CN108175726A - A kind of preparation method of the wax of seed peel containing tree peony and tree peony floral wax lipstick - Google Patents

A kind of preparation method of the wax of seed peel containing tree peony and tree peony floral wax lipstick Download PDF

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Publication number
CN108175726A
CN108175726A CN201711469559.9A CN201711469559A CN108175726A CN 108175726 A CN108175726 A CN 108175726A CN 201711469559 A CN201711469559 A CN 201711469559A CN 108175726 A CN108175726 A CN 108175726A
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Prior art keywords
tree peony
wax
peony
seed peel
lipstick
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CN201711469559.9A
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Inventor
杨永庆
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HENAN LUOYANG HONGMUDAN INDUSTRIAL R&D Co Ltd
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HENAN LUOYANG HONGMUDAN INDUSTRIAL R&D Co Ltd
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Priority to CN201711469559.9A priority Critical patent/CN108175726A/en
Publication of CN108175726A publication Critical patent/CN108175726A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02Preparations containing skin colorants, e.g. pigments
    • A61Q1/04Preparations containing skin colorants, e.g. pigments for lips
    • A61Q1/06Lipsticks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/001Preparations for care of the lips
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/82Preparation or application process involves sonication or ultrasonication

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Dermatology (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses the preparation methods of a kind of wax of seed peel containing tree peony and tree peony floral wax lipstick, it is primary raw material using tree peony seed peel and peony petal, it takes mechanical extraction technique and zymolysis technique extraction process is combined technique, with the tree peony fragrance of a flower, heavy metal free, it is harmless, it is nontoxic, it is hypo-allergenic, moisturizing moisturizing, enhance skin elasticity, strengthen skin natural protection ability, and be suitble to crowd use the advantages that the wax of seed peel containing tree peony and tree peony floral wax lipstick and preparation method, and additional income will be brought to tree peony farmer, this by be tree peony process deeply industry new approaches and new issue.

Description

A kind of preparation method of the wax of seed peel containing tree peony and tree peony floral wax lipstick
Technical field
The present invention relates to a kind of lipstick, more particularly to a kind of harmless, nontoxic, hypo-allergenic wax of seed peel containing tree peony and tree peony The lipstick and preparation method of floral wax.
Background technology
Lipstick is to make lip ruddy glossy, reaches moist, protection lip, and increasing facial aesthetic feeling and correcting lip outline has A kind of product of effect is set off, is one of the cosmetics of women indispensability, it is sexy, charming that women can be showed.
The base-material of manufacture lipstick is oil, grease and wax;Oil, based on the high viscosity castor oil of good adhesion, but in recent years Come it is rancid smelly to solve the problems, such as, mostly using it is similar to castor oil structure, to oxidation-stabilized synthetic oil.Lipstick will have Good companding, for the ease of gently drawing, generally with low viscosities such as isopropyl myristate, glyceryl triisostearates Synthesis ester oil is used in combination with high-viscosity oil.Wax is the fusing point in order to improve product, keeps rod-like morphology.Use a small amount of babassu Wax, candelila wax can improve the hardness of stick, make stick surface more bright.Lanolin and lanolin derivative can make oils and wax Class is easily mixed, and contributes to the dispersion of dyestuff, can be made into the uniform and sturdy lipstick of color;And lanolin complicated component, to mistake The people of quick constitution easily causes allergic reaction;In addition, lanolin have stronger adsorptivity, can by air dust, bacterium, The molecule of the harmful substances such as virus is adsorbed on lip mucosa, stimulation part.This not only adds cause allergy chance, And when people is when drinking water, feeding, by lipstick and attachment above band import, accumulate over a long period, these harmful substances are in vivo Accumulation, potential eutrophication is caused to body.
Since skin care lipstick is more or less on the market, all containing some chemical substances, therefore consumer increasingly favor in Lipstick prepared by natural material.
In recent years, China greatly develops and plants tree peony, and including phoenix Varieties of Peony, the plan of the Ministry of Agriculture of China strives 2020 Year, the plantation of tree peony reaches 1,000 ten thousand mu, and the planting site of tree peony is mostly knob, however, knob is all poor area, Young and middle-aged labour largely flow to developed regions, and remaining labour is mostly weaker labour, such as to be planted general Agricultural plant needs a large amount of labour, but if plantation tree peony, primary to plant, can obtain the picking time of 30-40, not only saves Power, and economic well-being of workers and staff harvest is larger.So, usually when planting tree peony, peony seeds can make oil, flower, root, the stem of tree peony It can be used as medicine, make full use of carry out deep processing by people, with requirement of the people to healthy living, now in peony seeds When squeezing edible oil, the casting skin that peony seeds wrap up is often required to remove, it is a large amount of so as to produce to pursue the oil plant of high-quality Casting skin, but the casting skin of peony seeds package is not used now, however the casting skin of peony seeds package is rich in anti-oxidant, anti- The same substance of the grease of radiation.
Not only fragrance is pleasant for peony, more containing abundant nutriment, containing 13 kinds of amino acid, has 8 kinds for needed by human body, And content is more, has the function of health care to human body, it is safe and free of toxic and side effects;And have on peony a thin layer of Ceride, this layer of ceride have natural skin care effect.
Therefore, if the lipstick of raw material being wanted to prepare based on tree peony seed peel can be produced, will turn waste into wealth, it is used to make the best, To bring additional income to farmer, this by be tree peony process deeply industry new approaches and new issue.
Invention content
The purpose of the present invention is to solve deficiencies existing for above-mentioned technical problem, provide a kind of utilize based on tree peony seed peel Want raw material, take mechanical extraction technique and zymolysis technique extraction process is combined technique, have heavy metal free, it is harmless, nontoxic, Containing for the advantages that hypo-allergenic, moisturizing moisturizing enhancing skin elasticity, strengthens skin natural protection ability, and suitable crowd uses is male The lipstick and preparation method of red seed peel.
The technical solution adopted in the present invention is that the preparation method of a kind of wax of seed peel containing tree peony and tree peony floral wax lipstick is:
Step 1: collecting tree peony seed peel, cleaned, the naturally dry in net bed is dried under 50-60 °C;It is ground into granularity For 200-300 mesh, tree peony seed peel powder is obtained;
Step 2: tree peony seed peel powder is impregnated 5-8 hour, stirred with being that the pure water of 5-6 times of mixed powder total weight is impregnated 0.2-1 hours, carry out vibration of ultrasonic wave 10-30 minutes, mixture with distillate is squeezed into and stirred after centrifugal dehydration by a certain percentage It mixes blending tank to be preheated, forms the preferable mixture of uniform mobility, after steam heats, be sent into extraction tower and extracted Dehydration is taken, mixture is discharged into the laggard gun barrel of condenser, oil and solid slag from tower top and enters settling tank progress with distillate Separation, solid slag sink to tank bottom, grease are separated, and obtain tree peony seed peel wax;
Step 3: peony petal in full bloom is picked, the strip of 1-2 centimetres long 3-5 millimeters of width is split into, is carried out with clear water Cleaning, naturally dry in net bed is placed on after cleaning by petal;Then petal is rubbed:Flower item after drying be put into rolling machine into Row is rubbed 30-40 minutes;It is dried under 50-60 °C;50-180 mesh is ground into, obtains peony petal powder;
Step 4: peony petal powder is put into Soxhlet extractor, appropriate small polar solvent is added in the round-bottomed flask of bottom, is carried out Vibration of ultrasonic wave 20-30 minutes, heating water bath extracts repeatedly;Extraction finishes, and extracting solution is evaporated under reduced pressure and removes solvent up to male Red petal wax;
Step 5: by tree peony seed peel wax, peony petal wax, softening agent, natural colorant, olive oil, natural essence is added to water In phase pot, 75-80 degree is heated, stirring and dissolving is uniform, keeps the temperature 10-15 minutes;It being put into the mold of lipstick, temperature is down to 30 degree, Depanning is packed.
Peony seeds Powder Particle Size 200-300 mesh after being ground wherein in step 1;Because peony seeds quality is hard, cell wall Compare thick, general crushing can not break the cell wall of tree peony powder of seeds completely, and the present invention is reached by way of grinding Ultramicro-powder can be completely severed the cell wall of tree peony powder of seeds, and intracellular active ingredient is made all fully to release, and Also improve the dissolution rate and dissolution rate of peony seeds wax in peony seeds.
Wherein step 2 uses vibration of ultrasonic wave 10-30 minutes, is in order to which the cell wall of peony seeds is broken, it is allowed to discharge The medical substance of cell interior.
Peony petal Powder Particle Size 50-180 mesh after being crushed wherein in step 3;It is effectively medicinal in peony petal flour cell The dissolution of composition needs guiding through several or even dozens of cell wall, and quite a few Cell Component can not possibly pass through cell wall, This part can only waste, therefore intracellular active ingredient can not be made all fully to release, and the present invention passes through The mode of crushing makes intracellular active ingredient all fully release, so as to improve the drug availability of peony petal powder, But also improve the dissolution rate and dissolution rate of peony petal wax in peony petal.
Wherein step 4 uses vibration of ultrasonic wave 20-30 minutes, is to break the cell wall of peony petal, it is allowed to release Put the substances such as flavonoids, the polyphenol of cell interior.
Beneficial effects of the present invention:The present invention provides the preparation method of a kind of wax of seed peel containing tree peony and tree peony floral wax lipstick, It is primary raw material using tree peony seed peel and peony petal, takes mechanical extraction technique and zymolysis technique extraction process is combined work Skill has the tree peony fragrance of a flower, heavy metal free, harmless, nontoxic, hypo-allergenic, moisturizing moisturizing, enhances skin elasticity, and it is natural to strengthen skin Defence capability, and the wax of seed peel containing tree peony and the lipstick and preparation method of tree peony floral wax the advantages that suitable crowd's use.
Specific embodiment
The specific embodiment of the present invention is described in further detail below in conjunction with specific embodiment, embodiment is only used In illustrating the present invention rather than limit the scope of the invention.
Embodiment 1
The preparation method of a kind of wax of seed peel containing tree peony and tree peony floral wax lipstick is:
Step 1: collecting tree peony seed peel, cleaned, the naturally dry in net bed is dried under 50-60 °C;It is ground into granularity For 200-300 mesh, tree peony seed peel powder is obtained;
Step 2: tree peony seed peel powder is impregnated 8 hours, stirring 1 with being that the pure water of 5-6 times of mixed powder total weight is impregnated Hour, carry out vibration of ultrasonic wave 30 minutes, mixture squeezes into auger tank by a certain percentage after centrifugal dehydration, with distillate It is preheated, forms the preferable mixture of uniform mobility, after steam heats, be sent into extraction tower and carry out extraction dehydration, Mixture is discharged into the laggard gun barrel of condenser from tower top, and oil and solid slag enter settling tank with distillate and detached, Gu Body slag sinks to tank bottom, and grease is separated, and obtains tree peony seed peel wax;
Step 3: peony petal in full bloom is picked, the strip of 1-2 centimetres long 3-5 millimeters of width is split into, is carried out with clear water Cleaning, naturally dry in net bed is placed on after cleaning by petal;Then petal is rubbed:Flower item after drying be put into rolling machine into Row is rubbed 30-40 minutes;It is dried under 60 °C;50-180 mesh is ground into, obtains peony petal powder;
Step 4: peony petal powder is put into Soxhlet extractor, appropriate small polar solvent is added in the round-bottomed flask of bottom, is carried out Vibration of ultrasonic wave 20 minutes, heating water bath extracts repeatedly;Extraction finishes, and extracting solution is evaporated under reduced pressure and removes solvent up to peony Valve wax;
Step 5: by tree peony seed peel wax, peony petal wax, softening agent, natural colorant, olive oil, natural essence is added to water In phase pot, 80 degree are heated, stirring and dissolving is uniform, keeps the temperature 15 minutes;It is put into the mold of lipstick, temperature is down to 30 degree, depanning packet Dress.
Embodiment 2
The preparation method of a kind of wax of seed peel containing tree peony and tree peony floral wax lipstick is:
Step 1: collecting tree peony seed peel, cleaned, the naturally dry in net bed is dried under 50-60 °C;It is ground into granularity For 200-300 mesh, tree peony seed peel powder is obtained;
Step 2: tree peony seed peel powder is impregnated 8 hours, stirring 0.2 with being that the pure water of 6 times of mixed powder total weight is impregnated Hour, carry out vibration of ultrasonic wave 10 minutes, mixture squeezes into auger tank by a certain percentage after centrifugal dehydration, with distillate It is preheated, forms the preferable mixture of uniform mobility, after steam heats, be sent into extraction tower and carry out extraction dehydration, Mixture is discharged into the laggard gun barrel of condenser from tower top, and oil and solid slag enter settling tank with distillate and detached, Gu Body slag sinks to tank bottom, and grease is separated, and obtains tree peony seed peel wax;
Step 3: peony petal in full bloom is picked, the strip of 1-2 centimetres long 3-5 millimeters of width is split into, is carried out with clear water Cleaning, naturally dry in net bed is placed on after cleaning by petal;Then petal is rubbed:Flower item after drying be put into rolling machine into Row is rubbed 30 minutes;It is dried under 50-60 °C;50-180 mesh is ground into, obtains peony petal powder;
Step 4: peony petal powder is put into Soxhlet extractor, appropriate small polar solvent is added in the round-bottomed flask of bottom, is carried out Vibration of ultrasonic wave 20 minutes, heating water bath extracts repeatedly;Extraction finishes, and extracting solution is evaporated under reduced pressure and removes solvent up to peony Valve wax;
Step 5: by tree peony seed peel wax, peony petal wax, softening agent, natural colorant, olive oil, natural essence is added to water In phase pot, 75 degree are heated, stirring and dissolving is uniform, keeps the temperature 10 minutes;It is put into the mold of lipstick, temperature is down to 30 degree, depanning packet Dress.

Claims (3)

1. a kind of preparation method of wax of seed peel containing tree peony and tree peony floral wax lipstick, it is characterised in that:Step 1: collect peony seeds Skin is cleaned, and the naturally dry in net bed is dried under 50-60 °C;Crushing obtains tree peony seed peel powder;Step 2: tree peony Seed peel powder is impregnated 5-8 hour with being that the pure water of 5-6 times of mixed powder total weight is impregnated, and stirring 0.2-1 hours is surpassed Acoustic wave vibrations 10-30 minutes, mixture after centrifugal dehydration, with distillate squeeze into auger tank and carry out pre-add by a certain percentage Heat forms the preferable mixture of uniform mobility, after steam heats, is sent into extraction tower and carries out extraction dehydration, mixture from Tower top is discharged into the laggard gun barrel of condenser, and oil and solid slag enter settling tank with distillate and detached, and solid slag is sunk to Tank bottom separates grease, obtains tree peony seed peel wax;Step 3: peony petal in full bloom is picked, it is split into long 1-2 Centimetre, the strip of 3-5 millimeters of width, cleaned with clear water, petal be placed on naturally dry in net bed after cleaning;Then flower is rubbed Valve:Flower item after drying, which is put into rolling machine, rub 30-40 minutes;It is dried under 50-60 °C;Crushing obtains peony Valve powder;Step 4: peony petal powder is put into Soxhlet extractor, appropriate small polar solvent is added in the round-bottomed flask of bottom, into Row vibration of ultrasonic wave 20-30 minutes, heating water bath extracts repeatedly;Extraction finishes, and extracting solution is evaporated under reduced pressure and removes solvent to obtain the final product Peony petal wax;Step 5: by tree peony seed peel wax, peony petal wax, softening agent, natural colorant, olive oil, natural perfume finishing Enter into water phase pot, heat 75-80 degree, stirring and dissolving is uniform, keeps the temperature 10-15 minutes;It is put into the mold of lipstick, temperature is down to 30 degree, depanning packaging.
2. the preparation method of a kind of wax of seed peel containing tree peony according to claim 1 and tree peony floral wax lipstick, it is characterised in that: Tree peony seed peel Powder Particle Size in step 1 is 200-300 mesh.
3. the preparation method of a kind of wax of seed peel containing tree peony according to claim 1 and tree peony floral wax lipstick, it is characterised in that: Peony petal Powder Particle Size in step 3 is 50-180 mesh.
CN201711469559.9A 2017-12-29 2017-12-29 A kind of preparation method of the wax of seed peel containing tree peony and tree peony floral wax lipstick Pending CN108175726A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111773817A (en) * 2020-07-13 2020-10-16 哈尔滨禄远科技有限公司 Skin cream and preparation system and preparation method thereof
CN113749991A (en) * 2021-09-03 2021-12-07 洛阳红牡丹产业科技发展有限公司 Multi-effect protective lipstick containing peony moisturizing components and preparation method thereof
CN115531261A (en) * 2022-08-31 2022-12-30 洛阳古草生物科技有限公司 Pure natural peony moisturizing lipstick and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1074601A (en) * 1992-01-25 1993-07-28 刘国荣 Natural colour lipstick
CN104887598A (en) * 2015-05-14 2015-09-09 北京同仁堂安徽中药材有限公司 Peony Chinese herbal medicine lipstick and preparation method thereof
CN105662923A (en) * 2016-01-22 2016-06-15 武汉市农业科学技术研究院林业果树科学研究所 Pure natural multi-effect repairing color-variable lip balm with peony seed oil and method for preparing pure natural multi-effect repairing color-variable lip balm

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1074601A (en) * 1992-01-25 1993-07-28 刘国荣 Natural colour lipstick
CN104887598A (en) * 2015-05-14 2015-09-09 北京同仁堂安徽中药材有限公司 Peony Chinese herbal medicine lipstick and preparation method thereof
CN105662923A (en) * 2016-01-22 2016-06-15 武汉市农业科学技术研究院林业果树科学研究所 Pure natural multi-effect repairing color-variable lip balm with peony seed oil and method for preparing pure natural multi-effect repairing color-variable lip balm

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111773817A (en) * 2020-07-13 2020-10-16 哈尔滨禄远科技有限公司 Skin cream and preparation system and preparation method thereof
CN111773817B (en) * 2020-07-13 2021-12-03 汕头市深特宝洁实业有限公司 Skin cream and preparation system and preparation method thereof
CN113749991A (en) * 2021-09-03 2021-12-07 洛阳红牡丹产业科技发展有限公司 Multi-effect protective lipstick containing peony moisturizing components and preparation method thereof
CN115531261A (en) * 2022-08-31 2022-12-30 洛阳古草生物科技有限公司 Pure natural peony moisturizing lipstick and preparation method thereof

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