CN110101602B - Cyperus esculentus shampoo added with cyperus esculentus root oil - Google Patents
Cyperus esculentus shampoo added with cyperus esculentus root oil Download PDFInfo
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- CN110101602B CN110101602B CN201910260079.4A CN201910260079A CN110101602B CN 110101602 B CN110101602 B CN 110101602B CN 201910260079 A CN201910260079 A CN 201910260079A CN 110101602 B CN110101602 B CN 110101602B
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- cyperus esculentus
- cyperus
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/06—Production of fats or fatty oils from raw materials by pressing
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- Life Sciences & Earth Sciences (AREA)
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- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
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- Cosmetics (AREA)
Abstract
The cyperus esculentus root oil added shampoo provided by the invention is characterized in that cyperus esculentus root oil is added in the shampoo, and has the functions of cleaning, moistening, resisting bacteria and diminishing inflammation, so that the hair can be deeply cleaned, hair silks can be moistened, the hair is elastic, the bifurcation is effectively inhibited, the hair quality is improved, the cyperus esculentus root oil is a pure plant extract, the character is mild, no damage is caused to a human body after long-term use, the hair quality is gradually improved, and the hair is enabled to recover the soft and bright elastic state.
Description
Technical Field
The invention relates to the field of daily chemical articles, in particular to cyperus esculentus shampoo added with cyperus esculentus root oil.
Background
With the acceleration of life rhythm and the increase of working pressure, more and more people are puzzled by the problem of hair quality, and the hair is often radiated by electronic products, so that the hair quality is deteriorated, the problems of much oil, dry and split hair and the like occur, and the personal image is influenced.
Although some shampoo and hair care products on the market have the effects of inhibiting oil from flowing out of scalp and improving dry hair and split ends of hair, the shampoo and hair care products are essentially added with moistening agents, the moistening agents can wrap the hair to form a film, the hair looks more smooth, the problem of poor hair quality cannot be fundamentally solved, and certain damage can be caused to the hair after the moistening agents are used for a long time.
The cyperus esculentus is a plant originally produced in Mediterranean areas, introduced to China from the Soviet Union in the last century and planted, the cyperus esculentus mainly harvests tuberous roots which are longer than underground, and the cyperus esculentus roots are rich in oil, so that the cyperus esculentus is commonly used for squeezing oil.
Therefore, a need exists for a cyperus esculentus shampoo containing cyperus esculentus root oil, which can deeply clean hair, moisten hair, make hair elastic, effectively inhibit hair split, and improve hair quality, and is added by pure plants without damaging hair.
Disclosure of Invention
The invention aims to provide cyperus esculentus shampoo added with cyperus esculentus root oil, which aims to solve the problems that the existing shampoo is mostly added with a moistening agent, the problem of hair cannot be fundamentally solved, and certain damage can be caused to the hair after long-time use.
In order to achieve the purpose, the invention provides the following scheme:
the invention provides cyperus esculentus shampoo added with cyperus esculentus root oil, which comprises the following components in percentage by mass:
preferably, the extraction method of the cyperus esculentus root oil comprises the following steps:
(1) (1) selecting, cleaning, drying in the sun or by baking, and pretreating cyperus esculentus roots for later use;
(2) extracting oily liquid of cyperus esculentus roots by adopting a cold pressing mode to obtain primary oil, and controlling the cold pressing temperature to be 15-35 ℃;
(3) the extracted oil is cyperus oil.
Preferably, the surfactant comprises the following components in percentage by mass:
preferably, the conditioner comprises the following components in percentage by mass:
preferably, the thickener is sodium chloride.
Preferably, the pH value regulator comprises the following components in percentage by mass:
0.01 to 0.1 percent of citric acid
0.01 to 0.1 percent of EDTA disodium
Preferably, the antimicrobial agent is DMDM hydantoin.
Preferably, the preservative comprises the following components in percentage by mass:
a preparation method of cyperus esculentus shampoo added with cyperus esculentus root oil comprises the following steps:
(1) keeping the Cyperus esculentus root oil at 40 ℃ under the pressure of 20MPa, and standing for 1h for later use;
(2) sterilizing in water bath, adding surfactant into the water bath, and adding part of the surfactant
Ionized water is stirred for 10min at the water bath temperature of 75-85 ℃, and then the temperature is reduced to 45-55 ℃;
(3) adding Cyperus esculentus root oil, conditioner, antibacterial agent, antiseptic and the rest
Keeping the temperature of the ionized water at 45-55 ℃ and stirring for 10 min;
(4) adding thickener into water bath, stirring to room temperature, and adding pH regulator
Mixing with plant essence for daily use, and stirring for 30min to obtain herba Cyperiae Pratentis shampoo containing herba Cyperiae Pratentis root oil.
Preferably, the pH value of the cyperus esculentus shampoo added with the cyperus esculentus root oil is adjusted to 5.0-6.5 by adding a pH value adjusting agent in the step (4).
The main functions of the components of the invention are as follows:
sodium laureth sulfate: is easy to dissolve in water, has strong foaming power, full foam, white and fine foam, has excellent emulsifying property and washing capacity, and is used as a surfactant for hair washing cream.
Ammonium lauryl sulfate: has good emulsifying, foaming, penetrating, decontaminating and dispersing properties, and can be used as a surfactant for hair washing emulsion.
Cocamidopropyl betaine: a zwitterionic surfactant has low irritation, good water solubility, good stability to acid and alkali, high foaminess, high detergency, and good thickening, softness, bactericidal, antistatic and hard water resistance.
Lauramide MEA: has good emulsifying, foaming, penetrating, decontaminating and dispersing properties, and can be used as a surfactant for hair washing emulsion.
Laureth-23: has high detergency and is used as the surfactant of hair lotion.
Dodecyl benzene sulfonic acid TEA salt: a surfactant which is easy to rinse and can generate a large amount of durable foam and is used for a hair washing cream.
Ethylene glycol stearate: can produce obvious pearl effect, can increase the viscosity of the product, has the functions of moistening skin, nourishing and protecting hair and resisting static electricity, and is used as a conditioner of shampoo.
Polydimethylsiloxane: can darken hair color, help hair keep natural luster, and is used as conditioner of shampoo.
Dimethiconol: can keep hair natural luster, and can be used as conditioner of shampoo.
Guar hydroxypropyltrimonium chloride: can provide good dry and wet hand feeling and is used as a conditioner of shampoo.
Polyquaternium-10: has strong affinity, can repair split hair, form transparent and continuous film on hair, provide excellent moisture retention, improve damaged hair quality, and can be used as conditioner of shampoo.
Cetostearyl alcohol: can make hair moist and soft, and can be used as conditioner of shampoo.
Compared with the prior art, the invention has the following beneficial technical effects:
the cyperus esculentus root oil added shampoo provided by the invention is characterized in that cyperus esculentus root oil is added in the shampoo, and has the functions of cleaning and moistening, so that hair can be deeply cleaned and hair can be moistened, the hair is enabled to have elasticity, the bifurcation is effectively inhibited, the hair quality is improved, the cyperus esculentus root oil is a pure plant extract, the character is mild, no damage is caused to a human body after long-term use, the hair quality is gradually improved, and the hair is enabled to recover the soft and bright elastic state.
Detailed Description
The technical solutions in the embodiments of the present invention are clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention aims to provide cyperus esculentus shampoo added with cyperus esculentus root oil, which solves the problems that most of existing shampoo products are added with moisturizers, the problem of hair cannot be fundamentally solved, and certain damage is caused to the hair after long-time use by adding cyperus esculentus root oil into the shampoo.
In order to make the above objects, features and advantages of the present invention more comprehensible, the present invention is described in further detail below with reference to examples, comparative examples and test examples.
Example 1:
table 1 shows the mass parts of the ingredients in the cyperus esculentus shampoo containing cyperus esculentus root oil provided in example 1.
TABLE 1
Selecting cyperus esculentus roots according to the fullness degree, selecting cyperus esculentus roots with plump and large fruits, repeatedly washing the cyperus esculentus roots with clear water, washing sand, drying in the sun in a natural state or drying, and then carrying out low-temperature cold pressing on the cyperus esculentus roots, wherein the cold pressing temperature is controlled at 30 ℃, and the extracted oil is cyperus esculentus root oil. Preparing the raw materials according to the parts by weight, putting 0.05g of cyperus rotundus oil into a high-pressure closed container, keeping the pressure in the container at 20MPa, standing for 1h in an environment of 40 ℃ to volatilize the active ingredients of the cyperus rotundus oil, taking a water bath kettle, sterilizing, putting a surfactant consisting of 2g of sodium laureth sulfate, 2g of ammonium laureth sulfate, 2g of cocamidopropyl betaine, 2g of laureth MEA, 1g of laureth-23 and 1g of TEA dodecylbenzene sulfonate and 20g of deionized water into the kettle, controlling the water bath temperature at 80 ℃, stirring for 10min by using a stirrer, regulating the rotating speed of the stirrer to 25r/min, naturally cooling the material to 50 ℃ after stirring, adding the pretreated cyperus rotundus oil into the cooled material, adding 0.2g of ethylene glycol stearate, and water, and stirring the mixture to obtain the cyperus rotundus oil, 0.1g of polydimethylsiloxane, 0.1g of dimethiconol, 0.2g of guar hydroxypropyl trimethyl ammonium chloride, 0.2g of polyquaternium-10 and 0.2g of cetostearyl alcohol, 0.01g of DMDM hydantoin serving as an antibacterial agent, 0.001g of methylchloroisothiazolinone, 0.001g of methylisothiazolinone, 0.001g of magnesium nitrate and 0.001g of magnesium chloride serving as preservatives are added, the rest deionized water is added, the mixture is kept at 50 ℃ and stirred for 10min, 0.5g of sodium chloride serving as a thickening agent is added, the mixture is continuously stirred to room temperature, a pH value regulator consisting of 0.01g of citric acid and 0.01g of EDTA disodium is added to regulate the pH value to 5.1, 0.3g of plant essence for daily use is added, and the cyperus oil added into the cyperus oil is stirred for 30min to obtain the cyperus oil shampoo.
In the cyperus esculentus shampoo added with cyperus esculentus root oil provided by the embodiment, in order to volatilize and release active substances in the cyperus esculentus root oil, the cyperus esculentus root oil is pretreated in a pressurized standing mode so as to thoroughly volatilize the active substances in the cyperus esculentus root oil.
In other embodiments, the volatilization of the effective components of the cyperus rotundus can be achieved by shaking the cyperus rotundus root oil, and the like, and the treatment method which can maximize the efficacy of the cyperus rotundus root oil is within the protection scope of the invention.
When the shampoo is used, the hair is completely soaked in warm water, a proper amount of cyperus esculentus oil-added cyperus esculentus shampoo is applied to the hair according to the length of the hair, the hair is slightly scratched by a hand until the hair foams, the hair is scratched for two minutes continuously, the foams are completely cleaned, the hair is wiped by a dry towel and then naturally dried, and the problem of hair quality can be solved after the hair is continuously used for one month.
Example 2:
table 2 shows the mass parts of the ingredients in the cyperus esculentus shampoo containing cyperus esculentus root oil provided in example 2.
TABLE 2
Example 3:
table 3 shows the mass parts of the ingredients in the cyperus esculentus shampoo containing cyperus esculentus root oil provided in example 3.
TABLE 3
Example 4:
table 4 shows the mass parts of the ingredients in the cyperus esculentus shampoo containing cyperus esculentus root oil provided in example 4.
TABLE 4
Example 5:
table 5 shows the mass parts of the ingredients in the cyperus esculentus shampoo containing cyperus esculentus root oil provided in example 5.
TABLE 5
Example 6:
table 6 shows the mass parts of the ingredients in the cyperus esculentus shampoo containing cyperus esculentus root oil provided in example 6.
TABLE 6
Example 7:
table 7 shows the mass parts of the ingredients in the cyperus esculentus shampoo containing cyperus esculentus root oil provided in example 7.
TABLE 7
Example 8:
table 8 shows the mass parts of the ingredients in the cyperus esculentus shampoo containing cyperus esculentus root oil provided in example 8.
TABLE 8
Comparative example 1:
table 9 shows the mass parts of the components in the shampoo to which the oil-free cyperus rotundus oil was added, provided in comparative example 1.
TABLE 9
Comparative example 2:
table 10 shows the parts by mass of each component in the shampoo to which the oil-free cyperus rotundus oil was added, provided in comparative example 2.
Watch 10
The preparation methods and the use methods of the above examples 2 to 8 and comparative examples 1 to 2 were the same as those of example 1, except that the raw material component ratios were different from those of example 1.
The ten shampoo creams prepared according to the formula are subjected to comparative experiments, 100 testers with the problems of head oil, dry and rough hair, split ends and the like are selected, 50 men and women of 100 testers are 50, the age range is 25-45 years old, the testers are divided into 10 groups, the number of men and women in each group is the same, the age of each group is about 35 years old, the ten shampoo creams are respectively used once every two days, the shampoo creams are continuously used for one month, the hair quality of the shampoo creams is detected after one month, and the use feeling of the testers is recorded.
The test results are as follows:
it can be seen from the above test examples that the hair lotions containing cyperus rotundus oil (examples 1 to 8) do not cause allergic reaction, and do not cause the problems of itching of the head after use, and do not cause damage to the scalp, while the hair lotions without cyperus rotundus oil (comparative examples 1 to 2) cause allergic reaction, and generally cause itching of the scalp after half a month of use, and do some damage to the skin, and it can be seen from the longitudinal comparison that the increase of the surfactant can only increase the amount of foam, the addition of too much surfactant can cause the problems of difficult rinsing, dry hair, and the like, while the conditioner has a certain effect on the split and dry hair, but the lasting time is not long, and the problems can not be fundamentally solved, and the problems of oil generation, split and dry hair and the like are thoroughly solved with the increase of cyperus rotundus oil, this indicates that the cyperus oil is purely natural, does not cause damage to the hair scalp, and is capable of nourishing the hair, so that the hair is not split and remains supple for a long time.
And (3) detection results:
the inventor tests the cyperus esculentus shampoo added with cyperus esculentus root oil provided by the embodiment 7 of the invention, and the test report is as follows:
the principle and the implementation mode of the invention are explained by applying specific examples, and the description of the above examples is only used for helping understanding the method and the core idea of the invention; meanwhile, for a person skilled in the art, according to the idea of the present invention, the specific embodiments and the application range may be changed. In summary, this summary should not be construed to limit the present invention.
Claims (5)
3. the cyperus esculentus shampoo as claimed in claim 1, wherein the cyperus esculentus root oil is added with the following components: the extraction method of the cyperus esculentus root oil comprises the following steps:
(1) selecting, cleaning, drying in the sun or by baking, and reserving pretreated cyperus esculentus roots for later use;
(2) extracting oily liquid of cyperus esculentus roots by adopting a cold pressing mode to obtain primary oil, and controlling the cold pressing temperature to be 15-35 ℃;
(3) the extracted oil is cyperus oil.
4. A method of preparing a cyperus esculentus hair shampoo containing cyperus esculentus root oil according to claim 1, which comprises: the preparation method comprises the following steps:
(1) keeping the Cyperus esculentus root oil at 40 ℃ under the pressure of 20MPa, and standing for 1h for later use;
(2) sterilizing a water bath, putting a surfactant into the water bath, adding part of deionized water, stirring for 10min at the water bath temperature of 75-85 ℃, and cooling to 45-55 ℃;
(3) adding cyperus oil, a conditioner, an antibacterial agent, a preservative and the rest deionized water into a water bath kettle, keeping the temperature at 45-55 ℃, and stirring for 10 min;
(4) adding the thickening agent into a water bath kettle, continuously stirring to room temperature, adding the pH value regulator and the plant essence for daily use, and stirring for 30min to obtain the cyperus esculentus shampoo containing cyperus esculentus root oil.
5. The method for preparing the cyperus esculentus hair shampoo added with cyperus esculentus root oil provided by the claim 4 is characterized in that: and (3) adding a pH value regulator in the step (4) to regulate the pH value of the cyperus esculentus shampoo added with the cyperus esculentus root oil to 5.0-6.5.
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Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102012203986A1 (en) * | 2012-03-14 | 2012-12-27 | Henkel Ag & Co. Kgaa | Composition, useful for treating hair, comprises a specified range of Cyperus esculentus tuber oil, a quaternary ammonium compound e.g. esterquat and an amino functional silicone |
WO2013113960A1 (en) * | 2012-01-30 | 2013-08-08 | The Colomer Group Spain, S.L. | Cosmetic composition for protecting the hair |
CN109394588A (en) * | 2018-12-21 | 2019-03-01 | 广州善草纪化妆品有限公司 | A kind of sunscreen composition, sunscreen product and its preparation method and application |
-
2019
- 2019-03-23 CN CN201910260079.4A patent/CN110101602B/en active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2013113960A1 (en) * | 2012-01-30 | 2013-08-08 | The Colomer Group Spain, S.L. | Cosmetic composition for protecting the hair |
DE102012203986A1 (en) * | 2012-03-14 | 2012-12-27 | Henkel Ag & Co. Kgaa | Composition, useful for treating hair, comprises a specified range of Cyperus esculentus tuber oil, a quaternary ammonium compound e.g. esterquat and an amino functional silicone |
CN109394588A (en) * | 2018-12-21 | 2019-03-01 | 广州善草纪化妆品有限公司 | A kind of sunscreen composition, sunscreen product and its preparation method and application |
Non-Patent Citations (1)
Title |
---|
《康如滋养柔顺洗发乳》;皮尔发伯康如化妆品公司;《国家药品监督管理局—进口化妆品查询》;20140730;"配方成分"部分 * |
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