DE69104461D1 - Verfahren zur Erzeugung von hochreinem Wasserstoff. - Google Patents

Verfahren zur Erzeugung von hochreinem Wasserstoff.

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Publication number
DE69104461D1
DE69104461D1 DE69104461T DE69104461T DE69104461D1 DE 69104461 D1 DE69104461 D1 DE 69104461D1 DE 69104461 T DE69104461 T DE 69104461T DE 69104461 T DE69104461 T DE 69104461T DE 69104461 D1 DE69104461 D1 DE 69104461D1
Authority
DE
Germany
Prior art keywords
production
purity hydrogen
purity
hydrogen
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Revoked
Application number
DE69104461T
Other languages
English (en)
Other versions
DE69104461T2 (de
Inventor
Wing-Chiu Francis Fong
Henry Choisun Chan
Robert Murray Suggitt
Manuel Eduardo Quintana
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Texaco Development Corp
Original Assignee
Texaco Development Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=27087214&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=DE69104461(D1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Priority claimed from US07/614,335 external-priority patent/US5152976A/en
Priority claimed from US07/669,796 external-priority patent/US5152975A/en
Application filed by Texaco Development Corp filed Critical Texaco Development Corp
Application granted granted Critical
Publication of DE69104461D1 publication Critical patent/DE69104461D1/de
Publication of DE69104461T2 publication Critical patent/DE69104461T2/de
Anticipated expiration legal-status Critical
Revoked legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/32Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air
    • C01B3/34Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents
    • C01B3/48Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents followed by reaction of water vapour with carbon monoxide
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02Processes for making hydrogen or synthesis gas
    • C01B2203/025Processes for making hydrogen or synthesis gas containing a partial oxidation step
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02Processes for making hydrogen or synthesis gas
    • C01B2203/0283Processes for making hydrogen or synthesis gas containing a CO-shift step, i.e. a water gas shift step
    • C01B2203/0288Processes for making hydrogen or synthesis gas containing a CO-shift step, i.e. a water gas shift step containing two CO-shift steps
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/042Purification by adsorption on solids
    • C01B2203/043Regenerative adsorption process in two or more beds, one for adsorption, the other for regeneration
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0435Catalytic purification
    • C01B2203/045Purification by catalytic desulfurisation
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465Composition of the impurity
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465Composition of the impurity
    • C01B2203/0485Composition of the impurity the impurity being a sulfur compound
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465Composition of the impurity
    • C01B2203/0495Composition of the impurity the impurity being water
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/08Methods of heating or cooling
    • C01B2203/0805Methods of heating the process for making hydrogen or synthesis gas
    • C01B2203/0811Methods of heating the process for making hydrogen or synthesis gas by combustion of fuel
    • C01B2203/0816Heating by flames
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/08Methods of heating or cooling
    • C01B2203/0805Methods of heating the process for making hydrogen or synthesis gas
    • C01B2203/0811Methods of heating the process for making hydrogen or synthesis gas by combustion of fuel
    • C01B2203/0822Methods of heating the process for making hydrogen or synthesis gas by combustion of fuel the fuel containing hydrogen
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/08Methods of heating or cooling
    • C01B2203/0805Methods of heating the process for making hydrogen or synthesis gas
    • C01B2203/0833Heating by indirect heat exchange with hot fluids, other than combustion gases, product gases or non-combustive exothermic reaction product gases
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/08Methods of heating or cooling
    • C01B2203/0805Methods of heating the process for making hydrogen or synthesis gas
    • C01B2203/0838Methods of heating the process for making hydrogen or synthesis gas by heat exchange with exothermic reactions, other than by combustion of fuel
    • C01B2203/0844Methods of heating the process for making hydrogen or synthesis gas by heat exchange with exothermic reactions, other than by combustion of fuel the non-combustive exothermic reaction being another reforming reaction as defined in groups C01B2203/02 - C01B2203/0294
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/08Methods of heating or cooling
    • C01B2203/0872Methods of cooling
    • C01B2203/0877Methods of cooling by direct injection of fluid
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/08Methods of heating or cooling
    • C01B2203/0872Methods of cooling
    • C01B2203/0883Methods of cooling by indirect heat exchange
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/08Methods of heating or cooling
    • C01B2203/0872Methods of cooling
    • C01B2203/0888Methods of cooling by evaporation of a fluid
    • C01B2203/0894Generation of steam
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/10Catalysts for performing the hydrogen forming reactions
    • C01B2203/1005Arrangement or shape of catalyst
    • C01B2203/1011Packed bed of catalytic structures, e.g. particles, packing elements
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/10Catalysts for performing the hydrogen forming reactions
    • C01B2203/1041Composition of the catalyst
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/10Catalysts for performing the hydrogen forming reactions
    • C01B2203/1041Composition of the catalyst
    • C01B2203/1047Group VIII metal catalysts
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/12Feeding the process for making hydrogen or synthesis gas
    • C01B2203/1205Composition of the feed
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/12Feeding the process for making hydrogen or synthesis gas
    • C01B2203/1205Composition of the feed
    • C01B2203/1211Organic compounds or organic mixtures used in the process for making hydrogen or synthesis gas
    • C01B2203/1235Hydrocarbons
    • C01B2203/1241Natural gas or methane
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/14Details of the flowsheet
    • C01B2203/146At least two purification steps in series
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/14Details of the flowsheet
    • C01B2203/148Details of the flowsheet involving a recycle stream to the feed of the process for making hydrogen or synthesis gas
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency
DE69104461T 1990-11-16 1991-10-24 Verfahren zur Erzeugung von hochreinem Wasserstoff. Revoked DE69104461T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US07/614,335 US5152976A (en) 1990-11-16 1990-11-16 Process for producing high purity hydrogen
US07/669,796 US5152975A (en) 1991-03-15 1991-03-15 Process for producing high purity hydrogen

Publications (2)

Publication Number Publication Date
DE69104461D1 true DE69104461D1 (de) 1994-11-10
DE69104461T2 DE69104461T2 (de) 1995-02-09

Family

ID=27087214

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69104461T Revoked DE69104461T2 (de) 1990-11-16 1991-10-24 Verfahren zur Erzeugung von hochreinem Wasserstoff.

Country Status (9)

Country Link
EP (1) EP0486174B1 (de)
JP (1) JP3638618B2 (de)
KR (1) KR100209982B1 (de)
CN (1) CN1025844C (de)
AU (1) AU645628B2 (de)
DE (1) DE69104461T2 (de)
ES (1) ES2061189T3 (de)
MX (1) MX9101972A (de)
TW (1) TW197997B (de)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5458808A (en) * 1994-01-07 1995-10-17 Texaco Inc. Process for continuously controlling the heat content of a partial oxidation unit feed-gas stream
CN1067348C (zh) * 1996-12-19 2001-06-20 中国石化茂名石油化工公司 氢气保温保压循环方法
DE19902926C2 (de) * 1999-01-26 2001-01-04 Daimler Chrysler Ag Reaktoranlage und Betriebsverfahren hierfür
AU2001268019A1 (en) * 2000-07-07 2002-01-21 National University Of Singapore Method for hydrogen production
JP4568448B2 (ja) * 2001-03-30 2010-10-27 出光興産株式会社 水素製造プラントおよび水素製造方法
DE10334590B4 (de) * 2003-07-28 2006-10-26 Uhde Gmbh Verfahren zur Gewinnung von Wasserstoff aus einem methanhaltigen Gas, insbesondere Erdgas und Anlage zur Durchführung des Verfahrens
DE102006045379B4 (de) * 2006-09-26 2008-07-31 Lurgi Ag Verfahren zur Herstellung von Wasserstoff
KR100884701B1 (ko) 2007-08-22 2009-02-19 한국에너지기술연구원 연료개질 장치에서 압력구동을 이용한 이산화탄소 흡착제재생방법
JP5288840B2 (ja) * 2008-03-17 2013-09-11 Jx日鉱日石エネルギー株式会社 水素製造システム
US7909913B2 (en) 2008-07-17 2011-03-22 Air Products And Chemicals, Inc. Gas purification by adsorption of hydrogen sulfide
AU2010230279B2 (en) * 2009-03-30 2013-10-10 Shell Internationale Research Maatschappij B.V. Process for producing purified synthesis gas
AU2010230278B2 (en) * 2009-03-30 2013-08-29 Shell Internationale Research Maatschappij B.V. Process for producing a purified synthesis gas stream
US8808654B2 (en) 2009-09-29 2014-08-19 Praxair Technology, Inc. Process for sulfur removal from refinery off gas
CN101773765B (zh) * 2010-01-14 2012-07-25 党延斋 炼厂干气中氢气的回收方法
US8518356B2 (en) * 2010-07-27 2013-08-27 Air Products And Chemicals, Inc. Method and apparatus for adjustably treating a sour gas
US8206669B2 (en) * 2010-07-27 2012-06-26 Air Products And Chemicals, Inc. Method and apparatus for treating a sour gas
CN102614764B (zh) * 2011-01-27 2014-03-26 中科合成油工程有限公司 一种费托合成尾气处理的工艺
CN103922280B (zh) * 2014-04-18 2017-10-20 四川省达科特能源科技股份有限公司 一种灵活焦化气化气制氢工艺方法
WO2016059566A1 (en) * 2014-10-15 2016-04-21 Sabic Global Technologies B.V. Integrated syngas-based production of dimethyl carbonate
MX2018013088A (es) * 2016-04-26 2019-03-06 Newcastle Innovation Ltd Un aparato de alimentacion para un separador de particulas, un separador de particulas y un metodo para separacion de particulas.
US10622656B2 (en) * 2017-10-11 2020-04-14 Saudi Arabian Oil Company Method and system for capturing high-purity CO2 in a hydrocarbon facility
CN110937573B (zh) * 2019-10-28 2023-08-22 中科液态阳光(苏州)氢能科技发展有限公司 氢气混合余气重整方法
CN112626560B (zh) * 2020-12-14 2022-04-08 阳光电源股份有限公司 电解槽设备及其气体回收装置、电解气体回收方法
CN114348962A (zh) * 2021-12-23 2022-04-15 甘肃银光聚银化工有限公司 一种基于排放火炬废气回收提氢方法

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BR6899414D0 (pt) * 1963-06-06 1973-01-02 Texaco Development Corp Processo para producao de hidrogenio
US4533981A (en) * 1982-08-16 1985-08-06 Ready Metal Manufacturing Company Light cornice
GB8519821D0 (en) * 1985-08-07 1985-09-11 Ici Plc Hydrogen streams
DE3667180D1 (de) * 1985-06-27 1990-01-04 Texaco Development Corp Verfahren zur teiloxydation.
DE3605811A1 (de) * 1986-02-22 1987-08-27 Uhde Gmbh Vorrichtung zum einsetzen in einem verfahren zur erzeugung von produktgas mit wasserstoff- und kohlenoxidgehalten

Also Published As

Publication number Publication date
JP3638618B2 (ja) 2005-04-13
CN1061386A (zh) 1992-05-27
AU8787691A (en) 1992-05-21
ES2061189T3 (es) 1994-12-01
KR920009687A (ko) 1992-06-25
EP0486174B1 (de) 1994-10-05
KR100209982B1 (ko) 1999-07-15
MX9101972A (es) 1992-07-08
AU645628B2 (en) 1994-01-20
JPH0624703A (ja) 1994-02-01
DE69104461T2 (de) 1995-02-09
CN1025844C (zh) 1994-09-07
TW197997B (de) 1993-01-11
EP0486174A1 (de) 1992-05-20

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