CN105982833B - Strong moisturizing gel film-forming composition and preparation method thereof - Google Patents
Strong moisturizing gel film-forming composition and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a strong moisturizing gel film-forming composition and a preparation method thereof, and discloses a composition containing essence containing various moisturizing components and a solid mixture containing alginate and calcium salt. This combination has the following advantages: strong moisturizing effect, mildness, no stimulation and suitability for various types of skin; the non-woven fabric is not used, so that skin irritation caused by the non-woven fabric is avoided, and the most challenge of the existing non-woven fabric mask is achieved; other functional components can be added into the essence to achieve various effects; the product forms a gel-like film on the skin during use and can be peeled off from the skin, thereby providing excellent use experience for consumers. This combination can be used for applications including skin care, cosmetic, and skin repair, treatment, etc.
Description
Technical Field
The invention relates to the related technology of skin care, beauty, skin repair and treatment products.
Background
The inventor is dedicated to developing safe, mild and natural cosmetic formulas for many years, and provides a safe and high-quality product for wide consumers. The moisturizing effect is the most basic effect requirement of all skin care products, the long-acting and strong moisturizing effects are one of the characteristics of high-quality skin care products, other skin care and beautifying effects can be exerted to the maximum, and the facial mask products which are mild, have no irritation and have the strong moisturizing effect are one of the main research directions of people.
The facial mask is a skin care single product which is sold in the largest quantity so far, and the two most common facial mask forms are a blending and smearing type facial mask and a non-woven facial mask. The blending and smearing type facial mask is a mud cream and a tearing type facial mask which are prepared by using mud powder, the mud powder and the like are generally used as raw materials, the raw materials are blended by water before use and are applied to the skin, the skin care effects of moisturizing and the like are basically not generated, the skin surface cleaning effect is mainly achieved, the skin cleaning effect is generally strong in alkalinity, and the skin can be dry after use. The non-woven fabric mask is prepared by soaking non-woven fabric with essence, is the most popular mask product with the largest using amount at present, but as is known, the pricking feeling, burning feeling and the like of the skin are common consumer complaints which are brought by non-woven fabric materials, and although the irritation feeling can be properly alleviated by adding a proper amount of anti-irritation components, the non-woven fabric mask is still a big defect of the products.
Disclosure of Invention
In order to overcome the defects of the prior art, the inventor finds that a composition containing a mixture of alginate and calcium salt and essence containing a plurality of moisturizing ingredients can form a gel membrane-shaped substance which has a strong moisturizing function and can be peeled from the skin when the two compositions are combined according to a specific ratio, and the combination can be used for facial mask products and has the following advantages compared with the two facial mask products: 1. strong moisturizing effect, mildness, no stimulation and suitability for various types of skin; 2. non-woven fabrics are not used, and the non-woven fabrics are one of the important reasons of the irritation of the mask product, so that the skin irritation caused by the non-woven fabrics is avoided; 3. other functional components can be added into the essence to achieve various effects; 4. the product forms a gel-like film on the skin during use and can be peeled off from the skin, thereby providing excellent use experience for consumers.
Besides the facial mask products, the combination can also be used for the purposes of skin care, beauty, skin repair, treatment and the like.
The invention provides a strong moisturizing gel film-forming composition which comprises a liquid mixture A and a solid mixture B, wherein the mixture A and the mixture B are mixed according to the weight ratio of A: B being 1: 4-1: 4.5, and a gel film which can be strongly moisturized and peeled from skin is formed, wherein: the mixture A consists of a moisturizing component, an antiseptic component, an efficacy component and water, wherein the moisturizing component is as follows: 0.01-5.0 parts of fructose, 0.01-5.0 parts of trehalose, 0.01-1.0 part of sodium pyrrolidone carboxylate, 0.01-1.0 part of sodium lactate, 0.04-0.2 part of sodium alginate, 0.01-1.0 part of urea, 1.0-10.0 parts of butanediol and 1.40-10.0 parts of glycerol, wherein the preservative comprises the following components in parts by weight: 1.24-5.4 parts of pentanediol, 0.36-0.48 part of hexanediol and 0.24-0.32 part of caprylyl glycol, wherein the functional components are as follows: 0.1-5.0 parts by weight of geranium extract or water-soluble neroli extract or aloe extract, and 81.2-93.2 parts by weight of water; the mixture B is composed of alginate, calcium carbonate, calcium sulfate, sodium citrate and sugar, wherein the alginate is as follows: 2-5.1 parts of sodium alginate or 2-5.1 parts of potassium alginate, 1.2-3.9 parts of calcium carbonate, 0.8-4.0 parts of dihydrate and calcium sulfate, 0.2-0.6 part of sodium citrate and 89.2-92.2 parts of sugar.
Preferably, the sugar in the mixture B is one or a mixture of two or more of glucose, fructose, sucrose, lactose and maltose.
The invention provides a powerful moisturizing gel film-forming composition, which consists of a liquid mixture A and a solid mixture B, wherein the mixture A and the mixture B are mixed according to the weight ratio of A: B to 1:4, wherein: the mixture A comprises 3.48 parts by weight of pentanediol, 0.48 part by weight of hexanediol, 0.32 part by weight of caprylyl glycol, 1.00 part by weight of 1, 3-butanediol, 1.98 parts by weight of glycerol, 0.04 part by weight of sodium alginate, 0.02 part by weight of sodium chloride, 0.24 part by weight of fructose, 0.10 part by weight of citric acid, 0.07 part by weight of sodium pyrrolidone carboxylate, 0.02 part by weight of trehalose, 0.05 part by weight of maltose, 0.05 part by weight of sodium hydroxide, 0.05 part by weight of sodium lactate, 0.12 part by weight of urea, 0.01 part by weight of allantoin, 0.25 part by weight of geranium extract and 91.72 parts by weight of water; the mixture B comprises 5.0 parts by weight of sodium alginate, 2.5 parts by weight of calcium carbonate, 0.8 part by weight of calcium sulfate dihydrate, 0.3 part by weight of trisodium citrate dihydrate and 91.4 parts by weight of glucose.
The invention provides a powerful moisturizing gel film-forming composition, which consists of a liquid mixture A and a solid mixture B, wherein the mixture A and the mixture B are mixed according to the weight ratio of A: B to 1:4.2, wherein: the mixture A comprises 5.40 parts by weight of pentanediol, 0.36 part by weight of hexanediol, 0.24 part by weight of caprylyl glycol, 1.00 part by weight of 1, 3-butanediol, 1.40 parts by weight of glycerol, 0.10 part by weight of sodium alginate, 0.02 part by weight of sodium chloride, 0.20 part by weight of fructose, 0.08 part by weight of citric acid, 0.06 part by weight of sodium pyrrolidone carboxylate, 0.02 part by weight of trehalose, 0.04 part by weight of maltose, 0.04 part by weight of sodium hydroxide, 0.04 part by weight of sodium lactate, 0.10 part by weight of urea, 0.01 part by weight of allantoin, 0.50 part by weight of aloe extract and 90.39 parts by weight of water; the composition of the mixture B is 5.1 parts by weight of sodium alginate, 3.9 parts by weight of calcium carbonate, 1.2 parts by weight of calcium sulfate dihydrate, 0.2 parts by weight of trisodium citrate dihydrate and 89.6 parts by weight of glucose.
The invention also provides a preparation method of the strong moisturizing gel film-forming composition, which comprises the following steps: mixing the liquid mixture A and the solid mixture B according to the weight ratio of A to B being 1: 4-1: 4.5, stirring the mixture into viscous liquid, coating the viscous liquid on the surface of skin, and standing the viscous liquid for 10-20 minutes to react to form a gel film-shaped substance which has strong moisturizing property and can be peeled off from the skin, wherein: the mixture A consists of a moisturizing component, an antiseptic component, an efficacy component and water, wherein the moisturizing component is as follows: 0.01-5.0 parts of fructose, 0.01-5.0 parts of trehalose, 0.01-1.0 part of sodium pyrrolidone carboxylate, 0.01-1.0 part of sodium lactate, 0.04-0.2 part of sodium alginate, 0.01-1.0 part of urea, 1.0-10.0 parts of butanediol and 1.40-10.0 parts of glycerol, wherein the preservative comprises the following components in parts by weight: 1.24-5.4 parts of pentanediol, 0.36-0.48 part of hexanediol and 0.24-0.32 part of caprylyl glycol, wherein the functional components are as follows: 0.1-5.0 parts by weight of geranium extract or water-soluble neroli extract or aloe extract, and 81.2-93.2 parts by weight of water; the mixture B is composed of alginate, calcium carbonate, calcium sulfate, sodium citrate and sugar, wherein the alginate is as follows: 2-5.1 parts of sodium alginate or 2-5.1 parts of potassium alginate, 1.2-3.9 parts of calcium carbonate, 0.8-4.0 parts of dihydrate and calcium sulfate, 0.2-0.6 part of sodium citrate and 89.2-92.2 parts of sugar.
The action principle is as follows: when the mixture B containing alginate and calcium salt is mixed with the mixture A, the calcium salt in the mixture B releases calcium ions, and the released calcium ions react with the alginate to generate calcium alginate, a gel-like substance, thereby forming a film. In order to moderate the speed of the film forming reaction, so that the film forming reaction can be applied to skin care, beauty treatment, skin repair and the like, sodium citrate is added to adjust the reaction speed, the saccharide in the solid mixture B is used as a dispersing agent to avoid agglomeration in the reaction, and the saccharide is an excellent humectant. The mixture A is added with moisturizing components to achieve the effect of strong moisturizing, and different active components can be added according to the effect requirement.
Drawings
FIG. 1 is a comparison graph of moisture measurements of dry skin before and after application to 51 year old female;
FIG. 2 is a comparison graph of moisture measurements of dry skin before and after application to a 26 year old female;
FIG. 3 is a comparison graph of moisture measurements of dry skin before and after application to a 26 year old female;
FIG. 4 is a comparison graph of moisture measurements taken on the skin before and after application to neutral skin of a 35 year old female;
FIG. 5 is a comparison graph of moisture measurements of dry skin before and after use in a 35 year old female;
FIG. 6 is a view of the membrane on the skin;
fig. 7 is a view showing a state where the membrane is peeled off the skin.
The specific implementation mode is as follows:
the present invention will be further described with reference to specific embodiments in order to make the original features, technical means and objectives of the invention easier to understand.
Preparation method of mixture A: the raw materials were mixed to make a liquid mixture a according to the formulation in table 1 below.
Preparation method of mixture B:
5.1 parts by weight of sodium alginate, 3.9 parts by weight of calcium carbonate, 1.2 parts by weight of calcium sulfate dihydrate, 0.2 parts by weight of trisodium citrate dihydrate and 89.6 parts by weight of glucose are uniformly mixed according to the weight ratio to prepare a solid mixture B1. Or
5.0 parts by weight of potassium alginate, 1.2 parts by weight of calcium carbonate, 4.0 parts by weight of calcium sulfate dihydrate, 0.6 parts by weight of trisodium citrate dihydrate and 89.2 parts by weight of glucose are uniformly mixed according to the weight ratio to prepare a solid mixture B2. Or
5.0 parts by weight of sodium alginate, 2.5 parts by weight of calcium carbonate, 0.8 part by weight of calcium sulfate dihydrate, 0.3 part by weight of trisodium citrate dihydrate and 91.4 parts by weight of glucose are uniformly mixed according to the weight ratio to prepare a solid mixture B3. Or
5.0 parts by weight of potassium alginate, 1.2 parts by weight of calcium carbonate, 4.0 parts by weight of calcium sulfate dihydrate, 0.6 parts by weight of trisodium citrate dihydrate and 89.2 parts by weight of sucrose are uniformly mixed according to the weight ratio to prepare a solid mixture B4. Or
5.1 parts by weight of sodium alginate, 3.9 parts by weight of calcium carbonate, 1.2 parts by weight of calcium sulfate dihydrate, 0.2 parts by weight of trisodium citrate dihydrate and 89.6 parts by weight of lactose are uniformly mixed according to the weight ratio to prepare a solid mixture B5. Or
5.0 parts by weight of sodium alginate, 2.5 parts by weight of calcium carbonate, 0.8 part by weight of calcium sulfate dihydrate, 0.4 part by weight of trisodium citrate dihydrate and 91.3 parts by weight of maltose are uniformly mixed according to the weight ratio to prepare a solid mixture B6. Or
5.1 parts by weight of sodium alginate, 3.9 parts by weight of calcium carbonate, 1.2 parts by weight of calcium sulfate dihydrate, 0.2 parts by weight of trisodium citrate dihydrate and 89.6 parts by weight of fructose are uniformly mixed according to the weight ratio to prepare a solid mixture B7. Or
2.0 parts by weight of sodium alginate, 3.9 parts by weight of calcium carbonate, 1.2 parts by weight of calcium sulfate dihydrate, 0.2 parts by weight of trisodium citrate dihydrate and 92.7 parts by weight of fructose are uniformly mixed according to the weight ratio to prepare a solid mixture B8. Or
2.0 parts by weight of potassium alginate, 1.2 parts by weight of calcium carbonate, 4.0 parts by weight of calcium sulfate dihydrate, 0.6 parts by weight of trisodium citrate dihydrate and 92.2 parts by weight of sucrose are uniformly mixed according to the weight ratio to prepare a solid mixture B9.
The preparation method of the gel membrane comprises the following steps: mixing the mixture A and the mixture B according to the weight ratio in the table, stirring into viscous liquid, coating the viscous substance on the skin surface, standing for 10-20 minutes after coating to form a gel-like film, and peeling off the film from the skin.
Moisture retention effect measurement of gel film:
measurement site: medial skin near the anterior half of the hand; first, the moisture value at the selected site was measured and measured as a value before use, and mixture A and mixture B were mixed to prepare a viscous mixture according to the preparation method of the film of example 11, the viscous mixture was applied to the selected site, the film was peeled off after 20 minutes, air-dried for 5 minutes, and the moisture value of the skin was measured after use and at different times after use. Fig. 1-5 show experimental results, where the data for the group near the front of the eye are control experimental data for the unused area, the data for the following group are experimental data using gel film, and the data after use are percentage increase of moisture value.
The tested person: women aged 26, 35, and 51 years old, and the skin is neutral and dry. The experimental results are as follows: after application of the film, the moisture value of the skin was greatly increased after application for all ages and skin types, and remained at a certain level for 3 hours, which is much higher than that of the control unused product. The gel film has long-acting and strong moisturizing effect.
The film can be completely peeled from the skin after use without leaving any residue, and fig. 6 to 7 show the form of the film during the coating process and the form when peeled.
Table 1:
the foregoing shows and describes the general principles, essential features, and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are given by way of illustration of the principles of the present invention, and that various changes and modifications may be made without departing from the spirit and scope of the invention as defined by the appended claims. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (4)
1. A strong moisturizing gel film-forming composition is composed of a liquid mixture A and a solid mixture B, wherein the mixture A and the mixture B are mixed according to the weight ratio of A to B being 1: 4-1: 4.5, and a gel film which is strong in moisturizing and can be peeled from skin is formed, wherein:
the mixture A consists of a moisturizing component, an antiseptic component, an effective component and water;
the moisture-keeping components are as follows: 0.01-5.0 parts by weight of fructose, 0.01-5.0 parts by weight of trehalose, 0.01-1.0 parts by weight of sodium pyrrolidone carboxylate, 0.01-1.0 parts by weight of sodium lactate, 0.04-0.2 parts by weight of sodium alginate, 0.01-1.0 parts by weight of urea, 1.0-10.0 parts by weight of butanediol and 1.40-10.0 parts by weight of glycerol;
the anticorrosive components are as follows: 1.24-5.4 parts by weight of pentanediol, 0.36-0.48 part by weight of hexanediol and 0.24-0.32 part by weight of octaethylene glycol;
the functional components are as follows: 0.1 to 5.0 parts by weight of a geranium extract or a water-soluble neroli extract or an aloe extract, and 81.2 to 93.2 parts by weight of water;
the mixture B consists of alginate, calcium carbonate, calcium sulfate, sodium citrate and sugar;
the alginate is as follows: 2-5.1 parts of sodium alginate or 2-5.1 parts of potassium alginate, 1.2-3.9 parts of calcium carbonate, 0.8-4.0 parts of calcium sulfate dihydrate, 0.2-0.6 parts of trisodium citrate dihydrate and 89.2-92.2 parts of sugar.
2. The film-forming composition according to claim 1, wherein the sugar in mixture B is selected from one or a mixture of two or more of glucose, fructose, sucrose, lactose and maltose.
3. A strong moisturizing gel-forming composition consisting of a mixture a and a mixture B, wherein the mixture a and the mixture B are mixed in a weight ratio a: B of 1:4, wherein: the composition of the mixture A is as follows: 3.48 parts by weight of pentanediol, 0.48 part by weight of hexanediol, 0.32 part by weight of caprylyl glycol, 1.00 part by weight of 1, 3-butanediol, 1.98 parts by weight of glycerol, 0.04 part by weight of sodium alginate, 0.02 part by weight of sodium chloride, 0.24 part by weight of fructose, 0.10 part by weight of citric acid, 0.07 part by weight of sodium pyrrolidone carboxylate, 0.02 part by weight of trehalose, 0.05 part by weight of maltose, 0.05 part by weight of sodium hydroxide, 0.05 part by weight of sodium lactate, 0.12 part by weight of urea, 0.01 part by weight of allantoin, 0.25 part by weight of geranium extract, and 91.72 parts by weight of water;
the composition of the mixture B is as follows: 5.0 parts by weight of sodium alginate, 2.5 parts by weight of calcium carbonate, 0.8 parts by weight of dihydrate and calcium sulfate, 0.3 parts by weight of trisodium citrate dihydrate and 91.4 parts by weight of glucose.
4. A strong moisturizing gel-forming composition consisting of a mixture a and a mixture B, wherein the mixture a and the mixture B are mixed in a weight ratio a: B of 1:4.2, wherein:
the composition of the mixture A is as follows: 5.40 parts by weight of pentanediol, 0.36 part by weight of hexanediol, 0.24 part by weight of caprylyl glycol, 1.00 part by weight of 1, 3-butanediol, 1.40 parts by weight of glycerol, 0.10 part by weight of sodium alginate, 0.02 part by weight of sodium chloride, 0.20 part by weight of fructose, 0.08 part by weight of citric acid, 0.06 part by weight of sodium pyrrolidone carboxylate, 0.02 part by weight of trehalose, 0.04 part by weight of maltose, 0.04 part by weight of sodium hydroxide, 0.04 part by weight of sodium lactate, 0.10 part by weight of urea, 0.01 part by weight of allantoin, 0.50 part by weight of aloe extract, 90.39 parts by weight of water;
the composition of the mixture B is as follows: 5.1 parts by weight of sodium alginate, 3.9 parts by weight of calcium carbonate, 1.2 parts by weight of calcium sulfate dihydrate, 0.2 parts by weight of trisodium citrate dihydrate and 89.6 parts by weight of glucose.
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| CN106377436A (en) * | 2016-10-26 | 2017-02-08 | 德之馨（上海）有限公司 | Water-soluble whitening formula based on 4-(1-phenethyl)-1,3-hydroquinone |
| CN108464952A (en) * | 2018-04-27 | 2018-08-31 | 花安堂生物科技集团有限公司 | A kind of film-forming composition and its cosmetics of application and its composition |
| CN108926493A (en) * | 2018-08-24 | 2018-12-04 | 广东丸美生物技术股份有限公司 | A kind of skin care mantle compound powder and the preparation method and application thereof |
| CN111297738B (en) * | 2020-04-24 | 2021-09-28 | 山东大学 | Seaweed mask and preparation method and application thereof |
| CN111467562B (en) * | 2020-05-25 | 2021-02-26 | 绽妍生物科技有限公司 | Liquid wound dressing for rapidly repairing skin superficial injury and preparation method thereof |
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| JPS53149183A (en) * | 1977-06-01 | 1978-12-26 | Takaragen Kk | Gel base material for fragrant deodorizing agent |
| CN102783589A (en) * | 2012-08-28 | 2012-11-21 | 青岛海之林生物科技开发有限公司 | Formulated gelatinizing powder and application thereof |
| CN104352356A (en) * | 2014-11-12 | 2015-02-18 | 深圳市永济泰科技有限公司 | Humectant as well as preparation method and application thereof |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS53149183A (en) * | 1977-06-01 | 1978-12-26 | Takaragen Kk | Gel base material for fragrant deodorizing agent |
| CN102783589A (en) * | 2012-08-28 | 2012-11-21 | 青岛海之林生物科技开发有限公司 | Formulated gelatinizing powder and application thereof |
| CN104352356A (en) * | 2014-11-12 | 2015-02-18 | 深圳市永济泰科技有限公司 | Humectant as well as preparation method and application thereof |
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