CN110037943B - Cyperus esculentus eye cream added with cyperus esculentus root oil - Google Patents

Cyperus esculentus eye cream added with cyperus esculentus root oil Download PDF

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CN110037943B
CN110037943B CN201910258939.0A CN201910258939A CN110037943B CN 110037943 B CN110037943 B CN 110037943B CN 201910258939 A CN201910258939 A CN 201910258939A CN 110037943 B CN110037943 B CN 110037943B
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cyperus esculentus
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宋超
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/005Preparations for sensitive skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

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Abstract

The invention provides a cyperus esculentus eye cream added with cyperus esculentus root oil, wherein cyperus esculentus root oil is added into a moisturizing and soft-moistening matrix consisting of a plurality of oily substances, and cyperus esculentus root oil has the effects of moistening and repairing skin, can deeply moisten eye skin, smooth fine lines of eyes, improve the problems of black eyes, eye bags and the like, is extracted from pure plants, has mild properties, does not stimulate the eye skin, does not cause any damage to the skin, enables the skin to be full of moisture, can inhibit the regeneration of wrinkles, black eyes, eye bags and the like after long-term use, and can continuously repair the eye skin.

Description

Cyperus esculentus eye cream added with cyperus esculentus root oil
Technical Field
The invention relates to the field of skin care products, in particular to cyperus esculentus eye cream added with cyperus esculentus root oil.
Background
Eyes are the window of soul, eye skin is the thinnest skin of a human body, is the part with the most frequent movement, is the place with the most skin pulling times in makeup, is very easy to grow wrinkles, and is difficult to disappear once growing.
Modern life style is gradually changed, the modern faces an electronic screen almost every moment in work, and the amateur life after work is occupied by electronic products such as mobile phones and flat panels, so that eye muscles are in a tight state for a long time, and aging of eye skin is aggravated.
The existing eye care products are mainly applied and dressed externally, the eye care products generally form a film on the skin around eyes by adding various moistening agents and film forming agents to cover wrinkles and black eyes on the skin around the eyes, the skin problem cannot be fundamentally solved, the moistening agents and the film forming agents are mostly chemical synthetic substances and can generate certain harm to the skin after long-term use, in order to minimize the harm of the skin care products to the skin of a human body, more and more skin care products adopt plant extracts as the components of the skin care products, the harm of the skin care products to the skin is greatly reduced by natural plant components, but common plants only have one or two skin care effects, and the problem of various skins cannot be solved.
The cyperus esculentus is a plant originally produced in Mediterranean areas, is introduced into China from the Soviet Union in the last century and starts to be planted, the cyperus esculentus mainly harvests tuberous roots which are longer than underground, and the root of the cyperus esculentus is rich in grease, so that oil is commonly used for squeezing.
Therefore, the cyperus esculentus eye cream added with cyperus esculentus root oil is pure plant extract, has mild properties, does not stimulate eye skin, does not cause any damage to the skin, enables the skin to be full of moisture, can inhibit the regeneration of wrinkles, black eye circles, eye bags and the like after long-term use, can continuously repair the special penetrating power of the eye skin, and can effectively enter the deep layer of the skin so as to achieve the effect of deep water replenishing, and the components in the cyperus esculentus root oil have the effects of moisturizing, removing wrinkles and lightening spots, and can deeply repair the skin.
Disclosure of Invention
The invention aims to provide cyperus esculentus eye cream added with cyperus esculentus root oil, which aims to solve the problems that the existing eye cream only has a concealing function and cannot fundamentally solve the skin problem, and most of cyperus esculentus root oil is chemical additive substances and causes certain harm to human body after long-term use.
In order to achieve the purpose, the invention provides the following scheme:
the invention provides cyperus esculentus eye cream added with cyperus esculentus root oil, which comprises the following components in parts by mass: 0.05-9 parts of cyperus esculentus root oil, 35-65 parts of moisturizing soft and moist matrix, 0.8-4 parts of skin repair component, 0.2-1 part of pH value regulator, 0.1 part of preservative, 0.3 part of daily plant extract essence, 100 parts in total, and the balance of deionized water;
the extraction method of the cyperus esculentus root oil comprises the following steps:
(1) selecting, cleaning, drying in the sun or by baking, and reserving pretreated cyperus esculentus roots for later use;
(2) extracting oily liquid of cyperus esculentus roots by adopting a cold pressing mode to obtain primary oil, and controlling the cold pressing temperature to be 15-35 ℃;
(3) the extracted oil is cyperus oil.
Preferably, the moisturizing and softening matrix comprises the following components:
Figure GSB0000181873850000021
Figure GSB0000181873850000031
preferably, the skin repair ingredients comprise:
Figure GSB0000181873850000032
preferably, the PH adjuster is:
0.1 to 0.5 portion of triethanolamine
0.1-0.5 part of EDTA disodium
Preferably, the preservative comprises:
0.05 part of phenoxyethanol
0.05 part of p-hydroxyacetophenone
A preparation method of cyperus esculentus eye cream added with cyperus esculentus root oil comprises the following steps:
(1) keeping the Cyperus esculentus root oil at 40 ℃ under the pressure of 20MPa, and standing for 1 h;
(2) adding the processed cyperus esculentus root oil into the moisture-preserving soft-moistening matrix, heating to 65-85 ℃, and stirring for 0.5h to prepare an oil phase;
(3) adding the skin repairing component into deionized water, mixing, and heating to 55-75 ℃ to prepare a water phase;
(4) mixing the oil phase and the water phase in a vacuum homogenizer, homogenizing and dissolving, controlling the temperature to be 45-60 ℃, adding a preservative, and stirring for 0.5 h; when the temperature is 40-55 ℃, adding the essence extracted from daily plants, stirring to 35 ℃, adding the pH value regulator, and continuing stirring for 1-2 hours to obtain the cyperus esculentus eye cream added with cyperus esculentus root oil.
Preferably, the stirring speed in the step (4) is 55-70 r/min.
Wherein, each component in the moisturizing soft and moist matrix has the functions of moisturizing and moistening the skin, and each component in the skin repairing component has the functions of repairing cells and improving the activity of the cells.
Compared with the prior art, the invention has the following beneficial technical effects:
the invention provides a cyperus esculentus eye cream added with cyperus esculentus root oil, wherein cyperus esculentus root oil is added into a moisturizing and soft-moistening matrix consisting of a plurality of oily substances, and cyperus esculentus root oil has the effects of moistening and repairing skin, can deeply moisten eye skin, smooth fine lines of eyes, improve the problems of black eyes, eye bags and the like, is extracted from pure plants, has mild properties, does not stimulate the eye skin, does not cause any damage to the skin, enables the skin to be full of moisture, can inhibit the regeneration of wrinkles, black eyes, eye bags and the like after long-term use, and can continuously repair the eye skin.
Detailed Description
The technical solutions in the embodiments of the present invention are clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention aims to provide cyperus esculentus eye cream added with cyperus esculentus root oil, which solves the problems that the existing eye cream only has a concealing function and cannot fundamentally solve skin problems, and most of cyperus esculentus root oil is chemical additive substances and causes certain harm to human body after long-term use by adding cyperus esculentus root oil into a moisturizing and soft substrate.
In order to make the above objects, features and advantages of the present invention more comprehensible, the present invention is described in further detail below with reference to examples, comparative examples and test examples.
Example 1:
table 1 shows the parts by mass of each component in a cyperus esculentus eye cream added with cyperus esculentus root oil provided in example 1.
Figure GSB0000181873850000051
TABLE 1
Taking 0.5g of cyperus esculentus root oil, keeping the temperature at 40 ℃ under the pressure of 20MPa, and standing for 1 h; 5g of cyclopentadimethylsiloxane, 5g of polydimethylsiloxane crosspolymer, 5g of polyvinylpyrrolidone, 5g of glycerol, 1g of hydrogenated polyisobutene, 1g of erythritol, 1g of sodium acrylate/sodium acryloyldimethyltaurate copolymer, 1g of isohexadecane, 1g of polysorbate-80, 1g of hydrolyzed vegetable protein, 1g of ethylhexyl glycerol, 1g of butanediol, 1g of sodium hyaluronate, 1g of PEG-60 hydrogenated castor oil, 1g of propylene glycol, 1g of acrylic acid (ester)/C10-30 alkanol acrylate crosspolymer, 1g of bis-PEG/PPG-16/16 PEG/PPG-16/16 polydimethylsiloxane, 0.5g of caprylic/capric triglyceride, 0.5g of 1, 2-hexanediol, 0.5g of 1, 6-hexanediol, a mixture of ethylene glycol, propylene glycol, and propylene glycol, and propylene glycol, Mixing 0.5g of moisturizing soft and moist matrix composed of acrylic acid (ester) copolymer sodium and pretreated cyperus oil, heating to 75 ℃, and stirring for 0.5h to obtain an oil phase; adding skin repairing component composed of 0.2g Bacillus/semen glycines fermented product extract, 0.2g folic acid, 0.2g tocopherol acetate and 0.2g hydroxydecyl ubiquinone into 63.1g deionized water, mixing, heating to 65 deg.C to obtain water phase; mixing the oil phase and the water phase in a vacuum homogenizer, homogenizing and dissolving, controlling the temperature at 57 ℃, adding a preservative consisting of 0.05g of phenoxyethanol and 0.05g of p-hydroxyacetophenone, stirring for 0.5h, adding 0.3g of daily plant extract essence when the temperature is reduced to 47 ℃, stirring to 35 ℃, adding 0.1g of triethanolamine and 0.1g of disodium EDTA to adjust the pH value, and continuously stirring for 2h at the stirring speed of 60r/min to obtain the cyperus esculentus eye cream added with cyperus esculentus root oil.
In the cyperus esculentus eye cream added with cyperus esculentus root oil provided by the embodiment, in order to volatilize and release active substances in the cyperus esculentus root oil, the cyperus esculentus root oil is pretreated in a pressurized standing mode so as to thoroughly volatilize the active substances in the cyperus esculentus root oil.
In other embodiments, the volatilization of the effective components of the cyperus rotundus can be achieved by shaking the cyperus rotundus root oil, and the like, and the treatment method which can maximize the efficacy of the cyperus rotundus root oil is within the protection scope of the invention.
When the eye cream is used, the face is cleaned firstly, the cyperus esculentus eye cream added with cyperus esculentus root oil provided by the invention is gently kneaded to be slightly transparent by hands, the finger abdomen is used for uniformly coating the eye cream around eyes, the eye cream is gently massaged until the eye cream is completely absorbed, and the eye cream is used twice a day, morning and evening, so that the effect is better.
Example 2:
table 2 shows the parts by mass of each component in the cyperus esculentus eye cream added with cyperus esculentus root oil provided in example 2.
Figure GSB0000181873850000061
Figure GSB0000181873850000071
TABLE 2
Example 3:
table 3 shows the parts by mass of each component in an cyperus esculentus eye cream added with cyperus esculentus root oil provided in example 3.
Figure GSB0000181873850000072
Figure GSB0000181873850000081
TABLE 3
Example 4:
table 4 shows the parts by mass of each component in the cyperus esculentus eye cream added with cyperus esculentus root oil provided in example 4.
Figure GSB0000181873850000082
Figure GSB0000181873850000091
TABLE 4
Example 5:
table 5 shows the parts by mass of each component in an cyperus esculentus eye cream added with cyperus esculentus root oil provided in example 5.
Figure GSB0000181873850000092
Figure GSB0000181873850000101
TABLE 5
Example 6:
table 6 shows the parts by mass of each component in an cyperus esculentus eye cream added with cyperus esculentus root oil provided in example 6.
Figure GSB0000181873850000102
Figure GSB0000181873850000111
TABLE 6
Example 7:
table 7 shows the parts by mass of each component in an cyperus esculentus eye cream added with cyperus esculentus root oil provided in example 7.
Figure GSB0000181873850000112
Figure GSB0000181873850000121
TABLE 7
Example 8:
table 8 shows the parts by mass of each component in the cyperus esculentus eye cream added with cyperus esculentus root oil provided in example 8.
Figure GSB0000181873850000122
TABLE 8
Comparative example 1:
table 9 shows the parts by mass of each component in the cyperus esculentus eye cream added with cyperus esculentus root oil provided in comparative example 1.
Figure GSB0000181873850000131
TABLE 9
Comparative example 2:
table 10 shows the parts by mass of each component in the cyperus esculentus eye cream added with cyperus esculentus root oil provided in comparative example 2.
Figure GSB0000181873850000141
Watch 10
The preparation methods and the use methods of the above examples 2 to 8 and comparative examples 1 to 2 were the same as those of example 1, except that the raw material component ratios were different from those of example 1.
The eye cream prepared according to the formula is used for a comparative test, 10 groups of women with the average age of 40 years are selected, 10 women in each group have eye skin problems, 100 women in each group use the eye creams in the embodiments 1-8 and the comparative examples 1-2 respectively, the eye cream is used after face cleaning in the morning and at night every day, and after 90 days, the skin of the women is detected, wherein the detection content comprises: whether allergy exists after the eye drop is used, whether black eye circles disappear, whether bags under the eyes disappear, and whether fine wrinkles in the eyes disappear.
The following are the recorded results for each test example:
test example 1:
table 11 shows the data records of test example 1.
Figure GSB0000181873850000151
TABLE 11
Test example 2:
table 12 shows the data records of test example 2.
Figure GSB0000181873850000152
TABLE 12
Test example 3:
table 13 shows the data records of test example 3.
Figure GSB0000181873850000153
Watch 13
Test example 4:
table 14 shows the data records of test example 4.
Figure GSB0000181873850000161
TABLE 14
Test example 5:
table 15 shows the data records of test example 5.
Figure GSB0000181873850000162
Watch 15
Test example 6:
table 16 shows data records of test example 6.
Figure GSB0000181873850000163
TABLE 16
Test example 7:
table 17 shows the data records of test example 7.
Figure GSB0000181873850000164
TABLE 17
Test example 8:
table 18 shows data records of test example 8.
Figure GSB0000181873850000171
Watch 18
Test example 9:
table 19 shows the data records of test example 9.
Figure GSB0000181873850000172
Watch 19
Test example 10:
table 20 shows data records of test example 10.
Figure GSB0000181873850000173
Watch 20
The experimental examples show that the eye cream containing cyperus rotundus root oil (examples 1-8) can not cause anaphylactic reaction and damage skin, the eye cream without cyperus rotundus root oil (comparative examples 1-2) can cause anaphylactic reaction and damage skin to a certain extent, and longitudinal comparison can also show that the eye cream has certain effect on skin care due to the number of the heat-preservation soft-moistening matrix and the skin repair components, but is not obvious, and eye skin problems such as dark circles, eye bags, fine lines and the like are well improved along with the increase of cyperus rotundus root oil, so that cyperus rotundus root oil is pure natural, can not cause damage to skin, can repair aged eye skin cells, and has good effect on eye skin care.
In test example 8, a 35-year-old female, a 40-year-old female, and a 45-year-old female were selected, followed, and skin condition was carefully examined for 90 days of use, with the following results:
Figure GSB0000181873850000181
after women of different ages use the eye cream added with the cyperus oil, the problem of eye skin is greatly improved, wherein the improvement is more obvious when the women of different ages use the eye cream, and the problems of under-eye bags, black eyes and fine lines of eyes can be gradually eliminated after the eye cream is used for a long time.
The principle and the implementation mode of the invention are explained by applying specific examples, and the description of the above examples is only used for helping understanding the method and the core idea of the invention; meanwhile, for a person skilled in the art, according to the idea of the present invention, the specific embodiments and the application range may be changed. In summary, this summary should not be construed to limit the present invention.

Claims (3)

1. The cyperus esculentus eye cream added with cyperus esculentus root oil is characterized in that: the cyperus esculentus eye cream added with cyperus esculentus root oil comprises the following components in parts by mass: 3-9 parts of cyperus esculentus root oil, 35-65 parts of moisturizing soft and moist matrix, 0.8-4 parts of skin repair ingredients, 0.2-1 part of pH value regulator, 0.1 part of preservative, 0.3 part of daily plant extract essence, 100 parts in total and the balance of deionized water;
the extraction method of the cyperus esculentus root oil comprises the following steps:
(1) selecting, cleaning, drying in the sun or by baking, and reserving pretreated cyperus esculentus roots for later use;
(2) extracting oily liquid of cyperus esculentus rhizomes in a cold pressing mode to obtain primary oil, and controlling the cold pressing temperature to be 15-35 ℃;
(3) the extracted oil is cyperus oil;
the moisturizing and softening matrix comprises the following components:
5-9 parts of cyclopenta dimethyl siloxane
5-9 parts of polydimethylsiloxane cross-linked polymer
5-9 parts of polyvinylpyrrolidone
5-8 parts of glycerol
1-2 parts of hydrogenated polyisobutene
1-2 parts of erythritol
1-2 parts of sodium acrylate/acryloyl dimethyl taurate copolymer
1-2 parts of isohexadecane
Polysorbate-801-2 parts
1-2 parts of hydrolyzed vegetable protein
1-2 parts of ethylhexyl glycerin
1-2 parts of butanediol
1-2 parts of sodium hyaluronate
1-2 parts of PEG-60 hydrogenated castor oil
1-2 parts of propylene glycol
1-2 parts of acrylic acid (ester)/C10-30 alkanol acrylate crosslinked polymer
1-2 parts of bis-PEG/PPG-16/16 PEG/PPG-16/16 polydimethylsiloxane
0.5-1 part of caprylic/capric triglyceride
0.5-1 part of 1, 2-hexanediol
0.5-1 part of 1, 6-hexanediol
0.5-1 part of acrylic acid (ester) copolymer sodium;
the skin repair ingredients include:
0.2-1 part of bacillus/soybean fermentation product extract
0.2-1 part of folic acid
0.2-1 part of tocopherol acetate
0.2-1 part of hydroxydecyl ubiquinone;
the pH value regulator is as follows:
0.1 to 0.5 portion of triethanolamine
0.1-0.5 part of EDTA disodium;
the preservative comprises:
0.05 part of phenoxyethanol
0.05 part of p-hydroxyacetophenone.
2. The method for preparing cyperus esculentus eye cream added with cyperus esculentus root oil according to claim 1, wherein: the manufacturing method comprises the following steps:
(1) keeping the Cyperus esculentus root oil at 40 ℃ under the pressure of 20MPa, and standing for 1 h;
(2) adding the processed cyperus esculentus root oil into the moisture-preserving soft-moistening matrix, heating to 65-85 ℃, and stirring for 0.5h to prepare an oil phase;
(3) adding the skin repairing component into deionized water, mixing, and heating to 55-75 ℃ to prepare a water phase;
(4) mixing the oil phase and the water phase in a vacuum homogenizer, homogenizing and dissolving, controlling the temperature to be 45-60 ℃, adding a preservative, and stirring for 0.5 h; when the temperature is 40-55 ℃, adding the essence extracted from daily-use plants, stirring to 35 ℃, adding the pH value regulator, and continuing stirring for 1-2 hours to obtain the cyperus esculentus eye cream added with cyperus esculentus root oil.
3. The method for preparing cyperus esculentus eye cream added with cyperus esculentus root oil according to claim 2, wherein: and (4) stirring at a rotating speed of 55-70 r/min.
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CN109394588A (en) * 2018-12-21 2019-03-01 广州善草纪化妆品有限公司 A kind of sunscreen composition, sunscreen product and its preparation method and application

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DE102012203986A1 (en) * 2012-03-14 2012-12-27 Henkel Ag & Co. Kgaa Composition, useful for treating hair, comprises a specified range of Cyperus esculentus tuber oil, a quaternary ammonium compound e.g. esterquat and an amino functional silicone
CN109394588A (en) * 2018-12-21 2019-03-01 广州善草纪化妆品有限公司 A kind of sunscreen composition, sunscreen product and its preparation method and application

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罗格珂天然化妆品公司.伊丽萃璞多重活效抗皱眼霜.《国家药品监督管理局—进口化妆品查询》.2013, *

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