CN102905787B - 钛-mww沸石的制造工艺 - Google Patents

钛-mww沸石的制造工艺 Download PDF

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Publication number
CN102905787B
CN102905787B CN201180008068.9A CN201180008068A CN102905787B CN 102905787 B CN102905787 B CN 102905787B CN 201180008068 A CN201180008068 A CN 201180008068A CN 102905787 B CN102905787 B CN 102905787B
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Prior art keywords
titanium
mww
technique
temperature
mixture
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CN201180008068.9A
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English (en)
Chinese (zh)
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CN102905787A (zh
Inventor
B·S·曼迪穆特西拉
J·F·米勒
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Lyondell Chemical Technology LP
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Lyondell Chemical Technology LP
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/005—Silicates, i.e. so-called metallosilicalites or metallozeosilites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/03—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by addition of hydroxy groups to unsaturated carbon-to-carbon bonds, e.g. with the aid of H2O2
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Epoxy Compounds (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN201180008068.9A 2010-02-01 2011-01-28 钛-mww沸石的制造工艺 Active CN102905787B (zh)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US12/658029 2010-02-01
US12/658,029 2010-02-01
US12/658,029 US8124555B2 (en) 2010-02-01 2010-02-01 Process for making titanium-MWW zeolite
PCT/US2011/022913 WO2012018408A2 (en) 2010-02-01 2011-01-28 Process for making titanium-mww zeolite

Publications (2)

Publication Number Publication Date
CN102905787A CN102905787A (zh) 2013-01-30
CN102905787B true CN102905787B (zh) 2015-04-29

Family

ID=44342209

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201180008068.9A Active CN102905787B (zh) 2010-02-01 2011-01-28 钛-mww沸石的制造工艺

Country Status (9)

Country Link
US (1) US8124555B2 (enExample)
EP (1) EP2531297B1 (enExample)
JP (1) JP5662481B2 (enExample)
KR (2) KR20120109603A (enExample)
CN (1) CN102905787B (enExample)
BR (1) BR112012019011B1 (enExample)
ES (1) ES2505615T3 (enExample)
SG (2) SG190585A1 (enExample)
WO (1) WO2012018408A2 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107074567A (zh) * 2014-09-09 2017-08-18 巴斯夫欧洲公司 制备包含硼和钛的mww沸石材料的方法

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102874834B (zh) * 2011-07-11 2014-10-15 中国石油化工股份有限公司 具有MWW结构Si/B分子筛的合成方法
BR112014019483B1 (pt) * 2012-02-07 2021-04-20 Basf Se processo para a preparação de um material zeolítico
FR2987046B1 (fr) 2012-02-17 2014-03-21 Rhodia Operations Procede d'hydroxylation de composes aromatiques, catalyseur d'hydroxylation et son procede de preparation
MY182905A (en) * 2013-02-05 2021-02-05 Basf Se Process for preparing a titanium-containing zeolitic material having an mww framework structure
HUE045051T2 (hu) * 2013-07-24 2019-12-30 Basf Se Eljárás propilén-oxid elõállítására
US20170275225A1 (en) * 2014-09-09 2017-09-28 Basf Se Method for the preparation of 2-alkoxy cyclohexanol
WO2016038033A1 (de) * 2014-09-09 2016-03-17 Basf Se Verfahren zur herstellung eines aromastoffs
CN107646032B (zh) * 2015-04-09 2019-07-12 利安德化学技术有限公司 在丙烯环氧化中改进的催化剂性能
KR101878627B1 (ko) 2015-04-09 2018-07-13 라이온델 케미칼 테크놀로지, 엘.피. 메틸벤질 알코올의 산화로부터 프로필렌 옥사이드를 형성하는 방법
JP7204636B2 (ja) * 2016-07-13 2023-01-16 ビーエーエスエフ ソシエタス・ヨーロピア エテンオキシドを製造する方法
CN106745038B (zh) * 2016-12-09 2018-11-13 卓悦环保新材料（上海）有限公司 一种Ti-MWW分子筛的合成方法
JP7296880B2 (ja) * 2016-12-20 2023-06-23 ビーエーエスエフ ソシエタス・ヨーロピア 骨格型ｍｗｗを有するチタン含有ゼオライト材料を含む組成物の可塑性を低下させるための酸処理の使用方法
CN109593072B (zh) * 2017-09-30 2020-09-22 中国石油化工股份有限公司 一种烯烃氧化的方法
CN110054198A (zh) * 2019-05-26 2019-07-26 福州大学 一种Ti-MWW分子筛的制备方法
CN112158856B (zh) * 2020-08-25 2021-11-19 郑州大学 一种制备Ti-MWW分子筛的方法

Citations (6)

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US6759540B2 (en) * 2000-09-29 2004-07-06 Showa Denko K.K. Crystalline MWW-type titanosilicate catalyst for producing oxidized compound, production process for the catalyst, and process for producing oxidized compound by using the catalyst
CN1686795A (zh) * 2005-04-18 2005-10-26 华东师范大学 一种 Ti－MWW 分子筛的合成方法
CN101148260A (zh) * 2007-08-20 2008-03-26 华东师范大学 具有mww结构的钛硅分子筛及其合成和应用
CN101374827A (zh) * 2006-01-11 2009-02-25 住友化学株式会社 生产环氧化合物的方法
US7501532B1 (en) * 2007-11-20 2009-03-10 Lyondell Chemical Technology, L.P. Process for producing hydrogen peroxide
CN100528854C (zh) * 2004-03-22 2009-08-19 住友化学株式会社 环氧丙烷的制备方法

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US4367342A (en) 1969-04-02 1983-01-04 Shell Oil Company Olefin epoxidation
IT1152299B (it) 1982-07-28 1986-12-31 Anic Spa Procedimento per l'espossidazione di composti olefinici
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Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6759540B2 (en) * 2000-09-29 2004-07-06 Showa Denko K.K. Crystalline MWW-type titanosilicate catalyst for producing oxidized compound, production process for the catalyst, and process for producing oxidized compound by using the catalyst
CN100528854C (zh) * 2004-03-22 2009-08-19 住友化学株式会社 环氧丙烷的制备方法
CN1686795A (zh) * 2005-04-18 2005-10-26 华东师范大学 一种 Ti－MWW 分子筛的合成方法
CN101374827A (zh) * 2006-01-11 2009-02-25 住友化学株式会社 生产环氧化合物的方法
CN101148260A (zh) * 2007-08-20 2008-03-26 华东师范大学 具有mww结构的钛硅分子筛及其合成和应用
US7501532B1 (en) * 2007-11-20 2009-03-10 Lyondell Chemical Technology, L.P. Process for producing hydrogen peroxide

Non-Patent Citations (2)

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A Novel Titanosilicate with MWW Structure. I. Hydrothermal Synthesis, Elimination of Extraframework Titanium, and Characterizations;Peng Wu et al;《Journal of Physical Chemistry B》;20010324;第105卷(第15期);第2898页左栏倒数第2段 *
Ti-MWW的合成及其对烯丙醇环氧化性能的研究;范志勇;《万方学位论文数据库》;20060831;第10页第2段，第15页第1段，第19页，第23页倒数第1段，第24页，第25页-第26页第1段，第34－35页，表3.1-1，表3.2-2，表4.2-1，表1.2-3 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107074567A (zh) * 2014-09-09 2017-08-18 巴斯夫欧洲公司 制备包含硼和钛的mww沸石材料的方法
CN107074567B (zh) * 2014-09-09 2020-01-03 巴斯夫欧洲公司 制备包含硼和钛的mww沸石材料的方法

Also Published As

Publication number Publication date
US8124555B2 (en) 2012-02-28
WO2012018408A2 (en) 2012-02-09
EP2531297B1 (en) 2014-08-20
JP2013518796A (ja) 2013-05-23
BR112012019011A8 (pt) 2018-05-29
US20110190517A1 (en) 2011-08-04
KR20160092034A (ko) 2016-08-03
KR20120109603A (ko) 2012-10-08
WO2012018408A3 (en) 2012-11-29
BR112012019011A2 (pt) 2016-09-13
EP2531297A2 (en) 2012-12-12
ES2505615T3 (es) 2014-10-10
SG182756A1 (en) 2012-08-30
BR112012019011B1 (pt) 2024-02-06
CN102905787A (zh) 2013-01-30
JP5662481B2 (ja) 2015-01-28
SG190585A1 (en) 2013-06-28

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