CN102795936A - Chinese medicinal herb-seaweed composite biological agent and preparation method thereof - Google Patents
Chinese medicinal herb-seaweed composite biological agent and preparation method thereof Download PDFInfo
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- CN102795936A CN102795936A CN2012103245035A CN201210324503A CN102795936A CN 102795936 A CN102795936 A CN 102795936A CN 2012103245035 A CN2012103245035 A CN 2012103245035A CN 201210324503 A CN201210324503 A CN 201210324503A CN 102795936 A CN102795936 A CN 102795936A
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Abstract
The invention provides a Chinese medicinal herb-seaweed fertilizer composite biological agent and a preparation method thereof. Effective constituents are extracted from Chinese medicinal herbs and seaweed, which are used as main raw materials, to prepare the biological composite preparation. The Chinese medicinal herb-seaweed fertilizer composite biological agent not only reserves biological active substances in seaweed, but also enhances the drug effect of the Chinese medicinal herbs as insecticide. The biological composite preparation contains rich Chinese medicinal herbs and multiple active substances in seaweed, thereby enhancing the photosynthesis of crops, enhancing the crop yield and product quality, enhancing the drought tolerance, cold tolerance and stress tolerance of the crops, accelerating prematurity and fruit setting rate, preventing and killing various soil insects and enhancing the disease resistance of the crops. The invention has the advantages of low cost, favorable solubility and environmental protection, and is convenient for popularization.
Description
Technical field
The present invention relates to biological technical field, specifically be meant a kind of composite biological agent by herbal medicine and seaweed fertilizer and preparation method thereof.
Background technology
At present, herbal medicine has been widely used in the control of agricultural pest as sterilant, and it is big, residual many to have solved original chemicals class agricultural chemical insecticide consumption, the problem of influence ecological environment and HUMAN HEALTH.
In recent years; Marine alga begins to occur and be applied in the agriculture prodn as new bio-fertilizer; Because marine alga contains abundant mineral element and various VITAMINs; Wherein, physiologically active substances such as the amino acid that contains, mineral substance, polysaccharide, VITAMINs and phytokinin, plant hormone and dormin effectively promote plant absorbing soil nutrient, moisture and gas; Increase chlorophyll content of plant, effectively improve photosynthetic efficiency; Can enhancing crop multiple degeneration-resistant functions such as drought resisting, cold-resistant, disease-resistant worm, improve crop yield, improve crop quality; Can also improve Soil structure, improve multiple efficacies such as retention capacity of soil.
Herbal medicine possesses excellent characteristic and good result of use as sterilant and marine alga as bio-feritlizer separately, if can both be combined, will be unusual ideal agricultural preparation; But, in production process in the past, herbal medicine and marine alga are carried out when composite; Because the complicacy of medicinal herb components, physiologically active substances such as amino acid that contains in the marine alga and polysaccharide are destroyed easily, are difficult to give full play to even reduce the fertilizer efficiency of seaweed fertilizer; Therefore, become insoluble technical problem.
Summary of the invention
Deficiency to the prior art existence; Technical problem to be solved by this invention is, composite biological agent of a kind of herbal medicine and seaweed fertilizer and preparation method thereof is provided, and is to be main raw material with natural Chinese medicinal herb and marine alga; Through pre-treatment, lixiviate, neutralization, process step such as concentrated, composite; With the extracts active ingredients in herbal medicine and the marine alga and process biological compound formulation, not only kept the physiologically active substance in the marine alga, and strengthened the property of medicine effect of herbal medicine as sterilant.
For solving the problems of the technologies described above, the technical scheme that the present invention taked is, composite biological agent of a kind of herbal medicine and marine alga and preparation method thereof, and the composite biological agent of herbal medicine and marine alga comprises following component, its weight proportion is:
The herbal medicine marine alga mixes 10 parts-80 parts of base fluids, 5 parts-25 parts of humic acidss, 5 parts-25 parts in urea, 5 parts-25 parts of monoammonium phosphates, 5 parts-25 parts of potassium primary phosphates, 2 parts-30 parts of vitriolate of tartar, 2 parts-20 parts of trace elements;
Wherein, the herbal medicine marine alga mixes base fluid and comprises following component, and its weight proportion is:
20 parts-45 parts of extracts of Chinese herbal medicine, 50 parts-80 parts of seaweed extracted liquors, 5 parts-20 parts of buffer reagent metalloproteases, 5 parts-20 parts in stablizer wood vinegar.
Above-mentioned herbal medicine and the composite biological agent of marine alga, the main raw material weight proportion of extracts of Chinese herbal medicine is following: tuber of stemona 40-70g, bark of eucommia 20-70g, root of langdu 30-80g; Herba Andrographis 30-70g, Herba Sophorae alopecuroidis 10-40g, Radix Astragali 30-80g, root of large-flowered skullcap 20-60g; Herba Houttuyniae 90-130g, kuh-seng 10-40g, Radix Glycyrrhizae 20-50g; Garlicin 30-60g, pipe tobacco 80-150g, Rangooncreeper Fruit 20-70g.
Above-mentioned herbal medicine and the composite biological agent of marine alga, the main raw material of seaweed extracted liquor are brown alga.
Above-mentioned herbal medicine and the composite biological agent of marine alga, trace element are one or more in magnesium, copper, manganese, iron, boron, zinc, molybdenum, the calcium.
The preparation method of above-mentioned herbal medicine and the composite biological agent of marine alga comprises following content:
The first step, produce extracts of Chinese herbal medicine: the herbal raw material of formula ratio is cleaned the back mix, be crushed to 300 orders, press (1), (3) or (2), (3) two kinds of technologies extractions as follows:
(1) herbal powder is mixed with water, pH value is adjusted to 9-11, add Sumizyme MP and extracted 24 hours at 45-65 degree Celsius;
(2) herbal powder is mixed with water, pH value is adjusted to 1-3, add aspartic protease and extracted 30 hours at 15-25 degree Celsius;
(3) cool to about 0 degree, pH value is adjusted to 7, separate to remove residue, to be concentrated into proportion be that 0.8-1.2g/ml promptly obtains extracts of Chinese herbal medicine to vacuum pressed then;
The weight proportion of said herbal raw material each component is: tuber of stemona 40-70g, bark of eucommia 20-70g, root of langdu 30-80g, Herba Andrographis 30-70g; Herba Sophorae alopecuroidis 10-40g, Radix Astragali 30-80g, root of large-flowered skullcap 20-60g; Herba Houttuyniae 90-130g, kuh-seng 10-40g, Radix Glycyrrhizae 20-50g; Garlicin 30-60g, pipe tobacco 80-150g, Rangooncreeper Fruit 20-70g;
In second step, produce seaweed extracted liquor: marine alga is cleaned oven dry be crushed to 300 orders, extract by (1), (3), (4) or (2), (3), (4) two kinds of technologies:
(1) marine algae powder is mixed with water, pH value is adjusted to 9-11, extracted 4-7 hour at 75-100 degree Celsius;
(2) marine algae powder is mixed with water, pH value is adjusted to 1-3, extracted 3-5 hour at 45-65 degree Celsius;
(3) pH value is adjusted to 7, then separating and removing impurities;
(4) to be concentrated into proportion be 1-1.4g/ml to vacuum pressed, promptly obtains seaweed extracted liquor;
In the 3rd step, produce the herbal medicine marine alga and mix base fluid: with extracts of Chinese herbal medicine and seaweed extracted liquor thorough mixing, add the buffer reagent metalloprotease then, with the stablizer wood vinegar;
The weight proportion of said each component is: 20 parts-45 parts of extracts of Chinese herbal medicine, 50 parts-80 parts of seaweed extracted liquors, 5 parts-20 parts of buffer reagent metalloproteases, 5 parts-20 parts in stablizer wood vinegar;
In the 4th step, process the composite biological agent of herbal medicine and marine alga: the herbal medicine marine alga is mixed in the base fluid add humic acids, urea, vitriolate of tartar, monoammonium phosphate, potassium primary phosphate and trace element, mix;
The weight proportion of said each component is: the herbal medicine marine alga mixes 10 parts-80 parts of base fluids, 5 parts-25 parts of humic acidss, 5 parts-25 parts in urea, 2 parts-30 parts of vitriolate of tartar, 5 parts-25 parts of monoammonium phosphates, 5 parts-25 parts of potassium primary phosphates, 2 parts-20 parts of trace elements.
The preparation method of above-mentioned herbal medicine and the composite biological agent of marine alga, the first step is produced in the extracts of Chinese herbal medicine, and the water consumption in (1) or (2) is 10-20 a times of herbal powder weight.
The preparation method of above-mentioned herbal medicine and the composite biological agent of marine alga, second step, to produce in the seaweed extracted liquor, the water consumption in (1) or (2) is 10-20 a times of marine algae powder weight.
The preparation method of above-mentioned herbal medicine and the composite biological agent of marine alga, the first step is produced in the extracts of Chinese herbal medicine, and the alkali that the adjusting pH value uses is Pottasium Hydroxide, sodium hydroxide, salt of wormwood or yellow soda ash, and the acid of using is hydrochloric acid, sulfuric acid or phosphoric acid.
The preparation method of above-mentioned herbal medicine and the composite biological agent of marine alga, second step, to produce in the seaweed extracted liquor, the alkali that the adjusting pH value uses is Pottasium Hydroxide, sodium hydroxide, salt of wormwood or yellow soda ash, the acid of using is hydrochloric acid, sulfuric acid or phosphoric acid.
The preparation method of above-mentioned herbal medicine and the composite biological agent of marine alga, trace element is one or more in magnesium, copper, manganese, iron, boron, zinc, molybdenum, the calcium.
The present invention has following advantage and beneficial effect:
The active substance extraction yield of leather medicine and marine alga is high in of the present invention, does not destroy the effective constituent in herbal medicine, the marine alga, contains multiple vegeto-alkali; Glycosides sugar, type mushroom sugar, protein, tannin enzyme, auxins benzazolyl compounds, Plant hormones regulators,gibberellins compounds; The cytokinin compounds; Tang oligosaccharide, amino acid and magnesium, copper, iron, zinc, boron, molybdenum etc., technology is simple, and production cost is lower; And can the composite biological agent of herbal medicine and marine alga be prepared into all kinds of herbal medicine seaweed fertilizer, effect is better.
Production cost of the present invention is low, and solvability is good, plant is not only had promote growth, the effect of extra-nutrition, and can also improve the resistance against diseases of plant self, repellent with kill subterranean pest-insect, harmless to people and animals and physical environment.Fast, the cold-resistant drought resisting so the crop plant of this organic fertilizer pouring of process is not only grown.And fruit-setting rate is high, ripe early, painted good, and the disease resistance ability is strong.
The present invention can be used for cash crop such as soybean, grape, paddy rice, corn, rape, cotton, strawberry, apple, tobacco, tomato, watermelon, cucumber, sponge gourd, greengrocery; Nontoxic, noresidue; Not only can coordinate plant growth; Improve the ability of plant disease-resistant evil, and can repellent with kill subterranean pest-insect; The marine alga as fertilizer sources can improve crop drought resistance, cold-resistant, etc. resistance, can also multiple highly active nutritive substance be provided to crop, promote plant growth; Improve product quality, improve crop yield, both combine and not only can improve fertilizer utilization ratio, reduce the access times of chemical pesticide; And various chemical residual in the minimizing farm crop; Alleviate the degree that hardens of soil, improve the breeding of profitable strain in the soil, strengthen the soil fertility of soil.
Embodiment
Embodiment 1
The herbal medicine of present embodiment and the composite biological agent of marine alga comprise following component, and its weight proportion is:
The herbal medicine marine alga mixes 10 parts of base fluids, 10 parts of humic acidss, 15 parts in urea, 5 parts of monoammonium phosphates, 10 parts of potassium primary phosphates, 5 parts of vitriolate of tartar, 5 parts in magnesium;
Wherein, the herbal medicine marine alga mixes base fluid and comprises following component, and its weight proportion is:
20 parts of extracts of Chinese herbal medicine, 60 parts of seaweed extracted liquors, 10 parts of buffer reagent metalloproteases, 10 parts in stablizer wood vinegar;
The main raw material weight proportion of extracts of Chinese herbal medicine is following: hundred step 40g, bark of eucommia 30g, root of langdu 30g, Herba Andrographis 40g, Herba Sophorae alopecuroidis 20g, Radix Astragali 30g, root of large-flowered skullcap 20g, Herba Houttuyniae 100g, kuh-seng 20g, Radix Glycyrrhizae 20g, garlicin 40g, pipe tobacco 90g Rangooncreeper Fruit 50g;
The main raw material of seaweed extracted liquor is a brown alga.
The preparation method of the herbal medicine of present embodiment and the composite biological agent of marine alga comprises following content:
The first step, produce extracts of Chinese herbal medicine: the herbal raw material of formula ratio is cleaned the back mix, be crushed to 300 orders, extract by following technology:
1, herbal powder is mixed with water, water consumption is 15 times of herbal powder weight, adds 30mol/l Pottasium Hydroxide pH value is adjusted to 9, adds Sumizyme MP and extracts 24 hours at 50 degree Celsius;
2, cool to about 0 degree, add 20mol/l hydrochloric acid pH value is adjusted to 7, separate and remove residue, obtain tawny liquid, to be concentrated into proportion be that 0.8g/ml promptly obtains extracts of Chinese herbal medicine to vacuum pressed then;
Wherein, the weight proportion of herbal raw material each component is: tuber of stemona 40g, bark of eucommia 30g, root of langdu 30g, Herba Andrographis 40g, Herba Sophorae alopecuroidis 20g, Radix Astragali 30g, root of large-flowered skullcap 20g, Herba Houttuyniae 100g, kuh-seng 20g, Radix Glycyrrhizae 20g, garlicin 40g, pipe tobacco 90g, Rangooncreeper Fruit 40g.
In second step, produce seaweed extracted liquor: marine alga is cleaned oven dry be crushed to 300 orders, extract by following technology:
1, marine algae powder is mixed with water, water consumption is 15 times of marine algae powder weight, adds 30mol/l Pottasium Hydroxide pH value is adjusted to 10, extracts 5 hours at 90 degrees centigrade;
2, add 20mol/l hydrochloric acid pH value is adjusted to 7, then separating and removing impurities;
3, to be concentrated into proportion be 1.2g/ml to vacuum pressed, promptly obtains seaweed extracted liquor.
In the 3rd step, produce the herbal medicine marine alga and mix base fluid: with extracts of Chinese herbal medicine and seaweed extracted liquor thorough mixing, add the buffer reagent metalloprotease then, the stablizer wood vinegar;
The weight proportion of each component is: 20 parts of extracts of Chinese herbal medicine, 60 parts of seaweed extracted liquors, 10 parts of buffer reagent metalloproteases, 10 parts in stablizer wood vinegar.
In the 4th step, process the composite biological agent of herbal medicine and marine alga: the herbal medicine marine alga is mixed in the base fluid add humic acids, urea, monoammonium phosphate, potassium primary phosphate, vitriolate of tartar and magnesium, mix;
The weight proportion of each component is: the herbal medicine marine alga mixes 10 parts of base fluids, 10 parts of humic acidss, 15 parts in urea, 5 parts of monoammonium phosphates, 10 parts of potassium primary phosphates, 5 parts of vitriolate of tartar, 5 parts in sal epsom.
The composite biological agent result of use of the herbal medicine of present embodiment and marine alga is following:
Subjects: plastic tent cucumber, experiment field and each 1 mu in contrast field;
Experimental plot: dash with every mu of the form of topdressing and to execute the composite biological agent 10kg of herbal medicine and marine alga;
Contrast the field: dash for every mu with the form of topdressing and execute nitrogen, phosphorus, the water-soluble fertile 10kg of potassium (20wt%-20wt%-20wt%) macroelement;
The contrast effect: it is harmful serious to dash the contrast field root knot nematode of executing nitrogen, phosphorus, the water-soluble fertilizer of potassium (15wt%-15wt%-15wt%) macroelement, yellow leaf, and sugar-preserved gourd dysplasia phenomenon is serious; Dash the experiment field of executing the Chinese medicine seaweed fertilizer and do not receive insect pest leaf look dark green basically, sugar-preserved gourd is straight, good colors, and the experiment field is to high by about 21% according to the real estate amount.
Embodiment 2
The herbal medicine of present embodiment and the composite biological agent of marine alga comprise following component, and its weight proportion is:
The herbal medicine marine alga mixes 20 parts of base fluids, 5 parts of humic acidss, 5 parts in urea, 10 parts of monoammonium phosphates, 5 parts of potassium primary phosphates, 10 parts of vitriolate of tartar, 5 parts of chelated irons, 5 parts in zinc sulfate;
Wherein, the herbal medicine marine alga mixes base fluid and comprises following component, and its weight proportion is:
45 parts of extracts of Chinese herbal medicine, 60 parts of seaweed extracted liquors, 5 parts of buffer reagent metalloproteases, 5 parts in stablizer wood vinegar;
The main raw material weight proportion of extracts of Chinese herbal medicine is following: tuber of stemona 50g, bark of eucommia 20g, root of langdu 50g, Herba Andrographis 30g, Herba Sophorae alopecuroidis 10g, Radix Astragali 50g, root of large-flowered skullcap 40g, Herba Houttuyniae 90g, kuh-seng 10g, Radix Glycyrrhizae 30g, garlicin 30g, pipe tobacco 80g, Rangooncreeper Fruit 30g;
The main raw material of seaweed extracted liquor is a brown alga.
The preparation method of the herbal medicine of present embodiment and the composite biological agent of marine alga comprises following content:
The first step, produce extracts of Chinese herbal medicine: the herbal raw material of formula ratio is cleaned the back mix, be crushed to 300 orders, extract by following technology:
1, herbal powder is mixed with water, water consumption is 15 times of herbal powder weight, adds 50mol/l sulfuric acid pH value is adjusted to 3, adds Sumizyme MP and extracts 30 hours at 20 degree Celsius;
2, cool to about 0 degree, add 60mol/l sodium hydroxide pH value is adjusted to 7, separate and remove residue, obtain tawny liquid, to be concentrated into proportion be that 0.8g/ml promptly obtains extracts of Chinese herbal medicine to vacuum pressed then;
Wherein, the weight proportion of herbal raw material each component is: tuber of stemona 50g, bark of eucommia 20g, root of langdu 50g, Herba Andrographis 30g, Herba Sophorae alopecuroidis 10g, Radix Astragali 50g, root of large-flowered skullcap 40g, Herba Houttuyniae 90g, kuh-seng 10g, Radix Glycyrrhizae 30g, garlicin 30g, pipe tobacco 80g, Rangooncreeper Fruit 30g.
In second step, produce seaweed extracted liquor: marine alga is cleaned oven dry be crushed to 300 orders, extract by following technology:
1, marine algae powder is mixed with water, water consumption is 15 times of marine algae powder weight, adds 50mol/l sulfuric acid pH value is adjusted to 1, extracts 4 hours at 50 degrees centigrade;
2, add 60mol/l sodium hydroxide pH value is adjusted to 7, then separating and removing impurities;
3, to be concentrated into proportion be 1g/ml to vacuum pressed, promptly obtains seaweed extracted liquor.
In the 3rd step, produce the herbal medicine marine alga and mix base fluid: with extracts of Chinese herbal medicine and seaweed extracted liquor thorough mixing, add the buffer reagent metalloprotease then, the stablizer wood vinegar;
The weight proportion of each component is: 45 parts of extracts of Chinese herbal medicine, 60 parts of seaweed extracted liquors, 5 parts of buffer reagent metalloproteases, 5 parts in stablizer wood vinegar.
In the 4th step, process the composite biological agent of herbal medicine and marine alga: the herbal medicine marine alga is mixed in the base fluid add humic acids, urea, monoammonium phosphate, potassium primary phosphate, vitriolate of tartar and magnesium, mix;
The weight proportion of each component is: the herbal medicine marine alga mixes 20 parts of base fluids, 5 parts of humic acidss, 5 parts in urea, 10 parts of monoammonium phosphates, 5 parts of potassium primary phosphates, 10 parts of vitriolate of tartar, 5 parts of chelated irons, 5 parts in zinc sulfate.
The composite biological agent result of use of the herbal medicine of present embodiment and marine alga is following:
Subjects: booth sponge gourd, experiment field and each 1 mu in contrast field;
Experimental plot: dash with every mu of the form of topdressing and to execute the composite biological agent 10kg of herbal medicine and marine alga;
Contrast the field: dash for every mu with the form of topdressing and execute nitrogen, phosphorus, the water-soluble fertile 10kg of potassium (20wt%-20wt%-20wt%) macroelement;
The contrast effect: it is harmful serious to dash the contrast field root knot nematode of executing nitrogen, phosphorus, the water-soluble fertilizer of potassium (20wt%-20wt%-20wt%) macroelement, yellow leaf, and sugar-preserved gourd eel-like figure phenomenon is serious, and bacterial disease is also heavier; Dash the experiment field of executing the Chinese medicine seaweed fertilizer and do not receive insect pest basically, blade is plump, and sugar-preserved gourd is straight and long, is beautiful in design and color, and does not have the disease of leaf class basically, and the experiment field is to high by about 23% according to the real estate amount.
Embodiment 3
The herbal medicine of present embodiment and the composite biological agent of marine alga comprise following component, and its weight proportion is:
The herbal medicine marine alga mixes 40 parts of base fluids, 15 parts of humic acidss, 15 parts in urea, 15 parts of monoammonium phosphates, 15 parts of potassium primary phosphates, 15 parts of vitriolate of tartar, 3 parts in copper sulfate, 3 parts of manganous sulfates, 2 parts of ammonium molybdates, 7 parts in zinc sulfate;
Wherein, the herbal medicine marine alga mixes base fluid and comprises following component, and its weight proportion is:
20 parts of extracts of Chinese herbal medicine, 55 parts of seaweed extracted liquors, 10 parts of buffer reagent metalloproteases, 15 parts in stablizer wood vinegar;
The main raw material weight proportion of extracts of Chinese herbal medicine is following: tuber of stemona 40g, bark of eucommia 20g, root of langdu 50g, Herba Andrographis 50g, Herba Sophorae alopecuroidis 30g, Radix Astragali 40g, root of large-flowered skullcap 50g, Herba Houttuyniae 120g, kuh-seng 30g, Radix Glycyrrhizae 40g, garlicin 60g, pipe tobacco 100g, Rangooncreeper Fruit 70g;
The main raw material of seaweed extracted liquor is a brown alga.
The preparation method of the herbal medicine of present embodiment and the composite biological agent of marine alga comprises following content:
The first step, produce extracts of Chinese herbal medicine: the herbal raw material of formula ratio is cleaned the back mix, be crushed to 300 orders, extract by following technology:
1, herbal powder is mixed with water, water consumption is 20 times of herbal powder weight, adds 40mol/l sulfuric acid pH value is adjusted to 1, adds Sumizyme MP and extracts 30 hours at 25 degree Celsius;
2, cool to about 0 degree, add 60mol/l salt of wormwood pH value is adjusted to 7, separate and remove residue, obtain tawny liquid, to be concentrated into proportion be that 1.2g/ml promptly obtains extracts of Chinese herbal medicine to vacuum pressed then;
Wherein, the weight proportion of herbal raw material each component is: tuber of stemona 40g, bark of eucommia 20g, root of langdu 50g, Herba Andrographis 50g, Herba Sophorae alopecuroidis 30g, Radix Astragali 40g, root of large-flowered skullcap 50g, Herba Houttuyniae 120g, kuh-seng 30g, Radix Glycyrrhizae 40g, garlicin 60g, pipe tobacco 100g, Rangooncreeper Fruit 70g.
In second step, produce seaweed extracted liquor: marine alga is cleaned oven dry be crushed to 300 orders, extract by following technology:
1, marine algae powder is mixed with water, water consumption is 10 times of marine algae powder weight, adds 60mol/l salt of wormwood pH value is adjusted to 9, extracts 7 hours at 75 degrees centigrade;
2, add 40mol/l sulfuric acid pH value is adjusted to 7, then separating and removing impurities;
3, to be concentrated into proportion be 1.4g/ml to vacuum pressed, promptly obtains seaweed extracted liquor.
In the 3rd step, produce the herbal medicine marine alga and mix base fluid: with extracts of Chinese herbal medicine and seaweed extracted liquor thorough mixing, add the buffer reagent metalloprotease then, the stablizer wood vinegar;
The weight proportion of each component is: 20 parts of extracts of Chinese herbal medicine, 55 parts of seaweed extracted liquors, 10 parts of buffer reagent metalloproteases, 15 parts in stablizer wood vinegar.
In the 4th step, process the composite biological agent of herbal medicine and marine alga: the herbal medicine marine alga is mixed in the base fluid add humic acids, urea, monoammonium phosphate, potassium primary phosphate, vitriolate of tartar and magnesium, mix;
The weight proportion of each component is: the herbal medicine marine alga mixes 40 parts of base fluids, 15 parts of humic acidss, 15 parts in urea, 15 parts of monoammonium phosphates, 15 parts of potassium primary phosphates, 15 parts of vitriolate of tartar, 3 parts in copper sulfate, 3 parts of manganous sulfates, 2 parts of ammonium molybdates, 7 parts in zinc sulfate.
The composite biological agent result of use of the herbal medicine of present embodiment and marine alga is following:
Subjects: shed capsicum, experiment field and each 1 mu in contrast field;
Experimental plot: dash with every mu of the form of topdressing and to execute the composite biological agent 10kg of herbal medicine and marine alga;
Contrast the field: dash for every mu with the form of topdressing and execute nitrogen, phosphorus, the water-soluble fertile 10kg of potassium (14wt%-6wt%-30wt%) macroelement;
The contrast effect: the contrast field root knot nematode insect pest towards executing nitrogen, phosphorus, the water-soluble fertilizer of potassium (14wt%-6wt%-30wt%) macroelement is heavier, and seat flower rate is few, and trialeurodes vaporariorum is more; Dash the experiment field of executing the Chinese medicine seaweed fertilizer and do not receive insect pest basically; The leaf look dark green, and pepper fruit is big, and the fruit type is straight; Basically do not have trialeurodes vaporariorum to occur, the experiment field is to high by about 19% according to the real estate amount.
Embodiment 4
The herbal medicine of present embodiment and the composite biological agent of marine alga comprise following component, and its weight proportion is:
The herbal medicine marine alga mixes 50 parts of base fluids, 25 parts of humic acidss, 20 parts in urea, 20 parts of monoammonium phosphates, 20 parts of potassium primary phosphates, 2 parts of vitriolate of tartar, 5 parts in sal epsom, 3 parts in copper sulfate, 3 parts of manganous sulfates, 3 parts of chelated irons, 3 parts of boron, 3 parts in nitrocalcite;
Wherein, the herbal medicine marine alga mixes base fluid and comprises following component, and its weight proportion is:
25 parts of extracts of Chinese herbal medicine, 50 parts of seaweed extracted liquors, 10 parts of buffer reagent metalloproteases, 15 parts in stablizer wood vinegar;
The main raw material weight proportion of extracts of Chinese herbal medicine is following: hundred step 60g, bark of eucommia 50g, root of langdu 60g, Herba Andrographis 30g, Herba Sophorae alopecuroidis 10g, Radix Astragali 60g, root of large-flowered skullcap 60g, Herba Houttuyniae 130g, kuh-seng 40g, Radix Glycyrrhizae 20g, garlicin 50g, pipe tobacco 130g, Rangooncreeper Fruit 30g;
The main raw material of seaweed extracted liquor is a brown alga.
The preparation method of the herbal medicine of present embodiment and the composite biological agent of marine alga comprises following content:
The first step, produce extracts of Chinese herbal medicine: the herbal raw material of formula ratio is cleaned the back mix, be crushed to 300 orders, extract by following technology:
1, herbal powder is mixed with water, water consumption is 20 times of herbal powder weight, adds 50mol/l Pottasium Hydroxide pH value is adjusted to 11, adds Sumizyme MP and extracts 24 hours at 45 degree Celsius;
2, cool to about 0 degree, add 40mol/l hydrochloric acid pH value is adjusted to 7, separate and remove residue, obtain tawny liquid, to be concentrated into proportion be that 0.9g/ml promptly obtains extracts of Chinese herbal medicine to vacuum pressed then;
Wherein, the weight proportion of herbal raw material each component is: tuber of stemona 60g, bark of eucommia 50g, root of langdu 60g, Herba Andrographis 30g, Herba Sophorae alopecuroidis 10g, Radix Astragali 60g, root of large-flowered skullcap 60g, Herba Houttuyniae 130g, kuh-seng 40g, Radix Glycyrrhizae 20g, garlicin 50g, pipe tobacco 130g, Rangooncreeper Fruit 30g.
In second step, produce seaweed extracted liquor: marine alga is cleaned oven dry be crushed to 300 orders, extract by following technology:
1, marine algae powder is mixed with water, water consumption is 20 times of marine algae powder weight, adds 50mol/l Pottasium Hydroxide pH value is adjusted to 11, extracts 4 hours at 100 degrees centigrade;
2, add 40mol/l hydrochloric acid pH value is adjusted to 7, then separating and removing impurities;
3, to be concentrated into proportion be 1.2g/ml to vacuum pressed, promptly obtains seaweed extracted liquor.
In the 3rd step, produce the herbal medicine marine alga and mix base fluid: with extracts of Chinese herbal medicine and seaweed extracted liquor thorough mixing, add the buffer reagent metalloprotease then, the stablizer wood vinegar;
The weight proportion of each component is: 25 parts of extracts of Chinese herbal medicine, 50 parts of seaweed extracted liquors, 10 parts of buffer reagent metalloproteases, 15 parts in stablizer wood vinegar.
In the 4th step, process the composite biological agent of herbal medicine and marine alga: the herbal medicine marine alga is mixed in the base fluid add humic acids, urea, monoammonium phosphate, potassium primary phosphate, vitriolate of tartar and magnesium, mix;
The weight proportion of each component is: the herbal medicine marine alga mixes 50 parts of base fluids, 25 parts of humic acidss, 20 parts in urea, 20 parts of monoammonium phosphates, 20 parts of potassium primary phosphates, 2 parts of vitriolate of tartar, 5 parts in sal epsom, 3 parts in copper sulfate, 3 parts of manganous sulfates, 3 parts of chelated irons, 3 parts of boron, 3 parts in nitrocalcite.
The composite biological agent result of use of the herbal medicine of present embodiment and marine alga is following:
Subjects: shed leek (only son and heir is red), experiment field and each 1 mu in contrast field;
Experimental plot: dash with every mu of the form of topdressing and to execute the composite biological agent 10kg of herbal medicine and marine alga;
Contrast the field: dash for every mu with the form of topdressing and execute nitrogen, phosphorus, the water-soluble fertile 10kg of potassium (14wt%-6wt%-30wt%) macroelement;
The contrast effect: dash the contrast field fragrant-flowered garlic maggot execute nitrogen, phosphorus, the water-soluble fertilizer of potassium (14wt%-6wt%-30wt%) macroelement and sting that to bite phenomenon heavier, stem is thin and the sharp phenomenon of doing is arranged, and dashing the experiment field of executing the Chinese medicine seaweed fertilizer does not have insect pest basically, and the leaf look blackish green, and stem is sturdy; Quality of vegetable is good, and the single batch of income in contrast contrast field, experiment field is high more than 30%.
Embodiment 5
The herbal medicine of present embodiment and the composite biological agent of marine alga comprise following component, and its weight proportion is:
The herbal medicine marine alga mixes 70 parts of base fluids, 20 parts of humic acidss, 25 parts in urea, 25 parts of monoammonium phosphates, 25 parts of potassium primary phosphates, 30 parts of vitriolate of tartar, 2 parts in magnesium;
Wherein, the herbal medicine marine alga mixes base fluid and comprises following component, and its weight proportion is:
30 parts of extracts of Chinese herbal medicine, 80 parts of seaweed extracted liquors, 20 parts of buffer reagent metalloproteases, 20 parts in stablizer wood vinegar;
The main raw material weight proportion of extracts of Chinese herbal medicine is following: tuber of stemona 70g, bark of eucommia 70g, root of langdu 80g, Herba Andrographis 70g, Herba Sophorae alopecuroidis 40g, Radix Astragali 80g, root of large-flowered skullcap 40g, Herba Houttuyniae 100g, kuh-seng 10g, Radix Glycyrrhizae 50g, garlicin 40g, pipe tobacco 150g, Rangooncreeper Fruit 60g;
The main raw material of seaweed extracted liquor is a brown alga.
The preparation method of the herbal medicine of present embodiment and the composite biological agent of marine alga comprises following content:
The first step, produce extracts of Chinese herbal medicine: the herbal raw material of formula ratio is cleaned the back mix, be crushed to 300 orders, extract by following technology:
1, herbal powder is mixed with water, water consumption is 10 times of herbal powder weight, adds 30mol/l phosphoric acid pH value is adjusted to 3, adds Sumizyme MP and extracts 30 hours at 15 degree Celsius;
2, cool to about 0 degree, add 50mol/l yellow soda ash pH value is adjusted to 7, separate and remove residue, obtain tawny liquid, to be concentrated into proportion be that 0.8g/ml promptly obtains extracts of Chinese herbal medicine to vacuum pressed then;
Wherein, the weight proportion of herbal raw material each component is: tuber of stemona 70g, bark of eucommia 70g, root of langdu 80g, Herba Andrographis 70g, Herba Sophorae alopecuroidis 40g, Radix Astragali 80g, root of large-flowered skullcap 40g, Herba Houttuyniae 100g, kuh-seng 10g, Radix Glycyrrhizae 50g, garlicin 40g, pipe tobacco 150g, Rangooncreeper Fruit 70g.
In second step, produce seaweed extracted liquor: marine alga is cleaned oven dry be crushed to 300 orders, extract by following technology:
1, marine algae powder is mixed with water, water consumption is 15 times of marine algae powder weight, adds 30mol/l phosphoric acid pH value is adjusted to 3, extracts 5 hours at 45 degrees centigrade;
2, add 50mol/l yellow soda ash pH value is adjusted to 7, then separating and removing impurities;
3, to be concentrated into proportion be 1.2g/ml to vacuum pressed, promptly obtains seaweed extracted liquor.
In the 3rd step, produce the herbal medicine marine alga and mix base fluid: with extracts of Chinese herbal medicine and seaweed extracted liquor thorough mixing, add the buffer reagent metalloprotease then, the stablizer wood vinegar;
The weight proportion of each component is: 30 parts of extracts of Chinese herbal medicine, 80 parts of seaweed extracted liquors, 20 parts of buffer reagent metalloproteases, 20 parts in stablizer wood vinegar;
In the 4th step, process the composite biological agent of herbal medicine and marine alga: the herbal medicine marine alga is mixed in the base fluid add humic acids, urea, monoammonium phosphate, potassium primary phosphate, vitriolate of tartar and magnesium, mix;
The weight proportion of each component is: the herbal medicine marine alga mixes 70 parts of base fluids, 20 parts of humic acidss, 25 parts in urea, 25 parts of monoammonium phosphates, 25 parts of potassium primary phosphates, 30 parts of vitriolate of tartar, 2 parts in sal epsom.
The composite biological agent result of use of the herbal medicine of present embodiment and marine alga is following:
Subjects: shed Da Jiang, experiment field and each 1 mu in contrast field;
Experimental plot: dash with every mu of the form of topdressing and to execute the composite biological agent 10kg of herbal medicine and marine alga;
Contrast the field: dash for every mu with the form of topdressing and execute nitrogen, phosphorus, the water-soluble fertile 10kg of potassium (18wt%-7wt%-30wt%) macroelement;
The contrast effect: it is heavier to dash the shameless disease in the contrast field execute nitrogen, phosphorus, the water-soluble fertilizer of potassium (18wt%-7wt%-30wt%) macroelement, wilts, to do sharp phenomenon serious; Dashing the experiment field of executing the Chinese medicine seaweed fertilizer does not have shameless sick phenomenon to take place basically; The growth of leaf look dark green is vigorous, and bacterial wilt of ginger also compares according to the field fewly 70%, and the experiment field is to high by about 26% according to the real estate amount.
Embodiment 6
The herbal medicine of present embodiment and the composite biological agent of marine alga comprise following component, and its weight proportion is:
The herbal medicine marine alga mixes 80 parts of base fluids, 5 parts of humic acidss, 5 parts in urea, 20 parts of monoammonium phosphates, 5 parts of potassium primary phosphates, 2 parts of vitriolate of tartar, 5 parts in sal epsom, 3 parts in copper sulfate, 3 parts of manganous sulfates, 3 parts in nitrocalcite;
Wherein, the herbal medicine marine alga mixes base fluid and comprises following component, and its weight proportion is:
35 parts of extracts of Chinese herbal medicine, 50 parts of seaweed extracted liquors, 5 parts of buffer reagent metalloproteases, 10 parts in stablizer wood vinegar;
The main raw material weight proportion of extracts of Chinese herbal medicine is following: tuber of stemona 60g, bark of eucommia 50g, root of langdu 50g, Herba Andrographis 30g, Herba Sophorae alopecuroidis 10g, Radix Astragali 50g, root of large-flowered skullcap 40g, Herba Houttuyniae 130g, kuh-seng 40g, Radix Glycyrrhizae 20g, garlicin 50g, pipe tobacco 100g, Rangooncreeper Fruit 20g;
The main raw material of seaweed extracted liquor is a brown alga.
The preparation method of the herbal medicine of present embodiment and the composite biological agent of marine alga comprises following content:
The first step, produce extracts of Chinese herbal medicine: the herbal raw material of formula ratio is cleaned the back mix, be crushed to 300 orders, extract by following technology:
1, herbal powder is mixed with water, water consumption is 10 times of herbal powder weight, adds 40mol/l Pottasium Hydroxide pH value is adjusted to 10, adds Sumizyme MP and extracts 24 hours at 65 degree Celsius;
2, cool to about 0 degree, add 40mol/l hydrochloric acid pH value is adjusted to 7, separate and remove residue, obtain tawny liquid, to be concentrated into proportion be that 1.1g/ml promptly obtains extracts of Chinese herbal medicine to vacuum pressed then;
Wherein, the weight proportion of herbal raw material each component is: tuber of stemona 60g, bark of eucommia 50g, root of langdu 50g, Herba Andrographis 30g, Herba Sophorae alopecuroidis 10g, Radix Astragali 50g, root of large-flowered skullcap 40g, Herba Houttuyniae 130g, kuh-seng 40g, Radix Glycyrrhizae 20g, garlicin 50g, pipe tobacco 100g, Rangooncreeper Fruit 20g.
In second step, produce seaweed extracted liquor: marine alga is cleaned oven dry be crushed to 300 orders, extract by following technology:
1, marine algae powder is mixed with water, water consumption is 20 times of marine algae powder weight, adds 40mol/l hydrochloric acid pH value is adjusted to 3, extracts 3 hours at 65 degrees centigrade;
2, add 40mol/l Pottasium Hydroxide pH value is adjusted to 7, then separating and removing impurities;
3, to be concentrated into proportion be 1.2g/ml to vacuum pressed, promptly obtains seaweed extracted liquor.
In the 3rd step, produce the herbal medicine marine alga and mix base fluid: with extracts of Chinese herbal medicine and seaweed extracted liquor thorough mixing, add the buffer reagent metalloprotease then, the stablizer wood vinegar;
The weight proportion of each component is: 35 parts of extracts of Chinese herbal medicine, 50 parts of seaweed extracted liquors, 5 parts of buffer reagent metalloproteases, 10 parts in stablizer wood vinegar.
In the 4th step, process the composite biological agent of herbal medicine and marine alga: the herbal medicine marine alga is mixed in the base fluid add humic acids, urea, monoammonium phosphate, potassium primary phosphate, vitriolate of tartar and magnesium, mix;
The weight proportion of each component is: the herbal medicine marine alga mixes 80 parts of base fluids, 5 parts of humic acidss, 5 parts in urea, 20 parts of monoammonium phosphates, 5 parts of potassium primary phosphates, 2 parts of vitriolate of tartar, 5 parts in sal epsom, 3 parts in copper sulfate, 3 parts of manganous sulfates, 3 parts in nitrocalcite.
The above only is to preferred embodiment of the present invention, is not to be that the present invention is done other forms of restriction, and any professional and technical personnel of being familiar with possibly utilize the technology contents of above-mentioned announcement to change or be modified as the equivalent embodiment of equivalent variations.But every the present invention program's content that do not break away to any simple modification, equivalent variations and remodeling that above embodiment did, still belongs to protection scope of the present invention according to technical spirit of the present invention.
Claims (10)
1. the composite biological agent of herbal medicine and marine alga, it is characterized in that: comprise following component, its weight proportion is:
The herbal medicine marine alga mixes 10 parts-80 parts of base fluids, 5 parts-25 parts of humic acidss, 5 parts-25 parts in urea, 5 parts-25 parts of monoammonium phosphates, 5 parts-25 parts of potassium primary phosphates, 2 parts-30 parts of vitriolate of tartar, 2 parts-20 parts of trace elements;
Wherein, the herbal medicine marine alga mixes base fluid and comprises following component, and its weight proportion is:
20 parts-45 parts of extracts of Chinese herbal medicine, 50 parts-80 parts of seaweed extracted liquors, 5 parts-20 parts of buffer reagent metalloproteases, 5 parts-20 parts in stablizer wood vinegar.
2. the composite biological agent of herbal medicine according to claim 1 and marine alga is characterized in that: the main raw material weight proportion of extracts of Chinese herbal medicine is following: tuber of stemona 40-70g, bark of eucommia 20-70g, root of langdu 30-80g; Herba Andrographis 30-70g, Herba Sophorae alopecuroidis 10-40g, Radix Astragali 30-80g, root of large-flowered skullcap 20-60g; Herba Houttuyniae 90-130g, kuh-seng 10-40g, Radix Glycyrrhizae 20-50g; Garlicin 30-60g, pipe tobacco 80-150g, Rangooncreeper Fruit 20-70g.
3. the composite biological agent of herbal medicine according to claim 1 and marine alga is characterized in that: the main raw material of seaweed extracted liquor is a brown alga.
4. the composite biological agent of herbal medicine according to claim 1 and marine alga is characterized in that: trace element is one or more in magnesium, copper, manganese, iron, boron, zinc, molybdenum, the calcium.
5. the preparation method of the composite biological agent of described herbal medicine of claim 1 and marine alga is characterized in that: comprise following content:
The first step, produce extracts of Chinese herbal medicine: the herbal raw material of formula ratio is cleaned the back mix, be crushed to 300 orders, press (1), (3) or (2), (3) two kinds of technologies extractions as follows:
(1) herbal powder is mixed with water, pH value is adjusted to 9-11, add Sumizyme MP and extracted 24 hours at 45-65 degree Celsius;
(2) herbal powder is mixed with water, pH value is adjusted to 1-3, add aspartic protease and extracted 30 hours at 15-25 degree Celsius;
(3) cool to about 0 degree, pH value is adjusted to 7, separate to remove residue, to be concentrated into proportion be that 0.8-1.2g/ml promptly obtains extracts of Chinese herbal medicine to vacuum pressed then;
The weight proportion of said herbal raw material each component is: tuber of stemona 40-70g, bark of eucommia 20-70g, root of langdu 30-80g, Herba Andrographis 30-70g; Herba Sophorae alopecuroidis 10-40g, Radix Astragali 30-80g, root of large-flowered skullcap 20-60g; Herba Houttuyniae 90-130g, kuh-seng 10-40g, Radix Glycyrrhizae 20-50g; Garlicin 30-60g, pipe tobacco 80-150g, Rangooncreeper Fruit 20-70g;
In second step, produce seaweed extracted liquor: marine alga is washed earned oven dry and be crushed to 300 orders, extract by (1), (3), (4) or (2), (3), (4) two kinds of technologies:
(1) marine algae powder is mixed with water, pH value is adjusted to 9-11, extracted 4-7 hour at 75-100 degree Celsius;
(2) marine algae powder is mixed with water, pH value is adjusted to 1-3, extracted 3-5 hour at 45-65 degree Celsius;
(3) pH value is adjusted to 7, then separating and removing impurities;
(4) to be concentrated into proportion be 1-1.4g/ml to vacuum pressed, promptly obtains seaweed extracted liquor;
In the 3rd step, produce the herbal medicine marine alga and mix base fluid: with extracts of Chinese herbal medicine and seaweed extracted liquor thorough mixing, add the buffer reagent metalloprotease then, with the stablizer wood vinegar;
The weight proportion of said each component is: 20 parts-45 parts of extracts of Chinese herbal medicine, 60 parts-80 parts of seaweed extracted liquors, 5 parts-20 parts of buffer reagent metalloproteases, 5 parts-20 parts in stablizer wood vinegar;
In the 4th step, process the composite biological agent of herbal medicine and marine alga: the herbal medicine marine alga is mixed in the base fluid add humic acids, urea, vitriolate of tartar, monoammonium phosphate, potassium primary phosphate and trace element, mix;
The weight proportion of said each component is: the herbal medicine marine alga mixes 10 parts-80 parts of base fluids, 5 parts-25 parts of humic acidss, 5 parts-25 parts in urea, 2 parts-30 parts of vitriolate of tartar, 5 parts-25 parts of monoammonium phosphates, 5 parts-25 parts of potassium primary phosphates, 2 parts-20 parts of trace elements.
6. the preparation method of the composite biological agent of herbal medicine according to claim 5 and marine alga is characterized in that: the first step, to produce in the extracts of Chinese herbal medicine, and the water consumption in (1) or (2) is 10-20 a times of herbal powder weight.
7. the preparation method of the composite biological agent of herbal medicine according to claim 5 and marine alga is characterized in that: second step, to produce in the seaweed extracted liquor, and the water consumption in (1) or (2) is 10-20 a times of marine algae powder weight.
8. the preparation method of the composite biological agent of herbal medicine according to claim 5 and marine alga; It is characterized in that: the first step; Produce in the extracts of Chinese herbal medicine, the alkali that the adjusting pH value uses is Pottasium Hydroxide, sodium hydroxide, salt of wormwood or yellow soda ash, and the acid of using is hydrochloric acid, sulfuric acid or phosphoric acid.
9. the preparation method of the composite biological agent of herbal medicine according to claim 5 and marine alga; It is characterized in that: second step; Produce in the seaweed extracted liquor, the alkali that the adjusting pH value uses is Pottasium Hydroxide, sodium hydroxide, salt of wormwood or yellow soda ash, and the acid of using is hydrochloric acid, sulfuric acid or phosphoric acid.
10. the preparation method of the composite biological agent of herbal medicine according to claim 5 and marine alga is characterized in that: said trace element is one or more in magnesium, copper, manganese, iron, boron, zinc, molybdenum, the calcium.
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