CN102860445B - Preparation method for honeycomb element cream - Google Patents
Preparation method for honeycomb element cream Download PDFInfo
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- CN102860445B CN102860445B CN2012103493764A CN201210349376A CN102860445B CN 102860445 B CN102860445 B CN 102860445B CN 2012103493764 A CN2012103493764 A CN 2012103493764A CN 201210349376 A CN201210349376 A CN 201210349376A CN 102860445 B CN102860445 B CN 102860445B
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Abstract
The invention discloses a preparation method for honeycomb element cream, wherein the method is simple in technological process, and the honeycomb element cream is made by extracting active ingredients in honeycombs and then mixing the active ingredients in the honeycombs with high-concentration mature honey. The honeycomb element cream has strong relieving effects on various rhinitis and symptoms including nasal obstruction, running nose, headache, discomfort throat and the like which are caused by the various rhinitis, and simultaneously has good prevention and healthcare effects on various chronic inflammatory diseases including hyperlipidemia, colitis and the like.
Description
Technical field
The present invention relates to a kind of preparation method of honeycomb element cream, belong to the health food technology field.
Background technology
Honeycomb is that honeybee perches part, it is the place that honeybee is used for producing ex ovum, breeds the offspring and store the foods such as royal jelly, honey and Bee Pollen, keeping the multiple particular matters such as honeybee husks (similar animal placenta), propolis, beeswax in honeycomb, before bimillennium, the effect that has recognized that honeycomb among the people, in B.C. Shennong's Herbal, " sweet, the tepor, nontoxic of beeswax (honeycomb) flavor is just arranged.Cure mainly diarrhea purulence blood, bowl spares, the continuous metal-inflicted wound of hindering absolutely, benefit gas " record; application honeycomb treatment sore furuncle and rhinitis also have very long history; the modern medicine scientific research finds, honeycomb element for treatment hepatitis, rhinitis, nasosinusitis, nose is responsive, chronic and allergic rhinitis, rheumatic arthritis etc. have good result.Can alleviate rapidly because of symptoms such as nasal obstruction that all kinds of rhinitis cause, runny nose, headache, dizziness, throat discomforts.Also have simultaneously just record in Compendium of Material Medica, honey is smeared outward also has better effects to rhinitis.If coordinate honeycomb element to use, be used for smearing nasal cavity, one day 2 times. smear before sleeping once, effect is best.Modern technologies the analysis showed that, the composition of honeycomb extract is very complicated, and main component has aliphatic acid, tannin, glucoside, protein, amino acid, taurine, enzyme and trace element etc.How to utilize the technical method of science, extract the active ingredient in honeycomb, then be equipped with that honey is refining forms honeycomb element cream, having no the art has similar report.
Summary of the invention
The object of the invention is to overcome defect of the prior art, a kind of preparation method of honeycomb element cream is provided, described method technological process is simple, extracts active ingredients in honeycomb is out allocated with the natural ripe honey of high concentration and make honeycomb element cream, the symptoms such as the nasal obstruction that described honeycomb element cream can cause various rhinitis and all kinds of rhinitis, runny nose, headache, throat discomfort have mitigation very doughtily, simultaneously the various chronic inflammation diseases such as high fat of blood, colitis are also had good functions of prevention and health care.
The present invention is achieved by the following technical programs.
A kind of preparation method of honeycomb element cream, preparation process is as follows:
(1) select the honey comb that does not go mouldy, with honeycomb clean, paraffin removal, and then honeycomb is pulverized;
(2) honeycomb after pulverizing adds in extractor, carry out water extraction take pure water as solvent and get, the mass ratio of pure water and honeycomb is 20 ︰ 1, and the Water Under that is 80-85 ℃ in temperature extracts 2-4 hour, and then through 60-80 purpose plate-frame filtering, filter residue is adopted supercritical CO
2Extract, obtain extract; Filtrate is pumped in settling tank with cooling coil, cooling-sedimentation 22-24 hour under the condition of-4～0 ℃, again with sedimentation liquid through 500 purpose plate-frame filterings, obtain smart filtrate, add the vacuum decompression evaporimeter to carry out Vacuum Concentration smart filtrate, thickening temperature is 50-70 ℃, and vacuum is more than 0.096MPa, to obtain concentrate;
(3) the natural ripe honey allotment of the concentrate of the extract of 5-10 part, 50-70 part and 30-40 part is mixed, can make honeycomb element cream.
The preparation method of above-mentioned a kind of honeycomb element cream, wherein, described honey comb is selected the honey comb that does not go mouldy more than 3 years.
The preparation method of above-mentioned a kind of honeycomb element cream, wherein, described wax removing process is carried out heating evaporation for the honey comb that will clean according to parallel the inserting in distiller of honeycomb rightabout of placement direction in beehive, heating-up temperature is 80-90 ℃, time 2-4h, wait beeswax all to be down to room temperature after outflow.
The preparation method of above-mentioned a kind of honeycomb element cream, wherein, described pulverizing is for to be crushed to the 5-10 order with honeycomb.
The preparation method of above-mentioned a kind of honeycomb element cream, wherein, described supercritical CO
2The extraction temperature of extraction is 33-36 ℃, and extracting pressure is 28-30MPa, and separation temperature is 40-45 ℃, and separating pressure is 7-8MPa, and extraction time is 2-3 hour, CO
2Flow is 350L/h.
The preparation method of above-mentioned a kind of honeycomb element cream, wherein, the biodiversity percentage composition of described concentrate is 8-16%.
The preparation method of above-mentioned a kind of honeycomb element cream, wherein, the biodiversity percentage composition of described natural ripe honey is less than 18%.
The preparation method of a kind of honeycomb element cream of the present invention, described method technological process is simple, and reaction condition is gentle, production process is environment friendly and pollution-free.The method of the invention is out allocated the extracts active ingredients in honeycomb and is made honeycomb element cream with the natural ripe honey of high concentration, but the traditional drug characteristic that has kept honeycomb dispersing swelling and dissipating binds, anti-inflammatory analgesic, the various active ingredients in the honeycomb have fully been extracted simultaneously, coordinate the sweet and bowl spares of honey nutriment, the effect of moistening lung, ease constipation, both combine with honeycomb, honey, the purpose of can play nutrition, diseases prevention, curing the disease, and instant, mouthfeel is fragrant and sweet.The symptoms such as the nasal obstruction that honeycomb element cream of the present invention can cause various rhinitis and all kinds of rhinitis, runny nose, headache, throat discomfort have mitigation very doughtily, simultaneously the various chronic inflammation diseases such as high fat of blood, colitis are also had good functions of prevention and health care.
The specific embodiment
Embodiment 1
A kind of preparation method of honeycomb element cream, preparation process is as follows: (1) selects the honey comb that does not go mouldy more than 3 years, honeycomb is cleaned, and carry out paraffin removal, the honeycomb that cleaned is carried out heating evaporation, 80 ℃ of heating-up temperatures, time 2h according to parallel the inserting in distiller of honeycomb rightabout of placement direction in beehive, all be down to room temperature after outflow in beeswax, then honeycomb be crushed to 5 orders; (2) honeycomb after pulverizing adds in extractor, carries out water extraction take pure water as solvent and gets, and the mass ratio of pure water and honeycomb is 20 ︰ 1, and the Water Under that is 80 ℃ in temperature extracted 2 hours, and then through 60 purpose plate-frame filterings, filter residue was adopted supercritical CO
2Extract, extraction temperature is 33 ℃, and extracting pressure is 28MPa, and separation temperature is 40 ℃, and separating pressure is 7MPa, and extraction time is 2 hours, CO
2Flow is 350L/h, obtains extract; Filtrate is pumped in settling tank with cooling coil, cooling-sedimentation is 22 hours under the condition of-4 ℃, again with sedimentation liquid through 500 purpose plate-frame filterings, obtain smart filtrate, add the vacuum decompression evaporimeter to carry out Vacuum Concentration smart filtrate, thickening temperature is 50 ℃, and vacuum is 0.096MPa, obtain concentrate, the biodiversity percentage composition of described concentrate is 16%; (3) extract of 5 parts, the concentrate of 50 parts and the natural ripe honey allotment of 30 parts are mixed, can make honeycomb element cream.
Embodiment 2
A kind of preparation method of honeycomb element cream, preparation process is as follows: (1) selects the honey comb that does not go mouldy more than 3 years, honeycomb is cleaned, and carry out paraffin removal, the honeycomb that cleaned is carried out heating evaporation, 85 ℃ of heating-up temperatures, time 3h according to parallel the inserting in distiller of honeycomb rightabout of placement direction in beehive, all be down to room temperature after outflow in beeswax, then honeycomb be crushed to 8 orders; (2) honeycomb after pulverizing adds in extractor, carries out water extraction take pure water as solvent and gets, and the mass ratio of pure water and honeycomb is 20 ︰ 1, and the Water Under that is 82 ℃ in temperature extracted 3 hours, and then through 70 purpose plate-frame filterings, filter residue was adopted supercritical CO
2Extract, extraction temperature is 34 ℃, and extracting pressure is 29MPa, and separation temperature is 42 ℃, and separating pressure is 7.5MPa, and extraction time is 2.5 hours, CO
2Flow is 350L/h, obtains extract; Filtrate is pumped in settling tank with cooling coil, cooling-sedimentation is 23 hours under the condition of-2 ℃, again with sedimentation liquid through 500 purpose plate-frame filterings, obtain smart filtrate, add the vacuum decompression evaporimeter to carry out Vacuum Concentration smart filtrate, thickening temperature is 60 ℃, and vacuum is 0.097MPa, obtain concentrate, the biodiversity percentage composition of described concentrate is 12%; (3) extract of 8 parts, the concentrate of 60 parts and the natural ripe honey allotment of 35 parts are mixed, can make honeycomb element cream.
Embodiment 3
A kind of preparation method of honeycomb element cream, preparation process is as follows: (1) selects the honey comb that does not go mouldy more than 3 years, honeycomb is cleaned, and carry out paraffin removal, the honeycomb that cleaned is carried out heating evaporation, 90 ℃ of heating-up temperatures, time 4h according to parallel the inserting in distiller of honeycomb rightabout of placement direction in beehive, all be down to room temperature after outflow in beeswax, then honeycomb be crushed to 10 orders; (2) honeycomb after pulverizing adds in extractor, carries out water extraction take pure water as solvent and gets, and the mass ratio of pure water and honeycomb is 20 ︰ 1, and the Water Under that is 85 ℃ in temperature extracted 4 hours, and then through 80 purpose plate-frame filterings, filter residue was adopted supercritical CO
2Extract, extraction temperature is 36 ℃, and extracting pressure is 30MPa, and separation temperature is 45 ℃, and separating pressure is 8MPa, and extraction time is 3 hours, CO
2Flow is 350L/h, obtains extract; Filtrate is pumped in settling tank with cooling coil, cooling-sedimentation is 24 hours under the condition of 0 ℃, again with sedimentation liquid through 500 purpose plate-frame filterings, obtain smart filtrate, add the vacuum decompression evaporimeter to carry out Vacuum Concentration smart filtrate, thickening temperature is 70 ℃, and vacuum is 0.098MPa, obtain concentrate, the biodiversity percentage composition of described concentrate is 8%; (3) extract of 10 parts, the concentrate of 70 parts and the natural ripe honey allotment of 40 parts are mixed, can make honeycomb element cream.
Clinical testing: 50 of nasopharyngitis patients, take the honeycomb element cream of the method for the invention preparation, sooner or later respectively take every day 1 time (getting up rear with just before going to bed), each 10-15 gram, serve on 3 months, treatment nasopharyngitis successful, effectively the sx↓ rate reaches 50%, and long-term taking can make the nasopharyngitis recovery from illness gradually.
Here description of the invention and application is illustrative, wants that not therefore, the present invention is not subjected to the restriction of the present embodiment with scope restriction of the present invention in the above-described embodiments, and the technical scheme that any employing equivalence replacement obtains is all in the scope of protection of the invention.
Claims (4)
1. the preparation method of a honeycomb element cream, is characterized in that, preparation process is as follows:
(1) select the honey comb that does not go mouldy, with honeycomb clean, paraffin removal, and then honeycomb is pulverized;
(2) honeycomb after pulverizing adds in extractor, carry out water extraction take pure water as solvent and get, the mass ratio of pure water and honeycomb is 20 ︰ 1, and the Water Under that is 80-85 ℃ in temperature extracts 2-4 hour, and then through 60-80 purpose plate-frame filtering, filter residue is adopted supercritical CO
2Extract described supercritical CO
2The extraction temperature of extraction is 33-36 ℃, and extracting pressure is 28-30MPa, and separation temperature is 40-45 ℃, and separating pressure is 7-8MPa, and extraction time is 2-3 hour, CO
2Flow is 350L/h, obtains extract; Filtrate is pumped in settling tank with cooling coil, cooling-sedimentation 22-24 hour under the condition of-4～0 ℃, again with sedimentation liquid through 500 purpose plate-frame filterings, obtain smart filtrate, add the vacuum decompression evaporimeter to carry out Vacuum Concentration smart filtrate, thickening temperature is 50-70 ℃, and vacuum is more than 0.096MPa, to obtain concentrate;
(3) the natural ripe honey allotment of the concentrate of the extract of 5-10 part, 50-70 part and 30-40 part is mixed, can make honeycomb element cream.
2. the preparation method of a kind of honeycomb element cream as claimed in claim 1, is characterized in that, described honey comb is selected the honey comb that does not go mouldy more than 3 years.
3. the preparation method of a kind of honeycomb element cream as claimed in claim 1, is characterized in that, described pulverizing is for to be crushed to the 5-10 order with honeycomb.
4. the preparation method of a kind of honeycomb element cream as claimed in claim 1, is characterized in that, the biodiversity percentage composition of described concentrate is 8-16%.
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| CN2012103493764A CN102860445B (en) | 2012-09-19 | 2012-09-19 | Preparation method for honeycomb element cream |
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| CN2012103493764A CN102860445B (en) | 2012-09-19 | 2012-09-19 | Preparation method for honeycomb element cream |
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| CN102860445B true CN102860445B (en) | 2013-11-20 |
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Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103230012B (en) * | 2013-05-08 | 2015-01-28 | 福建新之源生物制品有限公司 | Honeycomb essence buccal tablet and preparation process thereof |
| CN103271259A (en) * | 2013-05-29 | 2013-09-04 | 安徽省宿松县刘氏蜂产品有限责任公司 | Method for preparing honeycomb element concentrated pills |
| CN103549067B (en) * | 2013-11-21 | 2015-01-07 | 安徽惠隆中药饮片有限公司 | Health-care tea |
| CN103656275B (en) * | 2013-11-25 | 2015-08-26 | 陈文立 | A kind of Chinese medicine composition for the treatment of rhinitis and preparation method thereof |
| CN104839534A (en) * | 2015-04-25 | 2015-08-19 | 安徽蜂献蜂业有限公司 | Hericium erinaceus health care honeycomb element |
| CN104984949A (en) * | 2015-06-09 | 2015-10-21 | 上海鸿辉光通科技股份有限公司 | Wax removing washing method for V groove |
| CN104957457A (en) * | 2015-06-30 | 2015-10-07 | 广东省昆虫研究所 | Honeybee comb honey cream and making method for same |
| CN107890435A (en) * | 2017-11-28 | 2018-04-10 | 曾祥明 | The preparation method of honeycomb wax lip gloss |
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| CN1293043A (en) * | 1999-10-19 | 2001-05-02 | 梁霭 | Honeycomb honey and its preparing process |
| CN1634151A (en) * | 2004-10-11 | 2005-07-06 | 孙崇华 | Technology for processing honey comb element |
| CN102423032A (en) * | 2011-10-14 | 2012-04-25 | 安徽省宿松县刘氏蜂产品有限责任公司 | Processing technology of honeycomb element |
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| CN1293043A (en) * | 1999-10-19 | 2001-05-02 | 梁霭 | Honeycomb honey and its preparing process |
| CN1634151A (en) * | 2004-10-11 | 2005-07-06 | 孙崇华 | Technology for processing honey comb element |
| CN102423032A (en) * | 2011-10-14 | 2012-04-25 | 安徽省宿松县刘氏蜂产品有限责任公司 | Processing technology of honeycomb element |
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| 余林生 等.蜜蜂巢脾的陈旧过程及其开发利用.《中国蜂业》.2010,第61卷(第6期),第39、40、47页. |
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Owner name: JIANGSU JIANGDAYUAN ECOLOGICAL BIO-TECHNOLOGY CO., Free format text: FORMER NAME: JIANGSU NUCELL BIO-TECHNOLOGY CO., LTD. |
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Address after: 212009, No. 2, sailing Road, Zhenjiang hi tech Industrial Development Zone, Zhenjiang New District, Jiangsu, Zhenjiang Patentee after: JIANGSU JIANGDAYUAN ECOLOGICAL BIOLOGICAL TECHNOLOGY CO., LTD. Address before: 212200 hi tech Industrial Park, Jiangsu, Zhenjiang, No. four, No. 2 Patentee before: Jiangsu Jiangdayuan Ecology Biological Technology Co.,Ltd. |