CN103690392A - Baby shampoo containing marine bioactive substances, composition and preparation method thereof - Google Patents
Baby shampoo containing marine bioactive substances, composition and preparation method thereof Download PDFInfo
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- CN103690392A CN103690392A CN201310718513.1A CN201310718513A CN103690392A CN 103690392 A CN103690392 A CN 103690392A CN 201310718513 A CN201310718513 A CN 201310718513A CN 103690392 A CN103690392 A CN 103690392A
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Abstract
The invention discloses a baby shampoo containing marine bioactive substances, a composition and a preparation method thereof. The baby shampoo comprises the following components in percentage by weight: 2.0-4.0% of marine biological bactericide, 5.0-8.0% of seaweed polysaccharide, 8.0-15.0% of alkyl glucoside, 5.0-10.0% of cocamidopropyl betaine, 10.0-15.0% of alcohol ether carboxylate, 6.0-10.0% of stearamide ammonium salt, 1.0-1.5% of sodium chloride, 0.5-2.0% of citric acid, 0.5-2.0% of edible flavoring essence and the balance of pure water. The preparation method comprises the following steps: adding alkyl glucoside, cocamidopropyl betaine, alcohol ether carboxylate and stearamide ammonium salt into pure water, and stirring and emulsifying to obtain a mixed solution A; adding the marine biological bactericide and seaweed polysaccharide into the mixed solution A, and stirring and uniformly mixing to obtain a mixed solution B; adding sodium chloride, citric acid and the edible flavoring essence into the mixed solution B, and uniformly mixing to obtain the baby shampoo containing the marine bioactive substances. The baby shampoo containing the marine bioactive substances, disclosed by the invention, does not contain preservatives and can be used for preventing scalp and hair follicles of a baby from being damaged.
Description
Technical field
The present invention relates to shampoo, relate in particular to a kind of baby shampoo that contains marine bioactivity material and compositions, preparation method.
Background technology
At present, existing baby shampoo kind is a lot, and main adding ingredient is: surfactant, silicone oil and antiseptic.Baby's scalp has fast, the tender and lovely feature of metabolism, and shampoo as strong in frequent thigmic stimulus can cause pessimal stimulation, stop up hair follicle baby's scalp, affects the growth of hair.
Summary of the invention
Provide hereinafter about brief overview of the present invention, to the basic comprehension about some aspect of the present invention is provided.Should be appreciated that this general introduction is not about exhaustive general introduction of the present invention.It is not that intention is determined key of the present invention or pith, and nor is it intended to limit the scope of the present invention.Its object is only that the form of simplifying provides some concept, usings this as the preorder in greater detail of discussing after a while.
The object of the embodiment of the present invention is the defect for above-mentioned prior art, provides a kind of not containing antiseptic, to baby's scalp and the undamaged baby shampoo that contains marine bioactivity material of hair follicle.
Another object of the present invention is to provide a kind of preparation method of the baby shampoo that contains marine bioactivity material.
To achieve these goals, the technical scheme that the present invention takes is:
The invention provides a kind of compositions for the baby shampoo that contains marine bioactivity material, comprise the component of following weight percentage:
The present invention also provides a kind of method of using above-mentioned compositions to prepare the baby shampoo that contains marine bioactivity material, comprises the following steps:
Step S10: to the alkyl polyglucoside, cocamido propyl betaine, alcohol ether carboxylate and the stearmide ammonium salt that add proportional quantity in pure water, stir, carry out emulsifying, obtain mixed liquor A;
Step S20: marine organisms bacteria remover and Sargassum polysaccharides to adding proportional quantity in mixed liquor A, be uniformly mixed, obtain mixed liquid B;
Step S30: to the sodium chloride, citric acid and the edible essence that add proportional quantity in mixed liquid B, mix homogeneously, obtains the baby shampoo that contains marine bioactivity material.
The present invention also provides a kind of baby shampoo that contains marine bioactivity material of preparing according to above-mentioned method.
Compared with prior art, the invention has the beneficial effects as follows:
The baby shampoo that contains marine bioactivity material of the present invention, owing to containing marine organisms bacteria remover composition, therefore, after use, effectively degerming, and then there is antipruritic effect, and because each component of this baby shampoo that contains marine bioactivity material is nontoxic, non-stimulated, the free from corrosion material of skin, therefore this shampoo also has non-stimulated, the free from corrosion advantage of hair and hair, the interpolation of alternative antiseptic.The Sargassum polysaccharides containing can effectively moisten baby's scalp.
The selected surfactant of the baby shampoo that contains marine bioactivity material of the present invention is all environment-friendly type, and the novel surfactant minimum to skin irritation is without silicone oil composition, dry only smooth with back.
The preparation method of the baby shampoo that contains marine bioactivity material of the present invention, because order by merging and the mixing condition of each material are comparatively reasonable, make each component mix homogeneously of the baby shampoo that contains marine bioactivity material making by preparation method of the present invention, good stability.
The specific embodiment
For making object, technical scheme and the advantage of the embodiment of the present invention clearer, below the technical scheme in the embodiment of the present invention is clearly and completely described, obviously, described embodiment is the present invention's part embodiment, rather than whole embodiment.Element and the feature described in one embodiment of the invention can combine with element and feature shown in one or more embodiment.It should be noted that for purposes of clarity, in explanation, omitted expression and the description of unrelated to the invention, parts known to persons of ordinary skill in the art and processing.Embodiment based in the present invention, those of ordinary skills, not paying the every other embodiment obtaining under creative work prerequisite, belong to the scope of protection of the invention.
The invention provides a kind of compositions for the baby shampoo that contains marine bioactivity material, comprise the component of following weight percentage:
The baby shampoo that contains marine bioactivity material of the present invention, owing to containing marine organisms bacteria remover composition, therefore, after use, effectively degerming, and then there is antipruritic effect, and because each component of this baby shampoo that contains marine bioactivity material is nontoxic, non-stimulated, the free from corrosion material of skin, therefore this shampoo also has non-stimulated, the free from corrosion advantage of hair and hair, the interpolation of alternative antiseptic.The Sargassum polysaccharides containing can effectively moisten baby's scalp.
The selected surfactant of the baby shampoo that contains marine bioactivity material of the present invention is all environment-friendly type, and the novel surfactant minimum to skin irritation is without silicone oil composition, dry only smooth with back.
In the present embodiment, in order to obtain better antipruritic and antiseptic effect, for the compositions of the baby shampoo that contains marine bioactivity material, comprise the component of following weight percentage:
Preferred, the compositions for the baby shampoo that contains marine bioactivity material, is characterized in that, comprises the component of following weight percentage:
In the present embodiment, in order to obtain better antipruritic and anti-dandruff effect, preferred, described marine organisms bacteria remover by weight percent meter proportioning is as follows:
In the present embodiment, preferred, described edible essence can be selected edible strawberry essence, edible apple essence, edible Fructus Citri Limoniae essence etc.
In the present embodiment, in order to make the mixed effect of each component better, described hydromining pure water.
It is the cecropin described in CN101104637B that described cecropin can adopt notification number, can certainly adopt other cecropin.
The present invention also provides a kind of method of using above-mentioned compositions to prepare the baby shampoo that contains marine bioactivity material, comprises the following steps:
Step S10: to the alkyl polyglucoside, cocamido propyl betaine, alcohol ether carboxylate and the stearmide ammonium salt that add proportional quantity in pure water, stir, carry out emulsifying, obtain mixed liquor A;
Step S20: marine organisms bacteria remover and Sargassum polysaccharides to adding proportional quantity in mixed liquor A, be uniformly mixed, obtain mixed liquid B;
Step S30: to the sodium chloride, citric acid and the edible essence that add proportional quantity in mixed liquid B, mix homogeneously, obtains the baby shampoo that contains marine bioactivity material.
The preparation method of the baby shampoo that contains marine bioactivity material of the present embodiment, because order by merging and the mixing condition of each material are comparatively reasonable, make each component mix homogeneously of the baby shampoo that contains marine bioactivity material making by preparation method of the present invention, good stability.
Preferably, described marine organisms bacteria remover is prepared as follows:
Step S101: carboxymethyl chitosan and Sargassum polysaccharides to adding proportional quantity in the water of 30～35 ℃, stir and within 10～20 minutes, obtain the first mixed liquor;
Step S102: the cecropin toward adding proportional quantity in the first mixed liquor, stirs and within 3～7 minutes, obtains the second mixed liquor;
Step S103: the N-acetylmuramide lycanohydrlase toward adding proportional quantity in the second mixed liquor, stirs and within 3～7 minutes, obtains described degerming marine organisms bacteria remover.
In the present embodiment, in order to make each component obtain better mixed effect, in described step S10: the temperature of described pure water is 35-40 ℃, the time of stirring is 30-40 minute, and the speed of stirring is 80-90 rev/min.
In the present embodiment, in order to make each component obtain better mixed effect, in described step S20: the temperature of stirring is 25-35 ℃, the time of stirring is 15-20 minute, and the speed of stirring is 70-80 rev/min.In described step S30: the time of stirring is 10-15 minute, the speed of stirring is 70-80 rev/min.
In the present embodiment, in order to obtain portable shampoo, after step S30, also comprise step S40: after the baby shampoo that contains marine bioactivity material is cooling, carry out subpackage.
The present invention also provides a kind of baby shampoo that contains marine bioactivity material of preparing according to above-mentioned method.
Below by specific embodiment, the present invention is further illustrated:
Embodiment 1
The present embodiment provides a kind of baby shampoo that contains marine bioactivity material, and percent meter proportioning is as follows by weight:
The edible essence that the embodiment of the present invention is added can be selected the essence adding in shampoo in prior art or bath gel.For example can select edible strawberry essence, edible apple essence or edible Fructus Citri Limoniae essence.Edible essence in the present embodiment is edible strawberry essence.
Marine organisms bacteria remover in the present embodiment by weight percent meter proportioning is: carboxymethyl chitosan 1.5%; Sargassum polysaccharides 3.0%; Cecropin 7.0%; N-acetylmuramide lycanohydrlase 2.0%; Water 86.5%.
Marine organisms bacteria remover is prepared as follows:
Step S101: carboxymethyl chitosan and Sargassum polysaccharides to adding proportional quantity in the water of 32 ℃, stir and within 15 minutes, obtain the first mixed liquor;
Step S102: the cecropin toward adding proportional quantity in the first mixed liquor, stirs and within 6 minutes, obtains the second mixed liquor;
Step S103: the N-acetylmuramide lycanohydrlase toward adding proportional quantity in the second mixed liquor, stirs and within 5 minutes, obtains described degerming marine organisms bacteria remover.
The preparation method of the baby shampoo that contains marine bioactivity material of the present embodiment is carried out as follows:
Step S10: to the alkyl polyglucoside, cocamido propyl betaine, alcohol ether carboxylate AEC and the stearmide ammonium salt that add proportional quantity in the pure water of 35 ℃, take speed as 85 revs/min, stir 35 minutes, carry out emulsifying and obtain mixed liquor A;
Step S20: to the marine organisms bacteria remover and the Sargassum polysaccharides that add proportional quantity in mixed liquor A, at 35 ℃ of temperature, take speed as 75 revs/min, stir 15 minutes, mix homogeneously obtains mixed liquid B;
Step S30: to the sodium chloride, citrin and the edible essence that add proportional quantity in mixed liquid B, take speed as 75 revs/min, stir 15 minutes, mix homogeneously obtains the baby shampoo that contains marine bioactivity material.
Through experiment, the effectively decontamination of the baby shampoo that contains marine bioactivity material of the present embodiment, antipruritic, and after use, non-stimulated to scalp, hair is submissiveer.
Embodiment 2
The present embodiment provides a kind of baby shampoo that contains marine bioactivity material, and percent meter proportioning is as follows by weight:
Edible essence in the present embodiment is edible apple essence.
Marine organisms bacteria remover in the present embodiment by weight percent meter proportioning is: carboxymethyl chitosan 2.0%; Sargassum polysaccharides 4.0%; Cecropin 8.0%; N-acetylmuramide lycanohydrlase 3.5%; Water 82.5%.It is the cecropin described in CN101104637B that the present embodiment adopts Chinese notification number.
Marine organisms bacteria remover is prepared as follows:
Step S101: carboxymethyl chitosan and Sargassum polysaccharides to adding proportional quantity in the water of 30 ℃, stir and within 10 minutes, obtain the first mixed liquor;
Step S102: the cecropin toward adding proportional quantity in the first mixed liquor, stirs and within 7 minutes, obtains the second mixed liquor;
Step S103: the N-acetylmuramide lycanohydrlase toward adding proportional quantity in the second mixed liquor, stirs and within 3 minutes, obtains described degerming marine organisms bacteria remover.
The preparation method of the baby shampoo that contains marine bioactivity material of the present embodiment is carried out as follows:
Step S10: to the alkyl polyglucoside, cocamido propyl betaine, alcohol ether carboxylate AEC and the stearmide ammonium salt that add proportional quantity in the pure water of 40 ℃, take speed as 80 revs/min, stir 40 minutes, carry out emulsifying and obtain mixed liquor A;
Step S20: to the marine organisms bacteria remover and the Sargassum polysaccharides that add proportional quantity in mixed liquor A, at 27 ℃ of temperature, take speed as 70 revs/min, stir 14 minutes, mix homogeneously obtains mixed liquid B;
Step S30: to the sodium chloride, citrin and the edible essence that add proportional quantity in mixed liquid B, take speed as 80 revs/min, stir 13 minutes, mix homogeneously obtains the baby shampoo that contains marine bioactivity material.
Through test, the baby shampoo that contains marine bioactivity material of the present embodiment, dry only smooth with back.
Embodiment 3
The present embodiment provides a kind of baby shampoo that contains marine bioactivity material, and percent meter proportioning is as follows by weight:
Edible essence in the present embodiment is edible Fructus Citri Limoniae essence.
Marine organisms bacteria remover in the present embodiment by weight percent meter proportioning is: carboxymethyl chitosan 1.0%; Sargassum polysaccharides 2.0%; Cecropin 6.0%; N-acetylmuramide lycanohydrlase 1.5%; Water 89.5%.
Marine organisms bacteria remover is prepared as follows:
Step S101: carboxymethyl chitosan and Sargassum polysaccharides to adding proportional quantity in the water of 35 ℃, stir and within 20 minutes, obtain the first mixed liquor;
Step S102: the cecropin toward adding proportional quantity in the first mixed liquor, stirs and within 3 minutes, obtains the second mixed liquor;
Step S103: the N-acetylmuramide lycanohydrlase toward adding proportional quantity in the second mixed liquor, stirs and within 7 minutes, obtains described degerming marine organisms bacteria remover.
The preparation method of the baby shampoo that contains marine bioactivity material of the present embodiment is carried out as follows:
Step S10: to the alkyl polyglucoside, cocamido propyl betaine, alcohol ether carboxylate AEC and the stearmide ammonium salt that add proportional quantity in the pure water of 28 ℃, take speed as 90 revs/min, stir 30 minutes, carry out emulsifying and obtain mixed liquor A;
Step S20: to the marine organisms bacteria remover and the Sargassum polysaccharides that add proportional quantity in mixed liquor A, at 25 ℃ of temperature, take speed as 80 revs/min, stir 20 minutes, mix homogeneously obtains mixed liquid B;
Step S30: to the sodium chloride, citrin and the edible essence that add proportional quantity in mixed liquid B, take speed as 70 revs/min, stir 10 minutes, mix homogeneously obtains the baby shampoo that contains marine bioactivity material.
Through experiment, the effectively decontamination of the baby shampoo that contains marine bioactivity material of the present embodiment, antipruritic, and after use, non-stimulated to scalp, hair is submissiveer.
Pharmacodynamics research of the present invention:
One, from zoopery aspect checking antipruritic and antibacterial action of the present invention:
1 material
1.1 animal
Mice, regular grade, male and female half and half, body weight 18-22g, rat, male, body weight 180-220g.
1.2 medicines and reagent
Modeling reagent: depilatory cream: carrageenin: histamine phosphate; Dimethylbenzene.
Use medicine: the shampoo in the embodiment of the present invention 1
Key instrument
Electronic balance, electric-heated thermostatic water bath, sufficient sole of the foot capacity measurer
2 methods and result
2.1 itching-relieving actions:
Get 20 of mices and be divided at random two groups, 10 every group, male and female half and half, are respectively matched group, test group.24h before experiment, shaves hair to each group right back instep of Cavia porcellus, smears 1 time each 5 seconds with cotton swab.Test the same day, with coarse sandpaper, abrade right back foot and shave hair place, area 1cm
2.Smear 1 time with cotton swab part, each 5 second 1 time, at wound surface Chu Di 0.01% 0.05ml/ of histamine phosphate only after 10min, start, and after this every 3min0.02%, 0.03% ... progressive concentration is only 0.05ml/ at every turn.Until Cavia porcellus later licks the right back histamine phosphate's total amount (μ g) giving when sufficient, it is itch-threshold.Record the relatively itch-threshold of each group.Result shows: dehumidifying itching-relieving gels group itch-threshold (321 ± 350.8) μ g, and with matrix group (55 ± 47.2) μ g comparison, P < 0.01.Visible product of the present invention has the effect of pruritus due to obvious antagonism histamine phosphate.
2.2 bacteriostasis
Carry out external susceptibility minimum inhibitory concentration MIC test:
Test strain: fungus, Candida albicans, staphylococcus aureus, Escherichia coli.
Method: each test strain is made to bacteria suspension with normal saline, and to be diluted to turbidity be the above bacteria suspension of 2.0McF, use again 100 times of normal saline dilutions, 10 times of RPMIi640 culture fluid dilutions, test group (shampoo in the embodiment of the present invention 5) and matched group (health king's washing liquid) doubling dilution, in 96 well culture plates, cultivate 72-96h, slightly concussion, 490nm place carries out photoelectric colorimetry.
Table 1
2.3 conclusion
Referring to table 1, the present invention has the inhibitory action (P < 0.05 or P < 0.01) of highly significant to the guinea pig skin pruritus test due to histamine phosphate; Through external susceptibility MIC test, have a look at out: the present invention all has stronger antibacterial action to fungus, Candida albicans, staphylococcus aureus, Escherichia coli.More than test shows: the present invention has the effect of antipruritic antibacterial, the interpolation of alternative antiseptic.
The main clinical research of the present invention:
The shampoo of getting in the embodiment of the present invention 1, embodiment 2 and embodiment 3 is tested, occupation mode be every two days once, duration is 16 days, the results are shown in Table 2, the visible baby shampoo that contains marine bioactivity material of the present invention has the effect of antipruritic antibacterial, and non-stimulated, corrosion-free to scalp, after using, hair is submissive.
Table 2
In the various embodiments described above of the present invention, the sequence number of embodiment is only convenient to describe, and does not represent the quality of embodiment.Description to each embodiment all emphasizes particularly on different fields, and there is no the part of detailed description in certain embodiment, can be referring to the associated description of other embodiment.
In the embodiment such as apparatus and method of the present invention, obviously, each parts or each step reconfigure after can decomposing, combine and/or decomposing.These decomposition and/or reconfigure and should be considered as equivalents of the present invention.Simultaneously, in the above in the description of the specific embodiment of the invention, the feature of describing and/or illustrating for a kind of embodiment can be used in same or similar mode in one or more other embodiment, combined with the feature in other embodiment, or substitute the feature in other embodiment.
Should emphasize, term " comprises/comprises " existence that refers to feature, key element, step or assembly while using herein, but does not get rid of the existence of one or more further feature, key element, step or assembly or add.
Finally it should be noted that: although described above the present invention and advantage thereof in detail, be to be understood that in the situation that do not exceed the spirit and scope of the present invention that limited by appended claim and can carry out various changes, alternative and conversion.And scope of the present invention is not limited only to the specific embodiment of the described process of description, equipment, means, method and step.One of ordinary skilled in the art will readily appreciate that from disclosure of the present invention, can use carry out with the essentially identical function of corresponding embodiment described herein or obtain process, equipment, means, method or step result essentially identical with it, that existing and will be developed future according to the present invention.Therefore, appended claim is intended to comprise such process, equipment, means, method or step in their scope.
Claims (10)
1. for a compositions for the baby shampoo that contains marine bioactivity material, it is characterized in that, comprise the component of following weight percentage:
2. the compositions for the baby shampoo that contains marine bioactivity material according to claim 1, is characterized in that, comprises the component of following weight percentage:
3. the compositions for the baby shampoo that contains marine bioactivity material according to claim 1, is characterized in that, comprises the component of following weight percentage:
4. according to the compositions for the baby shampoo that contains marine bioactivity material described in claim 1-3 any one, it is characterized in that, described marine organisms bacteria remover by weight percent meter proportioning is as follows:
5. a method for the baby shampoo that the compositions preparation described in right to use requirement 1-4 any one contains marine bioactivity material, is characterized in that, comprises the following steps:
Step S10: to the alkyl polyglucoside, cocamido propyl betaine, alcohol ether carboxylate and the stearmide ammonium salt that add proportional quantity in pure water, stir, carry out emulsifying, obtain mixed liquor A;
Step S20: marine organisms bacteria remover and Sargassum polysaccharides to adding proportional quantity in mixed liquor A, be uniformly mixed, obtain mixed liquid B;
Step S30: to the sodium chloride, citric acid and the edible essence that add proportional quantity in mixed liquid B, mix homogeneously, obtains the baby shampoo that contains marine bioactivity material.
6. method according to claim 5, is characterized in that, described marine organisms bacteria remover is prepared as follows:
Step S101: carboxymethyl chitosan and Sargassum polysaccharides to adding proportional quantity in the water of 30～35 ℃, stir and within 10～20 minutes, obtain the first mixed liquor;
Step S102: the cecropin toward adding proportional quantity in the first mixed liquor, stirs and within 3～7 minutes, obtains the second mixed liquor;
Step S103: the N-acetylmuramide lycanohydrlase toward adding proportional quantity in the second mixed liquor, stirs and within 3～7 minutes, obtains described degerming marine organisms bacteria remover.
7. according to the method described in claim 5 or 6, it is characterized in that, in described step S10: the temperature of described pure water is 35-40 ℃, the time of stirring is 30-40 minute, and the speed of stirring is 80-90 rev/min.
8. according to the method described in claim 5 or 6, it is characterized in that, in described step S20: the temperature of stirring is 25-35 ℃, the time of stirring is 15-20 minute, and the speed of stirring is 70-80 rev/min; In described step S30: the time of stirring is 10-15 minute, the speed of stirring is 70-80 rev/min.
9. according to the method described in claim 5 or 6, it is characterized in that, after step S30, also comprise step S40: after the baby shampoo that contains marine bioactivity material is cooling, carry out subpackage.
10. a baby shampoo that contains marine bioactivity material of preparing according to the method described in claim 5-9 any one.
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| CN201310718513.1A CN103690392B (en) | 2013-12-23 | 2013-12-23 | Baby shampoo containing marine biomaterial and compositions, preparation method |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104586653A (en) * | 2015-02-13 | 2015-05-06 | 广东华润顺峰药业有限公司 | Hair and body wash suitable for infants and preparation method for hair and body wash |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103027857A (en) * | 2012-12-25 | 2013-04-10 | 青岛海芬海洋生物科技有限公司 | Shampoo containing marine biological degerming components and preparation method of shampoo |
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2013
- 2013-12-23 CN CN201310718513.1A patent/CN103690392B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103027857A (en) * | 2012-12-25 | 2013-04-10 | 青岛海芬海洋生物科技有限公司 | Shampoo containing marine biological degerming components and preparation method of shampoo |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104586653A (en) * | 2015-02-13 | 2015-05-06 | 广东华润顺峰药业有限公司 | Hair and body wash suitable for infants and preparation method for hair and body wash |
| CN104586653B (en) * | 2015-02-13 | 2017-09-29 | 广东华润顺峰药业有限公司 | Shampoo used also as bath lotion suitable for infant and preparation method thereof |
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