CN1025844C - 高纯度氢气的制备方法 - Google Patents

高纯度氢气的制备方法 Download PDF

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Publication number
CN1025844C
CN1025844C CN91110738A CN91110738A CN1025844C CN 1025844 C CN1025844 C CN 1025844C CN 91110738 A CN91110738 A CN 91110738A CN 91110738 A CN91110738 A CN 91110738A CN 1025844 C CN1025844 C CN 1025844C
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Prior art keywords
gas
gas mixture
raw material
defective
hydrogen
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Expired - Lifetime
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CN91110738A
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English (en)
Chinese (zh)
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CN1061386A (zh
Inventor
W-C·F·冯
H·C·钱
R·M·桑吉特
M·E·昆塔纳
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Texaco Development Corp
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Texaco Development Corp
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Priority claimed from US07/614,335 external-priority patent/US5152976A/en
Priority claimed from US07/669,796 external-priority patent/US5152975A/en
Application filed by Texaco Development Corp filed Critical Texaco Development Corp
Publication of CN1061386A publication Critical patent/CN1061386A/zh
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen; Reversible storage of hydrogen
    • C01B3/02—Production of hydrogen; Production of gaseous mixtures containing hydrogen
    • C01B3/32—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air
    • C01B3/34—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air by reaction of hydrocarbons with gasifying agents
    • C01B3/48—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air by reaction of hydrocarbons with gasifying agents followed by reaction of water vapour with carbon monoxide
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen; Reversible storage of hydrogen
    • C01B3/02—Production of hydrogen; Production of gaseous mixtures containing hydrogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02—Processes for making hydrogen or synthesis gas
    • C01B2203/025—Processes for making hydrogen or synthesis gas containing a partial oxidation step
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02—Processes for making hydrogen or synthesis gas
    • C01B2203/0283—Processes for making hydrogen or synthesis gas containing a CO-shift step, i.e. a water gas shift step
    • C01B2203/0288—Processes for making hydrogen or synthesis gas containing a CO-shift step, i.e. a water gas shift step containing two CO-shift steps
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/042—Purification by adsorption on solids
    • C01B2203/043—Regenerative adsorption process in two or more beds, one for adsorption, the other for regeneration
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0435—Catalytic purification
    • C01B2203/045—Purification by catalytic desulfurisation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465—Composition of the impurity
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465—Composition of the impurity
    • C01B2203/0485—Composition of the impurity the impurity being a sulfur compound
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465—Composition of the impurity
    • C01B2203/0495—Composition of the impurity the impurity being water
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/08—Methods of heating or cooling
    • C01B2203/0805—Methods of heating the process for making hydrogen or synthesis gas
    • C01B2203/0811—Methods of heating the process for making hydrogen or synthesis gas by combustion of fuel
    • C01B2203/0816—Heating by flames
    • C—CHEMISTRY; METALLURGY
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    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/08—Methods of heating or cooling
    • C01B2203/0805—Methods of heating the process for making hydrogen or synthesis gas
    • C01B2203/0811—Methods of heating the process for making hydrogen or synthesis gas by combustion of fuel
    • C01B2203/0822—Methods of heating the process for making hydrogen or synthesis gas by combustion of fuel the fuel containing hydrogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
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    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/08—Methods of heating or cooling
    • C01B2203/0805—Methods of heating the process for making hydrogen or synthesis gas
    • C01B2203/0833—Heating by indirect heat exchange with hot fluids, other than combustion gases, product gases or non-combustive exothermic reaction product gases
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    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/08—Methods of heating or cooling
    • C01B2203/0805—Methods of heating the process for making hydrogen or synthesis gas
    • C01B2203/0838—Methods of heating the process for making hydrogen or synthesis gas by heat exchange with exothermic reactions, other than by combustion of fuel
    • C01B2203/0844—Methods of heating the process for making hydrogen or synthesis gas by heat exchange with exothermic reactions, other than by combustion of fuel the non-combustive exothermic reaction being another reforming reaction as defined in groups C01B2203/02 - C01B2203/0294
    • C—CHEMISTRY; METALLURGY
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    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/08—Methods of heating or cooling
    • C01B2203/0872—Methods of cooling
    • C01B2203/0877—Methods of cooling by direct injection of fluid
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/08—Methods of heating or cooling
    • C01B2203/0872—Methods of cooling
    • C01B2203/0883—Methods of cooling by indirect heat exchange
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/08—Methods of heating or cooling
    • C01B2203/0872—Methods of cooling
    • C01B2203/0888—Methods of cooling by evaporation of a fluid
    • C01B2203/0894—Generation of steam
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/10—Catalysts for performing the hydrogen forming reactions
    • C01B2203/1005—Arrangement or shape of catalyst
    • C01B2203/1011—Packed bed of catalytic structures, e.g. particles, packing elements
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/10—Catalysts for performing the hydrogen forming reactions
    • C01B2203/1041—Composition of the catalyst
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/10—Catalysts for performing the hydrogen forming reactions
    • C01B2203/1041—Composition of the catalyst
    • C01B2203/1047—Group VIII metal catalysts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/12—Feeding the process for making hydrogen or synthesis gas
    • C01B2203/1205—Composition of the feed
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/12—Feeding the process for making hydrogen or synthesis gas
    • C01B2203/1205—Composition of the feed
    • C01B2203/1211—Organic compounds or organic mixtures used in the process for making hydrogen or synthesis gas
    • C01B2203/1235—Hydrocarbons
    • C01B2203/1241—Natural gas or methane
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/14—Details of the flowsheet
    • C01B2203/146—At least two purification steps in series
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/14—Details of the flowsheet
    • C01B2203/148—Details of the flowsheet involving a recycle stream to the feed of the process for making hydrogen or synthesis gas
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Hydrogen, Water And Hydrids (AREA)
  • Industrial Gases (AREA)
CN91110738A 1990-11-16 1991-11-15 高纯度氢气的制备方法 Expired - Lifetime CN1025844C (zh)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US07/614,335 US5152976A (en) 1990-11-16 1990-11-16 Process for producing high purity hydrogen
US614,335 1991-03-15
US07/669,796 US5152975A (en) 1991-03-15 1991-03-15 Process for producing high purity hydrogen
US669,796 1996-06-27

Publications (2)

Publication Number Publication Date
CN1061386A CN1061386A (zh) 1992-05-27
CN1025844C true CN1025844C (zh) 1994-09-07

Family

ID=27087214

Family Applications (1)

Application Number Title Priority Date Filing Date
CN91110738A Expired - Lifetime CN1025844C (zh) 1990-11-16 1991-11-15 高纯度氢气的制备方法

Country Status (9)

Country Link
EP (1) EP0486174B1 (online.php)
JP (1) JP3638618B2 (online.php)
KR (1) KR100209982B1 (online.php)
CN (1) CN1025844C (online.php)
AU (1) AU645628B2 (online.php)
DE (1) DE69104461T2 (online.php)
ES (1) ES2061189T3 (online.php)
MX (1) MX9101972A (online.php)
TW (1) TW197997B (online.php)

Families Citing this family (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5458808A (en) * 1994-01-07 1995-10-17 Texaco Inc. Process for continuously controlling the heat content of a partial oxidation unit feed-gas stream
CN1067348C (zh) * 1996-12-19 2001-06-20 中国石化茂名石油化工公司 氢气保温保压循环方法
DE19902926C2 (de) * 1999-01-26 2001-01-04 Daimler Chrysler Ag Reaktoranlage und Betriebsverfahren hierfür
AU2001268019A1 (en) * 2000-07-07 2002-01-21 National University Of Singapore Method for hydrogen production
JP4568448B2 (ja) * 2001-03-30 2010-10-27 出光興産株式会社 水素製造プラントおよび水素製造方法
DE10334590B4 (de) * 2003-07-28 2006-10-26 Uhde Gmbh Verfahren zur Gewinnung von Wasserstoff aus einem methanhaltigen Gas, insbesondere Erdgas und Anlage zur Durchführung des Verfahrens
DE102006045379B4 (de) * 2006-09-26 2008-07-31 Lurgi Ag Verfahren zur Herstellung von Wasserstoff
KR100884701B1 (ko) 2007-08-22 2009-02-19 한국에너지기술연구원 연료개질 장치에서 압력구동을 이용한 이산화탄소 흡착제재생방법
JP5288840B2 (ja) * 2008-03-17 2013-09-11 Ｊｘ日鉱日石エネルギー株式会社 水素製造システム
US7909913B2 (en) 2008-07-17 2011-03-22 Air Products And Chemicals, Inc. Gas purification by adsorption of hydrogen sulfide
JP2012521955A (ja) * 2009-03-30 2012-09-20 シエル・インターナシヨナル・リサーチ・マートスハツペイ・ベー・ヴエー 精製合成ガス流を生成する方法
EP2414074A1 (en) * 2009-03-30 2012-02-08 Shell Internationale Research Maatschappij B.V. Process for producing purified synthesis gas
US8808654B2 (en) 2009-09-29 2014-08-19 Praxair Technology, Inc. Process for sulfur removal from refinery off gas
CN101773765B (zh) * 2010-01-14 2012-07-25 党延斋 炼厂干气中氢气的回收方法
US8518356B2 (en) * 2010-07-27 2013-08-27 Air Products And Chemicals, Inc. Method and apparatus for adjustably treating a sour gas
US8206669B2 (en) * 2010-07-27 2012-06-26 Air Products And Chemicals, Inc. Method and apparatus for treating a sour gas
CN102614764B (zh) * 2011-01-27 2014-03-26 中科合成油工程有限公司 一种费托合成尾气处理的工艺
CN103922280B (zh) * 2014-04-18 2017-10-20 四川省达科特能源科技股份有限公司 一种灵活焦化气化气制氢工艺方法
WO2016059566A1 (en) * 2014-10-15 2016-04-21 Sabic Global Technologies B.V. Integrated syngas-based production of dimethyl carbonate
PL3448576T3 (pl) * 2016-04-26 2024-09-16 Newcastle Innovation Limited Urządzenie podające do separatora cząstek stałych, separator cząstek stałych i sposób separacji cząstek
US10622656B2 (en) * 2017-10-11 2020-04-14 Saudi Arabian Oil Company Method and system for capturing high-purity CO2 in a hydrocarbon facility
CN110937573B (zh) * 2019-10-28 2023-08-22 中科液态阳光(苏州)氢能科技发展有限公司 氢气混合余气重整方法
CN112626560B (zh) * 2020-12-14 2022-04-08 阳光电源股份有限公司 电解槽设备及其气体回收装置、电解气体回收方法
US11772966B2 (en) * 2021-03-29 2023-10-03 Uop Llc Integrated hydrogen production and bio-renewable conversion process
CN114348962A (zh) * 2021-12-23 2022-04-15 甘肃银光聚银化工有限公司 一种基于排放火炬废气回收提氢方法
CN117620915A (zh) * 2023-12-19 2024-03-01 青岛理工大学 一种仿生澳洲棘蜥磨削砂轮、磨削装置及制备工艺

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BR6899414D0 (pt) * 1963-06-06 1973-01-02 Texaco Development Corp Processo para producao de hidrogenio
US4533981A (en) * 1982-08-16 1985-08-06 Ready Metal Manufacturing Company Light cornice
GB8519821D0 (en) * 1985-08-07 1985-09-11 Ici Plc Hydrogen streams
DE3667180D1 (de) * 1985-06-27 1990-01-04 Texaco Development Corp Verfahren zur teiloxydation.
DE3605811A1 (de) * 1986-02-22 1987-08-27 Uhde Gmbh Vorrichtung zum einsetzen in einem verfahren zur erzeugung von produktgas mit wasserstoff- und kohlenoxidgehalten

Also Published As

Publication number Publication date
TW197997B (online.php) 1993-01-11
JP3638618B2 (ja) 2005-04-13
DE69104461T2 (de) 1995-02-09
CN1061386A (zh) 1992-05-27
KR920009687A (ko) 1992-06-25
MX9101972A (es) 1992-07-08
DE69104461D1 (de) 1994-11-10
KR100209982B1 (ko) 1999-07-15
AU645628B2 (en) 1994-01-20
EP0486174B1 (en) 1994-10-05
ES2061189T3 (es) 1994-12-01
JPH0624703A (ja) 1994-02-01
EP0486174A1 (en) 1992-05-20
AU8787691A (en) 1992-05-21

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