CN107034051B - One kind is containing amygdalate hair soap and preparation method thereof - Google Patents
One kind is containing amygdalate hair soap and preparation method thereof Download PDFInfo
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- CN107034051B CN107034051B CN201710319521.7A CN201710319521A CN107034051B CN 107034051 B CN107034051 B CN 107034051B CN 201710319521 A CN201710319521 A CN 201710319521A CN 107034051 B CN107034051 B CN 107034051B
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
Abstract
The invention discloses one kind containing amygdalate hair soap and preparation method thereof.The hair soap is composed of the following components by weight percentage: semen armeniacae amarae 10-55%, chlorogenic acid 1-5%, plant soap base 40-89%.Preparation method includes the following steps: (1) crushing semen armeniacae amarae, cross 12-100 mesh, obtain semen armeniacae amarae fine powder；(2) caustic alkali is soluble in water, it mixes, stirs evenly with vegetable oil, in 50-95 DEG C of progress saponification, reaction time 30-60min；(3) obtained plant soap base is cooled to 40-45 DEG C, semen armeniacae amarae fine powder and chlorogenic acid is added thereto according to the ratio, is uniformly mixed；(4) gained mixture is poured into mold, is placed until natural coagulation, sets shady place storage.The hair soap is pure natural, and quality is stablized, and preparation process is simple, at low cost, has effects that obviously profit hair.
Description
Technical field
The present invention relates to one kind containing amygdalate hair soap and preparation method thereof.
Background technique
Hair refers to the hair with back side of head position overhead.Hair can be divided into from bottom to top papilla, hair follicle, hair root and
Four parts of hair shaft.The physiological characteristic and function of hair depend primarily on scalp epidermis papilla below, hair follicle and sebaceous glands
Deng.Hair is withered to refer to that hair dries out and grease moistens, and hair is caused dry up frangibility, and hair tail bifurcated occurs and shows
As being phenomenon common at present.Hair is withered closely related with the function of human body viscera.Insufficiency of vital energy and blood in human body, viscera function
Imbalance, can all be such that hair loses and support, and cause hair withered.Furthermore cause dry hair related to following factors: not such as nutrition
Good, trophic disturbance, vitamin A deficiency, protein shortage etc.；It is inherent cause, the infringement of atmosphere pollution, solarization, ultraviolet in sunlight
The injury of line, the injury of chemicals, such as hair dyeing, hair-waving, blowing hot wind；Extended sleep is insufficient and excessive fatigue；Excessive smoking；Certain
The injury of a little diseases, such as anaemia, low potassium.
Dry hair is treated frequently with the methods of oral medicinal herb, the external application of Chinese medicine, catering therapy, massage, hair washing link
Also more important.Major daily use chemicals manufacturing enterprise, the world focuses on exploitation profit hair product, the shampoo with moisturizing profit hair function very much
Product up to hundreds of.
Semen armeniacae amarae is rosaceous plant ansu apricot, and summer harvests ripening fruits, removes pulp and nucleocapsid, takes out seed, dries.
Alias: almond.Curing mainly function has that sending down abnormally ascending is relieving cough and asthma, relax bowel and defecation.For cough and asthma, fullness sensation in chest abundant expectoration, deficiency of blood saliva is withered, intestinal dryness
Constipation.But be also it is toxic, more clothes can then be poisoned, few to take then heat-clearing.Semen armeniacae amarae is in flat heart, long 1~1.9cm, wide by 0.8~
1.5cm, 0.5~0.8cm of thickness.Surface yellowish-brown is to dark-brown, and one end point, another end blunt circle, plumpness are left-right asymmetry.Tip one
There is short-term shape hilum in side, has most dark-brown veins upwards at nose circle chalaza.Kind thin skin, cotyledon 2, milky are High oleic.Nothing
It is smelly, bitter.
Amygdalate chemical component contains amygdalin (amygdalin) about 3%, fat oil about 50%, and contains emulsin
(emulsin), amygdalase (amygdalase), prunase (prunase), oxynitrilase (oxynitrilase), Yi Jike
Soluble proteins.After seed is ground plus water is placed, and amygdalin is generated hydrogen cyanide, benzaldehyde and Portugal by the effect of emulsin
Grape sugar.Amygdalate toxicity hydrolyzes the hydrogen cyanide released from amygdalin.There is the document report to be to hydrogen cyanide content
0.1399% semen armeniacae amarae is impregnated 10 minutes with 60 DEG C of warm water, pulls rear peeling out and dry, hydrogen cyanide content is just fallen to
0.0667%.
Chlorogenic acid, 1,3,4,5- tetrahydroxy cyclohexane-carboxylic acid of chemical name-(3,4-dihydroxycinnamic acid ester).Molecular formula
For C16H18O9, molecular weight 354.31.Plant origin is the leaf of Eucommiaceae plant Cortex Eucommiae Eucommia ulmoides Oliv.,
Caprifoliaceae plant honeysuckle Lonicera japonica Thumb., Cortex Eucommiae Cortex Eucommiae lonicera hypoglauca miq Lonicera hypoglauca
Miq., the dry flower of Honeysuckle flower Lonicera confusa DC. or hair style honeysuckle Lonicera dasytyla Rehd.
Or with the flower just opened.Chlorogenic acid has extensive bioactivity, and modern science has been deep into the research of chlorogenic acid bioactivity
The multiple fields such as food, health care, medicine and daily-use chemical industry.Chlorogenic acid is a kind of important bioactive substance, has antibacterial, resists
Virus increases white blood cell, Hepatoprotective cholagogue, antitumor, lowering blood pressure and blood fat, removes free radical and stimulating central nervous system system etc.
Effect.Facino etc. has studied the natural polyphenol substance using chlorogenic acid as representative, find they can protect collagen not by
The injury of the free radicals such as active oxygen, and can effectively prevent the harmful effect that ultraviolet light generates human skin.It there is now multinomial add
Add after chlorogenic acid for antiurease cosmetics, antitan agent agent and prevents ultraviolet light and hair dye to the shampoo of hair damage
European patent document.
Patent document CN104161704A discloses a kind of pure natural shampoo of herbal raw material production.With following weight
Herbal raw material production of the part through processing, 25~30 parts of flax benevolence, peach kernel 15~20,20~25 parts of Radix Angelicae Sinensis, RADIX POLYGONI MULTIFLORI PREPARATA 25~30
Part, 20~25 parts of cacumen biotae, 5~7 parts of almond, 5~7 parts of wild chrysanthemum, windproof 5~7 parts, 5~7 parts of duckweed, eclipta 15~18
Part, 15~18 parts of the fruit of glossy privet, 10~12 parts of Rhizoma Chuanxiong, 10~15 parts and 5~7 parts of Radix Glycyrrhizae of dandelion；The big gun of the herbal raw material
Method processed is as follows: (1) flax benevolence: 250 grams of yellow rice wine are warmed, 500 grams of flax benevolence are poured into, is impregnated 1 hour, is pulled out and dry, on
Pot fry, appearing fragrance can take the dish out of the pot, spread out cool down system 200 mesh powder it is spare；(2) peach kernel: 500 milliliters of glutinous rice water boiled are put
150 grams of halite are added when to room temperature, is added 300 grams of peach kernel immersions after sufficiently stirring evenly, summer 12 hours, winter 24 hours, fishing
It is spare to spread the 200 mesh powder of system that dry in the shade after out out；Glutinous rice water is the water filtered out after 1 part of glutinous rice adds 3 parts of water to be sufficiently stirred；(3) Radix Angelicae Sinensis:
1000 milliliters of yellow rice wine are warmed, 500 grams of Radix Angelicae Sinensis investment is impregnated 2 hours, pull out dry it is rear spare；(4) RADIX POLYGONI MULTIFLORI PREPARATA: by semen sojae atricolor
500 grams cooked to pull and is pressed into beans mud out, and upper steamer is uniformly spread out on drawer cloth, then 500 grams of Radix Polygoni Multiflori are placed on beans mud and are spread
50 grams of upper halite end, lid pot cover, which steams 2 hours, to take the dish out of the pot, and spreads that 200 mesh powder are made after drying is spare out；(5) cacumen biotae: by 500 grams
Cacumen biotae is spread out, is first uniformly sprayed on medicinal material with 50% white wine of alcoholic strength, then is dissolved in 500 milliliters of water with 150 grams of halite
It is uniformly sprayed on medicinal material afterwards, it is spare that 200 mesh powder is made after drying in the shade；(6) almond: 50 grams of halite are dissolved in 300 milliliters of water,
50 grams of almond are poured into again and is wherein impregnated 2 hours, pulls that make 200 mesh powder after drying spare out；(7) wild chrysanthemum, duckweed and radix saposhnikoviae:
Wild chrysanthemum, duckweed and each 50 grams of radix saposhnikoviae, 50 grams of frutus cnidii are soaked in 500 milliliters of 50% white wine of alcoholic strength 2 hours, wine is filtered out
Liquid is uniformly sprayed on 150 grams of medicinal materials, and it is spare that 200 mesh powder are made after drying；(8) eclipta and the fruit of glossy privet: eclipta, the fruit of glossy privet are each
500 grams with 2500 milliliters of yellow rice wine, it is common impregnate 2 hours after pull out, add 500 milliliters of rice vinegar and mix well, be steamed in pot 4 small
When, pull that 200 mesh powder are made after drying is spare out；(9) Rhizoma Chuanxiong: mixed by 350 milliliters of white wine of 150 milliliters of yellow rice wine and alcoholic strength 50%
It is even, 500 grams of medicinal material are soaked in wine 2 hours, pot is entered when pulling micro- dry out fries to yellowish to take the dish out of the pot, 200 mesh powder are made after drying
It is spare；(10) dandelion: dandelion being poured into halite rice vinegar solution and is impregnated, and summer 3 hours, winter 5 hours, is pulled out and is dried in the air
Dry, slow fire is fried to medicine fragrance taste is appeared in upper hot pot, pours out that 200 mesh powder are made after drying is spare；Halite rice vinegar solution is by 1
The halite of parts by weight, which is placed in the rice vinegar of 2 parts by weight, sufficiently dissolves acquired solution；(11) Radix Glycyrrhizae: 200 mesh powder of licorice system
It is spare；By above-mentioned each medicinal powder end according to being mixed well after weight；By every bag of 30~35 grams of medicinal powder end, it is fitted into gauze bag
It seals to get the pure natural shampoo made to herbal raw material.
Patent document CN105395399A discloses a kind of shampoo with black hair function.The shampoo includes following weight
Measure the component of part: 60~80 parts of surfactant, 3~5 parts of foam improver, 1~2 part of conditioner, 0.1~0.3 part of essence, preservative
0.1~0.3 part, 10~40 parts of water, 15~25 parts of Chinese medicine extract.Chinese medicine extract is made by following raw materials: Herba Cistanches, day
Fiber crops, Radix Salviae Miltiorrhizae, amaranth are through son, eclipta, the fruit of glossy privet, radix achyranthis bidentatae, semen armeniacae amarae, rhizoma typhonii.Washing with black hair function provided by the invention
Shampoo, has many advantages, such as that toxic side effect is small, black hair effect is good.
Patent document CN1543925 discloses a kind of shampoo cream and preparation method thereof containing eclipta.Wherein, eclipta
The amount of extract is the 40~70% of total weight, and contains detergent, builder, moisturizer, the egg for accounting for total weight 30~60%
Bones of the dead collagen, preservative and pearling agent etc.." eclipta " shampoo cream of the invention, by natural plants " eclipta " extract with
Moisturizing agent combines with the washing base-material of shampoo cream, and Yeradetajo extract is made to play unique effect in shampoo cream,
The harm of addition other compound additive brings and stimulation in product are reduced, in addition the agent of HA biological moisture-keeping and animal bone glue has
Imitate booster action, moisten hair more soft, pitch-black glossy, dandruff significantly reduces, antipruritic effect up to 3 to 5 days,
And it is rapid, low-consuming, safe and reliable to blister, and has reached the optimum efficiency of " profit " after washing.
The effect of hair washing product is cleaning and removes hair and greasy dirt, the dust of scalp surface etc., to keep hair and head
The sanitation and hygiene of skin, they have foam abundant, mild clean effect and excellent using surfactant as main component
Dry and wet cardability.Contain almond or semen armeniacae amarae in above patent document CN105395399A and CN104161704A prescription, is
Shampoo；And in the rare patent document CN1543925 for being related to solid shampoo, it is natural plants " eclipta " extract
With moisturizing agent in conjunction with the washing base-material of shampoo cream, semen armeniacae amarae and its chlorogenic acid are free of, primary efficacy is black hair.
Summary of the invention
The purpose of the present invention is to provide one kind to contain amygdalate hair soap, and the hair soap is pure natural, and quality is stablized, and has
Obviously profit hair effect, and it is easy to carry.
Another object of the present invention is to provide a kind of preparation methods of hair soap, and preparation process is simple, at low cost.
To achieve the above object, the invention adopts the following technical scheme:
One kind containing amygdalate hair soap, and the hair soap is composed of the following components by weight percentage: semen armeniacae amarae 10-
55%, chlorogenic acid 1-5%, plant soap base 40-89%.
Wherein, the purity of the chlorogenic acid is 98%.
A kind of preparation method of the hair soap, method includes the following steps:
(1) semen armeniacae amarae is crushed, crosses 12-100 mesh, obtains semen armeniacae amarae fine powder；
(2) caustic alkali is soluble in water, it mixes, stirs evenly with vegetable oil, in 50-95 DEG C of progress saponification, reaction
Time is 30-60min, obtains plant soap base；
(3) obtained plant soap base is cooled to 40-45 DEG C, semen armeniacae amarae fine powder and green original is added thereto according to the ratio
Acid is uniformly mixed；
(4) gained mixture is poured into mold, is placed until natural coagulation, sets shady place storage.
Wherein, the vegetable oil be apricot kernel oil, Camellia oil, cupu oil, coconut oil, corn oil, linseed oil, olive oil,
One of palm oil, peanut oil, soybean oil, sunflower oil and wheat-germ oil are a variety of.
Wherein, the caustic alkali is sodium hydroxide or potassium hydroxide.
Wherein, in the step (2), relative to causticity base excess, the vegetable oil of 85%-95% be saponified anti-vegetable oil
It answers.
Wherein, in the step (2), water accounts for the 30-40% of vegetable oil weight.
Wherein, the water is distilled water, pure water or deionized water.
The present invention has the advantages that
Hair soap of the invention selects natural semen armeniacae amarae, and semen armeniacae amarae has the function of the moist hair quality of highly significant, place
Addition chlorogenic acid extracting ingredient from natural plants in side, chlorogenic acid have effects that repair damage hair quality, two natural component associations
With playing a role, the consumer psychology that consumer pursues Product Green and safety can be met.Hair soap quality of the invention is stablized, and takes
Band is convenient.Preparation process of the present invention is simple, and supplementary material is at low cost, has the prospect of marketing.
Detailed description of the invention
Fig. 1 is hair proteins loss amount measurement result.
Fig. 2 is that hair breaks function measurement result.
Specific embodiment
Below by way of specific embodiment, the present invention will be further described.Semen armeniacae amarae used in following embodiment is purchased from
Hebei province Laishui County Jin Gu oil and foodstuffs Co., Ltd, chlorogenic acid are purchased from the careless plant Trade Co., Ltd. of Xuancheng hundred, vegetable oil purchase
Supermarket is sent out in Beijing supermarket, caustic alkali is purchased from Beijing Reagent Company.Distilled water, deionized water, pure water: Beijing Union University is raw
The preparation of object chemistry engineering college's training base.
Embodiment 1
20g semen armeniacae amarae is weighed, crushed 12 meshes；Weigh chlorogenic acid 2.5g；Take sunflower oil 100g, the hydrogen of sunflower oil
Sodium oxide molybdena saponification number is 0.134, weighs sodium hydroxide 12g and is dissolved in distilled water 30mL, lye is poured into sunflower oil, water-bath adds
Heat, temperature are controlled at 80-90 DEG C, stir 45min；Semen armeniacae amarae powder and chlorogenic acid is added to 50 DEG C in Temperature fall, is stirred
It is even, it pours into mold, places until natural coagulation；Set shady place storage.The perceptual index test of hair soap the results are shown in Table 1, head
The result is shown in Figure 1 is determined in hair protein losses measurement, and hair breaks function measurement result and sees Fig. 2.Indices meet professional standard QB/
T 1974-2004。
Embodiment 2
20g semen armeniacae amarae is weighed, crushed 12 meshes；Weigh chlorogenic acid 2.5g；Take sunflower oil 100g, the hydrogen of sunflower oil
Potassium oxide saponification number is 0.1876, weighs potassium hydroxide 16.8g and is dissolved in distilled water 30mL, lye is poured into sunflower oil, water
Bath heating, temperature are controlled at 80-90 DEG C, stir 45min；Semen armeniacae amarae powder and chlorogenic acid is added to 50 DEG C in Temperature fall, and stirring is mixed
It closes uniformly, pours into mold, place until natural coagulation；Set shady place storage.The perceptual index test of hair soap the results are shown in Table
1.Indices meet professional standard QB/T1974-2004.
Embodiment 3
20g semen armeniacae amarae is weighed, crushed 14 meshes；Weigh chlorogenic acid 2g；Take coconut oil 100g, the sodium hydroxide of coconut oil
Saponification number is 0.19, weighs sodium hydroxide 17g and is dissolved in distilled water 30mL, lye is poured into coconut seed oil, heating water bath, temperature
Control stirs 60min at 80-85 DEG C；Temperature fall is added semen armeniacae amarae powder and chlorogenic acid, is uniformly mixed, pours into 45 DEG C
In mold, place until natural coagulation；Set shady place storage.The perceptual index test of hair soap the results are shown in Table 1, hair proteins
Loss amount measurement result is shown in Fig. 1.Indices meet professional standard QB/T 1974-2004.
Embodiment 4
30g semen armeniacae amarae is weighed, crushed 80 meshes；Weigh chlorogenic acid 5g；Take corn oil 100g, the sodium hydroxide of corn oil
Saponification number is 0.136, weighs sodium hydroxide 12.5g and is dissolved in distilled water 30mL, lye is poured into corn oil, heating water bath, temperature
Degree control stirs 35min at 90-95 DEG C, and Temperature fall is added semen armeniacae amarae powder and chlorogenic acid, is uniformly mixed, to 45 DEG C
Enter in mold, places until natural coagulation；Set shady place storage.Hair breaks function measurement result and sees Fig. 2.Indices meet
Professional standard QB/T 1974-2004.
Comparative example 1
Overlord's hair-loss preventing and hair-restoring cream (production of overlord (Guangzhou) Co., Ltd), packaging: 60g.Effect: anticreep, it is submissive, it nourishes.
Hair proteins loss amount measurement result is shown in that Fig. 1, hair break function measurement result and see Fig. 2.
It participates in tester and gets the hair soap of each embodiment and the hair shampoo article of comparative example, with test product hair washing one
It uses every other day in week, once a day.Hair soap perception evaluation one embodiment select 5 people (18-23 years old age), experience result with
Most selection result labels.Hair proteins loss amount measurement and hair breaks function measurement test, with test sample hair washing one
Last time after week detects (0h, 36h, 72h).
The evaluation of embodiment hair quality
1, the perception evaluation of hair soap
7 perceptual index tests are carried out to four kinds of hair soaps of embodiment 1-4, perceptual index test the results are shown in Table 1.Table 1
Middle impression degree is divided to two grades, and each perception index explanation is as follows:
1) foam degree refers to the ability of hair washing Water blown.Foam is more, and cleaning capacity is stronger, and degreasing ability is also stronger.+ table
Show foaming abundancy ,-indicate low bubble.
2) hair will not mutually be wound when wet and slippery degree is hair washing bath.+ indicate that hair does not tangle ,-indicate that hair tangles.
3) dry slippery is that equal hairs have smooth effect after doing after having one's hair wash.+ indicate smooth ,-indicate dry and astringent.
4) irritation refers to after use process and use to the comfort level of scalp, face.+ indicate stimulation ,-indicate not pierce
Swash.
5) anti-oil content is called out oil content and refers to that (about one day or two days) are produced in hair and scalp surface in the short time after hair washing
Raw excessive oil content, hair feel it is greasy or in scalp mo(u)ld top half at one layer of oil film.+ indicating easily fuel-displaced ,-expression is not easy fuel-displaced.
6) glossiness, which refers to, forms layer protecting film in hair surface after hair washing, keeps hair gloss beautiful.+ indicate nature
Gloss ,-indicate that hair quality is dark and gloomy.
7) anti-head is itched after finger is washed hair, and head is not itched in three days.+ indicate that head is not itched ,-indicate that head is itched.
The perceptual index test result of 1 hair soap of table
2, hair proteins loss amount measures
Measure protein using Coomassie Brilliant Blue: 50mg Coomassie brilliant blue is dissolved in 25mL 90% (v/v) ethyl alcohol, is added
50mL 85% (w/v) phosphoric acid, distilled water are settled to 500mL, and brilliant blue dye liquor is made.System is measured at maximum absorption wavelength 595nm
The absorbance of column standard solution.Calibration curve equation are as follows: y=2.982X+1.063.Wherein y is absorbance A BS, and x is series mark
The protein concentration of quasi- solution.Linearly dependent coefficient is 0.9995, and linear relationship is good.
Separately sampled when 0h, 36h, 72h after having one's hair wash to three groups of hairs, each test point is surveyed in parallel averages three times, knot
Fruit indicates with protein content, unit: mg protein/g hair.Healthy clean hair sample is cut into the broken hair of 1cm or so, is added
3mL, 5% (w/v) SDS aqueous solution, 45 DEG C of ultrasonic constant temps shake 4h, draw upper solution 1mL, and 5mL dye liquor is added and mixes, distillation
Water is settled to 10mL, obtains test liquid after setting 2min.
Protein structure is degenerated, and increases the protein content being dissolved in the water, hair damage degree is bigger, dissolves in water
Protein content it is higher.It can be seen from figure 1 that embodiment 1 and 3 protein losses of embodiment are below comparative example 1 in 0-72h.
3, hair breaks function measurement (measurement of human hair tensile mechanical properties)
Hair is one kind most full of elasticity in natural fiber, and the tensile property of hair depends on the a- keratin of cortical layer,
The telescopicing performance of a- keratin is fine, elongates hair twice of original length.After hair elongates to a certain extent,
Alpha-helix is destroyed, and is changed into β-conformation, loss of elasticity.Healthy hair cortex has certain elasticity and toughness, and the hair being destroyed
Cortex, elasticity and toughness decline, are easily broken off.
Select MTT175 hair tester, German Dio-stron company production.Hair to be tested first at 25 DEG C of temperature,
It is balanced for 24 hours in the environment of relative humidity 50%.Due to longitudinal three positions of hair: the tensile property presence of root, middle part, taper
Nuance, therefore remove root and taper, surplus middle part about 10cm are tested, by hair be fixed on instrument two copper sheets it
Between, clamp distance 30cm, tensile speed 12.5mm/min carry out breaking test, and record breaks the data such as function.Every group takes 20
Hair is tested.
Separately sampled when 0h, 36h, 72h after having one's hair wash to three groups of hairs, each test point is surveyed in parallel averages three times, knot
Fruit indicates with function is broken, unit: joule (J).Break that function is smaller to illustrate that hair damage is more serious, as it is clear from fig. 2 that embodiment 4 is drawn
Disconnected function is bigger, illustrates that hair quality is preferable；The hair quality after 12h of embodiment 1 is deteriorated, but is also better than comparative example 1.
Claims (7)
1. one kind contains amygdalate hair soap, the hair soap is composed of the following components by weight percentage: semen armeniacae amarae 10-
55%, chlorogenic acid 1-5%, plant soap base 40-89%；Preparation method includes the following steps:
(1) semen armeniacae amarae is crushed, crosses 12-100 mesh, obtains semen armeniacae amarae fine powder；
(2) caustic alkali is soluble in water, it mixes, stirs evenly with vegetable oil, in 50-95 DEG C of progress saponification, reaction time
For 30-60min, plant soap base is obtained；
(3) obtained plant soap base is cooled to 40-45 DEG C, semen armeniacae amarae fine powder and chlorogenic acid is added thereto according to the ratio, stirs
It mixes uniformly mixed；
(4) gained mixture is poured into mold, is placed until natural coagulation, sets shady place storage.
2. hair soap according to claim 1, which is characterized in that the purity of the chlorogenic acid is 98%.
3. hair soap according to claim 1, which is characterized in that the vegetable oil be apricot kernel oil, Camellia oil, cupu oil,
One in coconut oil, corn oil, linseed oil, olive oil, palm oil, peanut oil, soybean oil, sunflower oil and wheat-germ oil
Kind is a variety of.
4. hair soap according to claim 1, which is characterized in that the caustic alkali is sodium hydroxide or potassium hydroxide.
5. hair soap according to claim 1, which is characterized in that in the step (2), vegetable oil is relative to caustic alkali mistake
The vegetable oil of amount, 85%-95% carries out saponification.
6. hair soap according to claim 1, which is characterized in that in the step (2), water accounts for vegetable oil weight
30-40%.
7. hair soap according to claim 1, which is characterized in that the water is distilled water, pure water or deionized water.
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|---|---|---|---|---|
| CN105238597A (en) * | 2015-10-30 | 2016-01-13 | 南京科技职业学院 | Shampoo soap containing cacumen biotae and preparation method for shampoo soap |
| CN106265370A (en) * | 2016-09-30 | 2017-01-04 | 翟鸿宇 | A kind of shampoo effectively preventing pathologic alopecia and preparation method thereof |
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| CN105238597A (en) * | 2015-10-30 | 2016-01-13 | 南京科技职业学院 | Shampoo soap containing cacumen biotae and preparation method for shampoo soap |
| CN106265370A (en) * | 2016-09-30 | 2017-01-04 | 翟鸿宇 | A kind of shampoo effectively preventing pathologic alopecia and preparation method thereof |
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