CN105476877A - Facial cleanser - Google Patents

Facial cleanser Download PDF

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Publication number
CN105476877A
CN105476877A CN201511007866.6A CN201511007866A CN105476877A CN 105476877 A CN105476877 A CN 105476877A CN 201511007866 A CN201511007866 A CN 201511007866A CN 105476877 A CN105476877 A CN 105476877A
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Prior art keywords
parts
cleansing milk
minutes
surfactant
gained
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CN201511007866.6A
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Chinese (zh)
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CN105476877B (en
Inventor
徐万锡
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Suzhou Industrial Park Anewcos Cosmetics R & D Co Ltd
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Suzhou Industrial Park Anewcos Cosmetics R & D Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/736Chitin; Chitosan; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/733Alginic acid; Salts thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/85Polyesters
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/008Preparations for oily skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations

Abstract

The invention discloses a facial cleanser. According to the main points of the technical scheme, the facial cleanser is prepared from the following components in parts by weight: 0.1-10 parts of an acrylate/C10-C30 alkanol acrylate cross-linked polymer, 5-50 parts of a surfactant, 0.2-11 parts of a preservative, 5-50 parts of a humectant, 2.3-22 parts of skincare components, 0.1-10 parts of an anticaking agent, 5-10 parts of a chitosan affinity membrane, 1-3 parts of all-carbon aerogel, 5-10 parts of an aid-grinding material and 20-50 parts of deionized water. The facial cleanser has the advantages that the all-carbon aerogel is added to the surfactant-type facial cleanser, so that the oil-absorption and degreasing effects of the surfactant-type facial cleanser with relatively weak degreasing ability can be effectively improved; the facial cleanser has good moisturizing properties through coordination of the chitosan affinity membrane and the humectant; and the facial cleanser can be applicable to a user with dry skin.

Description

Cleansing milk
Technical field
The present invention relates to a kind of daily use chemicals cleaning supplies, more particularly, it relates to a kind of cleansing milk.
Background technology
Liking to be beautiful is the nature of people, keep that specious what first will accomplish is exactly keep clean, face is as the shop front of people, keep the clean particularly important of face, in order to realize effectively cleaning face, abundant removing spot on the face and oils and fats, people have invented this cleaning supplies being specifically designed to clean face of cleansing milk.Cleansing milk as facial cleansing agent gradually accept by consumer, it is the face cleaning product for the purpose of cleaning skin, and the good cleaning strength of existing soap, has again certain nursing function.Cleansing milk is different by production technology, can be divided into surfactant type and soap base type cleansing milk.Cleansing milk is a kind of senior agent that washes one's face.Colory cleansing milk should have the effects such as clean, nutrition, protection skin.In general, common cleansing milk does not have whitening effect.If add appropriate skin-whitening agents again in high-quality cleansing milk, for a long time with having white-skinned face function.Cleansing milk includes: the types such as facial milk cleanser, facial cleaning cream, clean skin liquid.
When selecting cleansing milk, people often restrict by the skin type of oneself, consumer for inclined dry skin just can not use soap base cleansing milk, soap base cleansing milk has very strong effect of deoiling, dry skin person can make skin very dry after using, and then skin can be caused uncomfortable, injury skin, therefore dry skin person must use surfactant type cleansing milk, same, oily skin person can not use surfactant type cleansing milk, because although surfactant type cleansing milk character is comparatively gentle, not easily injured skin, but for oily skin person, use the oils and fats that surfactant type cleansing milk is difficult on cleaning skin effectively and in pore, if things go on like this can make oils and fats and accumulation of mud in pore, and then breed bacteria, cause such as acne, a series of skin problem such as acne.
Summary of the invention
For the deficiency that prior art exists, the object of the present invention is to provide a kind of cleansing milk that simultaneously can be suitable for dry skin and oily skin.
For achieving the above object, the invention provides following technical scheme: a kind of cleansing milk, the recipe ingredient of this cleansing milk by weight mark is counted
Esters of acrylic acid/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer 0.1 ~ 10 part
5 ~ 50 parts, surfactant
Antiseptic 0.2 ~ 11 part
Wetting agent 5 ~ 50 parts
Skin care ingredient 2.3 ~ 22 parts
Anti-caking agent 0.1 ~ 10 part
Chitosan affinity membrane 5 ~ 10 parts
Full carbon aerogels 1 ~ 3 part
Grinding aid material 5 ~ 10 parts
Deionized water 20 ~ 50 parts.
Wherein: in surfactant type cleansing milk, add full carbon aerogels, can effectively for the more weak surfactant type cleansing milk of the ability of deoiling improves the effect of oil suction degreasing, oily skin user is made not have when using this cleansing milk unclean sensation of deoiling, optimize the cleaning effect of this cleansing milk, also in the formula of this cleansing milk, with the addition of chitosan affinity membrane simultaneously, complete with this cleansing milk clean to the washing of face after, chitosan affinity membrane can form layer protecting film at skin surface as a kind of film forming matter, esters of acrylic acid in addition in formula/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer is as a kind of cross linked polymer of macromolecule, the wetting agent that contains in this cleansing milk and skin care ingredient can be made evenly to be locked in cleansing milk by network-like cross linked polymer subregion, when using this cleansing milk to wash one's face, esters of acrylic acid/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer is opened gradually under the effect of moisture and surfactant, the wetting agent be coated on wherein and skin care ingredient are discharged gradually, make it to be coated on facial skin equably, coordinate chitosan affinity membrane, the protecting film that can realize lasting moisturizing and skin protection is defined at skin surface, thus enable dry skin person's skin after this cleansing milk of use washes one's face keep moistening, can not feel dry and astringent to feel bad.
Preferably, described surfactant is one or more in sodium lauroyl glutamate, lecithin and fluorocarbon surfactant.
Wherein: surfactant preferably lecithin and fluorocarbon surfactant, lecithin is the indispensable material of each cell of human body, if lacked, the regeneration capacity of Skin Cell will be reduced, cause pachylosis, there is wrinkle, if suitably absorb lecithin, skin regeneration vigor just can ensure, add the good hydrophilic of lecithin and lipophile, contribute to the glossiness improving user skin, coordinate the wetting agent in this cleansing milk and skin care ingredient to act on simultaneously simultaneously, better skin effect can be played, fluorocarbon surfactant fluorine element is the element that electronegativity is the strongest, it has high oxidation gesture, high ionization energy, this characteristic causes fluorine-carbon bond bond energy high on the one hand, in fact fluorine-carbon bond is the covalent bond that known bond energy is the highest, thus fluorocarbon chain structure is more than hydrocarbon Stability Analysis of Structures, fluorine atom is very difficult to polarized on the other hand, makes fluorocarbon chain polarity less than hydrocarbon chain.Exactly because this low polarity, make fluorocarbon chain hydrophobic interaction strong more than hydrocarbon chain, in fact, low polarity not only makes fluorocarbon chain hydrophobic, and the oil of but also oleophobic-here refers to hydrocarbon compound; In addition, low polarity causes again the mutual active force of fluorocarbon chain weak.These two factor combineds effect make fluorocarbon surfactant molecule have the tendency stronger than other surfactant molecule in aqueous to depart from aqueous solution, on liquid/gas interface, directed gathering is arranged in molecular film, thus makes it have the surface tension that just significantly can reduce aqueous solution with other surfactant difference two kinds of characteristics (1) under extremely low application concentration.Some fluorocarbon surfactant, just can drop to 18 ~ 20dyn/cm by aqueous solution surface tension when 50 ~ 100ppm.Mainly fluorocarbon chain hydrophobic interaction is strong for this, the reason that mutual molecular force is weak; (2) high surface activity, can drop to pole low-level by aqueous solution surface tension.Aqueous solution surface tension can be made to be down to 15 ~ 16dyn/cm as perfluorocarboxylic acid.This is because the fluorocarbon chain in fluorocarbon surfactant forms the monomolecular film of marshalling on aqueous solution surface, one deck fluorocarbons has been spread just as in solution surface, and fluorocarbons is typical low-surface-energy material, if ptfe surface can be 19dyn/cm.
Preferably, described antiseptic is one or more in trehalose, caprylyl glycol and potassium sorbate.
Wherein: trehalose can form unique protecting film at cell surface; protected protein matter molecule invariance inactivation effectively; thus the important component of cytoactive, moisturizing class cosmetics can be kept; here trehalose can either play good antisepsis; also the complementary element of skin care ingredient can be become; caprylyl glycol is that a kind of permeability is fine; and the anti-corrosion composition that toxicity is very little; potassium sorbate has very strong suppression putrefaction bacteria and mycete effect; and because of toxicity be low more than other antiseptic, therefore become topmost antiseptic in the world.
Preferably, described antiseptic is
Trehalose 0.1 ~ 10 part
Caprylyl glycol 0.1 ~ 1 part.
Preferably, described wetting agent is one or more in glycerol, chitin derivativ, ceramide and sorbitol.
Wherein: glycerol after absorption, can't discharge moisture again.And dynamically moisturizing can regulate moisture according to surrounding, if the moisture both in skin is less, so absorbed moisture can discharge by glycerol, thus realize the effect of long-acting moisturizing, moisture absorption, the performance of keeping humidity of chitin derivativ are close with hyaluronic acid, the hygroscopic capacity of every gram of wetting agent is approximately equal to moisture-holding capacity, its moistening effect long stable effect, be suitable as daily wetting agent, ceramide is also known as sphingolipid, be a kind of lipid being present in skin, play an important role in epidermal keratinocytes layer formation process.It is the structural units that sphingolipid has.Fatty acid has the structure of sour amido link on the amino of sphingol.If combine sugar thereon, just become glycosyl sphingolipid class, if in conjunction with phosphocholine, just become sphingomyelin.Ceramide is the mesostate of sphingolipid, especially on biosynthesis, important position is occupied, research in recent years shows, when drying, desquamation, cracking phenomena appear in skin, when its barrier function obviously reduces, skin supplements ceramide can recover rapidly moisturizing and barrier function, and sorbitol is used as the conditioning agent of toothpaste, cosmetics, Nicotiana tabacum L..Be sweet oil substitute, moisture retention comparatively glycerol relaxes, and taste is also better.Can with other wetting agents and use, in the hope of collaborative effect, be a kind of wetting agent adjuvant of good performance.
Preferably, described skin care ingredient is
Sensiva SC50 0.1 ~ 1 part
Arginine 0.1 ~ 10 part
Mactra veneriformis polysaccharide 0.1 ~ 1 part
Rhodiola crenulata extract 2 ~ 10 parts.
Wherein: Sensiva SC50 is moderate emollient, wetting agent and the wetting agent of a kind of spreading property.It can have again soft and smooth skinfeel while raising formula moisturizing effect.Be added in some cream frost system, can solve cream frost absorbs slow, shortcoming in the skinfeel such as to be clamminess and whitewash, Sensiva SC50 has deodorizing effect simultaneously, the material that sebum in human sweat and the epidermis cell etc. come off produce under the effect of gram positive bacteria has unhappy abnormal smells from the patient, Sensiva SC50 effectively can suppress the growth and breeding of the antibacterial causing abnormal flavour, do not affect the skin flora useful to human body simultaneously, thus play the effect of abnormal smells from the patient suppression, also can play antibacterial effect simultaneously, thus can skin health be protected, arginine is the indispensable nutrient of a kind of skin health, here as a kind of supplementary nutrient, Mactra veneriformis polysaccharide has good moistening effect, also there is the function of good antioxidation and reparation skin fiber, Rhodiola crenulata extract can significantly improve the activity of body superoxide dismutase, scavenging free radicals, LPO inhibitor, thus effectively suppress skin aging.
Preferably, described grinding aid material is the one or several in Semen Juglandis abrasive material and Herba bromi japonici abrasive material.
Wherein: the oils and fats that Semen Juglandis is rich in, be conducive to moist skin, Semen Juglandis also has stronger hardness simultaneously, supracutaneous cutin can be effectively ground off as grinding aid material, Herba bromi japonici contains a large amount of celluloses, as good grinding aid material, can be rich in magnesium, vitamin B1, phosphorus, potassium in Herba bromi japonici simultaneously, also containing nutrient substance such as ferrum, zinc, folic acid, pantothenic acid and copper, the function of nutrition skin-protection can be played.
Preferably, described anti-caking agent is the one in betanin and silicon dioxide.
Wherein: betanin is a kind of alkaline matter; there is strong moisture pick-up properties; so often anti-caking agent process can be used in processing technology; its advantage is soluble in water; effectively can clean dirt, indifferent equilibrium, not injure skin; silicon dioxide is then a kind of conventional anti-caking agent, and silicon dioxide also has good thickening effect simultaneously.
Prepare as arbitrary in claim 1-7 as described in the method for cleansing milk
Step one: by esters of acrylic acid/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer adds in the deionized water of 30 ~ 40 DEG C, insulation Keep agitation 15 ~ 20 minutes;
Step 2: surfactant, wetting agent and antiseptic are added successively in the product of gained in step one, is heated to 45 ~ 60 DEG C, is incubated and stirs 25 ~ 30 minutes, making it Homogeneous phase mixing;
Step 3: wetting agent and skin care ingredient are added in the product of step 2 gained, is cooled to 28 ~ 30 DEG C, is incubated and stirs 15 ~ 18 minutes;
Step 4: full carbon aerogels, anti-caking agent and grinding aid material are added in the product of step 3 gained, is incubated and vibrates 15 ~ 18 minutes;
Step 5: added by chitosan affinity membrane in the product of step 4 gained, is cooled to 25 DEG C, and insulation also mixes 8 ~ 10 minutes by ultrasound wave.
Wherein: preferentially putting into esters of acrylic acid/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer in step one is to process the entanglement result opening macromolecules cross-linking polymer under the environment of heating, make the follow-up component added can enter in macromolecular tangled structure, thus realize the abundant mixing of each component, surfactant is added subsequently in step 2, wetting agent and antiseptic are to effectively be mixed by these function ingredients at a higher temperature, in step 3, add wetting agent and skin care ingredient is again because these components are mostly and have bioactive material, need during heated and stirred to reduce temperature, these material inactive are made to prevent Yin Gaowen, and then reduction properties of product, vibrate in step 4 full carbon aerogels and grinding aid material is because these two components are solid granular material, simple stirring can increase the mobility of mixture, cause full carbon aerogels and grinding aid material generation sedimentation, be difficult to mix homogeneously, finally adding chitosan affinity membrane is because chitosan affinity membrane is film forming matter, need it in the end to be added obtain best covering property.
Compared with prior art the present invention has following advantage: in surfactant type cleansing milk, add full carbon aerogels, can effectively for the more weak surfactant type cleansing milk of the ability of deoiling improves the effect of oil suction degreasing, make this cleansing milk have good performance of keeping humidity by chitosan affinity membrane with coordinating of wetting agent, thus make dry skin person also can be suitable for this cleansing milk.
Detailed description of the invention
Embodiment 1
Esters of acrylic acid/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer 10 parts
Sodium lauroyl glutamate 50 parts
Trehalose 10 parts
Caprylyl glycol 1 part
Glycerol 50 parts
Sensiva SC50 1 part
Arginine 10 parts
Mactra veneriformis polysaccharide 1 part
Rhodiola crenulata extract 10 parts
Semen Juglandis abrasive material 10 parts
Betanin 10 parts
Chitosan affinity membrane 10 parts
Full carbon aerogels 3 parts
Deionized water 50 parts
Preparation method
Step one: by esters of acrylic acid/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer adds in the deionized water of 40 DEG C, insulation Keep agitation 20 minutes;
Step 2: sodium lauroyl glutamate, trehalose and caprylyl glycol are added successively in the product of gained in step one, is heated to 60 DEG C, is incubated and stirs 30 minutes, making it Homogeneous phase mixing;
Step 3: glycerol, Sensiva SC50, arginine, Mactra veneriformis polysaccharide and Rhodiola crenulata extract are added in the product of step 2 gained, be cooled to 30 DEG C, is incubated and stirs 18 minutes;
Step 4: full carbon aerogels, betanin and Semen Juglandis abrasive material are added in the product of step 3 gained, is incubated and vibrates 18 minutes;
Step 5: added by chitosan affinity membrane in the product of step 4 gained, is cooled to 25 DEG C, and insulation is also mixed 10 minutes by ultrasound wave.
Embodiment 2
Esters of acrylic acid/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer 0.1 part
Fluorocarbon surfactant 5 parts
Trehalose 0.1 part
Caprylyl glycol 0.1 part
Chitin derivativ 2 parts
Ceramide 3 part
Sensiva SC50 0.1 part
Arginine 0.1 part
Mactra veneriformis polysaccharide 0.1 part
Rhodiola crenulata extract 2 parts
Herba bromi japonici abrasive material 5 parts
Silicon dioxide 0.1 part
Chitosan affinity membrane 5 parts
Full carbon aerogels 1 part
Deionized water 20 parts
Preparation method
Step one: by esters of acrylic acid/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer adds in the deionized water of 30 ~ 40 DEG C, insulation Keep agitation 15 minutes;
Step 2: fluorocarbon surfactant, trehalose and caprylyl glycol are added successively in the product of gained in step one, is heated to 45 DEG C, is incubated and stirs 25 minutes, making it Homogeneous phase mixing;
Step 3: chitin derivativ, ceramide, Sensiva SC50, arginine, Mactra veneriformis polysaccharide and Rhodiola crenulata extract are added in the product of step 2 gained, be cooled to 28 DEG C, is incubated and stirs 15 minutes;
Step 4: full carbon aerogels, silicon dioxide and Herba bromi japonici abrasive material are added in the product of step 3 gained, is incubated and vibrates 15 minutes;
Step 5: added by chitosan affinity membrane in the product of step 4 gained, is cooled to 25 DEG C, and insulation also mixes 8 minutes by ultrasound wave.
Embodiment 3
Esters of acrylic acid/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer 5 parts
27 parts, lecithin
Potassium sorbate 7 parts
Sorbitol 32 parts
Sensiva SC50 0.6 part
Arginine 5 parts
Mactra veneriformis polysaccharide 0.8 part
Rhodiola crenulata extract 9 parts
Semen Juglandis abrasive material 4 parts
Herba bromi japonici abrasive material 4 parts
Betanin 3 parts
Silicon dioxide 2 parts
Chitosan affinity membrane 7 parts
Full carbon aerogels 1.9 parts
Deionized water 38 parts
Preparation method
Step one: by esters of acrylic acid/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer adds in the deionized water of 37 DEG C, insulation Keep agitation 16.5 minutes;
Step 2: lecithin and potassium sorbate are added successively in the product of gained in step one, be heated to 52 DEG C, is incubated and stirs 28.6 minutes, making it Homogeneous phase mixing;
Step 3: sorbitol, Sensiva SC50, arginine, Mactra veneriformis polysaccharide and Rhodiola crenulata extract are added in the product of step 2 gained, be cooled to 29.3 DEG C, is incubated and stirs 17 minutes;
Step 4: full carbon aerogels, betanin, silicon dioxide and grinding aid material are added in the product of step 3 gained, is incubated and vibrates 17 minutes;
Step 5: added by chitosan affinity membrane in the product of step 4 gained, is cooled to 25 DEG C, and insulation also mixes 9 minutes by ultrasound wave.
Embodiment 4
Esters of acrylic acid/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer 4 parts
11 parts, lecithin
Fluorocarbon surfactant 27 parts
Trehalose 7 parts
Potassium sorbate 3 parts
Glycerol 13 parts
Cer NS 1 point
Sensiva SC50 0.3 part
Arginine 1.4 parts
Mactra veneriformis polysaccharide 0.6 part
Rhodiola crenulata extract 8 parts
Semen Juglandis abrasive material 7 parts
Silicon dioxide 3.3 parts
Chitosan affinity membrane 6.2 parts
Full carbon aerogels 1.9 parts
Deionized water 36 parts
Preparation method
Step one: by esters of acrylic acid/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer adds in the deionized water of 32.4 DEG C, insulation Keep agitation 19 minutes;
Step 2: lecithin, fluorocarbon surfactant, trehalose and potassium sorbate are added successively in the product of gained in step one, is heated to 55 DEG C, is incubated and stirs 27 minutes, making it Homogeneous phase mixing;
Step 3: glycerol, ceramide, Sensiva SC50, arginine, Mactra veneriformis polysaccharide and Rhodiola crenulata extract are added in the product of step 2 gained, be cooled to 28.7 DEG C, is incubated and stirs 17 minutes;
Step 4: full carbon aerogels, silicon dioxide and Semen Juglandis abrasive material are added in the product of step 3 gained, is incubated and vibrates 16 minutes;
Step 5: added by chitosan affinity membrane in the product of step 4 gained, is cooled to 25 DEG C, and insulation also mixes 9.3 minutes by ultrasound wave.
Embodiment 5
Esters of acrylic acid/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer 4 parts
Sodium lauroyl glutamate 21 parts
Fluorocarbon surfactant 14 parts
Caprylyl glycol 0.4 part
Potassium sorbate 5 parts
Sorbitol 7 parts
Cer NS 6 points
Sensiva SC50 0.9 part
Arginine 8 parts
Mactra veneriformis polysaccharide 0.4 part
Rhodiola crenulata extract 10 parts
Herba bromi japonici abrasive material 7 parts
Silicon dioxide 4.3 parts
Chitosan affinity membrane 6.8 parts
Full carbon aerogels 1.7 parts
Deionized water 41 parts
Preparation method
Step one: by esters of acrylic acid/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer adds in the deionized water of 32.4 DEG C, insulation Keep agitation 19 minutes;
Step 2: sodium lauroyl glutamate, fluorocarbon surfactant, caprylyl glycol and potassium sorbate are added successively in the product of gained in step one, is heated to 55 DEG C, is incubated and stirs 27 minutes, making it Homogeneous phase mixing;
Step 3: sorbitol, ceramide, Sensiva SC50, arginine, Mactra veneriformis polysaccharide and Rhodiola crenulata extract are added in the product of step 2 gained, be cooled to 28.7 DEG C, is incubated and stirs 17 minutes;
Step 4: full carbon aerogels, silicon dioxide and Herba bromi japonici abrasive material are added in the product of step 3 gained, is incubated and vibrates 16 minutes;
Step 5: added by chitosan affinity membrane in the product of step 4 gained, is cooled to 25 DEG C, and insulation also mixes 9.3 minutes by ultrasound wave.
Embodiment 6
Esters of acrylic acid/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer 4 parts
Sodium lauroyl glutamate 19 parts
24 parts, lecithin
Caprylyl glycol 0.4 part
Potassium sorbate 5 parts
Trehalose 2 parts
Sorbitol 7 parts
Cer NS 6 points
Chitin derivativ 9 parts
Sensiva SC50 1 part
Arginine 4 parts
Mactra veneriformis polysaccharide 0.9 part
Rhodiola crenulata extract 4 parts
Herba bromi japonici abrasive material 7 parts
Betanin 3.3 parts
Chitosan affinity membrane 8.8 parts
Full carbon aerogels 2.2 parts
Deionized water 39 parts
Preparation method
Step one: by esters of acrylic acid/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer adds in the deionized water of 35.5 DEG C, insulation Keep agitation 18 minutes;
Step 2: sodium lauroyl glutamate, lecithin, caprylyl glycol, alginic acid and potassium sorbate are added successively in the product of gained in step one, is heated to 51 DEG C, is incubated and stirs 26 minutes, making it Homogeneous phase mixing;
Step 3: sorbitol, ceramide, chitin derivativ, Sensiva SC50, arginine, Mactra veneriformis polysaccharide and Rhodiola crenulata extract are added in the product of step 2 gained, be cooled to 27 DEG C, is incubated and stirs 18 minutes;
Step 4: full carbon aerogels, betanin and Herba bromi japonici abrasive material are added in the product of step 3 gained, is incubated and vibrates 17 minutes;
Step 5: added by chitosan affinity membrane in the product of step 4 gained, is cooled to 25 DEG C, and insulation also mixes 7.3 minutes by ultrasound wave.
Embodiment 7
Esters of acrylic acid/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer 4 parts
Sodium lauroyl glutamate 19 parts
9 parts, lecithin
Fluorocarbon surfactant 11 parts
Caprylyl glycol 0.8 part
Potassium sorbate 5 parts
Trehalose 2 parts
Sorbitol 7 parts
Cer NS 1 point
Chitin derivativ 9 parts
Glycerol 10 parts
Sensiva SC50 0.5 part
Arginine 6 parts
Mactra veneriformis polysaccharide 0.7 part
Rhodiola crenulata extract 5 parts
Semen Juglandis abrasive material 7 parts
Betanin 3.9 parts
Chitosan affinity membrane 7 parts
Full carbon aerogels 3 parts
Deionized water 48 parts
Preparation method
Step one: by esters of acrylic acid/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer adds in the deionized water of 32.4 DEG C, insulation Keep agitation 19 minutes;
Step 2: sodium lauroyl glutamate, lecithin, fluorocarbon surfactant, caprylyl glycol, alginic acid and potassium sorbate are added successively in the product of gained in step one, is heated to 55 DEG C, is incubated and stirs 27 minutes, making it Homogeneous phase mixing;
Step 3: sorbitol, ceramide, chitin derivativ, glycerol, Sensiva SC50, arginine, Mactra veneriformis polysaccharide and Rhodiola crenulata extract are added in the product of step 2 gained, be cooled to 28.7 DEG C, is incubated and stirs 17 minutes;
Step 4: full carbon aerogels, betanin and Semen Juglandis abrasive material are added in the product of step 3 gained, is incubated and vibrates 16 minutes;
Step 5: added by chitosan affinity membrane in the product of step 4 gained, is cooled to 25 DEG C, and insulation also mixes 9.3 minutes by ultrasound wave.
The above is only the preferred embodiment of the present invention, protection scope of the present invention be not only confined to above-described embodiment, and all technical schemes belonged under thinking of the present invention all belong to protection scope of the present invention.It should be pointed out that for those skilled in the art, some improvements and modifications without departing from the principles of the present invention, these improvements and modifications also should be considered as protection scope of the present invention.
Performance characterization is tested
(1) deoil measure of merit
Take the thermoplastic elastomer TPE plate of formed objects, this TPE plate evenly have the aperture that diameter is 1 millimeter, and evenly applying 10 grams of solid-state Adeps Sus domesticas above at TPE plate, adopt finished product in above-described embodiment it is washed required for grammes per square metre as following table
Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Embodiment 5 Embodiment 6 Embodiment 7
Grammes per square metre 2 grams 13 grams 9.2 gram 7.5 gram 8.1 gram 5.5 gram 3.6 gram
By the amount of the surfactant added in each embodiment of upper table Data Comparison and full carbon aerogels, visible the two all have impact to the ability of deoiling of product, and full carbon aerogels the impact of ability is deoiled on product will much larger than surfactant.
(2) moistening effect test
Take the thermoplastic elastomer TPE plate of formed objects, this TPE plate evenly has the aperture that diameter is 1 millimeter, the water of equivalent is injected in advance in opened aperture, and realize the pivot weight measuring accurate thermoplastic elastomer TPE plate, adopt each 5 grams of finished product in above-described embodiment to wash to it time that rear measurement thermoplastic elastomer TPE plate gross weight gets back to concentrated weight, the gained time is as following table
Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Embodiment 5 Embodiment 6 Embodiment 7
Time 53min 15min 46min 43min 44min 49min 48min
By the amount of the wetting agent added in each embodiment of upper table Data Comparison and chitosan affinity membrane, visible the two all have impact to the moisture-retaining capacity of product, and chitosan affinity membrane on the impact of product moisture-retaining capacity slightly larger than wetting agent.
(3) result measured by above-mentioned scale, the cleansing milk obtained by this formula all has good practicality to dry skin and oily skin.

Claims (9)

1. a cleansing milk, is characterized in that: the recipe ingredient of this cleansing milk by weight mark is counted
Esters of acrylic acid/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer 0.1 ~ 10 part
5 ~ 50 parts, surfactant
Antiseptic 0.2 ~ 11 part
Wetting agent 5 ~ 50 parts
Skin care ingredient 2.3 ~ 22 parts
Anti-caking agent 0.1 ~ 10 part
Chitosan affinity membrane 5 ~ 10 parts
Full carbon aerogels 1 ~ 3 part
Grinding aid material 5 ~ 10 parts
Deionized water 20 ~ 50 parts.
2. cleansing milk according to claim 1, is characterized in that: described surfactant is one or more in sodium lauroyl glutamate, lecithin and fluorocarbon surfactant.
3. cleansing milk according to claim 1, is characterized in that: described antiseptic is one or more in trehalose, caprylyl glycol and potassium sorbate.
4. cleansing milk according to claim 3, is characterized in that: described antiseptic is
Trehalose 0.1 ~ 10 part
Caprylyl glycol 0.1 ~ 1 part.
5. cleansing milk according to claim 1, is characterized in that: described wetting agent is one or more in glycerol, chitin derivativ, ceramide and sorbitol.
6. cleansing milk according to claim 1, is characterized in that: described skin care ingredient is
Sensiva SC50 0.1 ~ 1 part
Arginine 0.1 ~ 10 part
Mactra veneriformis polysaccharide 0.1 ~ 1 part
Rhodiola crenulata extract 2 ~ 10 parts.
7. cleansing milk according to claim 1, is characterized in that: described grinding aid material is the one or several in Semen Juglandis abrasive material and Herba bromi japonici abrasive material.
8. cleansing milk according to claim 1, is characterized in that: described anti-caking agent comprises the one in betanin and silicon dioxide.
9. preparation as arbitrary in claim 1-7 as described in the method for cleansing milk
Step one: by esters of acrylic acid/C10 ~ C30 alkylol acrylamide acid esters cross linked polymer adds in the deionized water of 30 ~ 40 DEG C, insulation Keep agitation 15 ~ 20 minutes;
Step 2: surfactant and antiseptic are added successively in the product of gained in step one, be heated to 45 ~ 60 DEG C, is incubated and stirs 25 ~ 30 minutes, making it Homogeneous phase mixing;
Step 3: wetting agent and skin care ingredient are added in the product of step 2 gained, is cooled to 28 ~ 30 DEG C, is incubated and stirs 15 ~ 18 minutes;
Step 4: full carbon aerogels, anti-caking agent and grinding aid material are added in the product of step 3 gained, is incubated and vibrates 15 ~ 18 minutes;
Step 5: added by chitosan affinity membrane in the product of step 4 gained, is cooled to 25 DEG C, and insulation also mixes 8 ~ 10 minutes by ultrasound wave.
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CN106176355A (en) * 2016-07-23 2016-12-07 扬中市创想驿站工业设计有限公司 Cleansing milk
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CN108938495A (en) * 2018-09-18 2018-12-07 广西壮族自治区农业科学院农产品加工研究所 A kind of Tea Saponin face cleaning cream and preparation method thereof
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CN109260052A (en) * 2018-11-03 2019-01-25 江苏贝塔仕生物科技有限公司 A kind of wider array of facial cleanser of the scope of application

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