CN105238597A - Shampoo soap containing cacumen biotae and preparation method for shampoo soap - Google Patents
Shampoo soap containing cacumen biotae and preparation method for shampoo soap Download PDFInfo
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- CN105238597A CN105238597A CN201510727448.8A CN201510727448A CN105238597A CN 105238597 A CN105238597 A CN 105238597A CN 201510727448 A CN201510727448 A CN 201510727448A CN 105238597 A CN105238597 A CN 105238597A
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Abstract
The invention discloses a shampoo soap containing cacumen biotae. The shampoo soap comprises the following main raw materials: a plant extraction solution and plant oil. The plant extraction solution is composed of a cacumen biotae extraction solution, a rosemary extraction solution, a Chinese honeylocust fruit extraction solution, a mint extraction solution, a fleece-flower root extraction solution and a nettle extraction solution. Particularly, the plant oil is composed of 10-60 parts of shea butter and 10-30 parts of coconut oil. The shampoo soap disclosed by the invention is made from fully natural raw materials, so that the shampoo soap is safe and non-irritant and has no side effects on human body. Meanwhile, the shampoo soap disclosed by the invention contains extract of cacumen biotae, so that the shampoo soap has the functions of cooling and arresting blood and restoring and blackening hairs.
Description
Technical field
The invention belongs to household chemicals production technical field, be specifically related to a kind of hair soap containing Leafy twigs of Oriental Arborvitae and preparation method thereof.
Background technology
Leafy twigs of Oriental Arborvitae has another name called CedarLeaves, Cong Baiye, Japan cypress, cloud sheet cypress etc., is spray and the leaf of Cupressaceae evergreen plant arbor-vitae.Modern many using arbor-vitae as Ornamental plant, and its health be worth rarely have understanding.
Leafy twigs of Oriental Arborvitae be doctor pay attention to control blood good medicine.The traditional Chinese medical science thinks Leafy twigs of Oriental Arborvitae bitter, and cold nature is nontoxic, enters the heart, liver, large intestine channel.There is the merit of cool blood, hemostasis, interior wet, loose pyogenic infections.The diseases such as haematemesis, nasal bleeding, hematuria, bloody flux, uterine bleeding, rheumatalgia, cough, scald can be controlled.
Show according to scientific research, Leafy twigs of Oriental Arborvitae is containing a large amount of volatile oil, and in oil, main component is thujene, fenchone etc., also containing various trace elements such as potassium, sodium, phosphorus, nitrogen, calcium, magnesium, manganese and zinc in leaf.Pharmacologically, Leafy twigs of Oriental Arborvitae decoction can significantly shorten bleeding time and clotting time, and its hemostasis effective constituent is Quercetin and tannin.In addition, effects such as also having antibechic, relieving asthma, eliminate the phlegm, be calm.Related experiment shows, Leafy twigs of Oriental Arborvitae all has good restraining effect to streptococcus aureus, dysentery bacterium, micrococcus catarrhalis, diphtheria corynebacterium, Corynebacterium diphtheriae etc., has effect that black beard and hair, hemostasis, cough-relieving are breathed heavily.
Common hair soap for have one's hair wash to wash rear sense not good, during hair washing, more puckery, hair comb all cannot be opened by finger; After drying up, feel again the not fluffy sense in road, even feel that hair sticks greasy; In addition, as dandruff, soap scum on hair is remained in addition.Its reason is that silicone oil is water insoluble containing silicone oil in common hair soap, can be wrapped on hair from level to level, so cause hair thick and heavy, and progressively follow the string along with access times, and pore is blocked thus cannot breathe.In addition, add animal raw materials, staining agent, nipagin esters and petroleum-type tensio-active agent etc., Long Term Contact can stimulate decortication grease body of gland, destroy scalp fungi balance, causes clogging of pores, hair dries up easily broken, hair loss alopecia.
Because hair soap has above-mentioned defect, therefore not by people are commonly used, more Leafy twigs of Oriental Arborvitae is not used for the report of hair soap.
Summary of the invention
Goal of the invention: for the corresponding shortcoming of hair soap of the prior art, the invention provides a kind of hair soap containing Leafy twigs of Oriental Arborvitae, and provides the preparation method of this hair soap.
Technical scheme: the invention provides a kind of hair soap containing Leafy twigs of Oriental Arborvitae, its main raw material comprises: plant extraction liquid, vegetables oil and sodium hydroxide, and described plant extraction liquid is made up of Chinese arborvitae twig extract, Rosmarinus officinalis extracting solution, Chinese honey locust extracting solution, peppermint extracting solution, tuber of multiflower knotweed extracting solution and nettle extracting solution.
Concrete, according to the mass fraction, each main raw materials in proportion is: Chinese arborvitae twig extract 20 ~ 50 parts, Rosmarinus officinalis extracting solution 5 ~ 20 parts, Chinese honey locust extracting solution 10 ~ 30 parts, peppermint extracting solution 5 ~ 20 parts, tuber of multiflower knotweed extracting solution 5 ~ 20 parts, nettle extracting solution 5 ~ 20 parts, vegetables oil 20 ~ 90 parts.
More specifically, described vegetables oil is made up of shea butter and cocounut oil, and the proportioning of shea butter and cocounut oil is: shea butter 10 ~ 60 parts, cocounut oil 10 ~ 30 parts.
Present invention also offers the preparation method of above-mentioned hair soap: Chinese arborvitae twig extract 20 ~ 50 parts, Rosmarinus officinalis extracting solution 5 ~ 20 parts, Chinese honey locust extracting solution 10 ~ 30 parts, peppermint extracting solution 5 ~ 20 parts, tuber of multiflower knotweed extracting solution 5 ~ 20 parts, nettle extracting solution 5 ~ 20 parts are mixed, then in mixed solution, add vegetables oil 20 ~ 90 parts, 1 ~ 3 part, sodium hydroxide, be heated with stirring to 55 ~ 80 degree, stir after 5 ~ 40 minutes and stop heating, pour grinding tool into, be cooled to room temperature, obtain hair soap.
Vegetables oil in above-mentioned steps is made up of shea butter and cocounut oil.The proportioning of shea butter and cocounut oil is: shea butter 10 ~ 60 parts, cocounut oil 10 ~ 30 parts.
Raw material selected by the present invention, is natural phant, and wherein Leafy twigs of Oriental Arborvitae, Chinese honey locust, the tuber of multiflower knotweed have hair tonic, the black function sent out, and Rosmarinus officinalis can stimulate circulation, and hair follicle stimulating is active to be regenerated, and makes healthy hair gloss beautiful.Nettle can delay the sebum secretion of root of hair, makes that hair is fluffy vigor, suitable especially oiliness, easily alopecia crowd.Shea butter has moist function, can strengthen the moisture-retaining capacity of hair, can consolidate root of hair, moistens impaired root of hair, improve dandruff problem.Cocounut oil contains natural phant cleaning gene C
19h
38n
2o
3, foam is fine and smooth soft, deeply can permeate pore, the greasy dirt at cleaning head fur hole depth place and dandruff.
But can by the extracts active ingredients in above-mentioned crude substance out, this point is most important, therefore, the invention provides a kind of extracting method, concrete steps are as follows: step 1) get raw material clean, dry, pulverize, cross 40 mesh sieves, add 5-20 times of water, mix; Step 2) then at the temperature of-40 ~-20 DEG C freezing 10 ~ 24 hours, ambient temperatare is put until it melts; Repeat freezing-thawing step 2 ~ 3 times; Step 3) then carry out ultrasonic extraction, ultrasonic power is 60 ~ 100W; Ultrasonic temperature is 40 ~ 80 DEG C; Ultrasonic time is 20 ~ 60min; Step 4) mixed solution of gained carry out centrifugal, filter, get supernatant liquor, obtain the extracting solution of corresponding raw material.
Further research finds, if the step 2 described) and step 3) between increase a step: to step 2) in add cellulase 500 ~ 2000U/g in the mixed solution that obtains, edible citric acid is appropriate, adjust ph 4 ~ 6, temperature is 40 ~ 65 DEG C, after reaction 20 ~ 200min, then carry out step 3).The activeconstituents of various natural matter then effectively can be made to overflow, and there is the plurality of advantages such as quick, extraction yield is high, cost is low.
Beneficial effect: 1, the present invention, without the chemical composition such as silicone oil, pore forming material, adopts All Pure Nature raw material, non-pigment, without essence, preservative-free, has no side effect to human body.Meanwhile, the extract containing Leafy twigs of Oriental Arborvitae in hair soap provided by the present invention, has effect of cooling blood for hemostasis, growing and blacking hair.
2, methods combining provided by the present invention freeze thawing and ultrasonic, the destruction of ultrasonic cavatition cell membrane contributes to release and the stripping of activeconstituents, ultrasonic wave makes extracting solution constantly shake, and contributes to solutes accumulation.Thus greatly can shorten extraction time, improve the utilization ratio of extraction yield and raw material, and the activity of composition of remaining valid.
3, method provided by the present invention additionally uses cellulase, and by the high specificity of enzyme, degradation of cell surface tissue, make intracellular organic matter stripping, operation is simple, can significantly improve the extraction yield of activeconstituents, is conducive to the preparation of hair soap.
Embodiment:
Embodiment 1
Step 1) get Leafy twigs of Oriental Arborvitae clean, dry, pulverize, cross 40 mesh sieves, add 5 times of water, mix.
Step 2) by step 1) mixed solution that obtains at the temperature of-40 ~-20 DEG C freezing 10 hours, ambient temperatare is put until it melts; Repeat freezing-thawing step 2 ~ 3 times; So, cell can, at formation ice pellets with while increasing residue cytosol salt concn, occur swelling, broken.Activeconstituents is fully discharged, and keeps active.
Step 3) by step 2) gained mixed solution carries out supersound extraction, ultrasonic power is 60W; Ultrasonic temperature is 40 DEG C; Ultrasonic time is 20min.
Step 4) by step 3) mixed solution of gained carry out centrifugal, filter, get supernatant liquor, obtain Chinese arborvitae twig extract.
Step 5) repeating step 1) ~ step 4) and produce respectively Rosmarinus officinalis, Chinese honey locust, peppermint, the tuber of multiflower knotweed, nettle extracting solution.
Step 6) get Chinese arborvitae twig extract 20 parts, Rosmarinus officinalis extracting solution 5 parts, Chinese honey locust extracting solution 10 parts, peppermint extracting solution 5 parts, tuber of multiflower knotweed extracting solution 5 parts, nettle extracting solution 5 parts, be heated to 55 degree, mix; Get shea butter 10 parts, cocounut oil 10 parts, be heated to 55 degree, mix; The extracting solution of equal temperature and vegetables oil are mixed, stirs, add 1 part, sodium hydroxide, stir under 55 DEG C of conditions after 5 minutes and stop heating, pour grinding tool into, be cooled to room temperature, obtain hair soap.
Embodiment 2
Step 1) get Leafy twigs of Oriental Arborvitae clean, dry, pulverize, cross 40 mesh sieves, add 20 times of water, mix.
Step 2) by step 1) mixed solution that obtains at the temperature of-40 ~-20 DEG C freezing 24 hours, ambient temperatare is put until it melts; Repeat freezing-thawing step 2 ~ 3 times; So, cell can, at formation ice pellets with while increasing residue cytosol salt concn, occur swelling, broken.Activeconstituents is fully discharged, and keeps active.
Step 3) by step 2) gained mixed solution carries out supersound extraction, ultrasonic power is 100W; Ultrasonic temperature is 80 DEG C; Ultrasonic time is 60min.
Step 4) by step 3) mixed solution of gained carry out centrifugal, filter, get supernatant liquor, obtain Chinese arborvitae twig extract.
Step 5) repeating step 1) ~ step 4) and produce respectively Rosmarinus officinalis, Chinese honey locust, peppermint, the tuber of multiflower knotweed, nettle extracting solution.
Step 6) get Chinese arborvitae twig extract 50 parts, Rosmarinus officinalis extracting solution 20 parts, Chinese honey locust extracting solution 30 parts, peppermint extracting solution 20 parts, tuber of multiflower knotweed extracting solution 20 parts, nettle extracting solution 20 parts be heated to 80 degree, mix; Get shea butter 30 parts, cocounut oil 60 parts is heated to 80 degree, mix, the extracting solution of equal temperature and vegetables oil are mixed, stir, add 3 parts, sodium hydroxide, stir under 80 DEG C of conditions after 40 minutes and stop heating, pour grinding tool into, be cooled to room temperature, obtain hair soap.
Embodiment 3
Step 1) get Leafy twigs of Oriental Arborvitae clean, dry, pulverize, cross 40 mesh sieves, add 10 times of water, mix.
Step 2) by step 1) mixed solution that obtains at the temperature of-40 ~-20 DEG C freezing 15 hours, ambient temperatare is put until it melts; Repeat freezing-thawing step 2 ~ 3 times; So, cell can, at formation ice pellets with while increasing residue cytosol salt concn, occur swelling, broken.Activeconstituents is fully discharged, and keeps active.
Step 3) by step 2) mixed solution of gained adds cellulase 250U/g, edible citric acid is appropriate, and adjust ph 4 ~ 6, temperature is 40 DEG C, reaction times 20min.
Step 4) by step 3) gained mixed solution carries out supersound extraction, ultrasonic power is 70W; Ultrasonic temperature is 50 DEG C; Ultrasonic time is 30min.
Step 5) mixed solution of step (4) gained carried out centrifugal, filter, get supernatant liquor, obtain Chinese arborvitae twig extract.
Step 6) repeating step 1) ~ step 5) and produce respectively Rosmarinus officinalis, Chinese honey locust, peppermint, the tuber of multiflower knotweed, nettle extracting solution.
Step 7) get Chinese arborvitae twig extract 30 parts, Rosmarinus officinalis extracting solution 10 parts, Chinese honey locust extracting solution 15 parts, peppermint extracting solution 10 parts, tuber of multiflower knotweed extracting solution 10 parts, nettle extracting solution 10 parts be heated to 60 degree, mix; Get shea butter 15 parts, cocounut oil 20 parts, be heated to 60 degree, mix; The extracting solution of equal temperature and vegetables oil are mixed, stir, add 2 parts, sodium hydroxide, stir under 60 DEG C of conditions after 5 minutes and stop heating, pour grinding tool into, be cooled to room temperature, obtain hair soap.
Embodiment 4
Step 1) get Leafy twigs of Oriental Arborvitae clean, dry, pulverize, cross 40 mesh sieves, add 15 times of water, mix.
Step 2) by step 1) mixed solution that obtains at the temperature of-40 ~-20 DEG C freezing 20 hours, ambient temperatare is put until it melts; Repeat freezing-thawing step 2 ~ 3 times; So, cell can, at formation ice pellets with while increasing residue cytosol salt concn, occur swelling, broken.Activeconstituents is fully discharged, and keeps active.
Step 3) by step 2) mixed solution of gained adds cellulase 2000U/g, edible citric acid is appropriate, and adjust ph 4 ~ 6, temperature is 65 DEG C, reaction times 200min.
Step 4) by step 3) gained mixed solution carries out supersound extraction, ultrasonic power is 80W; Ultrasonic temperature is 60 DEG C; Ultrasonic time is 50min.
Step 5) mixed solution of step (4) gained carried out centrifugal, filter, get supernatant liquor, obtain Chinese arborvitae twig extract.
Step 6) repeating step 1) ~ step 5) and produce respectively Rosmarinus officinalis, Chinese honey locust, peppermint, the tuber of multiflower knotweed, nettle extracting solution.
Step 7) get Chinese arborvitae twig extract 40 parts, Rosmarinus officinalis extracting solution 15 parts, Chinese honey locust extracting solution 20 parts, peppermint extracting solution 15 parts, tuber of multiflower knotweed extracting solution 15 parts, nettle extracting solution 15 parts be heated to 70 degree, mix; Get shea butter 20 parts, cocounut oil 40 parts is heated to 80 degree, mix, the extracting solution of equal temperature and vegetables oil are mixed, stir, add 3 parts, sodium hydroxide, stir under 80 DEG C of conditions after 40 minutes and stop heating, pour grinding tool into, be cooled to room temperature, obtain hair soap.
The product of above-described embodiment 1 ~ 4 gained is used for hair washing, after hair washing, hair is more fluffy, soft and non-greasy.Because the present invention adopts the raw material of All Pure Nature, human-body safety is had no side effect.In addition, add the extraction scheme of cellulase, the extraction for effective components in plants is more abundant, is conducive to cost-saving.
Claims (7)
1. the hair soap containing Leafy twigs of Oriental Arborvitae, it is characterized in that its main raw material comprises plant extraction liquid and vegetables oil, described plant extraction liquid is made up of Chinese arborvitae twig extract, Rosmarinus officinalis extracting solution, Chinese honey locust extracting solution, peppermint extracting solution, tuber of multiflower knotweed extracting solution and nettle extracting solution.
2. hair soap as claimed in claim 1, it is characterized in that according to the mass fraction, the proportioning of main raw material is: Chinese arborvitae twig extract 20 ~ 50 parts, Rosmarinus officinalis extracting solution 5 ~ 20 parts, Chinese honey locust extracting solution 10 ~ 30 parts, peppermint extracting solution 5 ~ 20 parts, tuber of multiflower knotweed extracting solution 5 ~ 20 parts, nettle extracting solution 5 ~ 20 parts, vegetables oil 20 ~ 90 parts.
3. hair soap as claimed in claim 1, it is characterized in that described vegetables oil is made up of shea butter and cocounut oil, the proportioning of shea butter and cocounut oil is: shea butter 10 ~ 60 parts, cocounut oil 10 ~ 30 parts.
4. the preparation method of hair soap described in claim 1, it is characterized in that carrying out according to the following steps: by Chinese arborvitae twig extract 20 ~ 50 parts, Rosmarinus officinalis extracting solution 5 ~ 20 parts, Chinese honey locust extracting solution 10 ~ 30 parts, peppermint extracting solution 5 ~ 20 parts, tuber of multiflower knotweed extracting solution 5 ~ 20 parts, nettle extracting solution 5 ~ 20 parts of Hybrid Heating, stir and obtain plant extraction liquid;
Then vegetables oil 20 ~ 90 parts is heated to the uniform temp of plant extraction liquid;
Plant milk extract is mixed with vegetables oil, at 55 ~ 80 DEG C, adds 1 ~ 3 part, sodium hydroxide, stir after 5 ~ 40 minutes and stop heating, pour grinding tool into, be cooled to room temperature, obtain hair soap.
5. preparation method as claimed in claim 4, it is characterized in that described vegetables oil is made up of shea butter and cocounut oil, the proportioning of shea butter and cocounut oil is: shea butter 10 ~ 60 parts, cocounut oil 10 ~ 30 parts.
6. preparation method as claimed in claim 4, is characterized in that the extracting solution of described each raw material obtains by the following method:
Step 1) get raw material clean, dry, pulverize, cross 40 mesh sieves, add 5-20 times of water, mix;
Step 2) then at the temperature of-40 ~-20 DEG C freezing 10 ~ 24 hours, ambient temperatare is put until it melts; Repeat freezing-thawing step 2 ~ 3 times;
Step 3) then carry out ultrasonic extraction, ultrasonic power is 60 ~ 100W; Ultrasonic temperature is 40 ~ 80 DEG C; Ultrasonic time is 20 ~ 60min;
Step 4) mixed solution of gained carry out centrifugal, filter, get supernatant liquor, obtain the extracting solution of corresponding raw material.
7. preparation method as claimed in claim 4, it is characterized in that in described step 2) and step 3) between increase a step: to step 2) in add cellulase 500 ~ 2000U/g in the mixed solution that obtains, edible citric acid is appropriate, adjust ph 4 ~ 6, temperature is 40 ~ 65 DEG C, after reaction 20 ~ 200min, then carry out step 3).
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Cited By (8)
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CN105586181A (en) * | 2016-01-15 | 2016-05-18 | 南京科技职业学院 | Natural mung bean soap and preparation method thereof |
CN106047538A (en) * | 2016-06-11 | 2016-10-26 | 张家界茶坤缘生物科技开发有限公司 | Healthy soap containing original eucommia ulmoide extract and preparation method of healthy soap |
CN107034050A (en) * | 2017-05-08 | 2017-08-11 | 北京联合大学 | One kind contains gleditsia sinensis and the two-in-one hair soap of semen armeniacae amarae and preparation method thereof |
CN107034051A (en) * | 2017-05-08 | 2017-08-11 | 北京联合大学 | One kind is containing amygdalate hair soap and preparation method thereof |
CN107502492A (en) * | 2017-08-22 | 2017-12-22 | 卢倩 | One kind hair care handmade soap formula and preparation method thereof |
CN109512757A (en) * | 2018-11-22 | 2019-03-26 | 刘真 | A kind of hair soap and preparation method thereof |
CN109825387A (en) * | 2019-04-02 | 2019-05-31 | 海南师范大学 | A kind of Anti-hair loss black hair hair soap and preparation method thereof |
CN110669598A (en) * | 2019-10-18 | 2020-01-10 | 王晓孟 | Traditional Chinese medicine shampoo soap and preparation method thereof |
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CN105586181A (en) * | 2016-01-15 | 2016-05-18 | 南京科技职业学院 | Natural mung bean soap and preparation method thereof |
CN106047538A (en) * | 2016-06-11 | 2016-10-26 | 张家界茶坤缘生物科技开发有限公司 | Healthy soap containing original eucommia ulmoide extract and preparation method of healthy soap |
CN107034050A (en) * | 2017-05-08 | 2017-08-11 | 北京联合大学 | One kind contains gleditsia sinensis and the two-in-one hair soap of semen armeniacae amarae and preparation method thereof |
CN107034051A (en) * | 2017-05-08 | 2017-08-11 | 北京联合大学 | One kind is containing amygdalate hair soap and preparation method thereof |
CN107034051B (en) * | 2017-05-08 | 2019-11-15 | 北京联合大学 | One kind is containing amygdalate hair soap and preparation method thereof |
CN107034050B (en) * | 2017-05-08 | 2019-11-15 | 北京联合大学 | One kind containing gleditsia sinensis and the two-in-one hair soap of semen armeniacae amarae and preparation method thereof |
CN107502492A (en) * | 2017-08-22 | 2017-12-22 | 卢倩 | One kind hair care handmade soap formula and preparation method thereof |
CN109512757A (en) * | 2018-11-22 | 2019-03-26 | 刘真 | A kind of hair soap and preparation method thereof |
CN109825387A (en) * | 2019-04-02 | 2019-05-31 | 海南师范大学 | A kind of Anti-hair loss black hair hair soap and preparation method thereof |
CN110669598A (en) * | 2019-10-18 | 2020-01-10 | 王晓孟 | Traditional Chinese medicine shampoo soap and preparation method thereof |
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