CN113749991A - Multi-effect protective lipstick containing peony moisturizing components and preparation method thereof - Google Patents
Multi-effect protective lipstick containing peony moisturizing components and preparation method thereof Download PDFInfo
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- CN113749991A CN113749991A CN202111029505.7A CN202111029505A CN113749991A CN 113749991 A CN113749991 A CN 113749991A CN 202111029505 A CN202111029505 A CN 202111029505A CN 113749991 A CN113749991 A CN 113749991A
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- peony
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/27—Zinc; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
Abstract
The invention discloses a multi-effect protective lipstick containing peony moisturizing components and a preparation method thereof, wherein organic plants such as peony seed skin and peony petals are used as main raw materials, a supercritical carbon dioxide extraction mode is adopted to extract waxy components and add the multi-effect protective components, artificial spice and pigment are not added, and the multi-effect protective lipstick which can effectively moisturize, has the advantages of preventing allergy, strengthening the natural ultraviolet ray defense capability of lip skin and the like is prepared by combining prevention and treatment through efficient and reasonable formula collocation; the lip care product has the advantages of harmlessness, no toxicity, moistening and moisturizing, strengthening the defense capacity of lip skin to ultraviolet rays, and has the effects of repairing damaged cells, activating cells, promoting lip skin metabolism, keeping the lip skin tender and delaying lip skin aging; the preparation method is simple, safe, convenient to use, high in safety, advanced in dosage form and remarkable in effect.
Description
Technical Field
The invention relates to a lipstick, in particular to a multi-effect protective lipstick containing peony moisturizing components and a preparation method thereof.
Background
The lipstick is one of the cosmetics essential for women to make lip ruddy and glossy, moisten, protect lip, increase face's aesthetic feeling and correct lip contour. With the influence of environmental damage, excessive pollutants in the air, irregular life rhythm and ozone layer damage ultraviolet irradiation, the dry climate environment and the increasingly worsened air quality enable the moisture of the skin of people to be rapidly lost, the sun protection consciousness of people on the skin is gradually improved, the skin protection and whitening are never required to be stopped by women, natural harmless cosmetics are more objects to be pursued by people, but the sun protection consciousness on lips is not strong, the lip mucous membrane is the only non-horny layer mucous membrane which is exposed in the environment for a long time, the lips are not protected by a sebum membrane, the effective moisture preservation can not be realized, the moisture evaporation is faster, the capability of resisting the external environment change is weaker, compared with the skin, the skin is more easily damaged, and the symptoms of cheilitis, lip cracks, dry lips, desquamation, redness and the like can be caused. And ultraviolet rays are an important factor that may cause damage to lips. At present, the commercially available lipstick mainly has a moistening effect, few lipstick can protect medium-wave ultraviolet rays, and almost has no protection effect on long-wave ultraviolet rays, and the long-wave ultraviolet rays have strong penetrating power on human skin, can reach the deep part of the skin dermis, damage cell DNA, damage elastic fibers, collagen fibers and the like, cause skin relaxation and aging, and even cause skin cancer.
In recent years, peonies are vigorously developed and planted in China, the planting area of the peonies reaches 1 million mu, the planting area of the peonies is mostly in hilly areas, the peonies have pleasant fragrance, contain rich nutrient substances, contain 13 amino acids, have 8 kinds of amino acids which are needed by human bodies, have high content, have a health care function on the human bodies, and are safe and free of toxic and side effects; and a thin layer of wax fat is arranged on the peony flowers, and the layer of wax fat has natural skin care effect. The peony seeds can be made into oil, flowers, roots and stems of peony can be used as medicines, deep processing is carried out by full utilization of people, and with the requirement of people on healthy life, when the peony seeds squeeze edible oil, black skin wrapped by the peony seeds is usually removed to pursue high-quality oil, so that a large amount of black skin is generated, the black skin wrapped by the peony seeds is rich in substances like antioxidant and anti-radiation grease, the black skin wrapped by the peony seeds is not fully utilized, and resource waste is caused.
Therefore, if the peony seed skin and peony flower are used as main raw materials to extract the biological wax, the natural moisturizing multi-effect protective lipstick is prepared, waste materials are changed into valuable materials, the materials are fully used, the treatment of peony waste is facilitated, and a new way is opened up for the deep processing and comprehensive utilization of peony.
Disclosure of Invention
The invention aims to solve the defects of the technical problems and provides a multi-effect protective lipstick which is prepared by taking natural organic plants such as peony seed skin and the like as main raw materials, adding no artificial spice and pigment, combining prevention and treatment through efficient and reasonable formula matching, and has the advantages of effectively moistening, preventing allergy, strengthening the natural ultraviolet ray defense capability of lip skin and the like.
The technical scheme adopted by the invention is that the multi-effect protective lipstick containing peony moisturizing components is prepared from the following raw materials in parts by weight: 15-25 parts of beeswax, 5-10 parts of peony seed peel wax, 5-10 parts of peony flower wax, 30-40 parts of peony seed oil, 5-8 parts of revived grass extract, 1-3 parts of chamomile extract, 2-4 parts of honeysuckle extract, 2-5 parts of mica powder, 1-2 parts of octyl methoxycinnamate, 1-3 parts of butyl methoxy dibenzoyl methane, 1-3 parts of nicotinamide, 1-3 parts of titanium dioxide and 1-3 parts of zinc oxide.
A preparation method of a multi-effect protective lipstick containing peony moisturizing components comprises the following steps:
collecting peony seed peels, cleaning, naturally airing on a net bed, and drying at 50-60 ℃; crushing into 150-mesh powder with the granularity of 100 meshes to obtain peony seed peel powder;
step two, mixing peony seed peel powder with a proper amount of 95% concentration (mass fraction) ethanol solution, performing ultrasonic vibration for 10-30 minutes, placing the mixture in a reaction kettle of a supercritical carbon dioxide extraction device, and performing continuous cyclic extraction by using a supercritical carbon dioxide fluid, wherein the extraction pressure is 15-25MPa, the extraction temperature is 35-55 ℃, and the extraction time is 2-4 hours; settling solid residues to the bottom of the tank, and separating oil to obtain peony seed husk wax;
picking the full-opened peony petals, splitting the peony petals into strips with the length of 1-2 cm and the width of 3-5 mm, cleaning the strips with clear water, and naturally airing the petals on a net bed after cleaning; then twisting petals: putting the dried flower strips into a rolling machine for rolling for 30-40 minutes; drying at 50-60 deg.C; pulverizing into 60-100 mesh to obtain peony petal powder;
putting the peony petal powder into a round-bottom flask, adding a proper amount of 95% ethanol solution for mixing, performing ultrasonic vibration for 10-20 minutes, putting the mixture into a reaction kettle of a supercritical carbon dioxide extraction device, and performing continuous cyclic extraction by using a supercritical carbon dioxide fluid, wherein the extraction pressure is 15-20MPa, the extraction temperature is 35-45 ℃, and the extraction time is 2-3 hours; settling solid residues to the bottom of the pot, and separating oil to obtain peony wax;
step five, weighing nicotinamide, zinc oxide and titanium dioxide according to the formula, adding the nicotinamide, zinc oxide and titanium dioxide into a proper amount of 95% ethanol solution, and heating and grinding until the ethanol solution is completely volatilized to obtain mixed fine powder;
putting the beeswax, the peony seed peel wax and the peony flower wax into a water phase pot by taking the beeswax, the peony seed peel wax, the peony flower wax and the peony seed oil as substrates, heating the substrates in a water bath at 75-80 ℃ until the substrates are melted, and then adding the octyl methoxycinnamate, the butyl methoxydibenzoylmethane and the mixed fine powder of the zinc oxide, the titanium dioxide and the nicotinamide which are weighed according to the dosage, fully shaking up and mixing; then rapidly adding the resurrection lily rhizome extract, the chamomile extract and the honeysuckle extract into the matrix, and fully mixing and shaking up; after slightly cooling, adding the softening agent, the natural coloring agent and the natural essence, stirring and dissolving uniformly, and keeping the temperature for 10-15 minutes; putting into a mould, cooling to 30 deg.C, demolding and packaging.
The plant contains waxy components and other non-volatile fat-soluble components, the chemical components of the plant are lipid compounds of higher fatty acid and higher monohydric alcohol, the plant is a high molecular weight thermoplastic solid, the plant is a valuable component, the plant has certain physiological activity, and particularly is used in the lipstick, because the low melting point of the plant improves the diffusivity of a lipstick finished product, and brings more comfortable feeling to a user. The flower wax is used for protecting petals, the thicker the flower is like peony petals, the higher the content of the flower wax is, the main components of the flower wax are natural fatty acid and glyceride components, and contain a certain amount of phytosterol and flavonoid components with functions, and the plant wax components of peony seed peel wax and peony flower wax are added into the lipstick, so that the emulsifying function is improved, the moisture retention is enhanced, and the effects of inflammation resistance, whitening and oxidation resistance are achieved.
In addition, the extracted flower wax contains a small amount of octacosanol which is a naturally existing monohydric higher aliphatic alcohol, has good biodegradability, is easy to be absorbed and utilized by human bodies, has the main effects of actively promoting the physiological functions of the human bodies, improving the metabolism rate of the human bodies, promoting the circulation of skin blood and activating cells, and has the effects of diminishing inflammation and preventing and treating skin diseases.
Revival grass is a desert plant known for its ability to "revive" in the sun almost completely. Under the condition of extreme drought, branches and leaves of the composite plant can be tightly contracted into balls to firmly lock the precious last drop of water in the body, and the composite plant can still survive for decades even if the water content of the composite plant reaches 98 percent from the height, because the composite plant contains abundant glycosyl trehalose in the body, the composite plant can play a strong water locking and moisturizing function, then the water containing life activity is led into each cell in the body, the water which is 450 times of the weight of the cell is locked, and the composite plant extracting solution is beneficial to locking the water content and enhancing the moisturizing effect.
Octyl methoxycinnamate is an cinnamate ultraviolet absorbent, can effectively prevent ultraviolet rays with the wavelength of 280-320 nm, and has high absorptivity, no stimulation to skin and good safety. Butyl methoxy dibenzoyl methane is a dibenzoylmethane chemical absorbent, is the only UVA sunscreen agents with limited safety in the world at present, has strong absorption on ultraviolet wavelength (320-400 nm), can absorb high-energy ultraviolet rays and release energy in a low-energy ray mode, and therefore prevents the skin from being damaged by the ultraviolet rays. The zinc oxide is non-toxic, harmless and nonirritating, and has special effects of ultraviolet resistance, astringency, moistening, proper sterilization and the like; the titanium dioxide has stable property and has the effects of resisting ultraviolet radiation, bacteria, aging and the like; titanium dioxide and zinc oxide are used as physical sun-screening agents, and the physical sun-screening agent is high in safety and stability. The chemical absorbent and the physical shielding agent are used together as the sun-screening agent, so that the damage of ultraviolet rays in different wave bands can be effectively prevented, and the sun-screening effect of the lipstick is improved.
Nicotinamide, also known as vitamin pp or vitamin B3, is an important coenzyme in cells, has high safety, and has the sunscreen effect of resisting inflammation, resisting light radiation, repairing DNA (deoxyribonucleic acid) induced by ultraviolet rays and the like on skin; the physical sun-screening agent and the chemical sun-screening agent are combined to form a formula, and the restoration function of the nicotinamide is combined, so that a PFA + + protection factor is provided, nutrients are provided for the skin at any time, the skin aging phenomenon is improved, the comprehensive care of the physical sun-screening agent and the chemical sun-screening agent is realized through 'prevention, care and protection', so that the effects of effectively inhibiting pigmentation and improving the skin glossiness are achieved, and the lipstick is combined with multiple protection functions of sun-screening, moisture retention and basic care.
Wherein the granularity of the peony seed peel powder ground in the step one is 100-150 meshes; because the peony seed skin is hard in texture and relatively thick in cell wall, the cell wall of the peony seed skin cannot be completely broken through common crushing, the peony seed skin ultrafine powder is prepared by grinding, the cell wall of the peony seed skin can be completely broken, active ingredients in cells can be completely released, and the dissolution speed and dissolution rate of wax in the peony seed skin are improved.
Wherein the granularity of the peony petal powder crushed in the third step is 60-100 meshes; the effective medicinal components in the peony petal powder cells need to penetrate through a plurality of cell walls or even dozens of cell walls, and a part of cell components cannot penetrate through the cell walls, and the part can only be wasted, so that the effective components in the cells cannot be fully released.
The peony seed peel wax and peony flower wax are obtained by supercritical carbon dioxide extraction and separation, the critical temperature of the carbon dioxide is 31.05 ℃, SCF technical operation can be realized near room temperature, so that energy consumption is saved, and the supercritical fluid for supercritical fluid extraction is stable, safe and easy to operate and has certain solubility and good selectivity on an extracted substance. The extraction process of supercritical carbon dioxide extraction is low in temperature, and has the characteristics of safe medium, no toxicity, no residue, environmental protection and the like, the change property of carbon dioxide supercritical fluid to the solubility of substances along with the change of temperature and pressure is utilized, the extraction and separation are coupled into a whole, namely, a refined product can be separated while extraction is carried out, the natural aroma of natural perfume can be effectively kept when the supercritical carbon dioxide is used for extracting plant volatile components, and the loss of top aroma of essential oil and the change of chemical structure of a thermosensitive substance caused by the operation temperature of the traditional steam distillation are overcome. The oil content in the prepared wax is low, the wax meets the requirements of fine chemical raw materials, and the oil separated from the wax can be further recycled.
Ultrasonic vibration is adopted in the second step and the fourth step respectively, so that cell walls of peony seed peels and peony petals are broken, and flavonoids, polyphenols and other substances in cells are released. And by utilizing the superiority of combining the supercritical extraction and the ultrasonic technology, in the process of extracting the active effective components of the natural biological resources by the supercritical fluid, a good extraction effect can be obtained by adopting a strengthening measure to reduce the external diffusion resistance of the extraction, the extraction time is shortened, and the extraction efficiency is improved.
The invention provides a multi-effect protective lipstick containing peony moisturizing components and a preparation method thereof, organic plants such as peony seed skin and peony petals are used as main raw materials, and the multi-effect protective components are added, so that the multi-effect protective lipstick has the advantages of harmlessness, no toxicity, moisturizing, enhancement of the defense capacity of lip skin to ultraviolet rays, prevention of lip damage caused by dryness, cold, ultraviolet rays and the like, and repair damage and antibacterial effects; repairing damaged cells, activating cells, promoting lip skin metabolism, keeping lip skin tender, and delaying lip skin aging; the multi-effect protective lipstick has convenient use, high safety and advanced formulation; the preparation method is simple, convenient and safe, combines prevention and treatment, and has remarkable effect.
Detailed Description
The following detailed description of the embodiments of the present invention is provided in connection with specific examples, which are provided for illustration only and are not intended to limit the scope of the present invention. All other embodiments, which can be obtained by a person skilled in the art without inventive effort based on the embodiments of the present invention, are within the scope of the present invention.
The lipstick which can effectively moisten and play a multi-effect protection role is prepared by taking organic plants of natural sources as main raw materials, adding no artificial perfume or pigment and no petroleum component through efficient and reasonable formula matching.
Example 1
A multi-effect protective lipstick containing peony moisturizing components is prepared from the following raw materials in parts by weight: 20 parts of beeswax, 5 parts of peony seed skin wax, 5 parts of peony flower wax, 36 parts of peony seed oil, 8 parts of revived grass extract, 3 parts of chamomile extract, 4 parts of honeysuckle extract, 5 parts of mica powder, 2 parts of octyl methoxycinnamate, 3 parts of butyl methoxy dibenzoyl methane, 3 parts of nicotinamide, 3 parts of titanium dioxide and 3 parts of zinc oxide.
A preparation method of a multi-effect protective lipstick containing peony moisturizing components comprises the following steps:
collecting peony seed peels, cleaning, naturally airing on a net bed, and drying at 50-60 ℃; crushing into 150-mesh powder with the granularity of 100 meshes to obtain peony seed peel powder;
step two, mixing peony seed peel powder with a proper amount of 95% ethanol solution, performing ultrasonic vibration for 10 minutes, placing the mixture in a reaction kettle of a supercritical carbon dioxide extraction device, and performing continuous cyclic extraction by using a supercritical carbon dioxide fluid, wherein the extraction pressure is 15MPa, the extraction temperature is 35 ℃, and the extraction time is 2 hours; settling solid residues to the bottom of the tank, and separating oil to obtain peony seed husk wax;
picking the full-opened peony petals, splitting the peony petals into strips with the length of 1-2 cm and the width of 3-5 mm, cleaning the strips with clear water, and naturally airing the petals on a net bed after cleaning; then twisting petals: putting the dried flower strips into a rolling machine for rolling for 30 minutes; drying at 50-60 deg.C; pulverizing into 60-100 mesh to obtain peony petal powder;
putting the peony petal powder into a round-bottom flask, adding a proper amount of 95% ethanol solution, mixing, vibrating with ultrasonic waves for 10 minutes, putting the mixture into a reaction kettle of a supercritical carbon dioxide extraction device, and performing continuous cyclic extraction with a supercritical carbon dioxide fluid at an extraction pressure of 15MPa and an extraction temperature of 35 ℃ for 2 hours; settling solid residues to the bottom of the pot, and separating oil to obtain peony wax;
step five, weighing nicotinamide, zinc oxide and titanium dioxide according to the formula, adding the nicotinamide, zinc oxide and titanium dioxide into a proper amount of 95% ethanol solution, and heating and grinding until the ethanol solution is completely volatilized to obtain mixed fine powder;
putting the beeswax, the peony seed peel wax and the peony flower wax into a water phase pot by taking the beeswax, the peony seed peel wax, the peony flower wax and the peony seed oil as substrates, heating the substrates in a water bath at 75 ℃ to be molten, and then adding the octyl methoxycinnamate, the butyl methoxydibenzoylmethane and the mixed fine powder of the zinc oxide, the titanium dioxide and the nicotinamide which are weighed according to the dosage, fully shaking up and mixing; then rapidly adding the resurrection lily rhizome extract, the chamomile extract and the honeysuckle extract into the matrix, and fully mixing and shaking up; after slightly cooling, adding the softening agent, the natural coloring agent and the natural essence, stirring and dissolving uniformly, and keeping the temperature for 10 minutes; putting into a mould, cooling to 30 deg.C, demolding and packaging.
Example 2
A multi-effect protective lipstick containing peony moisturizing components is prepared from the following raw materials in parts by weight: 25 parts of beeswax, 10 parts of peony seed skin wax, 10 parts of peony flower wax, 40 parts of peony seed oil, 5 parts of revived grass extract, 1 part of chamomile extract, 2 parts of honeysuckle extract, 2 parts of mica powder, 1 part of octyl methoxycinnamate, 1 part of butyl methoxy dibenzoyl methane, 1 part of nicotinamide, 1 part of titanium dioxide and 1 part of zinc oxide.
A preparation method of a multi-effect protective lipstick containing peony moisturizing components comprises the following steps:
collecting peony seed peels, cleaning, naturally airing on a net bed, and drying at 50-60 ℃; crushing into 150-mesh powder with the granularity of 100 meshes to obtain peony seed peel powder;
step two, mixing peony seed peel powder with a proper amount of 95% ethanol solution, performing ultrasonic vibration for 30 minutes, placing the mixture in a reaction kettle of a supercritical carbon dioxide extraction device, and performing continuous cyclic extraction by using a supercritical carbon dioxide fluid, wherein the extraction pressure is 25MPa, the extraction temperature is 50 ℃, and the extraction time is 4 hours; settling solid residues to the bottom of the tank, and separating oil to obtain peony seed husk wax;
picking the full-opened peony petals, splitting the peony petals into strips with the length of 1-2 cm and the width of 3-5 mm, cleaning the strips with clear water, and naturally airing the petals on a net bed after cleaning; then twisting petals: putting the dried flower strips into a rolling machine for rolling for 40 minutes; drying at 50-60 deg.C; pulverizing into 60-100 mesh to obtain peony petal powder;
putting the peony petal powder into a round-bottom flask, adding a proper amount of 95% ethanol solution for mixing, performing ultrasonic vibration for 20 minutes, putting the mixture into a reaction kettle of a supercritical carbon dioxide extraction device, and performing continuous cyclic extraction by using a supercritical carbon dioxide fluid, wherein the extraction pressure is 20MPa, the extraction temperature is 45 ℃, and the extraction time is 3 hours; settling solid residues to the bottom of the pot, and separating oil to obtain peony wax;
step five, weighing nicotinamide, zinc oxide and titanium dioxide according to the formula, adding the nicotinamide, zinc oxide and titanium dioxide into a proper amount of 95% ethanol solution, and heating and grinding until the ethanol solution is completely volatilized to obtain mixed fine powder;
putting the beeswax, the peony seed peel wax and the peony flower wax into a water phase pot by taking the beeswax, the peony seed peel wax, the peony flower wax and the peony seed oil as substrates, heating the substrates in a water bath at 80 ℃ to be molten, and then adding the octyl methoxycinnamate, the butyl methoxydibenzoylmethane and the mixed fine powder of the zinc oxide, the titanium dioxide and the nicotinamide which are weighed according to the dosage, fully shaking up and mixing; then rapidly adding the resurrection lily rhizome extract, the chamomile extract and the honeysuckle extract into the matrix, and fully mixing and shaking up; after slightly cooling, adding the softening agent, the natural coloring agent and the natural essence, stirring and dissolving uniformly, and keeping the temperature for 15 minutes; putting into a mould, cooling to 30 deg.C, demolding and packaging.
Example 3
A multi-effect protective lipstick containing peony moisturizing components is prepared from the following raw materials in parts by weight: 20 parts of beeswax, 8 parts of peony seed peel wax, 8 parts of peony flower wax, 35 parts of peony seed oil, 8 parts of revived grass extract, 3 parts of chamomile extract, 4 parts of honeysuckle extract, 3 parts of mica powder, 2 parts of octyl methoxycinnamate, 3 parts of butyl methoxy dibenzoyl methane, 2 parts of nicotinamide, 2 parts of titanium dioxide and 2 parts of zinc oxide.
A preparation method of a multi-effect protective lipstick containing peony moisturizing components comprises the following steps:
collecting peony seed peels, cleaning, naturally airing on a net bed, and drying at 50-60 ℃; crushing into 150-mesh powder with the granularity of 100 meshes to obtain peony seed peel powder;
step two, mixing peony seed peel powder with a proper amount of 95% ethanol solution, performing ultrasonic vibration for 20 minutes, placing the mixture in a reaction kettle of a supercritical carbon dioxide extraction device, and performing continuous cyclic extraction by using a supercritical carbon dioxide fluid, wherein the extraction pressure is 20MPa, the extraction temperature is 40 ℃, and the extraction time is 3 hours; settling solid residues to the bottom of the tank, and separating oil to obtain peony seed husk wax;
picking the full-opened peony petals, splitting the peony petals into strips with the length of 1-2 cm and the width of 3-5 mm, cleaning the strips with clear water, and naturally airing the petals on a net bed after cleaning; then twisting petals: putting the dried flower strips into a rolling machine for rolling for 35 minutes; drying at 50-60 deg.C; pulverizing into 60-100 mesh to obtain peony petal powder;
putting the peony petal powder into a round-bottom flask, adding a proper amount of 95% ethanol solution for mixing, performing ultrasonic vibration for 15 minutes, putting the mixture into a reaction kettle of a supercritical carbon dioxide extraction device, and performing continuous cyclic extraction by using a supercritical carbon dioxide fluid, wherein the extraction pressure is 18MPa, the extraction temperature is 40 ℃, and the extraction time is 3 hours; settling solid residues to the bottom of the pot, and separating oil to obtain peony wax;
step five, weighing nicotinamide, zinc oxide and titanium dioxide according to the formula, adding the nicotinamide, zinc oxide and titanium dioxide into a proper amount of 95% ethanol solution, and heating and grinding until the ethanol solution is completely volatilized to obtain mixed fine powder;
putting the beeswax, the peony seed peel wax and the peony flower wax into a water phase pot by taking the beeswax, the peony seed peel wax, the peony flower wax and the peony seed oil as substrates, heating the substrates in a water bath at 78 ℃ to melt, and then adding the octyl methoxycinnamate, the butyl methoxydibenzoylmethane and the mixed fine powder of the zinc oxide, the titanium dioxide and the nicotinamide which are weighed according to the dosage, fully shaking up and mixing; then rapidly adding the resurrection lily rhizome extract, the chamomile extract and the honeysuckle extract into the matrix, and fully mixing and shaking up; after slightly cooling, adding the softening agent, the natural coloring agent and the natural essence, stirring and dissolving uniformly, and keeping the temperature for 12 minutes; putting into a mould, cooling to 30 deg.C, demolding and packaging.
The lipsticks prepared in the above examples were tested, and two samples were prepared for each example, wherein samples Nos. 1-1 and 1-2 correspond to example 1; samples Nos. 2-1 and 2-2 correspond to example 2; samples No. 3-1 and 3-2 correspond to example 3.
1. Product safety assessment
(1) Subject: for a total of 30 people, 6 men and 24 women, the age is 25-35 years.
(2) The spot test method comprises the following steps: selecting a qualified spot tester, applying about 0.02-0.025 ml of a test object into the spot tester by a closed spot test method, externally applying a special adhesive tape to the curved side of the forearm of a subject, removing the test object after 24 hours, observing skin reaction 30min after the spot tester of the test object is removed, and recording the result according to the skin reaction grading standard in the cosmetic hygiene Specification (2007 edition).
(3) And (4) evaluating the results: the results were recorded as in Table 1 (grading Standard for adverse skin reactions).
Product safety evaluation results
As can be seen from the table, only 1 of 30 persons showed weak erythema reaction, and the product safety evaluation was qualified.
2. Product stability evaluation
(1) Quality stability check
The quality stability test includes 5 items of appearance stability test, cold resistance test, heat resistance test, illumination test and centrifugation test.
And (3) checking appearance stability: the glossiness of the appearance is good when the lipstick is observed, no bubbles appear on the surface, a small amount of finished lipstick is uniformly smeared on the face tissues, and the phenomenon that oil stains are diffused is observed.
Cold resistance test: taking two lipstick products, putting into a constant temperature freezer at-18 ℃, taking out after 24h, and the lipstick has no phenomena of water seepage, deformation and fracture.
Heat resistance test: taking two lipstick products, putting into a constant temperature box of 45 ℃, taking out after 24 hours, wherein the lipstick bodies are free from water seepage, deformation and fracture.
And (3) illumination experiment: placing a small amount of the finished product in a colorless closed container, and irradiating for 24h, 72h, 120h, 168h and 216h under natural light condition to observe the color, wherein the color is stable.
And (3) centrifugal experiment: and (3) placing a small amount of finished lip balm products in a centrifuge, adjusting to 5000r/min, centrifuging for 15min, and ensuring that the shape of the cream is complete and no layering phenomenon occurs.
(2) Evaluation results of lipstick appearance, color, hardness and spreadability indexes
3. The product has the use effect:
the lipstick product made from example 3 was used daily for three months by 30 women between the ages of 20 and 55 years, the use feedback being: the lipstick has good skin feeling and can be comfortable and moist for a long time. The natural moisturizing multi-effect protective lipstick provided by the invention is quite good in aspects of appearance, smell, color, smearing property, decoration and the like, and also good in aspects of moisturizing property, moistening property, trophism, repairability, safety and the like, and is proved to be capable of continuously caring the lip skin, having ultraviolet protection and repair functions, improving the lip skin and having a better effect after long-term use.
Claims (4)
1. A multi-effect protective lipstick containing peony moisturizing components is characterized in that: the feed is prepared from the following raw materials in parts by weight: 15-25 parts of beeswax, 5-10 parts of peony seed peel wax, 5-10 parts of peony flower wax, 30-40 parts of peony seed oil, 5-8 parts of revived grass extract, 1-3 parts of chamomile extract, 2-4 parts of honeysuckle extract, 2-5 parts of mica powder, 1-2 parts of octyl methoxycinnamate, 1-3 parts of butyl methoxy dibenzoyl methane, 1-3 parts of nicotinamide, 1-3 parts of titanium dioxide and 1-3 parts of zinc oxide.
2. A preparation method of a multi-effect protective lipstick containing peony moisturizing components is characterized by comprising the following steps:
collecting peony seed peels, cleaning, naturally airing on a net bed, and drying at 50-60 ℃; crushing into 150-mesh powder with the granularity of 100 meshes to obtain peony seed peel powder;
step two, mixing peony seed peel powder with a proper amount of 95% ethanol solution, performing ultrasonic vibration for 10-30 minutes, placing the mixture in a reaction kettle of a supercritical carbon dioxide extraction device, performing continuous cyclic extraction by using a supercritical carbon dioxide fluid, settling solid residues to the bottom of a tank, and separating oil to obtain peony seed peel wax;
picking the full-opened peony petals, splitting the peony petals into strips with the length of 1-2 cm and the width of 3-5 mm, cleaning the strips with clear water, and naturally airing the petals on a net bed after cleaning; then twisting petals: putting the dried flower strips into a rolling machine for rolling for 30-40 minutes; drying at 50-60 deg.C; pulverizing into 60-100 mesh to obtain peony petal powder;
putting the peony petal powder into a round-bottom flask, adding a proper amount of 95% ethanol solution, mixing, performing ultrasonic vibration for 10-20 minutes, putting the mixture into a reaction kettle of a supercritical carbon dioxide extraction device, performing continuous cyclic extraction by using a supercritical carbon dioxide fluid, settling solid residues to the bottom of the kettle, and separating oil to obtain peony flower wax;
step five, weighing nicotinamide, zinc oxide and titanium dioxide according to the formula, adding the nicotinamide, zinc oxide and titanium dioxide into a proper amount of 95% ethanol solution, and heating and grinding until the ethanol solution is completely volatilized to obtain mixed fine powder;
putting the beeswax, the peony seed peel wax and the peony flower wax into a water phase pot by taking the beeswax, the peony seed peel wax, the peony flower wax and the peony seed oil as substrates, heating the substrates in a water bath at 75-80 ℃ until the substrates are melted, and then adding the octyl methoxycinnamate, the butyl methoxydibenzoylmethane and the mixed fine powder of the zinc oxide, the titanium dioxide and the nicotinamide which are weighed according to the dosage, fully shaking up and mixing; then rapidly adding the resurrection lily rhizome extract, the chamomile extract and the honeysuckle extract into the matrix, and fully mixing and shaking up; after slightly cooling, adding the softening agent, the natural coloring agent and the natural essence, stirring and dissolving uniformly, and keeping the temperature for 10-15 minutes; putting into a mould, cooling to 30 deg.C, demolding and packaging.
3. The preparation method of the multi-effect protective lipstick containing peony moisturizing ingredients as claimed in claim 2, wherein the preparation method comprises the following steps: in the second step, the peony seed peel powder is subjected to supercritical carbon dioxide extraction at the extraction pressure of 15-25MPa, the extraction temperature of 35-55 ℃ and the extraction time of 2-4 hours.
4. The preparation method of the multi-effect protective lipstick containing peony moisturizing ingredients as claimed in claim 2, wherein the preparation method comprises the following steps: the extraction pressure of the peony petal powder in the fourth step is 15-20MPa, the extraction temperature is 35-45 ℃, and the extraction time is 2-3 hours.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN115531261A (en) * | 2022-08-31 | 2022-12-30 | 洛阳古草生物科技有限公司 | Pure natural peony moisturizing lipstick and preparation method thereof |
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Application publication date: 20211207 |