CN102884030B - 制备六氟-2-丁烯的方法 - Google Patents

制备六氟-2-丁烯的方法 Download PDF

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Publication number
CN102884030B
CN102884030B CN201180016420.3A CN201180016420A CN102884030B CN 102884030 B CN102884030 B CN 102884030B CN 201180016420 A CN201180016420 A CN 201180016420A CN 102884030 B CN102884030 B CN 102884030B
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hexafluoro
metal
catalyst
reaction
reactor
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CN102884030A (zh
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童雪松
H·王
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Sozhitech Performance Materials Usa
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Honeywell International Inc
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00—Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
    • C07C17/202—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
    • C07C17/206—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being HX
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/272—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
    • C07C17/278—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions of only halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/35—Preparation of halogenated hydrocarbons by reactions not affecting the number of carbon or of halogen atoms in the reaction
    • C07C17/358—Preparation of halogenated hydrocarbons by reactions not affecting the number of carbon or of halogen atoms in the reaction by isomerisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/09—Geometrical isomers

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
CN201180016420.3A 2010-03-26 2011-03-15 制备六氟-2-丁烯的方法 Active CN102884030B (zh)

Applications Claiming Priority (7)

Application Number Priority Date Filing Date Title
US31787910P 2010-03-26 2010-03-26
US61/317,879 2010-03-26
US61/317879 2010-03-26
US13/045926 2011-03-11
US13/045,926 2011-03-11
US13/045,926 US8461401B2 (en) 2010-03-26 2011-03-11 Method for making hexafluoro-2-butene
PCT/US2011/028476 WO2011119370A2 (en) 2010-03-26 2011-03-15 Method for making hexafluoro-2-butene

Publications (2)

Publication Number Publication Date
CN102884030A CN102884030A (zh) 2013-01-16
CN102884030B true CN102884030B (zh) 2015-11-25

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CN201180016420.3A Active CN102884030B (zh) 2010-03-26 2011-03-15 制备六氟-2-丁烯的方法

Country Status (7)

Country Link
US (1) US8461401B2 (enExample)
EP (1) EP2552873B1 (enExample)
JP (3) JP5913279B2 (enExample)
CN (1) CN102884030B (enExample)
ES (1) ES2654159T3 (enExample)
MX (1) MX2012011055A (enExample)
WO (1) WO2011119370A2 (enExample)

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US12421182B2 (en) 2020-01-23 2025-09-23 The Chemours Company Fc, Llc Synthesis of (e)-1,1,1,4,5,5,5-heptafluoro-4-(trifluoromethyl)pent-2-ene

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US9157018B2 (en) 2010-11-25 2015-10-13 Arkema France Compositions of chloro-trifluoropropene and hexafluorobutene
FR2968009B1 (fr) * 2010-11-25 2012-11-16 Arkema France Fluides frigorigenes contenant du (e)-1,1,1,4,4,4-hexafluorobut-2-ene
FR2968310B1 (fr) 2010-12-03 2012-12-07 Arkema France Compositions a base de 1,1,1,4,4,4-hexafluorobut-2-ene et de 3,3,4,4,4-pentafluorobut-1-ene
FR2977256B1 (fr) 2011-07-01 2013-06-21 Arkema France Compositions de 2,4,4,4-tetrafluorobut-1-ene et de cis-1,1,1,4,4,4-hexafluorobut-2-ene
CN103917507A (zh) * 2011-10-24 2014-07-09 纳幕尔杜邦公司 制备氢单氯氟丁烷和氢单氯氟戊烷化合物的催化方法
JP5790438B2 (ja) * 2011-11-21 2015-10-07 セントラル硝子株式会社 トランス−１−クロロ−３，３，３−トリフルオロプロペンの製造方法
FR2989084B1 (fr) 2012-04-04 2015-04-10 Arkema France Compositions a base de 2,3,3,4,4,4-hexafluorobut-1-ene
FR2989374A1 (fr) * 2012-04-11 2013-10-18 Arkema France Procede de preparation d'un compose olefinique sous forme d'un isomere specifique.
US9234123B2 (en) * 2013-03-21 2016-01-12 Hsi Fire & Safety Group, Llc Compositions for totally non-flammable aerosol dusters
US20170015607A1 (en) * 2014-03-21 2017-01-19 The Chemours Company Fc, Llc Processes for the production of z 1,1,1,4,4,4 hexafluoro 2-butene
US9353030B2 (en) * 2014-07-25 2016-05-31 Honeywell International Inc. One-step process for hexafluoro-2-butene
CN104370690B (zh) * 2014-11-20 2016-08-17 西安近代化学研究所 一种反式-1,1,1,4,4,4-六氟-2-丁烯的合成方法
CN104447186B (zh) * 2014-11-20 2016-08-17 西安近代化学研究所 一种2,4,4-三氯-1,1,1-三氟丁烷的制备方法
CN104529695B (zh) * 2015-01-26 2016-06-22 杭州芳环科技有限公司 一种制备1,1,1,4,4,4-六氟-2-丁烯的方法
JP6930962B2 (ja) * 2015-08-07 2021-09-01 ザ ケマーズ カンパニー エフシー リミテッド ライアビリティ カンパニー Ｚ−１，１，１，４，４，４−ヘキサフルオロ−２−ブテンのｅ−１，１，１，４，４，４−ヘキサフルオロ−２−ブテンへの接触異性化
EP3405516B1 (en) * 2016-01-22 2022-03-02 The Chemours Company FC, LLC Foaming of a reaction product of a polyisocyanate and an active hydrogen-containing compound
US11731925B2 (en) * 2016-07-27 2023-08-22 The Chemours Company Fc, Llc Process for producing halogenated olefins
KR102700055B1 (ko) * 2017-09-11 2024-08-29 더 케무어스 컴퍼니 에프씨, 엘엘씨 (e)-1,1,1,4,4,4-헥사플루오로부트-2-엔을 제조하는 액체상 공정
CN111094503B (zh) 2017-09-11 2022-04-01 科慕埃弗西有限公司 包含氟化氢和含氟烃的共沸组合物
CN107759440B (zh) * 2017-11-07 2020-07-03 中国民航大学 一种将含氟烯烃双键上的氟置换成氢的方法
CN111433177B (zh) * 2017-12-04 2024-04-16 科慕埃弗西有限公司 用于制备1,1,3-三氯-4,4,4-三氟丁-1-烯和(e)-1,1,1,4,4,4-六氟丁-2-烯的方法和中间体
CN109678650A (zh) * 2018-12-25 2019-04-26 西安近代化学研究所 一种1,1,1,3-四氯-4,4,4-三氟丁烷的制备方法
CN110590496A (zh) * 2019-09-24 2019-12-20 浙江三美化工股份有限公司 一种气相连续合成顺式-1,1,1,4,4,4-六氟-2-丁烯的方法
CN115210202B (zh) 2020-03-04 2025-01-21 科慕埃弗西有限公司 用于制备(z)-1,1,1,4,4,4-六氟-2-丁烯和中间体的方法
CN112159301B (zh) * 2020-09-29 2022-12-13 西安近代化学研究所 一种2-氯-1,1,1,4,4,4-六氟-2-丁烯的合成方法
US20230373887A1 (en) * 2020-10-15 2023-11-23 Resonac Corporation Method for storing fluorobutene
CN116472258A (zh) * 2020-10-15 2023-07-21 株式会社力森诺科 氟-2-丁烯的保存方法
KR102828130B1 (ko) * 2020-10-15 2025-07-03 가부시끼가이샤 레조낙 에칭 가스 및 그 제조 방법, 및 에칭 방법, 반도체 소자의 제조 방법
WO2022080275A1 (ja) * 2020-10-15 2022-04-21 昭和電工株式会社 フルオロ－２－ブテンの保管方法
US20230303469A1 (en) * 2020-10-15 2023-09-28 Resonac Corporation Method for storing fluoro-2-butene
KR102924118B1 (ko) * 2020-10-15 2026-02-09 가부시끼가이샤 레조낙 플루오로부텐의 보관 방법
WO2022085544A1 (ja) * 2020-10-22 2022-04-28 Ａｇｃ株式会社 電気設備
CN114716297B (zh) * 2021-01-06 2023-10-27 浙江省化工研究院有限公司 一种e-1,1,1,4,4,4-六氟-2-丁烯的制备方法
CN114292158B (zh) * 2021-12-01 2024-01-02 西安近代化学研究所 一种制备顺式-1,1,1,4,4,4-六氟-2-丁烯的方法
KR102788759B1 (ko) 2022-05-13 2025-04-01 (주)후성 1,1,1,4,4,4-헥사플루오로-2-부텐의 제조방법
CN116037120B (zh) * 2023-03-31 2023-07-14 北京宇极科技发展有限公司 1,1,1,4,4,4-六氟-2-丁烯的正反异构体的制备方法
CN116037117B (zh) * 2023-03-31 2023-07-25 北京宇极科技发展有限公司 引发剂、氟化催化剂和e-1,3,3,3-四氟丙烯与z-1,3,3,3-四氟丙烯的制备方法
CN121800603B (zh) * 2026-03-10 2026-05-26 山东联创聚合物有限公司 顺式-1,1,1,4,4,4-六氟-2-丁烯的制备方法

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US5463150A (en) * 1993-02-19 1995-10-31 Bayer Aktiengesellschaft Process for preparing hexafluorobutene
US5516951A (en) * 1992-11-20 1996-05-14 Daikin Industries Ltd. Process for preparing 1,1,1,4,4,4-hexafluoro-2-butene and 1,1,1,4,4,4-hexafluorobutane
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CN101500973A (zh) * 2005-01-19 2009-08-05 大湖化学公司 卤化碳制备方法，卤化碳分离方法和卤化碳制备系统
CN101578252A (zh) * 2006-09-05 2009-11-11 纳幕尔杜邦公司 1,2,3,3,3-五氟丙烯生产方法

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US5463150A (en) * 1993-02-19 1995-10-31 Bayer Aktiengesellschaft Process for preparing hexafluorobutene
CN101500973A (zh) * 2005-01-19 2009-08-05 大湖化学公司 卤化碳制备方法，卤化碳分离方法和卤化碳制备系统
CN101578252A (zh) * 2006-09-05 2009-11-11 纳幕尔杜邦公司 1,2,3,3,3-五氟丙烯生产方法

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US12421182B2 (en) 2020-01-23 2025-09-23 The Chemours Company Fc, Llc Synthesis of (e)-1,1,1,4,5,5,5-heptafluoro-4-(trifluoromethyl)pent-2-ene

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Publication number Publication date
WO2011119370A3 (en) 2011-12-22
JP6088618B2 (ja) 2017-03-01
EP2552873B1 (en) 2017-10-18
MX2012011055A (es) 2013-01-28
US8461401B2 (en) 2013-06-11
JP5913279B2 (ja) 2016-04-27
CN102884030A (zh) 2013-01-16
JP2017125023A (ja) 2017-07-20
JP2013523637A (ja) 2013-06-17
US20110237844A1 (en) 2011-09-29
EP2552873A2 (en) 2013-02-06
EP2552873A4 (en) 2014-09-10
ES2654159T3 (es) 2018-02-12
JP2016034970A (ja) 2016-03-17
WO2011119370A2 (en) 2011-09-29

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