ES2505615T3 - Proceso para fabricar zeolita de tipo MWW de titanio - Google Patents

Proceso para fabricar zeolita de tipo MWW de titanio Download PDF

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Publication number
ES2505615T3
ES2505615T3 ES11788621.8T ES11788621T ES2505615T3 ES 2505615 T3 ES2505615 T3 ES 2505615T3 ES 11788621 T ES11788621 T ES 11788621T ES 2505615 T3 ES2505615 T3 ES 2505615T3
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ES
Spain
Prior art keywords
mww
manufacturing
type titanium
mww type
titanium zeolite
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
ES11788621.8T
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English (en)
Inventor
Beaven S. Mandimutsira
Jay F. Miller
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Lyondell Chemical Technology LP
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Lyondell Chemical Technology LP
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Publication date
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Application filed by Lyondell Chemical Technology LP filed Critical Lyondell Chemical Technology LP
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Publication of ES2505615T3 publication Critical patent/ES2505615T3/es
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/005—Silicates, i.e. so-called metallosilicalites or metallozeosilites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/03—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by addition of hydroxy groups to unsaturated carbon-to-carbon bonds, e.g. with the aid of H2O2
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Epoxy Compounds (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Un proceso para producir una zeolita de tipo MWW de titanio, que consiste en: (a) calentar un gel formado a partir de un compuesto de titanio, una fuente de silicio, una fuente de boro, un agente molde de la MWW y agua a una temperatura comprendida entre 35ºC y 75ºC durante un período de 8 a 30 horas para formar un gel precristalizado; y (b) calentar el gel precristalizado a una temperatura comprendida entre 160ºC y 190ºC durante un período de 5 o más días para formar la zeolita de tipo MWW de titanio; en el que el agente molde de la MWW es la piperidina o la hexametilenimina.

Description

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Claims (1)

  1. imagen1
ES11788621.8T 2010-02-01 2011-01-28 Proceso para fabricar zeolita de tipo MWW de titanio Active ES2505615T3 (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US658029 1991-02-20
US12/658,029 US8124555B2 (en) 2010-02-01 2010-02-01 Process for making titanium-MWW zeolite
PCT/US2011/022913 WO2012018408A2 (en) 2010-02-01 2011-01-28 Process for making titanium-mww zeolite

Publications (1)

Publication Number Publication Date
ES2505615T3 true ES2505615T3 (es) 2014-10-10

Family

ID=44342209

Family Applications (1)

Application Number Title Priority Date Filing Date
ES11788621.8T Active ES2505615T3 (es) 2010-02-01 2011-01-28 Proceso para fabricar zeolita de tipo MWW de titanio

Country Status (9)

Country Link
US (1) US8124555B2 (es)
EP (1) EP2531297B1 (es)
JP (1) JP5662481B2 (es)
KR (2) KR20160092034A (es)
CN (1) CN102905787B (es)
BR (1) BR112012019011B1 (es)
ES (1) ES2505615T3 (es)
SG (2) SG190585A1 (es)
WO (1) WO2012018408A2 (es)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102874834B (zh) * 2011-07-11 2014-10-15 中国石油化工股份有限公司 具有MWW结构Si/B分子筛的合成方法
CN104302577A (zh) * 2012-02-07 2015-01-21 巴斯夫欧洲公司 沸石材料的制备方法
FR2987046B1 (fr) 2012-02-17 2014-03-21 Rhodia Operations Procede d'hydroxylation de composes aromatiques, catalyseur d'hydroxylation et son procede de preparation
MX2015010047A (es) * 2013-02-05 2016-03-04 Basf Se Proceso para preparar un material zeolitico que contiene titanio con una estructura marco mww.
SG11201600530YA (en) * 2013-07-24 2016-02-26 Basf Se A process for preparing propylene oxide
US20170275225A1 (en) * 2014-09-09 2017-09-28 Basf Se Method for the preparation of 2-alkoxy cyclohexanol
SG11201701622TA (en) * 2014-09-09 2017-03-30 Basf Se A process for the preparation of an mww zeolitic material comprising boron and titanium
US20170283352A1 (en) * 2014-09-09 2017-10-05 Basf Se Method for producing an aroma substance
US9643943B2 (en) 2015-04-09 2017-05-09 Lyondell Chemical Technology, L.P. Process for forming propylene oxide from oxidation of methyl benzyl alcohol
WO2016164585A1 (en) 2015-04-09 2016-10-13 Lyondell Chemical Technology, L.P. Improved catalyst performance in propylene epoxidation
WO2018011280A1 (en) * 2016-07-13 2018-01-18 Basf Se A process for preparing ethene oxide
CN106745038B (zh) * 2016-12-09 2018-11-13 卓悦环保新材料（上海）有限公司 一种Ti-MWW分子筛的合成方法
RU2761301C2 (ru) * 2016-12-20 2021-12-07 Басф Се Применение кислотной обработки для снижения пластичности композиции, содержащей титансодержащий цеолитный материал, имеющий структурный тип mww
CN109593072B (zh) * 2017-09-30 2020-09-22 中国石油化工股份有限公司 一种烯烃氧化的方法
CN110054198A (zh) * 2019-05-26 2019-07-26 福州大学 一种Ti-MWW分子筛的制备方法
CN112158856B (zh) * 2020-08-25 2021-11-19 郑州大学 一种制备Ti-MWW分子筛的方法

Family Cites Families (17)

* Cited by examiner, † Cited by third party
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US3013A (en) * 1843-03-21 James stewabt
US3351635A (en) * 1966-03-14 1967-11-07 Halcon International Inc Epoxidation process
US4367342A (en) * 1969-04-02 1983-01-04 Shell Oil Company Olefin epoxidation
IT1152299B (it) * 1982-07-28 1986-12-31 Anic Spa Procedimento per l'espossidazione di composti olefinici
JP3044836B2 (ja) 1991-05-28 2000-05-22 東ソー株式会社 プロピレンオキシドの製法
JP2000185912A (ja) * 1998-12-22 2000-07-04 Tosoh Corp 結晶性チタノシリケートゼオライトおよびその製造方法
JP2002102709A (ja) * 2000-09-29 2002-04-09 Showa Denko Kk 酸化化合物製造用結晶性ｍｗｗ型チタノシリケート触媒、該触媒の製造方法、及び該触媒を用いた酸化化合物の製造方法
JP4352771B2 (ja) 2003-06-11 2009-10-28 株式会社ジェイ・エム・エス カプラー連結具と該カプラー連結具を装着したカプラー
JP4433843B2 (ja) * 2004-03-22 2010-03-17 住友化学株式会社 プロピレンオキサイド製造用触媒及びプロピレンオキサイドの製造方法
CN1321061C (zh) * 2005-04-18 2007-06-13 华东师范大学 一种 Ti－MWW 分子筛的合成方法
US7994349B2 (en) * 2006-01-11 2011-08-09 Sumitomo Chemical Company, Limited Process for producing of epoxy compound
JP4938558B2 (ja) * 2007-06-18 2012-05-23 住友化学株式会社 チタノシリケートの製造方法およびオキシムの製造方法
CN101148260A (zh) * 2007-08-20 2008-03-26 华东师范大学 具有mww结构的钛硅分子筛及其合成和应用
US7501532B1 (en) * 2007-11-20 2009-03-10 Lyondell Chemical Technology, L.P. Process for producing hydrogen peroxide
US20090216033A1 (en) * 2008-02-27 2009-08-27 Lekhac Bi Epoxidation catalyst
JP2009233656A (ja) * 2008-03-05 2009-10-15 Sumitomo Chemical Co Ltd チタノシリケート触媒の再生方法
JP2010138032A (ja) * 2008-12-11 2010-06-24 Sumitomo Chemical Co Ltd チタノシリケートの製造方法

Also Published As

Publication number Publication date
CN102905787A (zh) 2013-01-30
US8124555B2 (en) 2012-02-28
JP2013518796A (ja) 2013-05-23
KR20160092034A (ko) 2016-08-03
CN102905787B (zh) 2015-04-29
EP2531297B1 (en) 2014-08-20
SG182756A1 (en) 2012-08-30
SG190585A1 (en) 2013-06-28
BR112012019011A8 (pt) 2018-05-29
EP2531297A2 (en) 2012-12-12
KR20120109603A (ko) 2012-10-08
BR112012019011A2 (pt) 2016-09-13
BR112012019011B1 (pt) 2024-02-06
JP5662481B2 (ja) 2015-01-28
WO2012018408A3 (en) 2012-11-29
US20110190517A1 (en) 2011-08-04
WO2012018408A2 (en) 2012-02-09

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