CN102906025A - 制备钛化合物的方法 - Google Patents

制备钛化合物的方法 Download PDF

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Publication number
CN102906025A
CN102906025A CN2011800250035A CN201180025003A CN102906025A CN 102906025 A CN102906025 A CN 102906025A CN 2011800250035 A CN2011800250035 A CN 2011800250035A CN 201180025003 A CN201180025003 A CN 201180025003A CN 102906025 A CN102906025 A CN 102906025A
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China
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approximately
titanium dioxide
tiocl
mixture
temperature range
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CN2011800250035A
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Chinese (zh)
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J.S.汤普森
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EIDP Inc
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EI Du Pont de Nemours and Co
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/04—Oxides; Hydroxides
    • C01G23/047—Titanium dioxide
    • C01G23/053—Producing by wet processes, e.g. hydrolysing titanium salts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/003—Titanates
    • C01G23/005—Alkali titanates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/04—Oxides; Hydroxides
    • C01G23/047—Titanium dioxide
    • C01G23/053—Producing by wet processes, e.g. hydrolysing titanium salts
    • C01G23/0536—Producing by wet processes, e.g. hydrolysing titanium salts by hydrolysing chloride-containing salts
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/485—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/11—Powder tap density
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Battery Electrode And Active Subsutance (AREA)
CN2011800250035A 2010-05-21 2011-05-20 制备钛化合物的方法 Pending CN102906025A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US34724910P 2010-05-21 2010-05-21
US61/347249 2010-05-21
PCT/US2011/037344 WO2011146838A2 (en) 2010-05-21 2011-05-20 Process for making titanium compounds

Publications (1)

Publication Number Publication Date
CN102906025A true CN102906025A (zh) 2013-01-30

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN2011800250035A Pending CN102906025A (zh) 2010-05-21 2011-05-20 制备钛化合物的方法

Country Status (7)

Country Link
US (1) US20130039844A1 (https=)
EP (1) EP2571811A4 (https=)
JP (1) JP2013531600A (https=)
KR (1) KR20130080019A (https=)
CN (1) CN102906025A (https=)
CA (1) CA2794633A1 (https=)
WO (1) WO2011146838A2 (https=)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105883917A (zh) * 2016-05-26 2016-08-24 宜宾天原集团股份有限公司 一种利用氯化法钛白粉废气制备TiO2及HCl溶液的方法

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101431693B1 (ko) 2011-12-29 2014-08-22 주식회사 포스코 이산화티타늄 나노분말, 타이타네이트, 리튬 타이타네이트 나노 분말 및 이들의 제조 방법
US20140363366A1 (en) * 2013-06-05 2014-12-11 E I Du Pont De Nemours And Company Process for making titanium compounds
KR102256399B1 (ko) * 2019-10-02 2021-05-26 더블유알씨 주식회사 이산화티탄 분말의 제조 방법
CN112174197B (zh) * 2020-09-29 2022-05-24 攀钢集团研究院有限公司 以四氯化钛为原料制备锂电负极材料钛酸锂的方法
KR102428917B1 (ko) * 2022-02-11 2022-08-02 김래희 개선된 티타늄옥시클로라이드의 제조 방법

Citations (9)

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Publication number Priority date Publication date Assignee Title
US4923682A (en) * 1989-03-30 1990-05-08 Kemira, Inc. Preparation of pure titanium dioxide with anatase crystal structure from titanium oxychloride solution
US4944936A (en) * 1987-04-10 1990-07-31 Kemira, Inc. Titanium dioxide with high purity and uniform particle size and method therefore
CN1242342A (zh) * 1998-07-16 2000-01-26 韩国原子力研究所 用均相沉淀由TiOCl2制作单分散结晶TiO2特细粉末方法
CN1622368A (zh) * 2004-12-17 2005-06-01 清华大学 锂离子电池负极材料球形Li4Ti5O12的制备方法
CN1884096A (zh) * 2006-07-07 2006-12-27 清华大学 一种掺碳球形Li4Ti5O12的制备方法
KR20080023831A (ko) * 2006-09-12 2008-03-17 주식회사 엘지화학 리튬티탄산화물 분말, 그 제조방법, 이를 포함하는 전극,및 이차전지
CN101378119A (zh) * 2008-10-06 2009-03-04 天津巴莫科技股份有限公司 锂离子电池用碳包覆型钛酸锂的制备方法
CN101428851A (zh) * 2008-12-04 2009-05-13 上海大学 锂离子电池负极材料钛酸锂的制备方法
CN101587948A (zh) * 2009-06-19 2009-11-25 中南大学 一种Li4Ti5O12/C复合电极材料的制备方法

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US2512807A (en) * 1947-09-23 1950-06-27 Nicholson Douglas Gillison Purification of titanium halides
DE69842254D1 (de) * 1997-07-15 2011-06-16 Ishihara Sangyo Kaisha Lithiumwasserstofftitanat und verfahren zu dessen herstellung
JP4642959B2 (ja) * 2000-01-26 2011-03-02 東邦チタニウム株式会社 チタン酸リチウムの製造方法
JP4540167B2 (ja) * 1999-02-16 2010-09-08 東邦チタニウム株式会社 チタン酸リチウムの製造方法
JP3894778B2 (ja) * 2000-11-20 2007-03-22 石原産業株式会社 チタン酸リチウム及びそれを用いてなるリチウム電池
US7211350B2 (en) * 2001-01-29 2007-05-01 Rutgers University Foundation Nanostructure lithium titanate electrode for high cycle rate rechargeable electrochemical cell
AU2002319587B2 (en) * 2001-07-20 2007-05-10 Altair Nanomaterials Inc. Process for making lithium titanate
CN1277749C (zh) * 2004-11-16 2006-10-04 浙江工业大学 一种金红石相二氧化钛纳米粉体的制备方法
JP4249727B2 (ja) * 2005-05-13 2009-04-08 株式会社東芝 非水電解質電池およびリチウムチタン複合酸化物
CN101074112B (zh) * 2007-06-27 2010-10-13 仙桃市中星电子材料有限公司 高纯超细二氧化钛的制备方法
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* Cited by examiner, † Cited by third party
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US4944936A (en) * 1987-04-10 1990-07-31 Kemira, Inc. Titanium dioxide with high purity and uniform particle size and method therefore
US4923682A (en) * 1989-03-30 1990-05-08 Kemira, Inc. Preparation of pure titanium dioxide with anatase crystal structure from titanium oxychloride solution
CN1242342A (zh) * 1998-07-16 2000-01-26 韩国原子力研究所 用均相沉淀由TiOCl2制作单分散结晶TiO2特细粉末方法
CN1622368A (zh) * 2004-12-17 2005-06-01 清华大学 锂离子电池负极材料球形Li4Ti5O12的制备方法
CN1884096A (zh) * 2006-07-07 2006-12-27 清华大学 一种掺碳球形Li4Ti5O12的制备方法
KR20080023831A (ko) * 2006-09-12 2008-03-17 주식회사 엘지화학 리튬티탄산화물 분말, 그 제조방법, 이를 포함하는 전극,및 이차전지
CN101378119A (zh) * 2008-10-06 2009-03-04 天津巴莫科技股份有限公司 锂离子电池用碳包覆型钛酸锂的制备方法
CN101428851A (zh) * 2008-12-04 2009-05-13 上海大学 锂离子电池负极材料钛酸锂的制备方法
CN101587948A (zh) * 2009-06-19 2009-11-25 中南大学 一种Li4Ti5O12/C复合电极材料的制备方法

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KANG RYEOL LEE ET AL.: "Photocatalytic Characteristics of Nanometer-Sized Titania Powders Fabricated by a Homogeneous-Precipitation Process", 《J. AM. CERAM. SOC.》, vol. 85, no. 2, 31 December 2002 (2002-12-31), pages 341 - 345 *
SUN-JAE KIM ET AL.: "Homogeneous Precipitation of TiO2 Ultrafine Powders from Aqueous TiOCl2 Solution", 《J. AM. CERAM. SOC.》, vol. 82, no. 4, 31 December 1999 (1999-12-31), pages 927 - 932, XP002271553 *
臧戈等: "水合氧化钛制备Li4Ti5O12及在电化学混合电容器中的应用", 《无机材料学报》, vol. 24, no. 3, 31 May 2009 (2009-05-31), pages 531 - 534 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105883917A (zh) * 2016-05-26 2016-08-24 宜宾天原集团股份有限公司 一种利用氯化法钛白粉废气制备TiO2及HCl溶液的方法

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CA2794633A1 (en) 2011-11-24
EP2571811A4 (en) 2016-02-17
EP2571811A2 (en) 2013-03-27
WO2011146838A3 (en) 2012-03-29
WO2011146838A2 (en) 2011-11-24
JP2013531600A (ja) 2013-08-08
KR20130080019A (ko) 2013-07-11
US20130039844A1 (en) 2013-02-14

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