyl sodium hydrogen alpha-aminoglutarate, stirring mixing
Uniformly；
(3) then it is cooled to room temperature and adds protease, Flos Camelliae Japonicae quintessence oil and natural botanical extraction liquid, is uniformly mixed；
(4) it is last, above-mentioned feed liquid is added in automatic packaging machine, the solidifying pearl product of laundry is packaged into PVA film.
Stirring described in step (1) is until mix homogeneously in 65～90 DEG C of stirrings until mix homogeneously.
Being cooled to described in step (2) is cooled to 40～55 DEG C.
Solidifying application of the pearl in household chemicals field of laundry of described infant.
The principle of the present invention：The present invention is a kind of gentle in order to obtain, and the low infant of zest is being matched somebody with somebody with the solidifying pearl of laundry
Meticulous selection is done in side, surfactant such as alkyl polyglucoside 0814 used, cocamido propyl betaine in the present invention
CBA-35, Dodecyl Polyoxyethylene Ether sulfosuccinate disodium, lauroyl musculamine acid sodium etc. are used as washing decontamination main body, foam
Abundant, clean effect is good, and zest is low, can be specially adapted to infant or child with degradable.Selection Flos Camelliae Japonicae quintessence oil,
Contain the compounds such as Radix Ophiopogonis polysaccharide, steroid saponin, polyphenol, flavonoid in the extract of Radix Ophiopogonis and Carlina acauliss, it is anti-that they have
Bacterium and antioxidative characteristic, instead of the preservative such as traditional triclosan, Kazon, sodium benzoate so as to will not be to Infant
Skin causes damage.
The present invention is had the following advantages and effect relative to prior art：
(1) present invention is gentle using decontamination main body, and the surfactant of low stimulation, the laundry for preparing coagulate Zhu Paomofeng
Richness, clean effect are good, and zest is low, and infant skin will not be caused damage.
(2) the natural botanical extraction liquid component added in the solidifying pearl of laundry that the present invention is provided, with excellent antibacterial and anti-
Oxidation effectiveness, while also having certain protection effect to infant skin.
Specific embodiment
With reference to embodiment, the present invention is described in further detail, but embodiments of the present invention not limited to this.
Embodiment 1
A kind of infant coagulates pearl with laundry, comprising component as follows by mass percentage：
The preparation method of described natural botanical extraction liquid, comprises the steps of：
(1) by dry root Radix Ophiopogonis and the mixing of Carlina acauliss leaf, crush, obtain mixture of powders；
(2) mixture of powders obtained in step (1) is mixed with the ethanol of 5 times of volumes, then carries out soxhlet type 4h；
After the completion of extraction, extracting solution is filtered, abandon filtering residue；
(3) extracting solution after step (2) filtration is dried, obtains extract dry powder；
(4) extract dry powder, dehydrated alcohol and deionized water obtained in step (3) are mixed into dissolving, obtains natural
Plant extraction liquid；
The mass ratio 2 of Radix Ophiopogonis and Carlina acauliss described in step (1):1；
The mode of the drying described in step (3) is preferably vacuum flashing and is dried；
The mass ratio of extract dry powder, second alcohol and water described in step (4) is 1:0.5:2；
The above-mentioned shield infant preparation method of the solidifying pearl of laundry, comprises the steps of：
By deionized water, cocoanut fatty acid diethanolamide, cocamido propyl betaine CAB-35 and lauryl alcohol it is poly-
Oxygen ethylene ether sulfosuccinates disodium is mixed in proportion, in 70 DEG C of stirrings until mix homogeneously
Then it is cooled to 55 DEG C and sequentially adds polyhydric alcohol, alkyl polyglucoside 0814 and N- lauroyl sodium hydrogen alpha-aminoglutarate, stirring is mixed
Close uniform；
Then it is cooled to room temperature and adds protease, Flos Camelliae Japonicae quintessence oil and natural botanical extraction liquid, is uniformly mixed.
Finally, above-mentioned feed liquid is added in automatic packaging machine, the solidifying pearl product of laundry is packaged into PVA film.
Embodiment 2
A kind of infant coagulates pearl with laundry, comprising component as follows by mass percentage：
The preparation method of described natural botanical extraction liquid, comprises the steps of：
(1) by dry root Radix Ophiopogonis and the mixing of Carlina acauliss leaf, crush, obtain mixture of powders；
(2) mixture of powders obtained in step (1) is mixed with the ethanol of 3 times of volumes, then carries out soxhlet type 8h；
After the completion of extraction, extracting solution is filtered, abandon filtering residue；
(3) extracting solution after step (2) filtration is dried, obtains extract dry powder；
(4) extract dry powder, dehydrated alcohol and deionized water obtained in step (3) are mixed into dissolving, obtains natural
Plant extraction liquid；
The mass ratio 1 of Radix Ophiopogonis and Carlina acauliss described in step (1):1；
The mode of the drying described in step (3) is preferably lyophilization；
The mass ratio of extract dry powder, second alcohol and water described in step (4) is 1:0.5:2；
The above-mentioned shield infant preparation method of the solidifying pearl of laundry, comprises the steps of：
By deionized water, cocoanut fatty acid diethanolamide, cocamido propyl betaine CAB-35 and lauryl alcohol it is poly-
Oxygen ethylene ether sulfosuccinates disodium is mixed in proportion, in 70 DEG C of stirrings until mix homogeneously
Then it is cooled to 40 DEG C and sequentially adds polyhydric alcohol, alkyl polyglucoside 0814 and N- lauroyl sodium hydrogen alpha-aminoglutarate, stirring is mixed
Close uniform；
Then it is cooled to room temperature and adds protease, Flos Camelliae Japonicae quintessence oil and natural botanical extraction liquid, is uniformly mixed.
Finally, above-mentioned feed liquid is added in automatic packaging machine, the solidifying pearl product of laundry is packaged into PVA film.
Embodiment 3
A kind of infant coagulates pearl with laundry, comprising component as follows by mass percentage：
The preparation method of described natural botanical extraction liquid, comprises the steps of：
(1) by dry root Radix Ophiopogonis and the mixing of Carlina acauliss leaf, crush, obtain mixture of powders；
(2) mixture of powders obtained in step (1) is mixed with the ethanol of 8 times of volumes, then carries out soxhlet type 3h；
After the completion of extraction, extracting solution is filtered, abandon filtering residue；
(3) extracting solution after step (2) filtration is dried, obtains extract dry powder；
(4) extract dry powder, dehydrated alcohol and deionized water obtained in step (3) are mixed into dissolving, obtains natural
Plant extraction liquid；
The mass ratio 3 of Radix Ophiopogonis and Carlina acauliss described in step (1):1；
The mode of the drying described in step (3) is preferably lyophilization；
The mass ratio of extract dry powder, second alcohol and water described in step (4) is 1:0.5:2；
The above-mentioned shield infant preparation method of the solidifying pearl of laundry, comprises the steps of：
By deionized water, cocoanut fatty acid diethanolamide, cocamido propyl betaine CAB-35 and lauryl alcohol it is poly-
Oxygen ethylene ether sulfosuccinates disodium is mixed in proportion, in 80 DEG C of stirrings until mix homogeneously
Then it is cooled to 50 DEG C and sequentially adds polyhydric alcohol, alkyl polyglucoside 0814 and N- lauroyl sodium hydrogen alpha-aminoglutarate, stirring is mixed
Close uniform；
Then it is cooled to room temperature and adds protease, Flos Camelliae Japonicae quintessence oil and natural botanical extraction liquid, is uniformly mixed.
Finally, above-mentioned feed liquid is added in automatic packaging machine, the solidifying pearl product of laundry is packaged into PVA film.
Embodiment 4
A kind of infant coagulates pearl with laundry, comprising component as follows by mass percentage：
The preparation method of described natural botanical extraction liquid, comprises the steps of：
(1) by dry root Radix Ophiopogonis and the mixing of Carlina acauliss leaf, crush, obtain mixture of powders；
(2) mixture of powders obtained in step (1) is mixed with the ethanol of 5 times of volumes, then carries out soxhlet type 4h；
After the completion of extraction, extracting solution is filtered, abandon filtering residue；
(3) extracting solution after step (2) filtration is dried, obtains extract dry powder；
(4) extract dry powder, dehydrated alcohol and deionized water obtained in step (3) are mixed into dissolving, obtains natural
Plant extraction liquid；
The mass ratio 2 of Radix Ophiopogonis and Carlina acauliss described in step (1):1；
The mode of the drying described in step (3) is preferably vacuum flashing and is dried；
The mass ratio of extract dry powder, second alcohol and water described in step (4) is 1:0.5:2；
The above-mentioned shield infant preparation method of the solidifying pearl of laundry, comprises the steps of：
By deionized water, cocoanut fatty acid diethanolamide, cocamido propyl betaine CAB-35 and lauryl alcohol it is poly-
Oxygen ethylene ether sulfosuccinates disodium is mixed in proportion, in 65 DEG C of stirrings until mix homogeneously
Then it is cooled to 45 DEG C and sequentially adds polyhydric alcohol, alkyl polyglucoside 0814 and N- lauroyl sodium hydrogen alpha-aminoglutarate, stirring is mixed
Close uniform；
Then it is cooled to room temperature and adds protease, Flos Camelliae Japonicae quintessence oil and natural botanical extraction liquid, is uniformly mixed.
Finally, above-mentioned feed liquid is added in automatic packaging machine, the solidifying pearl product of laundry is packaged into PVA film.
Embodiment 5
A kind of infant coagulates pearl with laundry, comprising component as follows by mass percentage：
The preparation method of described natural botanical extraction liquid, comprises the steps of：
(1) by dry root Radix Ophiopogonis and the mixing of Carlina acauliss leaf, crush, obtain mixture of powders；
(2) mixture of powders obtained in step (1) is mixed with the ethanol of 5 times of volumes, then carries out soxhlet type 4h；
After the completion of extraction, extracting solution is filtered, abandon filtering residue；
(3) extracting solution after step (2) filtration is dried, obtains extract dry powder；
(4) extract dry powder, dehydrated alcohol and deionized water obtained in step (3) are mixed into dissolving, obtains natural
Plant extraction liquid；
The mass ratio 2 of Radix Ophiopogonis and Carlina acauliss described in step (1):1；
The mode of the drying described in step (3) is preferably vacuum flashing and is dried；
The mass ratio of extract dry powder, second alcohol and water described in step (4) is 1:0.5:2；
The above-mentioned shield infant preparation method of the solidifying pearl of laundry, comprises the steps of：
By deionized water, cocoanut fatty acid diethanolamide, cocamido propyl betaine CAB-35 and lauryl alcohol it is poly-
Oxygen ethylene ether sulfosuccinates disodium is mixed in proportion, in 90 DEG C of stirrings until mix homogeneously
Then it is cooled to 55 DEG C and sequentially adds polyhydric alcohol, alkyl polyglucoside 0814 and N- lauroyl sodium hydrogen alpha-aminoglutarate, stirring is mixed
Close uniform；
Then it is cooled to room temperature and adds protease, Flos Camelliae Japonicae quintessence oil and natural botanical extraction liquid, is uniformly mixed.
Finally, above-mentioned feed liquid is added in automatic packaging machine, the solidifying pearl product of laundry is packaged into PVA film.
Effect example
According to QB/T 1224-2012《Dress material washes agent by liquid》The method of regulation, infant prepared by the detection present invention
With the detergency of the solidifying pearl of laundry.The method specified using QB/T 13174-2008 and soiled cotton, with machine determine the solidifying pearl sample of laundry and
The detergency of standard liquid detergent.As a result it is as shown in the table.
Above-described embodiment is the present invention preferably embodiment, but embodiments of the present invention not by above-described embodiment
Limit, other any spirit without departing from the present invention and the change, modification, replacement made under principle, combine, simplification,
Equivalent substitute mode is should be, is included within protection scope of the present invention.
Claims (10)
1. a kind of infant coagulates pearl with laundry, it is characterised in that comprising component as follows by mass percentage：
2. infant according to claim 1 coagulates pearl with laundry, it is characterised in that：
Described polyhydric alcohol is ethylene glycol, glycerol, polyethylene glycol 200 or PEG400.
3. infant according to claim 1 coagulates pearl with laundry, it is characterised in that：
Described natural botanical extraction liquid is the mixture of Radix Ophiopogonis extract and Carlina acauliss extracting solution.
4. the infant according to claim 1 or 3 coagulates pearl with laundry, it is characterised in that：
The preparation method of described natural botanical extraction liquid, comprises the steps of：
(1) by dry root Radix Ophiopogonis and the mixing of Carlina acauliss leaf, crush, obtain mixture of powders；
(2) mixture of powders obtained in step (1) is mixed with the ethanol of 3～8 times of volumes, then carries out soxhlet type；Carry
After the completion of taking, extracting solution is filtered, abandon filtering residue；
(3) extracting solution after step (2) filtration is dried, obtains extract dry powder；
(4) extract dry powder, dehydrated alcohol and deionized water obtained in step (3) are mixed into dissolving, obtains natural plants
Extracting solution.
5. infant according to claim 4 coagulates pearl with laundry, it is characterised in that：
The mass ratio of Radix Ophiopogonis and Carlina acauliss described in step (1) is (1～3)：1.
6. infant according to claim 4 coagulates pearl with laundry, it is characterised in that：
The time of the soxhlet type described in step (2) is 3～8h.
7. infant according to claim 4 coagulates pearl with laundry, it is characterised in that：
The mass ratio of extract dry powder, second alcohol and water described in step (4) is 1:0.5:2.
8. the infant described in any one of claim 1～7 coagulates the preparation method of pearl with laundry, it is characterised in that comprising following step
Suddenly：
(1) by deionized water, cocoanut fatty acid diethanolamide, cocamido propyl betaine CAB-35 and lauryl alcohol polyoxy
Ethylene ether sulfosuccinates disodium is mixed in proportion, and stirs until mix homogeneously；
(2) then cool down, sequentially add polyhydric alcohol, alkyl polyglucoside 0814 and N- lauroyl sodium hydrogen alpha-aminoglutarate, be uniformly mixed；
(3) then it is cooled to room temperature and adds protease, Flos Camelliae Japonicae quintessence oil and natural botanical extraction liquid, is uniformly mixed；
(4) it is last, above-mentioned feed liquid is added in automatic packaging machine, the solidifying pearl product of laundry is packaged into PVA film.
9. infant according to claim 8 coagulates the preparation method of pearl with laundry, it is characterised in that：
Stirring described in step (1) is until mix homogeneously in 65～90 DEG C of stirrings until mix homogeneously；
Being cooled to described in step (2) is cooled to 40～55 DEG C.
10. solidifying application of the pearl in household chemicals field of laundry of the infant described in any one of claim 1～7.
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| CN109468179A (en) * | 2018-11-05 | 2019-03-15 | 青岛美洁尔智能科技有限公司 | A kind of solidifying pearl of doing washing |
| CN115851384A (en) * | 2022-11-25 | 2023-03-28 | 浙江理工大学 | Preparation method of silk fibroin-polyaspartic acid-dodecyl glucoside disodium sulfosuccinate detergent |
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