CN109394588A - A kind of sunscreen composition, sunscreen product and its preparation method and application - Google Patents
A kind of sunscreen composition, sunscreen product and its preparation method and application Download PDFInfo
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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Abstract
The present invention relates to a kind of sunscreen compositions, sunscreen product and its preparation method and application.The sunscreen composition is grouped as by the group of following parts by weight: extra large 0.1 ~ 8.0 part of sandalwood seed oil, 0.1 ~ 10.0 part of foreign Hu Oleum Verniciae fordii, and 0.1 ~ 12.0 part of chufa root oil, bitter 0.1 ~ 8.0 part of oil of the seeds of trees of oil.Sunscreen composition provided by the invention has the group containing natural plant composition to be grouped as, and there is characteristic that is salubrious, quickly absorbing, good dispersion, stability is strong, spreadability is good, with preferable sun-proof result, higher spf value, water resistant ability and moisture-retaining capacity, it is easy to smear uniformly in skin surface, is not easy to rub mud pilling with the hands；And also has the effect of anti-inflammatory, removes free radical, anti-erythema.
Description
Technical field
The invention belongs to cosmetic fields, and in particular, to a kind of sunscreen composition, sunscreen product and preparation method thereof
And application.
Background technique
Ultraviolet light in sunlight, which has been shown to it, can cause skin sun burn, erythema, solarization to the direct irradiation of skin
It is black, or even skin photoage and cutaneum carcinoma can be caused, however ultraviolet light is either all ubiquitous at the fine day cloudy day, it is every when per
Skin is carved all in the injury by ultraviolet light.With the improvement of living standards, sunscreen product has become in people's life 1 year
The skincare product of four seasons indispensability.
Currently, sunscreen product on the market containing often through the content for increasing sun-screening agent, especially physical sunscreen agent
Amount, to reach higher SPF.But physical sunscreen agent content is higher, declines the spreading ratio of product, on skin compared with
Difficulty is pushed open, the problem of rubbing mud with the hands occurs, practical sun-proof result is caused to be had a greatly reduced quality.In addition, SPF is high and water repelling property is good
Sunscreen product can also carry out sticky sense to skin tape.Some products are often accomplished by adding the alcohol of higher dosage salubrious
Skin sense, but such product is to sensitive skin and unfriendly.High sun-proof value will often increase the dosage of chemical sun simultaneously,
And chemical sun can cause to bear to skin.Finally in order to increase the slipping of skin sense, a large amount of silicone oil component is added, and
Silicone oil component is not easy to be absorbed by the skin, and forms oil film, influences beauty.
Therefore, need to develop it is a kind of it is salubrious, it is not sticky it is easy absorb, spreading ratio it is high, and SPF is high, water repelling property is good
Sunscreen composition.
Summary of the invention
Sunscreen product is sticky, is not easy the defect absorbed or deficiency it is an object of the invention to overcoming in the prior art, provides
A kind of sunscreen composition.Sunscreen composition provided by the invention has the group containing natural plant composition to be grouped as, and has clear
Characteristic that is refreshing, quickly absorbing, good dispersion, stability is strong, and spreadability is good, have preferable sun-proof result, higher spf value,
Water resistant ability and moisture-retaining capacity are easy to smear uniformly, are not easy to rub mud pilling with the hands in skin surface；And also there is anti-inflammatory, remove freely
The effect of base, anti-erythema.
Another object of the present invention is to provide the preparation methods of above-mentioned sunscreen composition.
Another object of the present invention is to provide above-mentioned sunscreen compositions to prepare the application in sunscreen product.
Another object of the present invention is to a kind of sunscreen products.
For achieving the above object, the present invention adopts the following technical scheme:
A kind of sunscreen composition is grouped as by the group of following parts by weight:
Ximenia is dungarunga, the shrub category of Spain's monk's Franciso Ximenes name of the 17th century.Entirely
Southern Africa sheet grows extra large sandalwood, is commonly called as wild plum.Fruit is as plum, and color is from bright orange and scarlet to complete
Dark reddish brown when complete mature.South Africa women and the extra large sandalwood oil of young girl's traditional habit soften the skin of oneself and improve them
Hair.Treat drying, chapped skin this be especially welcome massage oil.Extra large sandalwood fruit vitamin all rich in
C. it in addition to eating it raw, is also used to cook jam, jelly and beverage.Unsaturated fatty acid rich in is (about in extra large sandalwood seed oil
92%), therefore there is comparable nutritive value.Oil helps to maintain the integrality of cell wall, and has and recombinate effect and to skin
The anti-aging effects of skin.Its long chain fatty acids bring good compatibility, and tax skin living moistens and moisturizing, softening.Extra large wingceltis
The wooden seed oil, which has proved to be one kind, can effectively treat dry skin, aging because it will increase skin moisture content and
Improve the function of sebaceous gland tissue.It also has anti-inflammatory property and improves skin blood circulation, it can also be effectively
For eczema, coarse skin and scar.The inventors discovered that its UVA/UVB in sun-proof field has absorption peak, have certain anti-
Shine and cooperate with sun-proof effect.
Foreign Hu Oleum Verniciae fordii is the oil produced from foreign poon seed through cold compaction process, be can be used in cosmetic formulations, peace
Quan Xinggao, human body nonhazardous effect have effects that soft and moist and conditioning skin.Foreign poon seed oil extract is from natural plants seed
Oil has antibiotic effect, inhibits scalp inflammation, and moisturizing simultaneously improves eczema capitis, and heel is dry and cracked etc., there is repair.This
Inventor has found that it has absorption peak in the UVA/UVB in sun-proof field, there is effect certain sun-proof and that collaboration is sun-proof.
Chufa is Cyperaceae herbaceos perennial, makees annual crop cultivation.Alias has: cyperue esculentus, sugared root fruit,
Underground Chinese chestnut, stem tuber oil-containing 27% or so, oil is shallow dark brown, and taste perfume (or spice) can be eaten, and food industry is usually with cream processed, candy, almond
Water, oil meal can make wine or make concentrated feed, and it is the excellent food of domestic animal that cauline leaf, which contains more fat and sugar point,.Can make oil plant and
Good forage is used, and lubricating oil and soapmaking can also be made, be a kind of high-quality, high yield and the wide collection grain of Prospects of Comprehensive Utilization, oil, herd,
It raises in the industrial crops of one.Chufa originates in Mediterranean Region, and nineteen fifty-two, China introduced from the Soviet Union, a province more than existing 20,
City, autonomous region's plantation.Chufa root oil is the grease extracted by its rhizome part, and environmentally friendly, as moisten and repair
Multiple ingredient is used in skin nursing, sun-proof, in hair reparation and baby products.Chufa root oil has in ultraviolet (UV) A/UVB
Obvious absorption peaks have effect certain sun-proof and that collaboration is sun-proof.
Since 1,100, American Indian of Amazon River basin Wayapi and Palikur use always bitter oil seeds of trees oil
Inflammation, flu, ulcer and the dermatozoon of this oil treatment skin and muscle.They also use it as natural lam-oil combustion
Material and pest repellant, especially it there is no tastes unpleasant possessed by other pest repellants.Nowadays, Brazilian is through commonly using it
Treatment of arthritis, psoriasis and rheumatism.The in vitro study of the ingredient proves that it has antibacterial activity and anti parasitic and resists
Tumor promotion.In cosmetics, its major function is anti-inflammatory and skin conditioning agent.Contain natural limonin in the oil,
They have been proved to that skin renewal can be made and have reduced inflammation.In addition to this, rouge needed by human is rich in bitter oily seeds of trees oil
Fat acid, such as oleic acid, palmitinic acid, stearic acid and linoleic acid.This makes it that can be divided into natural moisturizing factor (NMF).As a kind of guarantor
The wet factor, it can assist in keeping epidermal cell structure integrality and and effectively to antibacterium, be conducive to skin healing
Process prevents skin irritatin and makes skin regeneration.The inventors discovered that bitter oil seeds of trees oil has obvious suction in ultraviolet (UV) A/UVB
Peak is received, there is effect certain sun-proof and that collaboration is sun-proof.
The inventors of the present invention discovered through researches that extra large sandalwood seed oil, foreign Hu Oleum Verniciae fordii, chufa root oil and bitter oily seeds of trees oil
The sunscreen composition of composition can increase sun-proof UVA and UVB index, have apparent synergistic function to spf value, used
When in sunscreen product, the dosage of chemical sun can be reduced；It is natural plant product additionally, due to the sunscreen composition, contains
There is plant component, there is characteristic that is salubrious, quickly absorbing, can all dissolve each other with a variety of chemical suns, stablize composition system
Property enhancing, reduce the sticky sense of system, better disperse sun-screening agent, but also there is good spreadability, be easy to apply in skin
It smears uniformly, is not easy to rub mud pilling with the hands, further improves spf value, water resistant ability and the moisture-retaining capacity of composition.Also, the combination
Object also has the effect of anti-inflammatory, removes free radical, anti-erythema.
Preferably, the sunscreen composition is grouped as by the group of following parts by weight:
It is further preferable that the sunscreen composition is grouped as by the group of following parts by weight:
The preparation method of above-mentioned sunscreen composition, includes the following steps:
S1: the seed of extra large sandalwood is passed through into the isolated extra large sandalwood seed oil of squeezing or means of supercritical extraction；
S2: the seed of foreign poon was passed through into squeezing or the isolated foreign Hu Oleum Verniciae fordii of means of supercritical extraction；
S3: the rhizome of chufa is passed through into squeezing or the isolated chufa root oil of means of supercritical extraction；
S4: the seed of bitter oil tree is passed through into the isolated bitter oily seeds of trees oil of squeezing or means of supercritical extraction；
S5: extra large sandalwood seed oil, foreign Hu Oleum Verniciae fordii, chufa root oil and bitter oily seeds of trees oil are mixed up to described anti-
Shine composition.
The temperature separated in S1~S4 of above-mentioned sunscreen composition is 10~40 DEG C, in 10~40 DEG C of temperature conditions in S5
Lower stirring.
Above-mentioned sunscreen composition prepare in sunscreen product application it is also within the scope of the present invention.
A kind of sunscreen product is grouped as by the group of following mass fraction:
Above-mentioned sunscreen composition is added in sunscreen product, can be had under the dosage for significantly reducing chemical sunscreen product
There are higher spf value, good dispersion, salubrious non-greasy is not easy to rub mud pilling with the hands；In addition, also having preferable water resistant ability and guarantor
Wet ability and anti-inflammatory, the effect for removing free radical, anti-erythema.
Preferably, the sunscreen product is grouped as by the group of following mass fraction:
Preferably, the sunscreen product is grouped as by the group of following mass fraction:
Chemical sun, Synthetic Oil and the auxiliary agent of this field routine are used equally in the present invention.
Preferably, chemical sun is Uvinul T 150, ethylhexyl methoxy cinnamate, double ethyl hexyl oxygen benzene
One or more of phenol anisyl triazine, the own ester of diethyl oxybenzene formylbenzoate, Octocrilene or Homosalate.
Preferably, Synthetic Oil be hexanedioic acid dibutyl ester, carbonic acid dioctyl ester, isononyl isononanoate, lauric alcohol-caprylate/
Decylate, sad one or more of Propylheptyl or three isooctyl acid glyceride.
Preferably, auxiliary agent is bisabolol, ethyl alcohol, Phenoxyethanol, hexylene glycol, pentanediol, para hydroxybenzene propionamido- benzene
One or more of formic acid or butanediol.
Sunscreen product provided by the invention can be used in the spraying mode of inhalator jar or pump head.
Compared with prior art, the invention has the following beneficial effects:
Sunscreen composition provided by the invention has preferable sun-proof result, and has characteristic that is salubrious, quickly absorbing,
Good dispersion, stability is strong, and spreadability is good, spf value, water resistant ability and moisture-retaining capacity with higher, is easy in skin surface
It smears uniformly, is not easy to rub mud pilling with the hands；And also has the effect of anti-inflammatory, removes free radical, anti-erythema.
Specific embodiment
Below with reference to embodiment, the present invention will be further described.These embodiments are retouched to typical case of the invention
It states, however, the present invention is not limited thereto.Test method as used in the following examples unless otherwise specified, is conventional method, is made
Raw material, reagent etc. are unless otherwise specified the raw materials and reagents that can be obtained from commercial sources such as conventional markets.
Embodiment 1
The present embodiment provides a kind of sunscreen compositions, by extra large sandalwood seed oil 50g, foreign Hu Oleum Verniciae fordii 60g, chufa root oil
90g and hardship oil seeds of trees oil 50g is formed.
The sunscreen composition is prepared via a method which to obtain:
The preparation of extra large sandalwood seed oil: the seed of extra large sandalwood is isolated by squeezing or means of supercritical extraction；
The preparation of foreign Hu Oleum Verniciae fordii: the seed of foreign poon was passed through into squeezing or means of supercritical extraction is isolated；
The preparation of chufa root oil: the rhizome of chufa is isolated by squeezing or means of supercritical extraction；
The preparation of bitter oil seeds of trees oil: the seed of bitter oil tree is isolated by squeezing or means of supercritical extraction；
Being separated when preparation with the temperature of stirring is 10~40 DEG C.
Extra large sandalwood seed oil, foreign Hu Oleum Verniciae fordii, chufa root oil and bitter oily seeds of trees oil are mixed up to sunscreen composition, note
For 1# sunscreen composition.
Embodiment 2
The present embodiment provides a kind of sunscreen compositions, by extra large sandalwood seed oil 80g, foreign Hu Oleum Verniciae fordii 100g, chufa root oil
1g and hardship oil seeds of trees oil 1g is formed.
Preparation method and embodiment 1 are consistent, are denoted as 2# sunscreen composition.
Embodiment 3
The present embodiment provides a kind of sunscreen compositions, by extra large sandalwood seed oil 1g, foreign Hu Oleum Verniciae fordii 1g, chufa root oil
120g and hardship oil seeds of trees oil 80g is formed.
Preparation method and embodiment 1 are consistent, are denoted as 3# sunscreen composition.
Embodiment 4
The present embodiment provides a kind of sunscreen compositions, by extra large sandalwood seed oil 10g, foreign Hu Oleum Verniciae fordii 80g, chufa root oil
10g and hardship oil seeds of trees oil 60g is formed.
Preparation method and embodiment 1 are consistent, are denoted as 4# sunscreen composition.
Embodiment 5
The present embodiment provides a kind of sunscreen compositions, by extra large sandalwood seed oil 60g, foreign Hu Oleum Verniciae fordii 10g, chufa root oil
100g and hardship oil seeds of trees oil 10g is formed.
Preparation method and embodiment 1 are consistent, are denoted as 5# sunscreen composition.
In addition, the extra large sandalwood seed oil in embodiment 1 is replaced with carbonic acid dioctyl ester, object is closed as a control group, and it is anti-to be denoted as 1*
Shine composition；Foreign Hu Oleum Verniciae fordii in embodiment 1 is replaced with into carbonic acid dioctyl ester, object is closed as a control group, is denoted as sun-proof group of 2*
Close object；Chufa root oil in embodiment 1 is replaced with into carbonic acid dioctyl ester, object is closed as a control group, is denoted as 3* sunscreen composition
Object.The oily seeds of trees oil of hardship in embodiment 1 is replaced with into carbonic acid dioctyl ester, object is closed as a control group, is denoted as 4* sunscreen composition
Embodiment 6~14 and reference examples 1~5
Table 1,2 and 3 is respectively the formula of the sunscreen product of embodiment 6~10, embodiment 11~14 and reference examples 1~5
(unit: wt%).
The formula for the sunscreen product that 1 embodiment 6~10 of table provides
The formula for the sunscreen product that 2 embodiment 11~14 of table provides
The formula for the sunscreen product that 3 reference examples 1~5 of table provide
Auxiliary agent can be bisabolol, ethyl alcohol, Phenoxyethanol, hexylene glycol, pentanediol, para hydroxybenzene propionamido- benzoic acid
Or one or more of butanediol, select bisabolol as auxiliary agent in an embodiment of the present invention.
The following performance for the sunscreen product that embodiment 6~14 and reference examples 1~5 provide is tested:
(1) SPF performance test SPF performance test is measured according to following scheme using ex vivo technique:
Initially, shaggy PMMA substrate is measured (purchased from SCHONBERG GmbH&Co.KG, Hamburg/
Germany weight).Then to be tested batch is deposited on substrate and then with 7 microns of lower pull-rods (draw down bar)
Quickly smooth out to obtain thin conforming layer.So that the layer is about 20 minutes dry, and measure substrate+uniform drying layer weight.It is dry
The UV of dry conforming layer absorbs multiple points using LABSPHERE 2000S analyzer on layer and measures.The solid matter hundred of this layer
Divide than being measured using solid matter analyzer.Using the weight of dry film and the solid matter content of layer, can be calculated
The weight of instant original wet layer and its density is therefore calculated after deposition.Using this information, following formula can be passed through
Calculate SPF:
Wherein E (X)=standard solar spectrum spectral irradiance；S (λ)=af at wavelength lambda erythemal action spectrum
(erythemal action spectrum) and A (λ)=af at wavelength lambda spectral absorption (spectral absorbance) (meter
Correction factor is calculated to extrapolate for determining that under the wet layer density of 2.0mg/cm2, ((9 points, be averaged) are counted in sample test；
Scan number of Blank (8 times)；Solar irradiance (290nm-400nm).
UV-2000S is a stable top test equipment, can quickly detect product sample to 280nm-410nm wave
The diffusing transmission rate of light in long range.Double beam spectrometer with diffusion illumination functions can carry out essence to height scattering sample
It really tests, and prevents the overexposure of sample without using optical filter.Test data conversion can be by its application software automatically
Sun protection factor (SPF).
(2) test of UVAPF performance test UVA-PF uses COLIPA method
It is measured using UV-2000S analyzer, (9 points, be averaged) are counted in sample test；Scan number of Blank
(8 times)；Solar irradiance (290nm-400nm)
Principle steps are as follows: the measurement of UVAPF is carried out by following steps:
Step 1: passing through the in-vitro measurements for the absorbance A 0 (λ) being applied on PMMA panel products before any UV irradiation；
Step 2: the mathematics amendment that coefficient of utilization ' C ' carries out initial UV spectrum is equal to nominal (in vivo) SPF's to obtain
External SPF (0%UV dosage).Then initial UVA protection (UVAPF0) is calculated using A0 (λ) and C；
Step 3: single UV dosage D is calculated, it is proportional to UVAPF0 (D=UVAPF0 × 1.2)；
Step 4: being exposed to the sample under the UV for calculating UV dosage D；
The external transmission measurement of sunscreen product after step 5:UV irradiation obtains the 2nd UV spectrum with A (λ) data；
Step 6: the number of the second spectrum (after UV irradiation) is carried out according to the identical C coefficient previously measured in step 2；
Amendment is learned, external UVA protecting factor UVAPF is then calculated.Calculation formula is as follows:
Test data can be automatically UVA PF value by COLIPA method migration by its application software of UV-2000S analyzer.
(3) percutaneous loss of moist (transepidermalwaterloss, TEWL), TEWL are by measuring skin surface
Water vapor pressure gradient the case where showing moisture loss, to reflect the water permeability barrier of skin.Sample 1ML is taken to be applied to arm
Inside, the TEWL value after measurement 8 hours.When barrier function damage, TEWL value increases；On the contrary, TEWL is reduced, prompting screen
Barrier is repaired, unit g/m2h.The numerical value of TEWL is lower, indicates that the barrier function effect of product is better, and moisture of skin is lost
Also fewer, specific as follows: -0.50 is criterion of acceptability, and the lower numerical value the better.
(4) moisture retention is tested: mainly measuring skin keratin water with moisture of skin tester Corneometer CM 825
Divide content.Moisture of skin tester Corneometer CM 825 is normal much higher than other substance dielectrics using the dielectric constant of water
Several characteristics, the capacitance by measuring skin can reflect the water content in keratoderma.Capacitance is higher, cuticula
Water content is also higher, and vice versa.Side is bent in subject or so forearm and every half face chooses 4 test points, and uses orientation film
Label record test point position.It is measured with Corneometer CM 825 using preceding D0 and using the moisture of each test point of rear D28
Content, parallel replication 2 times, all test points in side are averaged, and compare the hydrauture of the keratoderma before and after use
Variation, is as a result indicated with moisture content difference, and unit is that a.u. test uses JMP software to carry out conspicuousness statistical to data
Analysis, the relative growth rate of obtained keratoderma water content, growth rate is higher, indicates that moistening effect is better, and vice versa,
Specific as follows: 25% is criterion of acceptability, and numerical value is the bigger the better.
(5) using effect is evaluated
Using effect evaluation is primarily referred to as the aspiration trier by 20 Jing Guo professional training, and the sample of 80ul is applied to
The back of the hand, smearing of mildly being circled round with another hand 8 times, the texture of sample is then successively evaluated in a manner of marking, is sprawled
Property, flexibility, absorbability, with rear pleasant feeling；Evaluation criterion: very good (8-10), good (6-8), general (4-6), poor (2-
4), poor (0-2), the scoring highest of properties are divided into 10 points, and minimum to be divided into 0 point, score is higher, represents the performance of the product
Better, total score is 50 points, and numerical value is higher, and effect is better.
The test result of SPF SPF and PA such as table 4.
The test result of the SPF SPF and PA of the sunscreen product that 4 embodiment 6~14 of table and comparative example 1~5 provide
As can be known from the results of Table 4, the effect in embodiment 6~14 is optimal to the spf value of embodiment 6 with PA value.It is real simultaneously
It applies example 6 and reference examples 1~4 compares, spf value is also that embodiment 6 is optimal with PA value, that is, proves extra large sandalwood seed oil, foreign poon seed
Oil, chufa root oil and oily every kind of the bitter oily seeds of trees can bring the promotion of spf value Yu PA value；Reference examples 5 are without in embodiment 6
Plant sun composition, reference examples 5 are to reach the SPF close with embodiment 6 by increasing the dosage of chemical synthesis sun-screening agent
Value and PA value, this can aggravate the burden of skin.
Percutaneous loss of moist and moisture retention test result such as table 5.
The percutaneous loss of moist of table 5 and moisture retention test result
| Sample | Percutaneous loss of moist | Moisture retention tests (relative growth rate) |
| Embodiment 6 | -0.78 | 38% |
| Embodiment 7 | -0.58 | 30% |
| Embodiment 8 | -0.62 | 31% |
| Embodiment 9 | -0.60 | 29% |
| Embodiment 10 | -0.61 | 32% |
| Embodiment 11 | -0.48 | 22% |
| Embodiment 12 | -0.74 | 36% |
| Embodiment 13 | -0.50 | 24% |
| Embodiment 14 | -0.72 | 34% |
| Reference examples 1 | -0.46 | 22% |
| Reference examples 2 | -0.46 | 22% |
| Reference examples 3 | -0.42 | 20% |
| Reference examples 4 | -0.45 | 21% |
| Reference examples 5 | -0.26 | 14% |
As can be known from the results of Table 5, from embodiment 6-14 compared with reference examples 1~5, the percutaneous moisture of embodiment 6 is lost
Mistake rate and the effect of moisture retention are optimal.Wherein in reference examples 5, because being free of plant sun composition, percutaneous loss of moist rate
It is obviously worst with the effect of moisture retention, that is, prove that the plant composition can bring percutaneous loss of moist rate and moisture retention effect
It is promoted.
The evaluation of 6 using effect of table
| Sample | Texture | Spreadability | Flexibility | Absorbability | With rear pleasant feeling | Comprehensive statistics |
| Embodiment 6 | 9.4 | 9.2 | 9.5 | 9.2 | 9.5 | 46.8 |
| Embodiment 7 | 9.3 | 9.2 | 9.4 | 9.1 | 9.4 | 46.4 |
| Embodiment 8 | 9.2 | 9.3 | 9.3 | 9.3 | 9.2 | 46.3 |
| Embodiment 9 | 9.1 | 9.2 | 9.3 | 9.4 | 9.3 | 46.3 |
| Embodiment 10 | 9.2 | 9.3 | 9.4 | 9.2 | 9.1 | 46.2 |
| Embodiment 11 | 8.3 | 8.3 | 8.0 | 7.9 | 7.9 | 40.4 |
| Embodiment 12 | 9.3 | 9.2 | 9.3 | 9.4 | 9.2 | 46.4 |
| Embodiment 13 | 8.4 | 8.4 | 8.2 | 8.0 | 8.0 | 41.0 |
| Embodiment 14 | 9.2 | 9.1 | 9.3 | 9.4 | 9.2 | 46.2 |
| Reference examples 1 | 8.4 | 9.1 | 8.5 | 9.1 | 8.5 | 43.6 |
| Reference examples 2 | 8.8 | 8.6 | 8.2 | 8.4 | 8.2 | 42.2 |
| Reference examples 3 | 8.3 | 8.8 | 8.4 | 8.0 | 8.0 | 41.5 |
| Reference examples 4 | 8.6 | 8.8 | 8.3 | 8.2 | 8.1 | 42.0 |
| Reference examples 5 | 8.0 | 8.0 | 7.9 | 7.4 | 7.4 | 38.7 |
As can be known from the results of Table 6, from the point of view of in-service evaluation, in embodiment 6~14, the synthesis in-service evaluation of embodiment 6 is most
It is excellent；Embodiment 6 is compared with reference examples 1~5, and as a result and the using effect of embodiment 6 is optimal.
In summary test evaluation, sunscreen composition provided by the invention have preferable sun-proof result, and have clear
Characteristic that is refreshing, quickly absorbing, good dispersion, stability is strong, and spreadability is good, spf value, water resistant ability and moisturizing with higher
Ability is easy to smear uniformly, is not easy to rub mud pilling with the hands in skin surface；And the vegetable fat of addition also brings anti-inflammatory, removes freely
The effect of base, anti-erythema.
Above-described specific embodiment has carried out further the purpose of the present invention, technical scheme and beneficial effects
It is described in detail, it should be understood that being not used to limit this hair the foregoing is merely a specific embodiment of the invention
Bright protection scope, all within the spirits and principles of the present invention, any modification, equivalent substitution, improvement and etc. done should all
It is included within protection scope of the present invention.
Claims (10)
1. a kind of sunscreen composition, which is characterized in that be grouped as by the group of following parts by weight:
Extra large 0.1 ~ 8.0 part of sandalwood seed oil,
0.1 ~ 10.0 part of foreign Hu Oleum Verniciae fordii,
0.1 ~ 12.0 part of chufa root oil,
Bitter 0.1 ~ 8.0 part of oil of the seeds of trees of oil.
2. sunscreen composition according to claim 1, which is characterized in that the sunscreen composition by following parts by weight group
It is grouped as:
Extra large 1.0 ~ 6.0 parts of sandalwood seed oil,
1.0 ~ 8.0 parts of foreign Hu Oleum Verniciae fordii,
1.0 ~ 10.0 parts of chufa root oil,
Bitter 1.0 ~ 6.0 parts of oil of the seeds of trees of oil.
3. sunscreen composition according to claim 2, which is characterized in that the sunscreen composition by following parts by weight group
It is grouped as:
Extra large 5 parts of sandalwood seed oil,
6 parts of foreign Hu Oleum Verniciae fordii,
9 parts of oil of chufa root,
5 parts of oil of the bitter oil seeds of trees.
4. the preparation method of any sunscreen composition of claim 1 ~ 3, which comprises the steps of:
S1: the seed of extra large sandalwood is passed through into the isolated extra large sandalwood seed oil of squeezing or means of supercritical extraction；
S2: the seed of foreign poon was passed through into squeezing or the isolated foreign Hu Oleum Verniciae fordii of means of supercritical extraction；
S3: the rhizome of chufa is passed through into squeezing or the isolated chufa root oil of means of supercritical extraction；
S4: the seed of bitter oil tree is passed through into the isolated bitter oily seeds of trees oil of squeezing or means of supercritical extraction；
S5: extra large sandalwood seed oil, foreign Hu Oleum Verniciae fordii, chufa root oil and bitter oily seeds of trees oil are mixed up to described sun-proof group
Close object.
5. preparation method according to claim 4, which is characterized in that the temperature separated in S1 ~ S4 be 10 ~ 40 DEG C, in S5
It is stirred under the conditions of 10 ~ 40 DEG C of temperature.
6. any sunscreen composition of claim 1 ~ 3 is preparing the application in sunscreen product.
7. a kind of sunscreen product, which is characterized in that be grouped as by the group of following mass fraction:
Any sunscreen composition 0.1 ~ 38.0% of claim 1 ~ 3,
Chemical sun 20.0 ~ 35.0%,
Synthetic Oil 42.0 ~ 65.0%,
Auxiliary agent 0.1 ~ 20.0%.
8. sunscreen product according to claim 7, which is characterized in that the sunscreen product is grouped by the group of following mass fraction
At:
Sunscreen composition 1.0 ~ 30.0%,
Chemical sun 22.0 ~ 30.0%,
Synthetic Oil 45.0 ~ 55.0%,
Auxiliary agent 0.2 ~ 10.0%.
9. sunscreen product according to claim 7, which is characterized in that the sunscreen product is grouped by the group of following mass fraction
At:
Sunscreen composition 25%,
Chemical sun 26%,
Synthetic Oil 46%,
Auxiliary agent TO 100%.
10. sunscreen product according to claim 7, which is characterized in that the chemical sun is Uvinul T 150, first
Oxygroup 2-Ethylhexyl cinnamate, double ethyl hexyl oxy phenol anisyl triazines, the own ester of diethyl oxybenzene formylbenzoate, Losec
Vertical one or more of woods or Homosalate；The Synthetic Oil is hexanedioic acid dibutyl ester, carbonic acid dioctyl ester, the different nonyl of isononanoic acid
Ester, lauric alcohol-caprylate/decylate, auxiliary agent is described in sad one or more of Propylheptyl or three isooctyl acid glyceride
One of bisabolol, ethyl alcohol, Phenoxyethanol, hexylene glycol, pentanediol, para hydroxybenzene propionamido- benzoic acid or butanediol or
It is several.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110029012A (en) * | 2019-03-23 | 2019-07-19 | 宋超 | A kind of high-purity chufa root oil and its extracting method |
| CN110037943A (en) * | 2019-03-23 | 2019-07-23 | 宋超 | A kind of chufa eye cream added with chufa root oil |
| CN110101602A (en) * | 2019-03-23 | 2019-08-09 | 宋超 | A kind of chufa leaves shampoo of chufa root oil addition |
| CN110527589A (en) * | 2019-09-12 | 2019-12-03 | 宋玉来 | A kind of preparation method and applications of tiger macadamia nut oil |
| CN113855591A (en) * | 2021-10-08 | 2021-12-31 | 露乐健康科技股份有限公司 | Pterocarpus marsupium seed oil composition simulating breast milk nervonic acid and having skin-touch soft feeling, skin care product, preparation method and application |
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2018
- 2018-12-21 CN CN201811572544.XA patent/CN109394588A/en not_active Withdrawn
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110029012A (en) * | 2019-03-23 | 2019-07-19 | 宋超 | A kind of high-purity chufa root oil and its extracting method |
| CN110037943A (en) * | 2019-03-23 | 2019-07-23 | 宋超 | A kind of chufa eye cream added with chufa root oil |
| CN110101602A (en) * | 2019-03-23 | 2019-08-09 | 宋超 | A kind of chufa leaves shampoo of chufa root oil addition |
| CN110037943B (en) * | 2019-03-23 | 2022-03-11 | 宋超 | Cyperus esculentus eye cream added with cyperus esculentus root oil |
| CN110101602B (en) * | 2019-03-23 | 2022-03-25 | 宋超 | Cyperus esculentus shampoo added with cyperus esculentus root oil |
| CN110527589A (en) * | 2019-09-12 | 2019-12-03 | 宋玉来 | A kind of preparation method and applications of tiger macadamia nut oil |
| CN113855591A (en) * | 2021-10-08 | 2021-12-31 | 露乐健康科技股份有限公司 | Pterocarpus marsupium seed oil composition simulating breast milk nervonic acid and having skin-touch soft feeling, skin care product, preparation method and application |
| CN113855591B (en) * | 2021-10-08 | 2022-08-16 | 露乐健康科技股份有限公司 | Pterocarpus marsupium seed oil composition simulating breast milk nervonic acid and having skin-touch soft feeling, skin care product, preparation method and application |
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Application publication date: 20190301 |