CN104688562A - HD and ZPT composite anti-dandruff liquid shampoo and preparation method thereof - Google Patents
HD and ZPT composite anti-dandruff liquid shampoo and preparation method thereof Download PDFInfo
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Abstract
The invention discloses HD and ZPT composite anti-dandruff liquid shampoo. The HD and ZPT composite anti-dandruff liquid shampoo is characterized by being prepared by mixing the following raw materials in percentage by weight: 0.3%-2.0% of a polyhydric alcohol humectant, 0.01-2.5% of sodium chloride, 10.0%-20.0% of a surfactant, 0.01%-0.5%of a cationic conditioner, 0.5%-2.6% of dimethiconol, 0.1%-0.2% of a preservative, 0.01%-0.1% of HD, 0.4%-1% of ZPT, 0.03%-0.1% of zinc chloride, 0.2%-0.6% of an essence and the balance of deionized water. The invention further discloses a preparation method of the HD and ZPT composite anti-dandruff liquid shampoo. The agency sense of water flushing of the liquid shampoo containing single ZPT is overcome; the defects of the anti-dandruff liquid shampoo containing single HD, such as high cost and the drug tolerance after long-time use are overcome; the HD and ZPT composite anti-dandruff liquid shampoo is low in cost and lasting in anti-dandruff effect; the hair is smooth and silky after the anti-dandruff liquid shampoo is used; the preparation technology is simple; the raw materials are safe and harmless; two anti-dandruff agents are reasonably combined; and the trouble of overmuch scurf is effectively solved.
Description
Technical field
The present invention relates to technical field of fine, be specifically related to compound dandruff control shampoo containing of a kind of HD and ZPT and preparation method thereof.
Background technology
The generation of the dandruff is that the horny layer face of constantly peeling off of epidermis produces, and is also metabolic result.The dandruff is many, and pore is blocked, just causes hair weak state, easy bacterial multiplication, and chafe produces head pruritus.Pathologic dandruff then refers to that scalp is because of bacteriological infection, fungal infection, or other physics, chemical injury cause scalp irritation.
Anion surfactant can remove fat secretion thing and the metabolism product at hair follicle place well, HD and ZPA has strong bactericidal action, dispels the dandruff, antipruritic completely, purification dandruff effect.Dandruff control shampoo containing is functional shampoo, is utilize some composition sterilization in product and clean, and without any dependency and side effect, can make daily shampoo life-time service.
Existing shampoo mostly is the single product of main component, and wherein, the shampoo product being main component with single ZPT, easily produces the deficiency relating to sense of bath when there is use; With the dandruff control shampoo containing that single HD is main component, then there is high cost and used of a specified duration the deficiency producing drug resistance.
Compound dandruff control shampoo containing is that common shampoo cannot be compared, and compound dandruff control shampoo containing thoroughly can effect a radical cure intractable dandruff for many years, builds healthy, value research very and inventing.But in the market, not yet occur better function, cost performance high, can the compound dandruff control shampoo containing of safe and efficient preparation.
Summary of the invention
For the above-mentioned deficiency of prior art, the object of the invention is to, the compound dandruff control shampoo containing of a kind of HD and ZPT and efficient, safe preparation method thereof are provided.What it had both overcome the bath that the shampoo containing single ZPT exists relates to sense, also overcome containing the dandruff control shampoo containing of single HD high cost and used to produce the deficiency of drug resistance of a specified duration.
The technical scheme that the present invention is adopted for achieving the above object is:
The compound dandruff control shampoo containing of a kind of HD and ZPT, is characterized in that: it is mixed with by weight percentage by following raw material components and forms:
Polyhydric alcohol wetting agent 0.3 ~ 2.0%;
Sodium chloride 0.01 ~ 2.5%;
Surfactant 10.0 ~ 20.0%;
Cation opsonizing agent 0.01 ~ 0.5%;
Dimethiconol 0.5 ~ 2.6%;
Antiseptic 0.01 ~ 0.2%;
HD 0.01～0.1%；
ZPT 0.4-1%；
Zinc chloride 0.03-0.1%;
Essence 0.2-0.6%;
Deionized water surplus.
Wherein, described polyhydric alcohol wetting agent is glycerol, propylene glycol or 1, more than one of 3 butanediols.Described sodium chloride is industrial chlorinations sodium or sea salt.Described surfactant be lauryl polyethers sodium sulfovinate, lauryl polyether thiourea acid esters ammonium, sodium lauryl sulfate, ammonium lauryl sulfate more than one.Described dimethiconol is the dimethiconol of 500,000 viscosity.Described HD is hexamidine two (hydroxyethylsulfonic acid .) salt; Described ZPT is the Zinc Pyrithione Zinc 2-pyridinethiol-1-oxide of 48% content.Described zinc chloride is analytical pure zinc chloride; Described cation opsonizing agent is C-14-S guar gum; Described antiseptic is Methylisothiazolinone.
A preparation method for the compound dandruff control shampoo containing of described HD and ZPT, is characterized in that: it comprises the steps:
1) component (preferably, before carrying out step 1), carrying out the pretreatment of equipment: after equipment and pipeline washed with de-ionized water are clean, the boric acid water soaking with 1% 30 minutes) of following mass percent is prepared:
Polyhydric alcohol wetting agent 0.3 ~ 2.0%;
Sodium chloride 0.01 ~ 2.5%;
Surfactant 10.0 ~ 20.0%;
Cation opsonizing agent 0.01 ~ 0.5%;
Dimethiconol 0.5 ~ 2.6%;
Antiseptic 0.01 ~ 0.2%;
HD 0.01～0.1%；
ZPT 0.4-1%；
Zinc chloride 0.03-0.1%;
Essence 0.2-0.6%;
Deionized water surplus;
2) being mixed with of the compound dandruff control shampoo containing of HD and ZPT:
First, by the deionized water in step 1), add in agitated kettle, start after adding cation opsonizing agent slowly to stir, start to heat after cation opsonizing agent fully disperses, temperature adds surfactant when arriving 75-78 DEG C and is stirred to surfactant and dimethiconol dissolves rear cooling completely, zinc chloride is added when 60 DEG C, then ZPT and HD is added, antiseptic, essence, polyhydric alcohol wetting agent is added when 45 DEG C, finally adjust viscosity to set point with sodium chloride, discharging after stirring, obtains the compound dandruff control shampoo containing of HD and ZPT.Wherein, the annual scope of described setting is 8000-10000mpa.s.
The invention has the advantages that: provide composite dandruff control shampoo containing of two kinds of anti-dandruff agent and preparation method thereof.Both overcome containing single ZPT that bath of shampoo relate to sense, also overcome containing the dandruff control shampoo containing of single HD high cost and used of a specified duration to produce the deficiency of drug resistance.HD and ZPT compound dandruff control shampoo containing cost is low, and anti-dandruff effect is lasting, sliding submissive with back luminescence.Its preparation technology is simple, and materials safety is harmless, reasonably two kinds of anti-dandruff agent is combined, the effectively firm worry of too much dandruff.
Detailed description of the invention
Embodiment 1
The compound dandruff control shampoo containing of a kind of HD and ZPT, it is mixed with by weight percentage by following raw material components and forms:
Polyhydric alcohol wetting agent 0.3 ~ 2.0%;
Sodium chloride 0.01 ~ 2.5%;
Surfactant 10.0 ~ 20.0%;
Cation opsonizing agent 0.01 ~ 0.5%;
Dimethiconol 0.5 ~ 2.6%;
Antiseptic 0.01 ~ 0.2%;
HD 0.01～0.1%；
ZPT 0.4-1%；
Zinc chloride 0.03-0.1%;
Essence 0.2-0.6%;
Deionized water surplus.
Wherein, described polyhydric alcohol wetting agent is glycerol, propylene glycol or 1, more than one of 3 butanediols.Described sodium chloride is industrial chlorinations sodium or sea salt.Described surfactant be lauryl polyethers sodium sulfovinate, lauryl polyether thiourea acid esters ammonium, sodium lauryl sulfate, ammonium lauryl sulfate more than one.Described dimethiconol is the dimethiconol of 500,000 viscosity.Described HD is hexamidine two (hydroxyethylsulfonic acid .) salt; Described ZPT is the Zinc Pyrithione Zinc 2-pyridinethiol-1-oxide of 48% content.Described zinc chloride is analytical pure zinc chloride; Described cation opsonizing agent is C-14-S guar gum; Described antiseptic is Methylisothiazolinone.
A preparation method for the compound dandruff control shampoo containing of described HD and ZPT, is characterized in that: it comprises the steps:
1) component (preferably, before carrying out step 1), carrying out the pretreatment of equipment: after equipment and pipeline washed with de-ionized water are clean, the boric acid water soaking with 1% 30 minutes) of following mass percent is prepared:
Polyhydric alcohol wetting agent 0.3 ~ 2.0%;
Sodium chloride 0.01 ~ 2.5%;
Surfactant 10.0 ~ 20.0%;
Cation opsonizing agent 0.01 ~ 0.5%;
Dimethiconol 0.5 ~ 2.6%;
Antiseptic 0.01 ~ 0.2%;
HD 0.01～0.1%；
ZPT 0.4-1%；
Zinc chloride 0.03-0.1%;
Essence 0.2-0.6%;
Deionized water surplus;
2) being mixed with of the compound dandruff control shampoo containing of HD and ZPT:
First, by the deionized water in step 1), add in agitated kettle, start after adding cation opsonizing agent slowly to stir, start to heat after cation opsonizing agent fully disperses, temperature adds surfactant when arriving 75-78 DEG C and is stirred to surfactant and dimethiconol dissolves rear cooling completely, zinc chloride is added when 60 DEG C, then ZPT and HD is added, antiseptic, essence, polyhydric alcohol wetting agent is added when 45 DEG C, finally adjust viscosity to set point with sodium chloride, discharging after stirring, obtains the compound dandruff control shampoo containing of HD and ZPT.Wherein, the annual scope of described setting is 8000-10000mpa.s.
Embodiment 2
The compound dandruff control shampoo containing of a kind of HD and ZPT, it is mixed with by weight percentage by following raw material components and forms:
Polyhydric alcohol wetting agent 0.3%;
Sodium chloride 0.01%;
Surfactant 10.0%;
Cation opsonizing agent 0.01%;
Dimethiconol 0.5%;
Antiseptic 0.01%;
HD 0.01%；
ZPT 0.4%；
Zinc chloride 0.03%;
Essence 0.2%;
Deionized water surplus.
Wherein, described polyhydric alcohol wetting agent is glycerol.Described sodium chloride is industrial chlorinations sodium or sea salt.Described surfactant (detergent) is lauryl polyethers sodium sulfovinate.Described dimethiconol is the dimethiconol of 500,000 viscosity.Described HD is hexamidine two (hydroxyethylsulfonic acid .) salt that BASF is produced.The Zinc Pyrithione Zinc 2-pyridinethiol-1-oxide of 48% content that described ZPT Shi Longsha company produces.Described zinc chloride is the analytical pure zinc chloride of western Gansu Province, Shantou Chemical Manufacture.Described essence CPL company produces.Described cation opsonizing agent is the sub-C-14-S guar gum in sieve ground.Described antiseptic is Methylisothiazolinone.
A preparation method for the compound dandruff control shampoo containing of described HD and ZPT, it comprises the steps:
1) component (preferably, before carrying out step 1), carrying out the pretreatment of equipment: after equipment and pipeline washed with de-ionized water are clean, the boric acid water soaking with 1% 30 minutes) of following mass percent is prepared:
Polyhydric alcohol wetting agent 0.3%;
Sodium chloride 0.01%;
Surfactant 10.0%;
Cation opsonizing agent 0.01%;
Dimethiconol 0.5%;
Antiseptic 0.01%;
HD 0.01%；
ZPT 0.4%；
Zinc chloride 0.03%;
Essence 0.2%;
Deionized water surplus;
2) being mixed with of the compound dandruff control shampoo containing of HD and ZPT:
First, by the deionized water in step 1), add in agitated kettle, start after adding cation opsonizing agent slowly to stir, start to heat after cation opsonizing agent fully disperses, temperature adds surfactant when arriving 75-78 DEG C and is stirred to surfactant and dimethiconol dissolves rear cooling completely, zinc chloride is added when 60 DEG C, then ZPT and HD is added, antiseptic, essence, polyhydric alcohol wetting agent is added when 45 DEG C, finally adjust viscosity to set point with sodium chloride, discharging after stirring, obtains the compound dandruff control shampoo containing of HD and ZPT.Wherein, the annual scope of described setting is 8000-10000mpa.s.
Embodiment 3
The compound dandruff control shampoo containing of a kind of HD and ZPT, it is mixed with by weight percentage by following raw material components and forms:
Polyhydric alcohol wetting agent 2.0%;
Sodium chloride 2.5%;
Surfactant 20.0%;
Cation opsonizing agent 0.5%;
Dimethiconol 2.6%;
Antiseptic 0.2%;
HD 0.1%；
ZPT 1%；
Zinc chloride 0.1%;
Essence 0.6%;
Deionized water surplus.
Wherein, described polyhydric alcohol wetting agent is propylene glycol.Described sodium chloride is industrial chlorinations sodium or sea salt.Described surfactant (detergent) is ammonium lauryl sulfate.Described dimethiconol is the dimethiconol of 500,000 viscosity.Described HD is hexamidine two (hydroxyethylsulfonic acid .) salt that BASF is produced.The Zinc Pyrithione Zinc 2-pyridinethiol-1-oxide of 48% content that described ZPT Shi Longsha company produces.Described zinc chloride is the analytical pure zinc chloride of western Gansu Province, Shantou Chemical Manufacture.Described essence CPL company produces.Described cation opsonizing agent is the sub-C-14-S guar gum in sieve ground.Described antiseptic is Methylisothiazolinone.
A preparation method for the compound dandruff control shampoo containing of described HD and ZPT, is characterized in that: it comprises the steps:
1) component (preferably, before carrying out step 1), carrying out the pretreatment of equipment: after equipment and pipeline washed with de-ionized water are clean, the boric acid water soaking with 1% 30 minutes) of following mass percent is prepared:
Polyhydric alcohol wetting agent 2.0%;
Sodium chloride 2.5%;
Surfactant 0.0%;
Cation opsonizing agent 0.5%;
Dimethiconol 2.6%;
Antiseptic 0.2%;
HD 0.1%；
ZPT 1%；
Zinc chloride 0.1%;
Essence 0.6%;
Deionized water surplus;
2) being mixed with of the compound dandruff control shampoo containing of HD and ZPT:
First, by the deionized water in step 1), add in agitated kettle, start after adding cation opsonizing agent slowly to stir, start to heat after cation opsonizing agent fully disperses, temperature adds surfactant when arriving 75-78 DEG C and is stirred to surfactant and dimethiconol dissolves rear cooling completely, zinc chloride is added when 60 DEG C, then ZPT and HD is added, antiseptic, essence, polyhydric alcohol wetting agent is added when 45 DEG C, finally adjust viscosity to set point with sodium chloride, discharging after stirring, obtains the compound dandruff control shampoo containing of HD and ZPT.Wherein, the annual scope of described setting is 8000-10000mpa.s.
Embodiment 4
The compound dandruff control shampoo containing of a kind of HD and ZPT, it is mixed with by weight percentage by following raw material components and forms:
Polyhydric alcohol wetting agent 1%;
Sodium chloride 1%;
Surfactant 15%;
Cation opsonizing agent 0.1%;
Dimethiconol 2%;
Antiseptic 0.1%;
HD 0.08%；
ZPT 0.5%；
Zinc chloride 0.05%;
Essence 0.4%;
Deionized water surplus.
Wherein, described polyhydric alcohol wetting agent is 1,3 butanediols.Described sodium chloride is industrial chlorinations sodium.Described surfactant is lauryl polyether thiourea acid esters ammonium, sodium lauryl sulfate mixture.Described dimethiconol is the dimethiconol of 500,000 viscosity.Described HD is hexamidine two (hydroxyethylsulfonic acid .) salt; Described ZPT is the Zinc Pyrithione Zinc 2-pyridinethiol-1-oxide of 48% content.Described zinc chloride is analytical pure zinc chloride; Described cation opsonizing agent is C-14-S guar gum; Described antiseptic is Methylisothiazolinone.
A preparation method for the compound dandruff control shampoo containing of described HD and ZPT, is characterized in that: it comprises the steps:
1) component (preferably, before carrying out step 1), carrying out the pretreatment of equipment: after equipment and pipeline washed with de-ionized water are clean, the boric acid water soaking with 1% 30 minutes) of following mass percent is prepared:
Polyhydric alcohol wetting agent 1%;
Sodium chloride 1%;
Surfactant 15%;
Cation opsonizing agent 0.1%;
Dimethiconol 2%;
Antiseptic 0.1%;
HD 0.08%；
ZPT 0.5%；
Zinc chloride 0.05%;
Essence 0.4%;
Deionized water surplus;
2) being mixed with of the compound dandruff control shampoo containing of HD and ZPT:
First, by the deionized water in step 1), add in agitated kettle, start after adding cation opsonizing agent slowly to stir, start to heat after cation opsonizing agent fully disperses, temperature adds surfactant when arriving 75-78 DEG C and is stirred to surfactant and dimethiconol dissolves rear cooling completely, zinc chloride is added when 60 DEG C, then ZPT and HD is added, antiseptic, essence, polyhydric alcohol wetting agent is added when 45 DEG C, finally adjust viscosity to set point with sodium chloride, discharging after stirring, obtains the compound dandruff control shampoo containing of HD and ZPT.Wherein, the annual scope of described setting is 8000-10000mpa.s.
Hair caring room test experiments:
Hair caring test utilizes China product H on the market to contrast for the M in reference product and embodiment.Experimenter is provided 0-10 by double blinding two products on probation to indices and divides, and 10 points represent that oneself is the most satisfied to this performance, and 0 point of representative is dissatisfied.Experimenter is the women of routine use hair care product.Specialty teacher adopt identical program very the time use H product on experimenter's half hair, second half hair used M product, then by identical amount and enough water rinse out.Application form, hair dryness finalization, is issued 18 professional teachers and 18 experimenters fill in corresponding project respectively by experimenter oneself.The experimenter participating in anti-dandruff effect assessment will fix half a head and use H sample, and another side uses M product, uses 14 days continuously.Every day carries out tracking evaluation marking by the dandruff situation of 18 professional teachers to every experimenter before using, and average is as the dandruff score value on the same day.Result gathers as follows:
| M | H | Difference | |
| Totally like degree | 7.05 | 6.50 | +0.55 |
| Top application type | 7.20 | 6.00 | +0.60 |
| Cardability (anti-entanglement) after dispersion | 8.0 | 6.45 | +1.55 |
| Slipping after top | 7.31 | 6.54 | +0.77 |
| The bath initial stage is smoothness | 7.20 | 6.67 | +0.53 |
| Bath is smoothness for mid-term | 7.22 | 6.50 | +0.72 |
| The bath later stage is smoothness | 7.00 | 6.45 | +0.55 |
| Bath later stage cardability (anti-entanglement) | 7.21 | 6.71 | +0.50 |
| A wet feel | 7.30 | 7.00 | +0.31 |
| Wet Comb rationality (anti-entanglement) | 6.95 | 6.6 | +0.35 |
| Antistatic | 6.23 | 6.18 | +0.05 |
| A dry feel | 7.58 | 7.03 | +0.5 |
| A dry elasticity | 6.11 | 6.25 | -0.14 |
The appreciable enhancing of positive difference representative energy, on antistatic property, difference is not obvious, and dry sending out in elasticity two performances is slightly worse than reference product H.
The experimenter participating in anti-dandruff effect assessment will fix half a head and use H sample, another side uses M product, continuous use 14 days, (10 are divided into dandruff little to carry out tracking evaluation marking by the dandruff situation of 18 professional teachers to every experimenter before using every day, 0 point of potential head bits especially severe), its average is as the dandruff score value on the same day.
| 1 day | 2 days | 3 days | 4 days | 5 days | 6 days | 7 days | 8 days | 9 days | 10 days | 11 days | 12 days | 13 days | 14 days | |
| M | 5 | 5.3 | 5.7 | 6.2 | 6.7 | 7.2 | 7.6 | 7.7 | 8.0 | 8.0 | 8.2 | 8.2 | 8.2 | 8.2 |
| H | 5 | 5.1 | 5.2 | 5.6 | 5.0 | 6.4 | 6.7 | 6.9 | 7.1 | 7.1 | 7.2 | 7.2 | 7.1 | 7.1 |
| Difference | 0.0 | 0.2 | 0.5 | 0.6 | 0.7 | 0.8 | 0.9 | 0.9 | 0.9 | 0.9 | 1.0 | 1.0 | 1.1 | 1.1 |
Embodiment M can be found in anti-dandruff to have clear superiority compared with market situation of selling well hit product H from above data.
The present invention is not limited to above-mentioned embodiment, the technical characteristic that all employings are identical or approximate with the above embodiment of the present invention, and compound dandruff control shampoo containing of other HD and ZPT obtained and preparation method thereof, all within protection scope of the present invention.
Claims (9)
1. the compound dandruff control shampoo containing of HD and ZPT, is characterized in that: it is mixed with by weight percentage by following raw material components and forms:
2. the compound dandruff control shampoo containing of HD and ZPT according to claim 1, is characterized in that: described polyhydric alcohol wetting agent is glycerol, propylene glycol or 1, more than one of 3 butanediols.
3. the compound dandruff control shampoo containing of HD and ZPT according to claim 1, is characterized in that: described sodium chloride is industrial chlorinations sodium or sea salt.
4. the compound dandruff control shampoo containing of HD and ZPT according to claim 1, is characterized in that: described surfactant be lauryl polyethers sodium sulfovinate, lauryl polyether thiourea acid esters ammonium, sodium lauryl sulfate, ammonium lauryl sulfate more than one.
5. the compound dandruff control shampoo containing of HD and ZPT according to claim 1, is characterized in that: described dimethiconol is the dimethiconol of 500,000 viscosity.
6. the compound dandruff control shampoo containing of HD and ZPT according to claim 1, is characterized in that: described HD is hexamidine two (hydroxyethylsulfonic acid .) salt; Described ZPT is the Zinc Pyrithione Zinc 2-pyridinethiol-1-oxide of 48% content.
7. the compound dandruff control shampoo containing of HD and ZPT according to claim 1, is characterized in that: described zinc chloride is analytical pure zinc chloride; Described cation opsonizing agent is C-14-S guar gum; Described antiseptic is Methylisothiazolinone.
8. a preparation method for the compound dandruff control shampoo containing of described HD and ZPT of one of claim 1-7, is characterized in that: it comprises the steps:
1) component of following mass percent is prepared:
2) being mixed with of the compound dandruff control shampoo containing of HD and ZPT:
First, by step 1) in deionized water, add in agitated kettle, start after adding cation opsonizing agent slowly to stir, start to heat after cation opsonizing agent fully disperses, temperature adds surfactant when arriving 75-78 DEG C and is stirred to surfactant and dimethiconol dissolves rear cooling completely, zinc chloride is added when 60 DEG C, then ZPT and HD is added, antiseptic, essence, polyhydric alcohol wetting agent is added when 45 DEG C, finally adjust viscosity to set point with sodium chloride, discharging after stirring, obtains the compound dandruff control shampoo containing of HD and ZPT.
9. the preparation method of the compound dandruff control shampoo containing of HD and ZPT according to claim 8, it is characterized in that, the annual scope of described setting is 8000-10000mpa.s.
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| CN107349123A (en) * | 2017-07-05 | 2017-11-17 | 广州臻颜化妆品有限公司 | A kind of desquamation compositions and dandruff control shampoo containing |
| CN107582447A (en) * | 2017-08-30 | 2018-01-16 | 曾万祥 | A kind of anti-dandruff ginger shampoo |
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| US20100189669A1 (en) * | 2009-01-29 | 2010-07-29 | Tomohiro Hakozaki | Regulation of Mammalian Keratinous Tissue Using Skin and/or Hair Care Actives |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107349123A (en) * | 2017-07-05 | 2017-11-17 | 广州臻颜化妆品有限公司 | A kind of desquamation compositions and dandruff control shampoo containing |
| CN107582447A (en) * | 2017-08-30 | 2018-01-16 | 曾万祥 | A kind of anti-dandruff ginger shampoo |
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Address after: Chenghai District 515800 of Guangdong Province under Shantou lotus Qianxi Industrial Zone Applicant after: Jin Qi baby life Polytron Technologies Inc Address before: Chenghai District 515800 of Guangdong Province under Shantou lotus Qianxi Industrial Zone Applicant before: Guangdong gold is very refined limited company |
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