KR100805692B1 - Chinese medicine extracts and a shampoo composition for stopping the hair from falling out - Google Patents

Abstract

An extract of Chinese medicines is provided to be added to prepare a shampoo, thereby being helpful for healing scalp, preventing hair loss and promoting hair growth. An extract of Chinese medicines for preventing hair loss is characterized in that it is prepared by heat-extracting 100 grams of pulverized Chinese medicines obtained by drying a mixture consisting of 8-20 wt.% of Angelica dahurica, 10-25 wt.% of Rubia akane Nakai, 5-20 wt.% of Lysimachiae Foenumgraeci Herba, 5-25 wt.% of Chrysanthemum indicum, 10-17 wt.% of Cnidium officinale, 5-15 wt.% of Eclipta prostrata, 7-15 wt.% of Mori Cotex Radicis, 9-12 wt.% of Sophora flavescens and 9-15 wt.% of Cynanchum wilfordii Hemsly in the shade to have the moisture content of 0.1-2% and pulverizing the mixture in 2l of distilled water at a temperature of 70-90 deg.C for 6-10 hours, centrifuging the extract for 30-50 minutes with the speed of 700-900 rpm, taking only an upper layer extract solution therefrom and cryopreserving the extract solution. A shampoo for preventing hair loss comprises 5-30 wt.% of the extract of Chinese medicines.

Description

Herbal extract for hair loss prevention and hair loss prevention shampoo using the same {CHINESE MEDICINE EXTRACTS AND A SHAMPOO COMPOSITION FOR STOPPING THE HAIR FROM FALLING OUT}

The present invention relates to a medicinal herb extract and a shampoo using the same, which can help scalp healing, hair loss prevention, hair growth promotion, and the like, which can be added at a predetermined ratio during the preparation of the shampoo.

The symptoms of hair loss are increasing in various age groups and women by various causes such as environmental factors and social factors according to the development of society.

As described above, hair loss is caused by environmental and social factors. Especially, due to frequent perming, staining, stress, and severe diet, hair loss symptoms are not limited to men in recent years. The age at which it develops is also gradually decreasing.

Our bodies move according to their functions and roles, and in relation to hair loss, the scalp essentially protects and absorbs all organs in the body from the external environment such as mechanical external force, chemical poisoning, microorganism invasion, and sunlight. Has the function of action, respiration and excretion, sensory function. These scalp also excrete harmful substances and wastes in the body. When keratin and wastes accumulate on the scalp and accumulate on the surface, they block the pores of the scalp, prevent skin breathing, inflame the scalp, and thin the hair. do. If the breathing and excretion is not smooth, it accumulates in the body and eventually distracts the body's balance, which greatly affects other functions, causing abnormal scalp phenomenon. The health of the scalp is an important factor in determining the health of the hair.

In general, a lot of soap or shampoo is generally used to wash the hair, and in particular, recently, as the interest in the health of the consumer's hair has increased, not only simple washing but also functional for preventing hair loss through the health of the scalp and hair. The development of shampoo is actively being developed.

For example, Korean Patent Publication No. 1994-0018084 (published on Aug. 16, 1994) includes licorice (Glycyrrhizae Radix), Lonicerae Flos, mint (Menthae Herba), Sessin (Asiasari Radix), Gardenia (Gardeniae Fructus), and Golden ( Disclosed is a fragrance dandruff shampoo composition containing herbal extracts such as Scutellariae Radix)

Korean Patent Publication No. 2002-0037796 (published on May 23, 2002) discloses a content of a hair shampoo composition and shampoo containing herbal extracts and natural vinegar,

Korean Patent Publication No. 2002-0078547 (published date 2002.10.19) discloses a shampoo for hair loss prevention using aroma oil, and Korea Patent Registration 10-0469658 (published date 2005.02.02) herbal composition such as mugwort and ginseng A shampoo containing hair loss prevention and hair regrowth composition is disclosed.

However, the patents have a problem in that the washing function, which is the basic function of the shampoo, or the hair loss function is inferior by enhancing functionality for hair loss or hair growth.

In order to solve the problems as described above, in the present invention, white paper, cheoncho, Yeongneung, Yeonggung, Gamuk, Cheongung, Hanyeoncho, Sangbaekpi, Gosam, white so as to have an effect on hair loss without dropping the hair washing function which is a basic function of the shampoo By adding the extract taken from the herbal ingredients composed of sewage in the range of 5 to 30% by weight based on the total weight of the shampoo, herbal extracts that can help to heal the scalp, prevent hair loss, promote hair growth, and hair loss using the same. It aims at providing the prevention shampoo.

In order to achieve the above object, the present invention is 8 to 20% by weight, 10 to 25% by weight Cheoncho, 5 to 20% by weight Yeongneung, 5 to 25% by weight, 10 to 17% by weight Cheonggung, Hanyeoncho 5 ~ 15% by weight, sangbaekpi 7 ~ 15% by weight, red ginseng 9 ~ 12% by weight, Baek Sewao 9 ~ 15% by weight of the composition is dried in the shade so that the moisture content of 0.1 ~ 2% 70 ~ 95 mesh (mesh Based on 100 g of the herbal mixture pulverized), using 2 liters of distilled water and extracting by heating at 70 ~ 90 ℃ for 6 to 10 hours, the extracted extract was centrifuged at 700 ~ 900rpm for 30 to 50 minutes to discard the residue Herbal extract for hair loss prevention and taking frozen extract only and

Hair loss prevention shampoo prepared by adding the prepared herbal extract in 5 to 30% by weight based on the total weight of the shampoo as the main technical configuration.

The herbal extract is dried in the shade so that the moisture content is 0.1 ~ 2% and then mixed with white paper, Cheoncho, Yeongneunghyang, Gamguk, Cheongung, Hannyeoncho, Sangbaekpi, Gosam, Baekshou, crushed into 70 ~ 95 mesh. Based on 100 g of the herbal mixture prepared, 2 liters of distilled water was used for 6-10 hours extraction at 70-90 ° C., and the extracted extract was centrifuged at 700-900 rpm for 30-50 minutes to discard the residue. After taking the bay is characterized in that it is stored frozen.

Hereinafter, the technical configuration will be described in more detail.

The Angelica dahurica BENTHAM et Hooker is a perennial herb belonging to the Umbelliferae and distributed throughout our country. Root stem contains angelicol, edultin, pelletopterin and the like and imperatorin for analgesic and pain relief. Its main medicinal effects are analgesic and small-species efficacies, and the applied disease is known to exhibit medicinal effects such as headache, migraine, various neuralgia, abdominal pain and the like. In addition, the extract of white paper has been reported to have antimicrobial effect, blood phase and vascular system improvement effect and significant hepatoprotective effect. The white paper is about 1 ~ 2m high, the roots are thick, large and straight, sometimes divided into several. The stem is large and thick, and close to the circumference. The leaves at the bottom of the stem are large and long, and the leaf is wrapped around the stem.

The white paper is used in a ratio of 8 to 20% by weight based on the total mixture, when used at less than 8% by weight, the antibacterial activity is reduced and the anti-hair loss function by dandruff is reduced, more than 20% by weight If the problem is not balanced with other active ingredients occurs, the white paper is preferably used in a ratio of 8 to 20% by weight based on the total mixture.

The cheoncho is 5 ~ 9 leaves are turned, long oval egg-shaped, pointed end, with a thorn on the back edge and vein, the fruit is 2 pieces of berries, round and ripen black. Roots are used as dyes and young leaves are eaten. In particular, the root is called chonchogeun (爽 草根) is used for arthritis, neuralgia, dysmenorrhea, soil blood, bloody stool, uterine bleeding, hepatitis, jaundice, chronic bronchitis, boils, bruises.

The cheoncho is used in a ratio of 10 to 25% by weight based on the total mixture, when using less than 10% by weight it is difficult to expect the effect of improving the scalp condition, when used in excess of 25% by weight Since a problem occurs that is not balanced with other active ingredients, it is preferable to use the cheoncho in a ratio of 10 to 25% by weight based on the total mixture.

The Yeongneunghyang is a biennial herbaceous, its shape is 40 ~ 60 cm long stem, 4 ~ 6 cm in diameter, the tip has a long and long leaf disease. The outer side of the leaf is green, the peduncle is relatively thin and weak, about 2-3cm long.

Yeongneunghyang is used in a ratio of 5 to 20% by weight based on the total mixture, if less than 5% by weight is used to prevent hair loss due to improvement of the scalp condition, it will be used in excess of 20% by weight In this case, since the balance with other active ingredients occurs, it is preferable to use the Youngneung in a ratio of 5 to 20% by weight based on the total mixture.

It is a plant belonging to the genus Chrysanthemum of Chrysanthemum indicum Linn'e (= Dendranthema indicum Des Moulins) and belonging to the genus Chrysanthemum of compositae. The leaves are dark green, alternate, petioles, egg-shaped, usually divided into quills and pointed ends, and the fragments are long oval and have serrated teeth.

In Chinese medicine, Chrysanthemum indicum L. is used to reduce blood pressure due to antipyretic, anti-inflammatory, coronary artery dilation and increase in coronary blood flow. It is known to have a therapeutic effect on vertigo, and is used for diseases such as flatulence, playing window, dizziness, headache and tears.

The main ingredients of Chrysanthemum indicum L. are found to contain adenine, stachydrine, choline and volatile essential oils, and the flavonoid compounds luteolin and apizezin Cumambrin A, cumambrin B, and ateglasin A, which are apigenin compounds, are contained.

In terms of quality, in the case of 50.0 g of powdered pharmaceuticals, foreign body less than 3.0%, dry weight less than 20.0%, ash less than 5.0%, acid insoluble ash less than 1.0%, essential oil content more than 0.1mL, water extract more than 17.0%, diluted ethanol More than 25% of the extract, more than 17% of the ether extract and the content of ash and each extract to meet the standard and yellowish heading, because the fragrance is strong, rather the less fragrance is evaluated as a good material.

Persimmon soup is used at a ratio of 5 to 25% by weight based on the total mixture. When used at less than 5% by weight, the effect of improving scalp is reduced. Since the problem occurs that the balance is not made, it is preferable to use the gamguk at a ratio of 5 to 25% by weight based on the total mixture.

The Cnidium officinale is cultivated as a medicinal plant as a perennial plant of the Apiaceae, which promotes blood circulation and clears blood, and has mild properties. It contains chemical components such as).

The arch is used in the form of powder milled in the range 70 ~ 95 mesh using a bead mill (Bead Mill) dried so that the moisture content is 2% or less. Cheongung is used at a ratio of 10 to 17% by weight based on the total mixture. When it is used at less than 10% by weight, scalp protection is not effective and prevents hair loss, and is used in excess of 17% by weight. When the problem occurs that the balance with other active ingredients is not made, it is preferable to use the cheongung at a ratio of 10 to 17% by weight based on the total mixture.

The nasturtium (旱 蓮 草) is a year-round plant belonging to the genus (Compositae), the scientific name is an outpost of the Eclipta prostrata (Compositae) is native to the marsh, the stem is vine-like, flexible, upright or crawled sideways It is 30 ~ 60cm high, with bristles on outpost, leaves are regenerated, lotus leaf shape, few or extremely short, lanceolate, thick veins near base, with fine teeth on edge.

The nasturtium contains saponin, tannin, ecriptin, coumarin compound, wetelolactin, vitamin A, and the like, and the dried nasturtium so that the moisture content is 2% or less using a bead mill (70 ~ 70). Use powder ground in the 95 mesh range. Nasturtium is used at a ratio of 5 to 15% by weight based on the total mixture. When it is used at less than 5% by weight, blackening and hair loss of the hair are reduced, and when it is used in excess of 15% by weight, Since the balance with the active ingredient is not achieved, the nasturtium is preferably used in a proportion of 5 to 15% by weight based on the total mixture.

The Morus Cortex Radicis is a plant belonging to the genus Morus alba Linne, Morus bombycis Koidzumi or other plants of the genus Morus. The root bark from which the cork layer has been removed is dried, and the physiological activity of the cortex is diuretic, coercive, hypoglycemic, antibacterial, antifungal, anti-inflammatory, and anti-inflammatory.

The baekbaekpi is composed of flavonoids, essential oils, organic acids, hinokiflavones, hinokichiol and the like as a main component, dried baekbaekpi so that the moisture content is less than 2% using a bead mill (Bead Mill) range of 70 ~ 95 mesh (mesh) Use crushed lettuce powder. It is used in the ratio of 7 to 15% by weight with respect to the entire mixture. When used at less than 7% by weight, the antibacterial activity is reduced and the hair loss prevention function by dandruff is reduced, and it is used in excess of 15% by weight. If so, the addition amount of the ingredients of other herbal ingredients is reduced, so there is a problem that the balance of the active ingredient is not made, it is preferable to use the baekryepi at a ratio of 7 to 15% by weight based on the total mixture.

The ginseng is a perennial herb that belongs to the legumes and grows in the mountains and fields of Korea, and is 80-120 cm tall, with short yellow hairs all over, the roots are hypertrophy, very bitter, standing upright, the leaves are regenerated, and the feathers overlap. , 10 pairs of small leaves, 2 ~ 4cm, flat edge, chin leaf.

The ginseng uses a ginseng powder ground in a range of 70 ~ 95 mesh (mesh) using a bead (Bead Mill) dried so that the moisture content is less than 2%. Ginseng is used in a ratio of 9 to 12% by weight based on the total mixture, when less than 9% by weight of the antibacterial to the dandruff is less, and when used in excess of 12% by weight with other active ingredients Since there is a problem of unbalance, the ginseng is preferably used in a ratio of 9 to 12% by weight based on the total mixture.

Cyna chum wilfordii Hemsley is a perennial vine herb belonging to the genus Asclepiadaceae and Cinnanchum, and as a root form, acetophenone and polyoxypreg as physiologically active substances of white sewage. Polyoxypregnane glycoside.

The constituents of Baek Sewao contain lecithin, sugar, fat, and the like. Acetophenones (acetophenones (Hwang et al, 1999)) such as cynandione A, sarcostin, and lineo Polyoxypregnane glycosides are contained in polyoxypregs such as lineolon.

White sewage used in the present invention is a powder form obtained by grinding white sewage dried to a moisture content of 2% or less using a bead mill in the range of 70 to 95 mesh. It is used in the ratio of 9-15 weight%. If it is used in less than 9% by weight, the blackening and antioxidant function of the hair is reduced, and when used in excess of 15% by weight, there is a problem that the balance is not balanced with other active ingredients, the white sewage Preference is given to using in proportions of 9-15% by weight relative to the mixture.

The white paper, Cheoncho, Yeongneunghyang, Gamguk, Cheonggung, Hanryokcho, Sangbaekpi, Gosam, Baekhasuo are used for the preparation of the shampoo after extracting the pulverized extraction process. After drying in the shade so that the moisture content is 0.1 ~ 2% and pulverized to 70 ~ 95mesh using a bead mill (Bead Mill).

The moisture content of the herbal material is adjusted to facilitate the grinding and extraction, when the moisture content is less than 0.1% is easy to grind, but the problem that the component extraction is not easy, and exceeds 2% Since there is a problem that the grinding is not easily made, it is preferable to use the dried so that the moisture content of the herbal material is 0.1 to 2%.

The herbal material pulverized as described above is subjected to the extraction process using distilled water, and the mixing ratio is extracted by heating at 70-90 ° C. for 6-10 hours using 2 L of distilled water based on 100 g of the herbal material.

The heat extraction temperature and time is related to the amount of the extraction liquid to be extracted, when the heat extraction to less than 70 ℃ or less than 6 hours, the extraction is not enough because the extraction amount is reduced, it is uneconomical, or exceeds 90 ℃ Alternatively, if the extraction by heating for more than 10 hours no further extraction process is meaningless. Therefore, the extraction temperature and extraction time is preferably based on 6 to 10 hours at 70 ~ 90 ℃.

Thus, the extract extracted through the extraction process is centrifuged for 30 to 50 minutes at 700 ~ 900rpm discarded the residue, take only the extract of the upper layer and store frozen.

The rpm and time of the centrifugation affect the degree of separation, and if the centrifugation is performed at less than 700 rpm or less than 30 minutes, the separation of the upper layer is insufficient, and is greater than 900 rpm or more than 50 minutes. In the case of centrifugation, there is no significant change in the degree of separation. Therefore, the rpm and time in the centrifugation is preferably based on 30 to 50 minutes at 700 to 900 rpm.

As such, the hair loss prevention shampoo composition that has undergone the extraction process is added in an amount of 5 to 30% by weight based on the total weight of the shampoo. In this case, when less than 5% by weight is added, scalp protection and hair loss prevention effect are reduced, and 30% by weight When used in excess, since the washing function, which is a unique function of the shampoo, cannot be exerted as a shampoo, the hair loss prevention shampoo composition is preferably added in an amount of 5 to 30% by weight based on the total weight of the shampoo. .

The shampoo is a common shampoo raw material, and specific examples thereof include anionic surfactants ALES (Ammonium Laureth-3 Sulfate), ALS (Ammonium Lauryl Sulfate), purified water, sodium hydroxide (NaOH) as a pH regulator, sodium chloride as a thickener ( NaCl) is used and the mixing ratio thereof is as described in Example 6 below.

As described above, the hair loss prevention shampoo composition according to the present invention protects the scalp from dandruff equality to maintain the health of the scalp, by using a shampoo containing natural substances to reduce the irritation of the scalp than conventional shampoos To prevent hair loss.

Hereinafter, a detailed description of the technical configuration described above will be described through examples and comparative examples.

Herbal Extract for Hair Loss Prevention

Example 1

20 g of white paper, 10 g of Cheoncho, 10 g of Yeongneunghyang, 10 g of Gamkook, 10 g of Cheonggung, 10 g of Hanyeoncho, 10 g of Sangbaekpi, 10 g of red ginseng, and 10 g of white sewage were added to the mixture and extracted by heating at 90 ° C. for 7 hours. The extract was centrifuged at 900 rpm for 40 minutes and the residue was discarded. The extract was taken from the upper layer and stored frozen.

Example 2

White paper 17g, Cheoncho 13g, Yeongneunghyang 10g, Gamuk 10g, Cheonggung 10g, Nayeoncho 10g, Sangbaekpi 10g, 10 g of red ginseng, 10g of white sewage is mixed, through the same extraction process as in Example 1 to prepare a herbal extract.

Example 3

White ginseng 15g, Cheoncho 10g, Yeongneunghyang 15g, Gamuk 10g, Cheonggung 10g, Hanryokcho 10g, Sangbaekpi 10g, 10 g of red ginseng, 10g of white sewage is mixed, through the same extraction process as in Example 1 to prepare a herbal extract.

Example 4

White ginseng 13g, Cheoncho 10g, Yeongneunghyang 10g, Gamuk 17g, Cheonggung 10g, Nayeoncho 10g, Sangbaekpi 10g, 10 g red ginseng, 10g of white sewage is mixed, through the same extraction process as in Example 1 to prepare a herbal extract.

Example 5

White paper 10g, Cheoncho 10g, Yeongneunghyang 10g, Gamuk 10g, Cheonggung 15g, Hanryokcho 15g, Sangbaekpi 10g, 10 g of red ginseng, 10g of white sewage is mixed, through the same extraction process as in Example 1 to prepare a herbal extract.

Hair Loss Prevention Shampoo

Example 6

38ml herbal extract prepared as in Example 1

Anionic Surfactant Amlesium Laureth-3 Sulfate 39.75ml

15 ml of Ammonium Lauryl Sulfate (ALS)

6 ml of purified water

PH regulator NaOH 0.25g

Thickener NaCl 1g was prepared by stirring and mixing at a rate of 25rpm so that bubbles do not occur.

Example 7

Prepared in the same manner as in Example 6, in selecting the herbal extract, the one prepared in Example 2 is used.

Example 8

Manufactured in the same manner as in Example 6, in selecting the herbal extract, the one prepared in Example 3 is used.

Example 9

Manufactured in the same manner as in Example 6, in selecting the herbal extract, the one prepared in Example 4 is used.

Example 10

Manufactured in the same manner as in Example 6, in selecting the herbal extract, the same as in Example 5 is used.

Test Example 1

The shampoos of Examples 6 to 10 prepared as described above were used for 20 days (including 15 people with dandruff and itching) for 30 days, and the results were examined, and the results are shown in Table 1 below. .

Table 1: Hair Growth and Hair Nutrition Test

division Example 6 Example 7 Example 8 Example 9 Example 10  Hair growth condition Very good 11 11 10 9 9 good 9 9 9 10 9 No change 0 0 One One 2  Hair nutrition Very good 14 13 13 11 10 good 6 7 6 7 8 No change 0 0 One 2 2

The evaluation was made in the case of the hair growth state, 'very good' if there is a hair growth on the whole head, 'good' if there is a hair growth on a part of the head, 'no change' if there is no hair growth. In the case of hair nourishment, there is almost no hair damage and it is 'very good' if it is smooth, and the hair damage state is limited to one minute and the hair is smooth. It was.

As can be seen from Table 1, as a result of irradiation, the hair loss rate was reduced by about half in all users, the thin hair or fine hair had the effect of thickening. In addition, people with dandruff and itching had the effect of completely eliminating dandruff and itching.

Claims (2)

White paper 8-20 wt%, Cheoncho 10-25 wt%, Yeongneung-hyang 5-20 wt%, Gamguk 5-25 wt%, Cheongung 10-17 wt%, Nasturtium 5-15 wt%, Sangbaekpi 7-15 wt%, 2 liters of distilled water based on 100 g of the herbal mixture mixed with 9 to 12% by weight of red ginseng and 9 to 15% by weight of white sewage, dried in the shade to obtain a water content of 0.1 to 2%, and then ground to 70 to 95 mesh. Heat-extract for 6 to 10 hours at 70 ~ 90 ℃ using, centrifuged the extracted extract at 700 ~ 900rpm for 30 to 50 minutes, discard the residue, take only the extract of the upper layer and freeze storage, characterized in that Herbal Extract. Hair loss prevention shampoo using the herbal extract, characterized in that it is prepared by adding the herbal extract prepared in 5 to 30% by weight based on the total weight of the shampoo.